#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:13:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180985 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/65/2206599.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206599_Fobs loop_ _publ_author_name 'Huang, Peng-Mian' 'Li, Jiang-Sheng' 'Duan, Xue-Min' 'Zeng, Tao' 'Yan, Xi-Long' _publ_section_title ; 3,6-Dibromo-9-ethyl-9H-carbazole ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2366 _journal_page_last o2367 _journal_volume 61 _journal_year 2005 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.733 _cell_angle_gamma 90.000 _cell_length_a 4.2588 _cell_length_b 10.9305 _cell_length_c 13.7243 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.8018 _cod_data_source_file xu6016Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50502C in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 154.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 -4 0 386.45 366.28 24.30 o 4 -4 0 20.75 12.59 13.78 o 5 -4 0 14.46 26.71 16.46 o 2 -3 0 1002.32 1012.26 34.90 o 3 -3 0 191.76 193.72 15.49 o 4 -3 0 231.95 219.88 19.94 o 5 -3 0 23.50 38.23 16.41 o 1 -2 0 3979.52 3908.98 141.07 o 2 -2 0 1618.67 1581.85 60.89 o 3 -2 0 64.57 69.43 6.06 o 4 -2 0 46.30 58.81 12.83 o 5 -2 0 3.35 13.15 15.00 o 1 -1 0 1254.52 1236.04 45.49 o 2 -1 0 200.61 203.55 8.71 o 3 -1 0 644.26 624.05 24.68 o 4 -1 0 43.14 56.50 12.52 o 5 -1 0 59.48 65.78 16.85 o 1 0 0 1299.70 1351.81 47.33 o 2 0 0 2920.33 3010.05 104.86 o 3 0 0 17.00 25.99 6.84 o 4 0 0 197.11 196.59 11.71 o 5 0 0 11.10 5.19 15.12 o 1 1 0 1321.51 1367.22 45.66 o 2 1 0 206.76 201.59 10.55 o 3 1 0 687.73 681.34 24.91 o 4 1 0 50.14 51.82 7.48 o 5 1 0 69.39 90.15 17.58 o 0 2 0 10398.06 10474.52 305.01 o 1 2 0 4030.29 4187.26 118.15 o 2 2 0 1819.30 1833.25 43.22 o 3 2 0 83.22 92.51 10.36 o 4 2 0 41.44 45.41 7.60 o 5 2 0 3.16 5.37 9.03 o 1 3 0 174.22 170.94 4.34 o 2 3 0 907.40 937.81 24.58 o 3 3 0 200.67 198.51 9.57 o 4 3 0 233.76 230.67 13.21 o 5 3 0 31.71 30.98 9.96 o 0 4 0 1030.34 1122.28 32.95 o 1 4 0 5935.72 6534.54 145.06 o 2 4 0 53.27 52.57 4.05 o 3 4 0 392.11 408.85 11.57 o 4 4 0 23.68 29.42 7.70 o 5 4 0 14.93 12.46 9.53 o 1 5 0 137.56 166.02 4.89 o 2 5 0 1102.51 1161.72 29.71 o 3 5 0 18.73 20.28 3.40 o 4 5 0 325.46 293.32 21.97 o 0 6 0 1305.28 1492.64 44.42 o 1 6 0 4683.36 5251.83 117.54 o 2 6 0 10.24 10.20 3.17 o 3 6 0 492.26 494.91 14.32 o 4 6 0 3.83 15.36 7.91 o 1 7 0 324.32 367.35 9.47 o 2 7 0 189.57 180.85 8.16 o 3 7 0 11.35 15.79 4.18 o 4 7 0 43.37 56.04 9.33 o 0 8 0 1044.44 1117.20 33.89 o 1 8 0 586.57 637.40 15.58 o 2 8 0 419.12 436.01 16.95 o 3 8 0 93.14 99.30 6.17 o 4 8 0 2.13 -4.74 11.68 o 1 9 0 323.08 326.57 9.23 o 2 9 0 23.18 29.57 5.09 o 3 9 0 106.15 115.51 6.91 o 0 10 0 1229.46 1266.26 46.61 o 1 10 0 95.04 100.10 4.99 o 2 10 0 440.22 474.20 17.03 o 3 10 0 4.01 6.98 5.41 o 1 11 0 210.03 221.70 8.67 o 2 11 0 53.15 64.02 7.76 o 3 11 0 64.11 66.84 6.85 o 0 12 0 379.71 403.22 18.36 o 1 12 0 14.03 7.23 4.59 o 2 12 0 161.56 159.29 12.71 o 1 13 0 9.84 8.98 5.06 o 4 -5 1 16.81 8.21 14.00 o -5 -4 1 13.00 2.36 15.66 o -4 -4 1 112.65 111.00 16.73 o -3 -4 1 234.84 224.60 17.92 o 2 -4 1 224.83 207.70 14.85 o 3 -4 1 26.29 31.78 10.64 o 4 -4 1 0.68 2.56 12.88 o 5 -4 1 1.38 34.82 16.71 o -5 -3 1 2.28 21.94 16.80 o -4 -3 1 11.64 4.46 12.44 o -3 -3 1 33.01 33.48 9.62 o -2 -3 1 614.09 604.95 22.65 o -1 -3 1 1489.68 1512.27 84.04 o 2 -3 1 1871.91 1892.10 67.22 o 3 -3 1 790.88 725.77 38.50 o 4 -3 1 160.66 158.05 17.19 o 5 -3 1 13.50 31.00 15.76 o -5 -2 1 61.53 63.27 17.36 o -4 -2 1 72.33 91.30 14.03 o -3 -2 1 703.82 688.20 25.67 o -2 -2 1 1114.81 1061.98 38.29 o -1 -2 1 4047.53 4153.29 206.36 o 1 -2 1 1899.10 1906.04 66.17 o 2 -2 1 369.99 383.13 14.41 o 3 -2 1 74.06 76.29 7.93 o 4 -2 1 9.56 14.42 11.32 o 5 -2 1 7.79 22.45 14.42 o -5 -1 1 1.73 1.66 14.83 o -4 -1 1 97.46 108.34 14.39 o -3 -1 1 34.33 34.42 6.82 o -2 -1 1 305.45 303.94 12.49 o -1 -1 1 5855.91 5886.15 206.72 o 1 -1 1 1729.95 1787.63 59.48 o 2 -1 1 3698.79 3747.66 132.50 o 3 -1 1 259.90 248.02 12.12 o 4 -1 1 219.65 205.14 17.56 o 5 -1 1 1.43 4.58 14.20 o -5 0 1 13.85 27.10 15.51 o -4 0 1 0.85 4.78 6.14 o -3 0 1 1764.60 1766.24 62.80 o -2 0 1 7.44 8.50 2.53 o -1 0 1 1787.87 1788.03 62.50 o 0 0 1 58.70 40.81 3.09 o 1 0 1 5788.99 5971.13 206.84 o 2 0 1 4.18 3.28 1.30 o 3 0 1 19.15 13.68 4.49 o 4 0 1 1.00 -5.30 6.05 o 5 0 1 1.70 34.68 15.61 o -5 1 1 0.72 -7.94 14.44 o -4 1 1 86.17 97.69 9.26 o -3 1 1 23.28 23.40 4.73 o -2 1 1 321.12 327.52 8.60 o -1 1 1 5823.20 6019.35 206.68 o 0 1 1 688.59 749.96 28.20 o 1 1 1 1555.08 1620.10 49.74 o 2 1 1 3821.48 3820.12 93.92 o 3 1 1 285.86 302.10 12.65 o 4 1 1 188.89 192.27 11.80 o 5 1 1 2.74 8.62 14.76 o -5 2 1 51.88 52.96 9.77 o -4 2 1 79.25 89.76 8.75 o -3 2 1 648.24 666.22 25.75 o -2 2 1 1091.28 1084.19 27.01 o -1 2 1 3774.68 3833.35 96.47 o 0 2 1 2985.84 3113.49 64.44 o 1 2 1 1852.99 1883.68 55.40 o 2 2 1 328.70 372.12 10.11 o 3 2 1 82.86 92.19 7.30 o 4 2 1 5.36 3.31 6.61 o 5 2 1 4.45 13.24 9.16 o -5 3 1 2.35 9.73 9.16 o -4 3 1 7.02 18.70 6.99 o -3 3 1 36.77 33.50 4.47 o -2 3 1 589.67 617.86 15.85 o -1 3 1 1552.95 1619.19 39.77 o 0 3 1 2357.25 2504.68 51.42 o 1 3 1 2689.11 2673.27 152.52 o 2 3 1 1818.89 1926.08 47.66 o 3 3 1 754.10 747.92 19.64 o 4 3 1 140.68 160.84 13.05 o 5 3 1 10.94 23.25 9.59 o -5 4 1 10.04 6.96 9.32 o -4 4 1 112.37 123.20 10.52 o -3 4 1 241.61 243.04 9.96 o -2 4 1 1983.91 1966.58 39.60 o -1 4 1 761.46 833.97 19.11 o 0 4 1 4411.98 4719.90 119.61 o 1 4 1 1410.88 1614.83 36.28 o 2 4 1 217.94 226.02 6.02 o 3 4 1 35.68 36.67 4.25 o 4 4 1 3.31 2.47 7.34 o 5 4 1 1.10 4.65 15.66 o -4 5 1 35.29 36.78 7.98 o -3 5 1 53.39 57.90 4.09 o -2 5 1 218.22 232.91 7.37 o -1 5 1 1101.60 1163.75 26.59 o 0 5 1 454.75 515.08 13.72 o 1 5 1 2872.76 2986.98 66.89 o 2 5 1 6.95 5.54 1.73 o 3 5 1 533.65 553.10 15.36 o 4 5 1 14.59 14.72 7.78 o -4 6 1 56.16 56.07 8.76 o -3 6 1 270.63 258.38 8.82 o -2 6 1 1822.07 1837.00 46.08 o -1 6 1 128.85 128.47 4.29 o 0 6 1 3199.24 3520.38 72.39 o 1 6 1 190.99 204.14 5.87 o 2 6 1 331.59 360.83 12.33 o 3 6 1 51.80 56.42 4.62 o 4 6 1 4.21 8.30 8.08 o -4 7 1 18.77 27.42 8.35 o -3 7 1 22.91 20.07 6.22 o -2 7 1 51.95 57.27 4.92 o -1 7 1 356.07 378.20 9.65 o 0 7 1 666.89 721.07 15.67 o 1 7 1 1269.72 1362.44 31.37 o 2 7 1 1110.38 1213.54 36.65 o 3 7 1 277.27 311.77 10.56 o 4 7 1 28.98 37.45 9.37 o -4 8 1 36.24 47.38 9.14 o -3 8 1 273.28 276.64 9.86 o -2 8 1 264.94 288.57 11.22 o -1 8 1 1139.38 1187.77 27.67 o 0 8 1 710.63 728.30 16.07 o 1 8 1 472.14 490.39 12.42 o 2 8 1 125.76 129.76 8.27 o 3 8 1 14.04 11.33 4.71 o 4 8 1 9.02 0.57 8.86 o -3 9 1 26.01 28.29 5.12 o -2 9 1 7.37 4.65 4.40 o -1 9 1 83.82 90.82 4.41 o 0 9 1 525.99 563.82 15.68 o 1 9 1 264.29 273.62 8.20 o 2 9 1 558.64 626.54 20.70 o 3 9 1 76.01 94.68 6.64 o -3 10 1 182.45 187.27 8.81 o -2 10 1 4.26 5.14 5.03 o -1 10 1 537.34 543.87 14.14 o 0 10 1 63.48 66.85 4.66 o 1 10 1 358.85 390.10 10.89 o 2 10 1 4.24 1.85 8.10 o 3 10 1 51.02 44.86 7.49 o -3 11 1 16.02 18.15 5.84 o -2 11 1 54.38 54.03 6.53 o -1 11 1 0.34 -1.41 3.94 o 0 11 1 144.06 140.79 6.95 o 1 11 1 153.02 158.93 7.51 o 2 11 1 192.38 202.06 10.84 o 3 11 1 2.53 0.39 5.95 o -2 12 1 152.62 152.32 12.44 o -1 12 1 122.63 116.45 11.88 o 0 12 1 68.83 61.26 5.45 o 1 12 1 135.88 123.72 7.04 o 2 12 1 0.89 6.96 7.89 o -1 13 1 18.27 11.05 8.10 o 0 13 1 52.81 50.33 7.31 o 1 13 1 106.02 100.26 6.81 o -1 -6 2 277.94 211.30 15.39 o -1 -5 2 1.10 -2.70 5.21 o 3 -5 2 8.45 13.73 10.81 o 4 -5 2 52.77 18.63 14.17 o -5 -4 2 54.72 43.91 17.36 o -4 -4 2 35.13 21.62 13.49 o -2 -4 2 519.07 498.93 28.15 o -1 -4 2 1685.14 1721.11 100.11 o 2 -4 2 61.93 66.24 8.06 o 3 -4 2 744.90 739.62 39.89 o 4 -4 2 10.46 21.75 13.34 o -5 -3 2 2.25 -9.42 16.34 o -4 -3 2 7.00 14.98 13.03 o -3 -3 2 41.07 40.38 10.33 o -2 -3 2 1181.42 1197.23 65.53 o -1 -3 2 3387.38 3547.21 175.65 o 2 -3 2 1389.95 1378.27 70.38 o 3 -3 2 413.37 416.74 24.28 o 4 -3 2 78.30 101.26 14.27 o 5 -3 2 4.92 9.13 15.32 o -5 -2 2 37.90 48.22 17.02 o -4 -2 2 157.69 154.81 17.10 o -3 -2 2 396.73 382.71 15.89 o -2 -2 2 1602.72 1620.82 59.53 o -1 -2 2 6412.85 6540.97 357.30 o 1 -2 2 71.63 69.28 8.12 o 2 -2 2 416.79 399.49 14.63 o 3 -2 2 251.30 250.01 12.07 o 4 -2 2 172.22 164.55 16.80 o 5 -2 2 15.32 24.04 14.27 o -5 -1 2 1.17 2.12 15.15 o -4 -1 2 49.47 50.87 12.54 o -3 -1 2 232.83 233.99 11.40 o -2 -1 2 557.02 561.52 18.99 o -1 -1 2 22904.74 21981.29 780.49 o 1 -1 2 7754.78 7974.82 274.78 o 2 -1 2 462.67 464.06 16.44 o 3 -1 2 1153.34 1124.01 41.50 o 4 -1 2 10.92 17.61 10.81 o 5 -1 2 1.24 14.34 14.17 o -5 0 2 8.99 6.06 15.17 o -4 0 2 122.45 138.62 10.18 o -3 0 2 221.39 217.56 10.47 o -2 0 2 1300.97 1292.76 45.84 o -1 0 2 286.16 317.85 11.82 o 0 0 2 100.13 76.37 6.45 o 1 0 2 1957.34 2019.12 70.44 o 2 0 2 1888.81 1841.47 46.03 o 3 0 2 12.67 12.86 4.40 o 4 0 2 220.25 221.85 12.40 o 5 0 2 0.17 17.51 14.54 o -5 1 2 1.65 5.07 14.95 o -4 1 2 49.97 49.91 8.43 o -3 1 2 276.05 267.72 12.31 o -2 1 2 448.77 470.87 13.12 o -1 1 2 23807.50 22725.69 640.47 o 0 1 2 2238.76 2278.83 58.00 o 1 1 2 7663.29 7788.07 230.40 o 2 1 2 403.19 418.67 11.46 o 3 1 2 1148.04 1165.46 41.73 o 4 1 2 9.29 8.72 6.51 o 5 1 2 1.04 4.07 14.90 o -5 2 2 37.89 40.66 9.43 o -4 2 2 174.63 174.11 11.32 o -3 2 2 376.49 385.78 16.03 o -2 2 2 1684.50 1737.30 42.10 o -1 2 2 6664.78 6928.43 167.33 o 0 2 2 719.22 763.49 16.09 o 1 2 2 69.03 68.98 2.37 o 2 2 2 365.93 360.34 10.23 o 3 2 2 275.62 295.47 12.76 o 4 2 2 199.29 196.79 12.08 o 5 2 2 8.58 5.25 9.17 o -5 3 2 2.00 10.36 8.76 o -4 3 2 9.49 7.07 6.77 o -3 3 2 50.90 54.01 4.20 o -2 3 2 1226.09 1255.01 31.10 o -1 3 2 3167.69 3258.46 102.12 o 0 3 2 6765.00 7149.64 147.41 o 1 3 2 1469.58 1405.79 57.24 o 2 3 2 1474.82 1554.64 43.09 o 3 3 2 395.48 422.33 11.96 o 4 3 2 89.63 89.77 9.29 o 5 3 2 7.30 10.49 9.63 o -5 4 2 52.80 55.59 10.14 o -4 4 2 34.88 30.76 7.35 o -3 4 2 615.18 619.99 19.45 o -2 4 2 535.73 530.00 11.17 o -1 4 2 1848.91 1955.48 42.62 o 0 4 2 691.98 730.62 15.46 o 1 4 2 521.57 571.08 13.31 o 2 4 2 41.23 41.31 2.44 o 3 4 2 739.99 761.53 20.22 o 4 4 2 18.46 16.12 7.70 o -4 5 2 61.68 62.51 8.42 o -3 5 2 121.42 121.68 5.66 o -2 5 2 1756.40 1865.75 37.66 o -1 5 2 0.26 2.12 1.69 o 0 5 2 6803.78 7381.33 151.49 o 1 5 2 44.71 49.17 3.54 o 2 5 2 1531.96 1579.52 36.03 o 3 5 2 7.53 12.80 3.46 o 4 5 2 74.34 78.65 9.41 o -4 6 2 13.11 14.28 7.50 o -3 6 2 215.46 209.71 7.73 o -2 6 2 399.81 391.52 11.22 o -1 6 2 169.44 181.18 5.35 o 0 6 2 38.68 47.58 3.02 o 1 6 2 587.50 622.03 14.85 o 2 6 2 21.73 17.25 3.48 o 3 6 2 354.51 359.77 11.40 o 4 6 2 3.72 6.77 8.35 o -4 7 2 33.42 15.34 9.55 o -3 7 2 93.11 97.82 5.48 o -2 7 2 569.21 554.92 15.20 o -1 7 2 696.43 757.59 17.82 o 0 7 2 2730.30 2934.35 60.91 o 1 7 2 716.83 731.27 17.49 o 2 7 2 945.36 980.02 30.37 o 3 7 2 56.05 61.75 6.06 o 4 7 2 52.22 48.53 9.89 o -4 8 2 43.21 53.87 9.29 o -3 8 2 154.48 148.57 7.22 o -2 8 2 513.19 518.05 14.55 o -1 8 2 105.64 101.17 4.59 o 0 8 2 16.91 17.89 2.18 o 1 8 2 70.36 71.36 3.64 o 2 8 2 1.71 2.70 4.46 o 3 8 2 72.16 81.54 6.13 o 4 8 2 38.17 27.76 9.92 o -3 9 2 52.05 55.49 5.45 o -2 9 2 168.98 183.09 7.49 o -1 9 2 727.90 751.79 18.18 o 0 9 2 280.13 283.88 9.23 o 1 9 2 848.80 915.10 21.96 o 2 9 2 142.41 147.24 8.45 o 3 9 2 141.83 142.55 12.23 o -3 10 2 15.72 23.92 5.33 o -2 10 2 301.97 296.28 10.16 o -1 10 2 70.53 76.16 4.32 o 0 10 2 133.93 127.78 6.32 o 1 10 2 2.43 3.17 3.24 o 2 10 2 58.41 58.30 6.32 o 3 10 2 1.48 4.10 5.71 o -3 11 2 63.44 58.51 7.48 o -2 11 2 7.66 9.68 5.54 o -1 11 2 495.54 504.97 20.85 o 0 11 2 2.41 8.53 4.33 o 1 11 2 566.33 579.14 16.80 o 2 11 2 14.16 11.89 5.97 o -2 12 2 86.17 80.85 9.72 o -1 12 2 91.11 90.88 6.22 o 0 12 2 30.05 27.75 4.81 o 1 12 2 2.82 12.14 4.72 o 2 12 2 20.71 25.87 6.79 o -1 13 2 99.85 99.14 20.37 o 0 13 2 169.09 153.59 8.28 o 1 13 2 113.56 112.78 7.51 o -1 -6 3 702.58 607.90 39.89 o 3 -5 3 135.91 156.00 15.03 o -2 -4 3 129.54 118.28 8.38 o -1 -4 3 1376.63 1288.94 78.75 o 2 -4 3 1855.61 1833.23 89.06 o 3 -4 3 189.04 186.32 16.05 o 4 -4 3 125.10 120.86 16.54 o -5 -3 3 7.23 -8.77 15.88 o -4 -3 3 78.95 72.96 14.73 o -3 -3 3 409.48 364.53 23.11 o -1 -3 3 1214.03 1154.24 62.22 o 1 -3 3 2884.55 2806.49 135.50 o 2 -3 3 292.14 299.90 20.43 o 3 -3 3 24.98 20.46 8.65 o 4 -3 3 19.35 27.98 11.62 o -5 -2 3 12.50 8.11 16.10 o -4 -2 3 65.51 55.55 13.61 o -3 -2 3 89.23 87.90 10.42 o -2 -2 3 2175.36 2128.69 73.33 o 1 -2 3 3825.55 3965.12 182.06 o 2 -2 3 930.15 920.83 35.12 o 3 -2 3 553.91 500.90 19.74 o 4 -2 3 29.39 26.35 11.47 o 5 -2 3 56.98 60.73 15.90 o -5 -1 3 0.49 6.45 15.56 o -4 -1 3 134.38 140.24 15.59 o -3 -1 3 41.87 50.56 5.56 o -2 -1 3 3291.53 3188.88 104.24 o 1 -1 3 929.74 938.84 35.53 o 2 -1 3 511.75 505.12 18.70 o 3 -1 3 23.18 29.09 5.05 o 4 -1 3 23.17 26.96 11.40 o 5 -1 3 22.04 28.00 13.98 o -5 0 3 18.69 20.85 15.46 o -4 0 3 1.33 8.85 6.28 o -3 0 3 1.91 2.90 4.27 o -2 0 3 1624.48 1504.71 47.58 o -1 0 3 375.74 349.89 9.39 o 0 0 3 29.59 21.45 4.48 o 1 0 3 3703.14 3875.14 204.24 o 2 0 3 818.10 851.56 21.80 o 3 0 3 803.18 759.64 28.61 o 4 0 3 18.47 14.36 6.50 o 5 0 3 38.48 69.40 15.73 o -5 1 3 0.00 9.01 14.51 o -4 1 3 130.43 134.54 10.13 o -3 1 3 64.12 73.58 6.35 o -2 1 3 2806.31 2867.12 73.71 o -1 1 3 20.38 20.81 1.51 o 0 1 3 8028.65 7549.35 197.07 o 1 1 3 722.88 764.12 47.05 o 2 1 3 494.78 493.19 13.11 o 3 1 3 36.07 44.88 6.42 o 4 1 3 16.89 24.82 6.97 o 5 1 3 21.68 29.15 15.20 o -5 2 3 11.06 11.86 8.56 o -4 2 3 60.87 71.48 7.89 o -3 2 3 97.30 99.12 7.30 o -2 2 3 1979.31 2061.23 51.80 o -1 2 3 145.61 158.39 4.67 o 0 2 3 3318.79 3312.88 84.82 o 1 2 3 3986.08 3882.63 118.26 o 2 2 3 947.92 963.13 24.12 o 3 2 3 514.55 498.27 20.10 o 4 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