#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/66/2206624.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206624_Fobs loop_ _publ_author_name 'Nengfang, She' 'Guo, Huizhen' 'Yin, Guodong' 'Wu, Anxin' _publ_section_title ; 2,2,6,6-Tetramethylpiperidin-4-ol ; _journal_coeditor_code BH6018 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2902 _journal_page_last o2903 _journal_volume 61 _journal_year 2005 _space_group_IT_number 64 _symmetry_space_group_name_Hall '-C 2ac 2' _symmetry_space_group_name_H-M 'C m c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.1493 _cell_length_b 10.1346 _cell_length_c 13.3806 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file bh6018Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' t in Cmca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 212.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 38431.90 43357.85 475.25 o 4 0 0 4713.20 4721.90 94.81 o 6 0 0 1638.75 1684.83 68.42 o 8 0 0 2213.40 2319.14 93.66 o 10 0 0 4461.17 4328.82 145.37 o 12 0 0 4214.13 4501.55 165.35 o 14 0 0 74.95 78.88 29.98 o 16 0 0 37.89 37.81 24.02 o 18 0 0 9.38 28.62 24.13 o 0 2 0 45284.33 41855.02 300.81 o 2 2 0 6948.21 6475.42 116.68 o 4 2 0 4597.84 4494.10 87.95 o 6 2 0 4906.10 5294.09 73.53 o 8 2 0 26.33 26.90 13.01 o 10 2 0 1427.29 1432.01 60.00 o 12 2 0 896.82 772.23 48.97 o 14 2 0 27.79 35.89 15.35 o 16 2 0 96.07 93.02 25.26 o 0 4 0 8201.38 8416.43 320.83 o 2 4 0 65.94 63.57 7.75 o 4 4 0 2800.09 3002.08 44.50 o 6 4 0 14005.94 14695.83 352.94 o 8 4 0 1571.72 1443.90 97.03 o 10 4 0 16.18 13.32 9.84 o 12 4 0 0.99 8.20 10.72 o 14 4 0 0.04 -9.32 8.83 o 16 4 0 195.13 264.25 44.14 o 0 6 0 63.70 76.77 14.82 o 2 6 0 14.67 10.10 4.99 o 4 6 0 739.47 671.12 25.25 o 6 6 0 2442.60 2349.34 48.96 o 8 6 0 1019.01 1073.51 45.26 o 10 6 0 17.01 17.16 9.83 o 12 6 0 79.99 109.52 25.73 o 14 6 0 21.52 23.63 16.90 o 16 6 0 144.24 217.49 42.58 o 0 8 0 1970.45 1828.85 66.39 o 2 8 0 148.12 124.89 15.34 o 4 8 0 162.80 160.70 21.58 o 6 8 0 28.85 25.28 11.02 o 8 8 0 17.30 33.79 12.44 o 10 8 0 124.01 163.88 25.89 o 12 8 0 221.94 316.98 45.37 o 14 8 0 6.70 -1.25 16.53 o 0 10 0 566.75 613.39 44.68 o 2 10 0 103.38 121.24 20.97 o 4 10 0 32.60 48.23 14.91 o 6 10 0 4.55 7.18 10.07 o 8 10 0 41.25 53.88 16.40 o 10 10 0 64.83 68.45 20.05 o 0 12 0 4.53 5.22 17.86 o 2 12 0 19.52 24.27 13.97 o 4 12 0 3.77 -2.69 12.10 o 6 12 0 1.12 13.89 17.04 o 1 1 1 2059.21 1982.81 26.24 o 3 1 1 871.48 567.90 156.36 o 5 1 1 6498.31 6801.39 57.25 o 7 1 1 1164.45 1278.72 32.62 o 9 1 1 17.06 16.28 6.09 o 11 1 1 250.79 246.09 22.14 o 13 1 1 155.07 183.71 21.57 o 15 1 1 1.14 -0.56 6.63 o 17 1 1 9.53 17.70 10.40 o 0 2 1 1238.25 1214.41 19.71 o 2 2 1 7150.29 5824.22 647.37 o 4 2 1 860.07 725.87 14.73 o 6 2 1 4.37 2.54 3.16 o 8 2 1 1081.20 1053.64 28.79 o 10 2 1 289.39 317.83 23.14 o 12 2 1 21.19 28.95 9.22 o 14 2 1 84.20 76.84 14.87 o 16 2 1 25.44 33.86 11.74 o 1 3 1 1485.90 1500.13 22.20 o 3 3 1 2321.59 2377.95 23.84 o 5 3 1 5111.15 5380.49 82.46 o 7 3 1 474.38 521.60 15.37 o 9 3 1 2.92 -0.84 3.75 o 11 3 1 424.50 350.64 26.16 o 13 3 1 243.78 226.96 24.02 o 15 3 1 0.80 -1.13 7.77 o 17 3 1 8.12 18.43 11.97 o 0 4 1 0.82 -0.21 2.59 o 2 4 1 163.97 137.31 24.91 o 4 4 1 643.81 660.59 14.68 o 6 4 1 10.68 4.34 2.84 o 8 4 1 13.15 13.34 5.28 o 10 4 1 34.53 30.87 6.97 o 12 4 1 2.62 4.37 6.68 o 14 4 1 3.73 -2.47 6.88 o 16 4 1 0.17 2.50 8.83 o 1 5 1 0.55 4.46 2.60 o 3 5 1 74.04 73.33 6.73 o 5 5 1 427.21 407.59 14.14 o 7 5 1 210.22 222.72 13.95 o 9 5 1 100.72 103.58 13.10 o 11 5 1 9.39 2.47 6.13 o 13 5 1 0.75 5.68 7.38 o 15 5 1 0.02 10.79 9.36 o 0 6 1 132.78 68.69 34.00 o 2 6 1 764.27 614.45 83.46 o 4 6 1 371.72 350.61 13.11 o 6 6 1 24.02 41.11 7.10 o 8 6 1 514.68 525.22 22.55 o 10 6 1 186.58 177.83 18.81 o 12 6 1 15.78 13.69 8.53 o 14 6 1 3.70 7.78 9.84 o 1 7 1 1.72 2.18 3.61 o 3 7 1 187.86 171.69 11.68 o 5 7 1 1084.19 1006.61 26.58 o 7 7 1 141.83 130.61 14.16 o 9 7 1 83.10 78.00 11.91 o 11 7 1 4.89 11.64 8.15 o 13 7 1 43.38 48.49 14.57 o 15 7 1 2.84 -1.12 10.44 o 0 8 1 0.12 0.73 5.10 o 2 8 1 5.55 2.70 3.89 o 4 8 1 17.77 15.99 5.84 o 6 8 1 11.47 7.72 5.95 o 8 8 1 51.45 41.51 9.34 o 10 8 1 2.68 1.69 6.88 o 12 8 1 17.21 14.76 9.79 o 14 8 1 6.80 -0.13 13.49 o 1 9 1 90.70 108.51 10.99 o 3 9 1 84.28 101.29 12.00 o 5 9 1 73.03 82.19 12.32 o 7 9 1 0.95 4.82 6.05 o 9 9 1 0.00 -2.56 6.25 o 11 9 1 2.50 -1.74 9.89 o 0 10 1 52.44 41.07 11.35 o 2 10 1 162.95 163.17 15.12 o 4 10 1 74.12 87.92 13.21 o 6 10 1 3.06 1.39 6.89 o 8 10 1 13.82 42.43 12.48 o 10 10 1 31.47 57.78 15.20 o 1 11 1 5.79 10.38 7.87 o 3 11 1 10.88 11.45 7.83 o 5 11 1 1.72 1.06 8.69 o 7 11 1 4.78 11.20 10.58 o 9 11 1 10.04 14.33 11.14 o 0 12 1 34.35 39.60 24.70 o 2 12 1 18.42 22.77 11.77 o 4 12 1 1.12 -1.31 9.16 o 6 12 1 0.01 -2.12 10.35 o 0 0 2 4701.79 4456.40 286.38 o 2 0 2 4092.27 3831.44 65.86 o 4 0 2 142.06 147.20 11.89 o 6 0 2 973.30 984.34 28.32 o 8 0 2 91.45 93.52 16.96 o 10 0 2 339.64 334.71 33.22 o 12 0 2 531.08 517.48 66.42 o 14 0 2 58.94 40.29 16.65 o 16 0 2 25.26 28.17 15.49 o 1 1 2 18900.29 17124.28 347.74 o 3 1 2 9599.35 9778.84 101.67 o 5 1 2 2014.24 2062.27 45.97 o 7 1 2 33.78 46.31 7.13 o 9 1 2 2.98 9.37 5.44 o 11 1 2 547.64 488.94 26.35 o 13 1 2 64.63 57.74 12.78 o 15 1 2 113.95 116.47 18.83 o 17 1 2 2.62 0.40 8.38 o 0 2 2 6126.78 5793.99 234.77 o 2 2 2 1313.07 1277.56 21.28 o 4 2 2 804.48 878.22 13.37 o 6 2 2 2017.97 2100.31 40.57 o 8 2 2 175.34 182.22 14.43 o 10 2 2 242.13 258.15 21.61 o 12 2 2 290.59 306.66 25.99 o 14 2 2 9.51 11.76 7.83 o 16 2 2 44.16 62.43 15.39 o 1 3 2 1696.09 1334.56 171.42 o 3 3 2 6052.45 6135.10 62.47 o 5 3 2 212.91 206.59 28.63 o 7 3 2 81.25 111.60 8.23 o 9 3 2 974.43 1038.25 31.29 o 11 3 2 234.93 224.52 19.52 o 13 3 2 57.79 52.38 12.53 o 15 3 2 9.48 17.18 9.67 o 17 3 2 47.27 47.88 15.39 o 0 4 2 4610.79 4743.89 91.44 o 2 4 2 81.85 91.14 6.38 o 4 4 2 2739.03 2434.68 291.63 o 6 4 2 1592.85 1664.38 26.95 o 8 4 2 62.78 70.29 9.31 o 10 4 2 112.16 103.90 12.11 o 12 4 2 64.80 85.32 14.89 o 14 4 2 7.11 9.32 8.82 o 16 4 2 55.48 86.96 18.26 o 1 5 2 4.42 1.24 2.37 o 3 5 2 907.81 938.91 25.36 o 5 5 2 487.47 522.69 14.46 o 7 5 2 690.47 481.67 86.13 o 9 5 2 40.64 30.24 7.41 o 11 5 2 51.77 58.57 11.50 o 13 5 2 8.83 4.54 8.30 o 15 5 2 0.07 2.36 8.58 o 0 6 2 736.92 777.05 26.06 o 2 6 2 32.68 29.91 5.18 o 4 6 2 595.02 560.19 25.85 o 6 6 2 417.07 385.43 16.37 o 8 6 2 5.88 2.18 4.69 o 10 6 2 42.07 50.54 11.43 o 12 6 2 18.77 26.95 9.45 o 14 6 2 3.97 4.77 9.54 o 1 7 2 66.96 63.38 10.97 o 3 7 2 1051.63 1023.12 24.95 o 5 7 2 805.51 739.18 23.08 o 7 7 2 601.06 460.39 77.90 o 9 7 2 220.34 277.95 23.03 o 11 7 2 19.42 28.30 10.19 o 13 7 2 1.10 -2.63 7.61 o 15 7 2 81.86 139.51 28.78 o 0 8 2 48.69 47.89 10.59 o 2 8 2 44.20 46.53 7.26 o 4 8 2 0.72 -1.31 4.07 o 6 8 2 17.75 18.46 7.58 o 8 8 2 0.41 -0.65 5.27 o 10 8 2 21.41 29.72 10.53 o 12 8 2 24.63 40.60 14.04 o 14 8 2 3.22 10.39 14.32 o 1 9 2 88.49 65.44 13.32 o 3 9 2 279.85 257.79 44.83 o 5 9 2 175.93 189.96 17.68 o 7 9 2 23.66 17.41 7.85 o 9 9 2 10.57 8.28 9.96 o 11 9 2 12.90 13.76 11.31 o 0 10 2 14.55 12.65 9.67 o 2 10 2 46.20 49.11 9.18 o 4 10 2 48.73 42.70 10.92 o 6 10 2 2.42 8.63 7.84 o 8 10 2 1.20 0.34 8.28 o 10 10 2 17.25 10.71 11.76 o 1 11 2 143.02 203.62 21.25 o 3 11 2 66.71 88.45 15.26 o 5 11 2 3.34 11.28 9.68 o 7 11 2 19.86 34.45 12.92 o 9 11 2 44.05 88.22 20.63 o 0 12 2 1.37 1.24 15.43 o 2 12 2 1.46 1.40 12.59 o 4 12 2 0.23 6.83 11.93 o 6 12 2 0.37 3.91 10.80 o 1 1 3 5958.62 4336.60 869.73 o 3 1 3 1.12 3.89 1.86 o 5 1 3 960.05 1011.02 18.25 o 7 1 3 681.28 643.08 60.40 o 9 1 3 50.57 41.26 7.97 o 11 1 3 202.96 190.79 19.94 o 13 1 3 44.74 54.74 12.15 o 15 1 3 2.84 2.02 7.29 o 17 1 3 12.89 15.13 10.51 o 0 2 3 1340.24 1264.02 21.70 o 2 2 3 0.78 2.21 1.96 o 4 2 3 1122.10 1165.60 20.93 o 6 2 3 2028.65 2196.59 36.62 o 8 2 3 111.19 64.62 24.12 o 10 2 3 0.03 -0.08 4.25 o 12 2 3 667.64 668.01 32.64 o 14 2 3 25.20 24.41 9.78 o 16 2 3 2.80 1.67 8.00 o 1 3 3 4543.46 4738.92 88.38 o 3 3 3 66.50 78.12 6.87 o 5 3 3 389.33 401.00 14.24 o 7 3 3 397.41 393.82 16.00 o 9 3 3 193.99 135.72 28.85 o 11 3 3 276.65 279.53 21.58 o 13 3 3 48.23 47.46 12.07 o 15 3 3 2.32 -0.27 7.42 o 17 3 3 11.78 16.43 11.61 o 0 4 3 3459.35 3664.81 68.30 o 2 4 3 2052.80 2093.82 32.76 o 4 4 3 884.43 865.76 21.00 o 6 4 3 94.50 94.84 9.74 o 8 4 3 33.36 20.47 5.54 o 10 4 3 301.19 221.02 37.95 o 12 4 3 423.63 411.05 26.30 o 14 4 3 55.36 57.81 14.21 o 16 4 3 0.62 5.68 9.53 o 1 5 3 18.36 22.41 4.12 o 3 5 3 7.26 22.10 4.11 o 5 5 3 433.49 431.68 16.94 o 7 5 3 99.42 65.76 8.93 o 9 5 3 59.75 56.15 9.44 o 11 5 3 0.85 4.85 6.45 o 13 5 3 2.93 5.48 7.71 o 15 5 3 0.01 2.61 10.63 o 0 6 3 1182.94 1237.80 40.92 o 2 6 3 813.51 777.53 18.58 o 4 6 3 122.13 114.16 10.29 o 6 6 3 822.54 622.50 104.34 o 8 6 3 75.24 83.81 11.25 o 10 6 3 310.46 320.17 24.41 o 12 6 3 5.29 -2.24 6.37 o 14 6 3 2.73 3.37 8.89 o 1 7 3 76.39 87.87 8.57 o 3 7 3 37.35 38.05 6.86 o 5 7 3 352.59 246.34 41.45 o 7 7 3 163.12 166.21 16.45 o 9 7 3 0.04 0.24 5.75 o 11 7 3 2.57 3.68 8.40 o 13 7 3 6.69 10.59 10.59 o 0 8 3 83.90 89.41 13.77 o 2 8 3 54.72 62.91 8.87 o 4 8 3 1260.51 1259.98 36.85 o 6 8 3 1104.20 1059.94 33.27 o 8 8 3 80.52 76.91 15.65 o 10 8 3 1.89 2.09 8.65 o 12 8 3 4.62 6.34 9.99 o 1 9 3 80.50 94.57 11.29 o 3 9 3 15.24 19.30 7.06 o 5 9 3 26.73 24.74 7.84 o 7 9 3 14.93 16.74 10.18 o 9 9 3 0.73 -2.72 9.05 o 11 9 3 31.01 34.56 13.90 o 0 10 3 53.97 58.17 20.32 o 2 10 3 44.49 35.36 8.73 o 4 10 3 361.99 323.51 62.46 o 6 10 3 227.43 227.67 23.69 o 8 10 3 129.48 140.26 22.30 o 10 10 3 2.27 2.21 10.59 o 1 11 3 63.15 84.96 17.11 o 3 11 3 5.88 6.36 10.71 o 5 11 3 26.14 23.61 12.33 o 7 11 3 6.41 12.31 12.16 o 0 12 3 160.12 182.96 36.21 o 2 12 3 68.83 98.96 23.67 o 4 12 3 1.01 1.96 12.57 o 6 12 3 10.86 24.13 19.04 o 0 0 4 16270.58 16019.07 1474.99 o 2 0 4 98.55 94.14 7.57 o 4 0 4 596.51 566.08 18.75 o 6 0 4 4845.23 4121.05 678.31 o 8 0 4 247.49 312.85 19.63 o 10 0 4 47.65 56.49 15.30 o 12 0 4 268.73 263.66 34.40 o 14 0 4 17.42 15.69 13.36 o 16 0 4 0.00 9.12 14.00 o 1 1 4 3679.01 2958.99 530.34 o 3 1 4 36.80 52.77 4.56 o 5 1 4 65.08 79.59 6.45 o 7 1 4 781.79 819.31 19.74 o 9 1 4 132.51 128.99 12.95 o 11 1 4 0.50 -0.67 5.17 o 13 1 4 3.82 8.92 7.20 o 15 1 4 24.62 40.62 12.94 o 17 1 4 22.76 25.21 12.63 o 0 2 4 68.76 69.27 5.54 o 2 2 4 24.59 23.67 2.75 o 4 2 4 82.32 104.31 7.64 o 6 2 4 41.49 27.66 5.89 o 8 2 4 51.46 64.81 9.29 o 10 2 4 10.25 10.93 5.20 o 12 2 4 0.66 2.72 6.34 o 14 2 4 3.98 4.83 7.77 o 16 2 4 0.03 -2.25 8.44 o 1 3 4 872.97 895.54 18.37 o 3 3 4 103.79 101.47 7.40 o 5 3 4 341.48 357.97 13.67 o 7 3 4 24.88 27.15 6.02 o 9 3 4 55.03 63.22 9.23 o 11 3 4 44.19 22.89 15.99 o 13 3 4 0.09 7.25 7.09 o 15 3 4 8.89 19.34 10.53 o 17 3 4 2.30 0.81 12.75 o 0 4 4 4550.29 4597.30 60.39 o 2 4 4 49.81 40.37 5.52 o 4 4 4 36.42 50.59 6.68 o 6 4 4 1261.34 1257.25 28.24 o 8 4 4 1.89 1.52 4.00 o 10 4 4 0.34 -1.73 4.43 o 12 4 4 163.25 68.53 39.29 o 14 4 4 0.05 4.26 9.70 o 16 4 4 0.25 -4.50 10.96 o 1 5 4 2275.97 2368.15 43.79 o 3 5 4 54.74 59.19 7.44 o 5 5 4 68.63 68.20 8.62 o 7 5 4 233.32 241.38 15.68 o 9 5 4 244.85 244.59 21.56 o 11 5 4 75.33 81.49 11.73 o 13 5 4 6.01 13.70 9.96 o 15 5 4 0.02 0.97 11.88 o 0 6 4 5.30 1.22 4.64 o 2 6 4 4.37 12.25 4.27 o 4 6 4 5.93 3.80 3.90 o 6 6 4 19.07 19.31 6.00 o 8 6 4 3.32 7.76 6.25 o 10 6 4 2.43 4.65 6.31 o 12 6 4 0.23 4.13 8.21 o 14 6 4 2.82 1.68 9.85 o 1 7 4 192.95 202.52 12.23 o 3 7 4 10.21 17.94 5.81 o 5 7 4 2.50 2.54 5.22 o 7 7 4 45.26 24.92 9.81 o 9 7 4 28.62 42.40 10.45 o 11 7 4 11.71 20.74 10.82 o 13 7 4 4.82 4.44 10.08 o 0 8 4 361.34 324.67 21.87 o 2 8 4 0.04 5.00 4.83 o 4 8 4 18.98 17.40 7.27 o 6 8 4 77.64 81.65 13.47 o 8 8 4 4.84 9.15 8.49 o 10 8 4 1.77 -0.49 8.31 o 12 8 4 19.47 15.60 11.60 o 1 9 4 50.51 57.31 13.09 o 3 9 4 7.80 12.14 6.78 o 5 9 4 2.23 5.16 6.78 o 7 9 4 18.64 19.88 10.27 o 9 9 4 13.12 19.88 11.03 o 11 9 4 0.91 5.46 10.84 o 0 10 4 1.76 8.54 12.09 o 2 10 4 29.47 35.22 11.79 o 4 10 4 57.10 70.57 15.69 o 6 10 4 19.22 8.52 11.80 o 8 10 4 14.14 13.39 10.97 o 10 10 4 12.88 3.29 11.35 o 1 11 4 43.44 51.65 14.56 o 3 11 4 0.55 -0.71 9.34 o 5 11 4 5.36 5.98 13.13 o 7 11 4 31.12 30.05 17.93 o 0 12 4 6.85 9.40 16.01 o 2 12 4 1.84 6.18 13.25 o 4 12 4 0.55 -5.22 12.23 o 1 1 5 883.14 940.79 18.08 o 3 1 5 438.62 463.92 10.94 o 5 1 5 1252.85 1272.54 21.71 o 7 1 5 261.96 250.27 11.87 o 9 1 5 2.63 6.42 4.75 o 11 1 5 143.56 126.78 14.65 o 13 1 5 72.71 71.38 14.16 o 15 1 5 6.03 8.99 9.06 o 17 1 5 2.58 1.13 10.57 o 0 2 5 7271.95 7748.66 100.70 o 2 2 5 23.54 17.63 3.45 o 4 2 5 1755.12 1731.87 30.51 o 6 2 5 34.34 33.54 5.78 o 8 2 5 3.62 6.44 4.61 o 10 2 5 78.81 64.19 10.76 o 12 2 5 108.61 53.87 21.39 o 14 2 5 13.93 23.49 10.39 o 16 2 5 1.55 -5.81 10.78 o 1 3 5 1030.33 1150.94 32.46 o 3 3 5 253.38 261.22 8.22 o 5 3 5 749.52 722.83 19.29 o 7 3 5 67.29 62.86 8.33 o 9 3 5 10.18 12.65 5.60 o 11 3 5 246.01 239.62 18.20 o 13 3 5 108.35 127.28 16.86 o 15 3 5 11.04 13.48 12.52 o 0 4 5 3143.69 3515.25 149.35 o 2 4 5 543.64 509.39 17.96 o 4 4 5 133.04 152.25 10.34 o 6 4 5 137.00 138.21 11.66 o 8 4 5 120.71 135.45 12.81 o 10 4 5 246.80 249.30 20.69 o 12 4 5 78.42 71.12 13.15 o 14 4 5 5.95 4.63 8.74 o 16 4 5 2.68 -3.75 11.32 o 1 5 5 8.95 13.54 4.23 o 3 5 5 6.85 4.45 3.67 o 5 5 5 256.33 232.86 17.10 o 7 5 5 123.77 109.61 13.22 o 9 5 5 54.48 52.79 10.57 o 11 5 5 10.68 10.85 7.04 o 13 5 5 0.33 3.64 8.52 o 15 5 5 0.60 -3.00 9.21 o 0 6 5 297.07 316.42 27.14 o 2 6 5 397.92 441.74 20.77 o 4 6 5 1.61 5.12 4.67 o 6 6 5 351.15 350.14 21.84 o 8 6 5 0.05 1.21 5.41 o 10 6 5 92.62 75.88 13.57 o 12 6 5 39.30 14.59 9.49 o 14 6 5 15.09 26.70 12.87 o 1 7 5 12.68 10.51 6.57 o 3 7 5 0.09 2.99 4.87 o 5 7 5 292.81 257.66 20.62 o 7 7 5 27.85 33.57 10.11 o 9 7 5 97.35 95.98 15.38 o 11 7 5 0.46 -1.91 8.47 o 13 7 5 7.95 9.77 11.56 o 0 8 5 34.21 24.63 12.59 o 2 8 5 0.81 1.83 6.13 o 4 8 5 271.60 241.70 24.53 o 6 8 5 556.95 534.07 27.70 o 8 8 5 209.90 213.04 21.86 o 10 8 5 11.20 13.88 10.46 o 12 8 5 58.63 73.00 18.80 o 1 9 5 63.57 63.99 13.43 o 3 9 5 12.64 10.68 8.28 o 5 9 5 9.99 13.99 9.66 o 7 9 5 0.63 -1.79 7.84 o 9 9 5 0.01 0.09 9.96 o 11 9 5 2.02 6.40 10.90 o 0 10 5 272.59 276.57 41.23 o 2 10 5 2.92 7.10 9.08 o 4 10 5 261.83 276.09 29.30 o 6 10 5 286.66 272.68 35.28 o 8 10 5 64.00 70.12 20.52 o 10 10 5 42.59 63.17 20.69 o 1 11 5 0.26 16.22 10.46 o 3 11 5 33.15 38.85 14.35 o 5 11 5 7.57 10.51 14.14 o 7 11 5 13.01 25.91 15.58 o 0 12 5 335.97 386.37 53.43 o 2 12 5 102.53 136.04 24.15 o 4 12 5 24.09 29.91 17.07 o 0 0 6 12754.83 13610.89 963.58 o 2 0 6 2613.63 2816.02 104.91 o 4 0 6 122.78 121.27 11.40 o 6 0 6 83.80 81.11 11.33 o 8 0 6 402.18 384.12 21.56 o 10 0 6 250.11 129.86 111.93 o 12 0 6 199.47 189.03 30.33 o 14 0 6 82.62 118.82 27.14 o 16 0 6 3.69 2.60 14.83 o 1 1 6 1839.48 2076.90 22.19 o 3 1 6 298.78 296.03 9.36 o 5 1 6 1.29 1.90 2.82 o 7 1 6 5.47 6.13 3.78 o 9 1 6 15.53 9.98 5.53 o 11 1 6 347.09 355.83 25.08 o 13 1 6 160.19 84.80 46.75 o 15 1 6 13.38 13.95 12.70 o 0 2 6 2007.11 680.42 972.34 o 2 2 6 292.62 267.77 29.57 o 4 2 6 95.33 62.15 10.70 o 6 2 6 1.34 7.00 3.87 o 8 2 6 4.40 4.57 4.58 o 10 2 6 32.23 34.80 8.31 o 12 2 6 93.84 98.76 19.58 o 14 2 6 31.94 39.09 14.69 o 16 2 6 0.00 0.54 12.73 o 1 3 6 1660.24 1850.43 41.57 o 3 3 6 950.25 934.99 19.40 o 5 3 6 218.80 211.21 11.57 o 7 3 6 50.33 38.18 8.22 o 9 3 6 424.53 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39.68 o 4 2 8 307.06 350.21 16.57 o 6 2 8 856.15 823.14 26.74 o 8 2 8 64.02 71.03 11.10 o 10 2 8 286.05 136.97 80.69 o 12 2 8 367.71 361.20 35.44 o 14 2 8 13.20 8.28 13.10 o 1 3 8 51.06 51.63 10.66 o 3 3 8 75.76 33.29 21.20 o 5 3 8 275.25 199.92 46.13 o 7 3 8 38.50 36.06 8.56 o 9 3 8 3.94 3.21 5.54 o 11 3 8 1.02 7.36 7.88 o 13 3 8 0.83 10.42 9.95 o 15 3 8 9.08 18.69 12.90 o 0 4 8 52.50 60.02 15.65 o 2 4 8 0.17 -0.73 4.56 o 4 4 8 1948.06 1808.30 47.69 o 6 4 8 3535.66 3499.61 67.03 o 8 4 8 107.93 95.21 12.99 o 10 4 8 108.16 102.82 15.06 o 12 4 8 0.04 0.42 8.64 o 14 4 8 3.47 0.81 10.55 o 1 5 8 53.26 32.78 9.10 o 3 5 8 263.38 241.86 21.98 o 5 5 8 122.53 112.14 16.04 o 7 5 8 0.78 2.16 6.90 o 9 5 8 2.21 2.44 7.21 o 11 5 8 0.27 3.16 7.58 o 13 5 8 0.06 0.93 10.19 o 0 6 8 480.88 407.69 37.45 o 2 6 8 32.84 33.01 9.47 o 4 6 8 548.03 520.81 28.98 o 6 6 8 615.90 584.70 31.51 o 8 6 8 22.58 13.71 8.46 o 10 6 8 48.71 63.87 14.87 o 12 6 8 18.50 18.75 11.85 o 1 7 8 62.44 69.29 13.73 o 3 7 8 2.82 0.44 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1 13 4.67 1.10 13.37 o 0 2 13 35.20 39.90 23.82 o 2 2 13 143.73 153.31 22.84 o 4 2 13 141.81 154.96 23.69 o 6 2 13 62.32 57.56 20.73 o 8 2 13 91.99 102.28 40.12 o 10 2 13 29.74 34.47 29.25 o 1 3 13 148.90 147.58 28.29 o 3 3 13 5.23 1.69 8.85 o 5 3 13 3.06 8.05 11.04 o 7 3 13 49.89 36.25 27.79 o 9 3 13 6.91 12.01 21.52 o 0 4 13 8.42 17.02 17.96 o 2 4 13 0.14 2.19 10.48 o 4 4 13 41.88 46.95 18.61 o 6 4 13 99.35 129.94 23.41 o 8 4 13 18.72 16.12 16.99 o 10 4 13 0.68 -0.45 13.90 o 1 5 13 15.40 26.37 16.85 o 3 5 13 0.00 -4.23 8.48 o 5 5 13 2.08 7.10 10.71 o 7 5 13 4.97 6.77 12.16 o 9 5 13 0.70 -1.02 15.65 o 0 6 13 176.34 229.19 38.41 o 2 6 13 97.00 106.66 22.36 o 4 6 13 6.06 17.74 13.36 o 6 6 13 70.45 89.65 21.16 o 8 6 13 0.97 14.92 13.03 o 1 7 13 18.30 15.19 10.72 o 3 7 13 27.35 39.72 13.42 o 5 7 13 2.11 5.13 15.61 o 0 8 13 184.88 263.06 44.41 o 2 8 13 30.72 30.33 14.15 o 0 0 14 2.23 12.01 17.86 o 2 0 14 33.92 66.12 29.14 o 4 0 14 134.12 165.62 45.66 o 6 0 14 65.25 78.56 35.00 o 8 0 14 3.27 -1.46 18.70 o 10 0 14 1.62 22.98 24.86 o 1 1 14 10.16 22.87 11.36 o 3 1 14 0.66 -7.67 10.63 o 5 1 14 0.29 0.38 12.09 o 7 1 14 7.74 33.32 16.47 o 9 1 14 1.47 3.05 13.76 o 0 2 14 5.06 0.31 15.88 o 2 2 14 9.87 17.22 10.98 o 4 2 14 22.33 18.61 14.89 o 6 2 14 7.14 11.78 14.20 o 8 2 14 2.52 1.87 12.16 o 1 3 14 33.23 52.90 19.40 o 3 3 14 40.09 54.61 17.13 o 5 3 14 0.20 8.69 13.44 o 7 3 14 0.46 7.09 13.34 o 9 3 14 11.36 4.60 23.50 o 0 4 14 1.54 11.91 19.64 o 2 4 14 0.37 4.21 12.07 o 4 4 14 21.07 39.89 19.14 o 6 4 14 27.26 52.43 30.92 o 8 4 14 0.26 11.07 20.78 o 1 5 14 2.22 6.05 12.70 o 3 5 14 3.35 4.80 11.70 o 5 5 14 23.67 47.69 18.36 o 7 5 14 7.99 12.64 22.04 o 0 6 14 3.59 -0.21 18.80 o 2 6 14 4.62 15.53 13.84 o 4 6 14 25.54 30.20 18.24 o 6 6 14 26.03 37.25 17.49 o 1 7 14 10.58 11.73 16.53 o 3 7 14 54.38 71.23 21.16 o 1 1 15 7.51 4.01 12.95 o 3 1 15 3.19 1.03 12.91 o 5 1 15 0.06 2.42 13.40 o 7 1 15 5.81 17.82 16.27 o 0 2 15 14.73 9.50 18.70 o 2 2 15 2.76 -0.84 12.76 o 4 2 15 0.99 4.76 14.00 o 6 2 15 48.85 33.27 18.80 o 8 2 15 12.43 4.04 16.57 o 1 3 15 51.06 41.94 20.24 o 3 3 15 28.01 25.63 22.20 o 5 3 15 25.89 13.10 16.94 o 7 3 15 59.23 103.34 30.33 o 0 4 15 10.86 10.24 17.96 o 2 4 15 12.19 6.02 14.58 o 4 4 15 51.37 54.11 21.03 o 6 4 15 102.54 123.70 32.58 o 1 5 15 3.15 -2.72 12.80 o 3 5 15 13.06 29.54 20.26 o 5 5 15 84.27 102.12 28.70 o 0 6 15 37.25 30.61 28.52 o 2 6 15 1.56 -7.91 14.52 o 2 0 16 36.16 89.10 34.37 o 4 0 16 25.20 60.58 33.22 o 6 0 16 47.62 64.76 35.93 o 1 1 16 20.95 19.32 21.93 o 3 1 16 8.15 12.13 15.30 o 5 1 16 43.59 58.24 24.48 o 0 2 16 41.52 85.65 34.78 o 2 2 16 4.05 -0.42 19.74 o 4 2 16 41.13 83.55 25.99 o 1 3 16 0.30 -1.14 12.39 o 3 3 16 4.27 -15.25 17.86 o 0 4 16 1.78 -1.15 21.20 o 2 4 16 1.48 -0.37 13.41 o