#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:14:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/66/2206630.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206630_Fobs loop_ _publ_author_name 'Reinoso, Santiago' 'Vitoria, Pablo' 'San Felices, Leire' 'Lezama, Luis' 'Guti\'errez-Zorrilla, Juan M.' _publ_section_title ; \m-Oxalato-\k^4^O^1^,O^2^:O^1'^,O^2'^-bis[aqua(2,2'-bipyridyl-\k^2^N,N')copper(II)] bis(hydrogen squarate) ; _journal_coeditor_code BT6702 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1677 _journal_page_last m1679 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.049 _cell_angle_beta 94.860 _cell_angle_gamma 109.283 _cell_length_a 8.0147 _cell_length_b 9.2276 _cell_length_c 21.7280 _exptl_crystal_F_000 524.00 _reflns_d_resolution_high 0.7107 _cod_data_source_file bt6702Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' XYZN file = SHELXL INS file, from DIRDIF output for CUOXBY' _shelx_refln_list_code 4 _shelx_f_calc_maximum 195.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17.64 16.66 5.78 o 3 0 0 958.03 990.18 35.73 o 4 0 0 472.94 490.06 20.14 o 5 0 0 7037.86 6935.57 98.16 o 6 0 0 252.94 238.93 35.66 o 7 0 0 120.36 93.75 35.40 o 8 0 0 1037.76 1039.82 70.40 o 9 0 0 10.62 30.34 34.19 o 10 0 0 105.72 140.95 63.12 o -10 1 0 68.21 82.23 49.43 o -9 1 0 120.82 128.31 46.77 o -8 1 0 87.69 90.57 42.74 o -7 1 0 1.98 63.26 80.79 o -6 1 0 2038.65 2031.66 41.49 o -5 1 0 1240.95 1170.53 38.51 o -4 1 0 111.14 98.11 14.26 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