#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:14:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/66/2206660.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206660_Fobs loop_ _publ_author_name 'Mahendra, M.' 'Khanum, S. A.' 'Singh, A.K.' 'Shashikanth, S.' 'Doreswamy, B. H.' 'Sridhar, M. A.' 'Shashidhara Prasad, J.' _publ_section_title ; (4-Methoxyphenyl)(2-methylphenyl)methanone ; _journal_coeditor_code CI6630 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2990 _journal_page_last o2991 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.231 _cell_angle_gamma 90.000 _cell_length_a 7.592 _cell_length_b 14.147 _cell_length_c 11.342 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8400 _cod_data_source_file ci6630Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ssk15' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 4.29 3.63 0.23 o 4 0 0 188.00 201.39 3.46 o 5 0 0 149.24 150.35 2.73 o 6 0 0 408.47 412.11 8.92 o 7 0 0 338.53 352.91 5.54 o 8 0 0 76.57 72.19 1.67 o 9 0 0 29.31 28.38 1.15 o 1 1 0 498.71 505.08 8.93 o 2 1 0 10565.67 18515.72 490.35 o 3 1 0 78.68 66.72 0.79 o 4 1 0 52.67 61.69 0.80 o 5 1 0 180.62 172.56 2.47 o 6 1 0 15.70 14.22 0.42 o 7 1 0 0.65 0.01 0.41 o 8 1 0 1.27 0.69 0.35 o 0 2 0 323.01 44.85 5.64 o 1 2 0 150.81 145.22 1.87 o 2 2 0 541.00 518.51 10.26 o 3 2 0 208.20 198.67 3.07 o 4 2 0 92.57 92.18 1.10 o 5 2 0 42.52 39.17 1.04 o 6 2 0 9.07 8.80 0.45 o 7 2 0 13.62 13.11 0.72 o 8 2 0 1.78 3.26 0.59 o 1 3 0 147.87 150.95 1.80 o 2 3 0 617.00 594.10 8.10 o 3 3 0 84.11 67.58 0.83 o 4 3 0 9.63 10.19 0.37 o 5 3 0 67.97 62.22 0.87 o 6 3 0 25.38 27.82 0.55 o 7 3 0 6.51 6.38 0.36 o 8 3 0 0.37 -0.24 0.40 o 0 4 0 26.28 21.92 0.38 o 1 4 0 167.09 150.89 1.89 o 2 4 0 140.16 126.43 2.18 o 3 4 0 689.79 706.87 20.67 o 4 4 0 52.56 48.10 1.12 o 5 4 0 9.27 11.67 0.33 o 6 4 0 17.27 17.37 0.57 o 7 4 0 5.96 5.47 0.42 o 8 4 0 0.96 1.14 0.71 o 1 5 0 190.53 175.66 2.44 o 2 5 0 647.88 715.14 9.85 o 3 5 0 28.70 28.91 0.67 o 4 5 0 1.88 3.17 0.20 o 5 5 0 194.71 194.15 3.09 o 6 5 0 43.25 41.59 0.71 o 7 5 0 51.48 49.97 0.85 o 8 5 0 24.86 26.07 1.08 o 0 6 0 21.57 20.14 0.38 o 1 6 0 327.48 336.54 4.96 o 2 6 0 1358.82 1536.35 19.61 o 3 6 0 74.03 69.06 1.63 o 4 6 0 180.50 186.61 2.64 o 5 6 0 30.55 30.50 0.75 o 6 6 0 14.21 13.76 0.52 o 7 6 0 3.18 3.95 0.36 o 8 6 0 20.66 18.76 1.26 o 2 7 0 132.73 141.96 3.01 o 3 7 0 70.61 72.15 0.96 o 4 7 0 1.96 2.12 0.20 o 5 7 0 2.57 2.57 0.33 o 6 7 0 9.46 8.87 0.58 o 7 7 0 175.41 188.78 2.33 o 8 7 0 3.02 2.01 0.60 o 0 8 0 9.09 11.23 0.39 o 1 8 0 78.73 96.64 1.36 o 2 8 0 46.40 43.05 1.12 o 3 8 0 210.89 217.70 2.51 o 4 8 0 0.00 0.20 0.21 o 5 8 0 3.34 3.66 0.31 o 6 8 0 21.29 18.15 0.65 o 7 8 0 2.49 1.77 0.34 o 1 9 0 48.32 45.13 1.25 o 2 9 0 2.30 2.64 0.20 o 3 9 0 62.41 64.93 0.90 o 4 9 0 0.80 1.10 0.26 o 5 9 0 0.16 0.03 0.20 o 6 9 0 11.96 13.29 0.41 o 7 9 0 1.67 1.95 0.31 o 0 10 0 13.75 14.19 0.78 o 1 10 0 4.35 3.18 0.13 o 2 10 0 2.46 2.61 0.17 o 3 10 0 97.32 91.75 1.50 o 4 10 0 14.14 13.28 0.33 o 5 10 0 44.31 47.63 0.74 o 6 10 0 0.54 0.88 0.30 o 7 10 0 0.02 0.12 0.26 o 1 11 0 10.04 9.96 0.56 o 2 11 0 69.28 73.55 1.16 o 3 11 0 109.58 117.41 1.67 o 4 11 0 10.86 16.06 0.36 o 5 11 0 0.73 0.53 0.25 o 6 11 0 7.72 6.41 0.33 o 0 12 0 35.65 35.73 1.11 o 1 12 0 3.83 6.50 0.47 o 2 12 0 32.44 26.63 0.44 o 3 12 0 2.69 2.21 0.41 o 4 12 0 99.03 98.21 1.50 o 5 12 0 26.15 28.50 1.02 o 6 12 0 33.72 32.66 1.72 o 1 13 0 6.22 3.72 0.15 o 2 13 0 0.27 1.17 0.13 o 3 13 0 18.60 12.00 0.49 o 4 13 0 33.65 36.15 1.05 o 5 13 0 1.10 1.81 0.22 o 0 14 0 43.48 37.78 0.78 o 1 14 0 5.16 3.38 0.21 o 2 14 0 3.91 4.03 0.21 o 3 14 0 9.91 11.18 0.59 o 4 14 0 2.64 1.47 0.47 o 5 14 0 3.92 4.21 0.33 o 1 15 0 16.65 17.02 0.51 o 2 15 0 1.77 1.69 0.16 o 3 15 0 3.64 1.97 0.17 o 4 15 0 3.28 1.96 0.34 o 0 16 0 3.82 3.00 0.25 o 1 16 0 6.31 6.33 0.23 o 2 16 0 5.59 6.46 0.40 o -9 1 1 7.36 6.20 0.48 o -8 1 1 29.17 24.15 1.37 o -7 1 1 2.51 2.38 0.33 o -6 1 1 118.26 118.93 2.01 o -5 1 1 57.24 57.00 0.78 o -4 1 1 395.32 419.49 5.59 o -3 1 1 1196.99 1273.37 51.94 o -2 1 1 14858.85 29195.13 667.66 o -1 1 1 19.90 16.79 0.29 o 0 1 1 2591.57 -0.02 0.02 o 1 1 1 2072.59 1630.69 64.92 o 2 1 1 1280.00 1391.89 22.75 o 3 1 1 0.02 0.21 0.17 o 4 1 1 1847.38 2045.48 21.46 o 5 1 1 6.63 9.47 0.32 o 6 1 1 57.31 57.79 0.87 o 7 1 1 15.82 16.32 1.03 o 8 1 1 0.06 0.35 0.35 o -8 2 1 22.12 23.32 1.01 o -7 2 1 2.41 2.53 0.40 o -6 2 1 0.01 -0.35 0.23 o -5 2 1 69.22 74.24 1.22 o -4 2 1 123.14 116.61 1.49 o -3 2 1 105.09 105.48 3.65 o -2 2 1 0.82 1.74 0.10 o -1 2 1 1103.18 1222.60 18.94 o 1 2 1 381.90 366.48 4.26 o 2 2 1 1905.13 2025.31 37.45 o 3 2 1 443.12 433.01 5.00 o 4 2 1 1.30 2.34 0.21 o 5 2 1 34.92 36.06 0.59 o 6 2 1 62.66 63.76 1.53 o 7 2 1 36.89 37.08 0.72 o 8 2 1 0.00 0.00 0.40 o -8 3 1 0.28 0.07 0.33 o -7 3 1 1.28 1.38 0.29 o -6 3 1 0.03 0.59 0.27 o -5 3 1 0.07 0.16 0.18 o -4 3 1 1.29 1.33 0.23 o -3 3 1 96.23 87.35 2.82 o -2 3 1 612.56 638.75 7.47 o -1 3 1 234.24 240.11 3.14 o 0 3 1 935.72 971.67 23.43 o 1 3 1 3.17 4.33 0.10 o 2 3 1 43.16 42.53 1.21 o 3 3 1 0.91 1.71 0.15 o 4 3 1 16.69 14.56 0.60 o 5 3 1 23.14 24.56 0.49 o 6 3 1 2.14 1.45 0.28 o 7 3 1 2.07 2.64 0.33 o 8 3 1 0.12 -0.05 0.47 o -8 4 1 12.66 13.15 0.53 o -7 4 1 3.07 2.54 0.34 o -6 4 1 29.06 29.61 0.74 o -5 4 1 6.68 5.61 0.29 o -4 4 1 326.79 333.05 6.04 o -3 4 1 52.19 43.38 0.56 o -2 4 1 360.29 365.33 4.87 o -1 4 1 49.52 53.42 0.74 o 0 4 1 637.32 634.09 13.51 o 1 4 1 1186.29 1243.08 15.76 o 2 4 1 62.93 57.74 0.69 o 3 4 1 9.52 8.22 0.21 o 4 4 1 220.47 221.72 3.95 o 5 4 1 9.56 8.76 0.38 o 6 4 1 41.45 42.72 0.72 o 7 4 1 0.25 0.22 0.33 o 8 4 1 4.23 5.31 0.51 o -8 5 1 5.38 5.26 0.41 o -7 5 1 2.83 2.41 0.38 o -6 5 1 0.00 0.08 0.23 o -5 5 1 391.19 411.73 4.67 o -4 5 1 37.53 37.35 0.65 o -3 5 1 340.48 348.50 7.46 o -2 5 1 75.57 83.70 2.24 o -1 5 1 13.96 12.26 0.24 o 0 5 1 622.53 615.77 13.31 o 1 5 1 1.90 1.25 0.10 o 2 5 1 82.27 100.68 1.60 o 3 5 1 89.45 79.29 1.44 o 4 5 1 49.80 48.93 0.78 o 5 5 1 13.06 13.75 0.53 o 6 5 1 63.16 64.48 1.15 o 7 5 1 71.64 75.84 1.30 o 8 5 1 0.02 0.48 0.37 o -8 6 1 8.16 8.67 1.45 o -7 6 1 7.91 6.97 0.39 o -6 6 1 6.12 6.61 0.33 o -5 6 1 0.98 1.23 0.39 o -4 6 1 73.90 76.22 0.94 o -3 6 1 817.68 914.12 11.09 o -2 6 1 1.77 0.55 0.17 o -1 6 1 1537.40 1944.53 29.60 o 0 6 1 615.23 727.05 13.05 o 1 6 1 771.26 847.20 18.15 o 2 6 1 3.31 5.23 0.20 o 3 6 1 22.29 22.52 0.37 o 4 6 1 153.55 171.28 1.95 o 5 6 1 47.92 49.08 0.85 o 6 6 1 34.85 34.84 1.48 o 7 6 1 24.19 23.69 1.44 o 8 6 1 0.49 0.51 0.38 o -8 7 1 23.31 23.26 0.69 o -7 7 1 5.53 6.60 0.72 o -6 7 1 1.20 1.32 0.61 o -5 7 1 11.58 12.07 0.33 o -4 7 1 1.99 2.18 0.18 o -3 7 1 20.50 28.98 0.46 o -2 7 1 14.31 12.20 0.24 o -1 7 1 5.72 9.64 0.18 o 0 7 1 1616.29 1890.34 48.27 o 1 7 1 388.56 426.28 13.78 o 2 7 1 1419.45 1639.97 22.20 o 3 7 1 232.70 234.99 3.17 o 4 7 1 203.31 206.87 2.53 o 5 7 1 36.45 34.70 0.99 o 6 7 1 68.32 71.94 1.05 o 7 7 1 3.09 3.70 0.45 o 8 7 1 11.00 10.98 0.55 o -7 8 1 2.39 2.70 0.45 o -6 8 1 89.24 98.96 1.43 o -5 8 1 41.87 42.89 0.68 o -4 8 1 0.21 0.32 0.41 o -3 8 1 67.86 72.59 1.30 o -2 8 1 216.56 211.81 3.90 o -1 8 1 38.30 42.46 1.32 o 0 8 1 325.20 341.53 9.31 o 1 8 1 44.06 53.09 0.81 o 2 8 1 80.92 88.94 1.38 o 3 8 1 0.22 -0.02 0.14 o 4 8 1 2.41 1.55 0.21 o 5 8 1 140.87 147.03 2.56 o 6 8 1 1.06 1.44 0.28 o 7 8 1 55.70 52.96 0.92 o -7 9 1 24.56 25.52 0.89 o -6 9 1 12.97 12.18 0.63 o -5 9 1 94.97 102.82 1.79 o -4 9 1 78.40 74.12 2.06 o -3 9 1 9.33 8.70 0.41 o -2 9 1 5.28 6.11 0.29 o -1 9 1 60.97 53.80 1.51 o 0 9 1 94.16 100.55 1.41 o 1 9 1 64.36 66.36 1.66 o 2 9 1 27.23 23.35 1.29 o 3 9 1 17.34 16.23 0.32 o 4 9 1 2.13 1.78 0.28 o 5 9 1 3.83 3.62 0.26 o 6 9 1 2.25 2.13 0.31 o 7 9 1 29.38 32.41 0.91 o -7 10 1 1.86 1.98 0.34 o -6 10 1 7.71 7.80 0.39 o -5 10 1 5.90 5.76 0.27 o -4 10 1 14.10 14.55 1.07 o -3 10 1 138.65 144.64 2.04 o -2 10 1 20.83 18.47 0.36 o -1 10 1 299.15 299.00 9.15 o 0 10 1 41.52 42.44 1.09 o 1 10 1 8.39 9.83 0.43 o 2 10 1 34.48 35.01 0.54 o 3 10 1 18.09 16.68 0.59 o 4 10 1 0.89 1.25 0.21 o 5 10 1 13.11 14.44 0.55 o 6 10 1 0.48 0.83 0.26 o 7 10 1 5.23 5.00 0.39 o -6 11 1 1.54 1.49 0.54 o -5 11 1 21.92 20.62 0.80 o -4 11 1 52.80 52.04 1.80 o -3 11 1 91.99 89.49 1.40 o -2 11 1 62.74 60.02 1.09 o -1 11 1 234.92 237.03 7.79 o 0 11 1 35.57 35.07 1.59 o 1 11 1 85.55 84.06 1.07 o 2 11 1 2.35 2.79 0.17 o 3 11 1 0.04 0.44 0.18 o 4 11 1 214.30 217.77 2.76 o 5 11 1 2.07 2.46 0.32 o 6 11 1 84.39 84.51 1.18 o -6 12 1 7.62 7.33 0.43 o -5 12 1 285.24 313.49 4.70 o -4 12 1 45.81 43.19 0.64 o -3 12 1 392.52 375.78 5.62 o -2 12 1 14.09 11.74 0.31 o -1 12 1 3.74 1.93 0.11 o 0 12 1 0.33 1.24 0.65 o 1 12 1 22.04 19.03 0.39 o 2 12 1 359.36 339.38 4.75 o 3 12 1 4.18 3.61 0.29 o 4 12 1 266.88 279.44 7.00 o 5 12 1 40.82 39.87 0.66 o 6 12 1 4.79 4.43 0.41 o -5 13 1 22.93 21.82 0.80 o -4 13 1 9.11 7.09 0.66 o -3 13 1 81.88 83.89 1.50 o -2 13 1 18.07 15.52 0.36 o -1 13 1 78.95 62.73 2.60 o 0 13 1 59.84 50.02 0.99 o 1 13 1 10.22 8.73 0.34 o 2 13 1 75.49 75.38 1.35 o 3 13 1 9.47 9.90 0.28 o 4 13 1 57.54 52.25 1.83 o 5 13 1 13.36 11.39 0.48 o -5 14 1 5.08 5.71 0.52 o -4 14 1 6.94 7.19 0.47 o -3 14 1 19.55 19.00 0.61 o -2 14 1 7.23 4.35 0.22 o -1 14 1 7.73 7.72 0.25 o 0 14 1 15.41 15.00 0.56 o 1 14 1 8.06 5.33 0.23 o 2 14 1 3.71 2.43 0.19 o 3 14 1 8.17 7.96 0.30 o 4 14 1 0.70 0.77 0.22 o -4 15 1 0.01 0.36 0.39 o -3 15 1 21.21 23.59 0.71 o -2 15 1 0.13 0.51 0.34 o -1 15 1 0.66 0.37 0.11 o 0 15 1 1.79 2.14 0.17 o 1 15 1 1.32 1.53 0.16 o 2 15 1 0.02 -0.06 0.31 o 3 15 1 10.48 7.98 0.53 o -2 16 1 0.39 0.04 0.24 o -1 16 1 0.43 0.72 0.27 o 0 16 1 0.06 0.46 0.26 o 1 16 1 3.99 4.14 0.19 o 2 16 1 0.55 0.53 0.16 o -9 0 2 6.83 5.81 0.64 o -8 0 2 110.24 108.76 2.11 o -7 0 2 4.62 5.47 0.51 o -6 0 2 182.50 191.14 3.15 o -5 0 2 476.38 487.20 7.25 o -4 0 2 2140.47 2554.17 37.94 o -3 0 2 610.97 671.53 11.52 o -2 0 2 226.80 262.76 5.83 o 1 0 2 948.96 877.79 13.77 o 3 0 2 1079.37 1027.95 15.42 o 4 0 2 254.17 255.98 3.92 o 5 0 2 9.83 8.42 0.50 o 6 0 2 77.11 80.92 1.54 o 7 0 2 0.92 1.36 0.45 o 8 0 2 1.02 0.20 0.49 o -9 1 2 1.83 1.02 0.78 o -8 1 2 10.87 10.72 0.59 o -7 1 2 16.58 17.08 0.58 o -6 1 2 102.96 106.31 1.54 o -5 1 2 27.65 27.29 0.81 o -4 1 2 1108.03 1220.71 15.57 o -3 1 2 778.39 797.63 9.16 o -2 1 2 5295.90 7484.39 177.68 o -1 1 2 2001.01 2401.70 58.48 o 0 1 2 294.65 293.85 4.45 o 2 1 2 1485.37 1592.95 17.66 o 3 1 2 2640.89 2905.21 32.76 o 4 1 2 1813.57 1976.41 23.31 o 5 1 2 164.61 161.31 1.87 o 6 1 2 6.08 5.97 0.34 o 7 1 2 9.93 9.65 0.55 o 8 1 2 24.27 23.21 0.64 o -8 2 2 1.94 1.58 0.56 o -7 2 2 2.98 3.49 0.38 o -6 2 2 28.57 33.20 1.16 o -5 2 2 30.76 29.21 0.51 o -4 2 2 166.66 149.01 4.65 o -3 2 2 317.25 310.72 10.19 o -2 2 2 1817.32 2030.76 70.27 o -1 2 2 482.69 453.00 6.97 o 0 2 2 75.39 73.26 1.24 o 1 2 2 491.31 495.41 5.71 o 2 2 2 44.99 43.96 0.55 o 3 2 2 1.26 1.49 0.18 o 4 2 2 9.76 10.31 0.30 o 5 2 2 161.35 167.12 2.08 o 6 2 2 79.16 76.89 1.08 o 7 2 2 1.04 1.40 0.32 o 8 2 2 1.05 1.79 0.41 o -8 3 2 5.45 5.91 0.40 o -7 3 2 9.83 10.02 0.68 o -6 3 2 8.04 8.92 0.56 o -5 3 2 26.41 28.16 0.50 o -4 3 2 563.91 628.26 8.43 o -3 3 2 692.05 713.70 8.41 o -2 3 2 139.39 138.83 5.68 o -1 3 2 343.94 311.88 3.61 o 1 3 2 18.31 15.69 0.35 o 2 3 2 49.84 48.71 0.81 o 3 3 2 136.29 125.08 1.65 o 4 3 2 0.70 0.70 0.19 o 5 3 2 3.99 2.96 0.25 o 6 3 2 5.43 5.89 0.35 o 7 3 2 6.89 6.49 0.39 o 8 3 2 11.15 11.22 0.51 o -8 4 2 2.34 3.31 0.49 o -7 4 2 19.53 18.17 0.55 o -6 4 2 40.47 39.89 0.78 o -5 4 2 2.57 2.60 0.22 o -4 4 2 703.06 724.29 9.11 o -3 4 2 472.64 516.76 5.57 o -2 4 2 668.85 634.37 21.42 o -1 4 2 1300.56 1419.09 23.05 o 0 4 2 68.83 74.81 1.07 o 1 4 2 603.35 626.82 7.71 o 2 4 2 82.56 94.78 1.11 o 3 4 2 564.39 565.49 6.31 o 4 4 2 81.19 70.66 1.80 o 5 4 2 12.46 11.77 0.37 o 6 4 2 0.75 1.20 0.27 o 7 4 2 3.74 3.87 0.41 o 8 4 2 0.10 0.37 0.39 o -8 5 2 14.76 12.39 0.57 o -7 5 2 2.63 1.97 0.32 o -6 5 2 173.30 179.54 2.83 o -5 5 2 0.23 0.68 0.21 o -4 5 2 274.49 279.48 4.96 o -3 5 2 5.27 6.36 0.17 o -2 5 2 81.02 85.73 1.18 o -1 5 2 248.57 249.51 10.83 o 0 5 2 732.49 817.70 11.17 o 1 5 2 106.25 110.93 1.36 o 2 5 2 149.03 138.64 1.60 o 3 5 2 8.77 3.96 0.21 o 4 5 2 68.09 72.92 0.97 o 5 5 2 18.07 17.04 0.41 o 6 5 2 40.97 43.63 0.74 o 7 5 2 18.79 20.61 0.68 o 8 5 2 15.61 15.34 0.59 o -8 6 2 6.92 8.31 0.45 o -7 6 2 8.44 9.38 0.46 o -6 6 2 9.39 9.42 0.65 o -5 6 2 8.70 9.12 0.29 o -4 6 2 38.86 34.80 0.57 o -3 6 2 1.23 0.70 0.25 o -2 6 2 92.87 87.79 1.31 o -1 6 2 74.58 71.93 2.51 o 0 6 2 92.94 92.54 1.19 o 1 6 2 37.37 37.04 0.83 o 2 6 2 4.01 3.68 0.15 o 3 6 2 188.50 194.37 2.25 o 4 6 2 509.52 541.76 13.81 o 5 6 2 137.90 139.62 1.67 o 6 6 2 10.41 10.41 0.45 o 7 6 2 36.34 36.06 0.74 o 8 6 2 9.49 9.59 1.46 o -8 7 2 42.96 44.48 1.37 o -7 7 2 8.35 8.33 0.47 o -6 7 2 2.12 3.14 0.32 o -5 7 2 154.47 162.72 2.02 o -4 7 2 0.46 0.68 0.15 o -3 7 2 8.82 10.84 0.28 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