#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:14:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180986 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/66/2206670.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206670_Fobs loop_ _publ_author_name 'Backiel, Stanley' 'Bajrami, Besnik' 'Hunter, Allen D.' 'Zeller, Matthias' 'Lesley, M. J. Gerald' _publ_section_title ; Bis(benzylsulfanyl)maleonitrile ; _journal_coeditor_code CV6553 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2817 _journal_page_last o2819 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.138 _cell_angle_gamma 90.000 _cell_length_a 18.1665 _cell_length_b 11.0409 _cell_length_c 32.1972 _exptl_crystal_F_000 2688.00 _reflns_d_resolution_high 0.7492 _cod_data_source_file cv6553Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 03mz24am in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 631.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 53.21 11.48 1.53 o 2 0 0 18913.36 20366.57 679.36 o 3 0 0 364.08 383.92 11.69 o 4 0 0 7774.43 8425.59 228.76 o 5 0 0 67.73 62.78 4.56 o 6 0 0 2727.26 2050.51 57.70 o 7 0 0 540.74 557.21 18.17 o 8 0 0 3879.75 4284.72 118.74 o 9 0 0 826.88 847.59 26.90 o 10 0 0 2707.78 3071.86 87.05 o 11 0 0 829.45 830.53 27.50 o 12 0 0 24881.65 26895.34 728.90 o 13 0 0 62.97 91.72 9.52 o 14 0 0 3093.74 2867.00 104.69 o 15 0 0 332.88 321.88 23.13 o 16 0 0 2886.12 2872.14 106.72 o 17 0 0 71.62 81.10 20.28 o 18 0 0 58.61 34.16 16.50 o 19 0 0 143.69 166.12 22.45 o 20 0 0 28.90 49.93 18.66 o 21 0 0 60.93 53.05 20.41 o 22 0 0 4.34 29.97 21.52 o 23 0 0 84.26 131.32 27.58 o 24 0 0 2562.48 2727.71 110.91 o 1 1 0 148.04 193.40 6.03 o 2 1 0 23.71 46.04 2.27 o 3 1 0 251992.64 254534.45 5940.77 o 4 1 0 306.51 303.83 8.35 o 5 1 0 1188.43 1034.92 23.64 o 6 1 0 310.72 297.88 8.95 o 7 1 0 7453.85 8555.06 180.64 o 8 1 0 428.40 434.04 12.60 o 9 1 0 386.26 607.00 14.97 o 10 1 0 0.06 0.78 8.95 o 11 1 0 3460.79 3692.86 81.36 o 12 1 0 487.49 499.12 15.86 o 13 1 0 4160.65 4025.85 88.91 o 14 1 0 49.02 112.21 17.56 o 15 1 0 14263.72 14599.40 347.76 o 16 1 0 252.77 275.28 16.10 o 17 1 0 929.20 868.32 29.88 o 18 1 0 184.95 225.04 16.40 o 19 1 0 2454.78 2341.64 65.13 o 20 1 0 26.38 55.85 13.84 o 21 1 0 677.87 691.77 28.82 o 22 1 0 0.54 2.66 13.95 o 23 1 0 248.93 283.09 22.50 o 24 1 0 62.63 91.14 19.21 o 0 2 0 245728.78 234378.86 10954.65 o 1 2 0 5.58 25.86 4.24 o 2 2 0 3377.77 3281.40 63.57 o 3 2 0 51.68 59.54 4.31 o 4 2 0 30107.21 33007.43 629.79 o 5 2 0 24.64 37.37 3.86 o 6 2 0 4586.18 4644.45 99.40 o 7 2 0 544.82 541.03 17.48 o 8 2 0 11469.99 12268.91 259.00 o 9 2 0 220.68 211.31 8.88 o 10 2 0 13811.74 14581.55 307.76 o 11 2 0 0.07 -4.92 4.92 o 12 2 0 2209.92 2292.75 52.95 o 13 2 0 0.02 -4.67 5.99 o 14 2 0 15363.05 14900.39 315.83 o 15 2 0 90.74 104.91 9.98 o 16 2 0 763.77 693.82 25.28 o 17 2 0 129.80 143.95 14.33 o 18 2 0 688.89 673.48 26.06 o 19 2 0 631.29 616.13 25.48 o 20 2 0 479.11 439.82 22.18 o 21 2 0 212.55 201.08 18.20 o 22 2 0 141.90 174.09 18.71 o 23 2 0 73.29 87.92 18.17 o 24 2 0 35.51 53.29 20.54 o 1 3 0 3757.87 4103.46 79.63 o 2 3 0 35.53 51.89 3.54 o 3 3 0 54387.13 58668.63 1117.27 o 4 3 0 218.81 215.72 6.60 o 5 3 0 2005.57 1929.24 42.39 o 6 3 0 201.40 194.47 7.60 o 7 3 0 5302.35 6279.04 133.96 o 8 3 0 17.50 23.13 4.93 o 9 3 0 6219.09 6910.89 147.99 o 10 3 0 27.33 32.54 5.94 o 11 3 0 65.06 93.07 7.73 o 12 3 0 5.83 10.61 6.95 o 13 3 0 0.27 1.30 6.67 o 14 3 0 52.42 68.68 8.93 o 15 3 0 476.18 443.52 21.51 o 16 3 0 19.70 43.96 11.02 o 17 3 0 4.05 12.33 10.16 o 18 3 0 53.29 42.21 12.24 o 19 3 0 1791.35 1831.74 53.64 o 20 3 0 52.94 80.96 14.75 o 21 3 0 277.15 273.12 20.20 o 22 3 0 4.25 17.98 14.92 o 23 3 0 338.24 330.14 23.80 o 0 4 0 9103.61 10786.69 293.18 o 1 4 0 0.66 11.77 4.98 o 2 4 0 4639.52 4797.88 93.37 o 3 4 0 14.78 16.14 3.41 o 4 4 0 21968.63 23310.60 445.65 o 5 4 0 2.93 4.68 3.35 o 6 4 0 174.43 88.11 5.11 o 7 4 0 10.27 12.79 3.78 o 8 4 0 7201.83 7104.59 152.06 o 9 4 0 203.01 187.66 9.23 o 10 4 0 6427.23 5740.17 141.02 o 11 4 0 7.04 12.05 6.29 o 12 4 0 536.99 451.03 15.69 o 13 4 0 79.85 90.10 9.36 o 14 4 0 3184.78 2794.01 64.76 o 15 4 0 229.29 203.82 12.61 o 16 4 0 1403.11 1331.48 37.21 o 17 4 0 38.94 44.73 11.69 o 18 4 0 918.65 918.66 32.07 o 19 4 0 23.06 18.79 12.30 o 20 4 0 275.22 257.74 19.18 o 21 4 0 227.17 260.33 20.33 o 22 4 0 1761.52 1870.86 57.31 o 23 4 0 223.44 252.15 23.31 o 1 5 0 8484.11 9983.10 192.47 o 2 5 0 74.93 106.57 13.20 o 3 5 0 6525.87 7164.13 138.79 o 4 5 0 51.39 55.32 4.89 o 5 5 0 556.77 758.02 17.76 o 6 5 0 234.50 216.42 13.92 o 7 5 0 5815.77 6068.75 118.79 o 8 5 0 96.69 99.53 6.56 o 9 5 0 10039.43 9963.32 212.19 o 10 5 0 0.88 -3.39 6.05 o 11 5 0 2111.37 1953.07 46.51 o 12 5 0 129.75 131.31 10.44 o 13 5 0 5697.72 5391.45 132.89 o 14 5 0 473.60 431.17 17.06 o 15 5 0 4044.35 3852.53 102.34 o 16 5 0 17.10 25.10 10.17 o 17 5 0 1738.32 1730.90 44.87 o 18 5 0 32.05 32.82 12.93 o 19 5 0 14116.78 14268.75 342.92 o 20 5 0 387.94 357.05 21.64 o 21 5 0 1520.41 1524.66 48.69 o 22 5 0 17.45 -3.01 15.39 o 0 6 0 78103.88 90148.00 2429.09 o 1 6 0 29.60 31.51 5.16 o 2 6 0 3473.20 3472.42 69.31 o 3 6 0 52.26 57.28 5.99 o 4 6 0 627.01 591.16 15.11 o 5 6 0 30.31 45.89 6.93 o 6 6 0 5767.21 5538.94 109.06 o 7 6 0 9.66 20.86 5.26 o 8 6 0 2300.68 2269.02 47.71 o 9 6 0 15.89 6.86 5.82 o 10 6 0 2247.65 2284.20 53.43 o 11 6 0 127.16 146.66 14.43 o 12 6 0 1731.79 1620.51 42.55 o 13 6 0 0.49 -6.18 8.06 o 14 6 0 12552.88 12286.15 263.10 o 15 6 0 4.11 4.01 9.32 o 16 6 0 2477.80 2445.35 59.55 o 17 6 0 384.15 362.08 17.89 o 18 6 0 247.77 263.03 18.60 o 19 6 0 595.07 627.18 27.24 o 20 6 0 371.74 436.29 23.73 o 21 6 0 8.42 -10.81 17.25 o 22 6 0 655.10 733.91 38.06 o 1 7 0 51.89 37.43 5.22 o 2 7 0 36.13 43.76 5.43 o 3 7 0 1484.45 1452.94 31.70 o 4 7 0 12.79 14.87 5.15 o 5 7 0 656.15 556.38 15.11 o 6 7 0 23.77 18.65 5.61 o 7 7 0 605.39 526.19 15.25 o 8 7 0 578.08 541.21 18.85 o 9 7 0 11890.10 11396.98 221.43 o 10 7 0 2.42 27.09 8.91 o 11 7 0 2321.99 2190.50 52.51 o 12 7 0 178.86 216.47 12.88 o 13 7 0 987.01 915.24 27.02 o 14 7 0 29.81 29.70 9.78 o 15 7 0 1290.78 1240.78 34.66 o 16 7 0 731.78 707.53 24.40 o 17 7 0 681.21 658.47 24.19 o 18 7 0 4.54 22.03 14.04 o 19 7 0 532.58 477.17 28.60 o 20 7 0 13.34 36.17 18.16 o 21 7 0 2362.43 2732.01 111.99 o 0 8 0 50640.20 52799.15 1426.29 o 1 8 0 215.98 229.34 13.37 o 2 8 0 433.58 347.26 11.93 o 3 8 0 79.99 89.59 7.34 o 4 8 0 1303.46 1346.26 30.55 o 5 8 0 13.61 -0.55 12.90 o 6 8 0 1987.78 1599.81 47.10 o 7 8 0 303.68 352.43 13.68 o 8 8 0 179.40 165.30 10.42 o 9 8 0 48.67 59.31 9.30 o 10 8 0 262.79 255.87 13.51 o 11 8 0 15.41 20.94 8.64 o 12 8 0 341.53 326.63 15.25 o 13 8 0 64.29 76.09 10.79 o 14 8 0 62.63 58.04 10.93 o 15 8 0 0.86 9.50 13.66 o 16 8 0 5.25 -11.70 11.70 o 17 8 0 121.59 113.96 18.91 o 18 8 0 82.93 75.67 18.73 o 19 8 0 1.51 11.49 21.51 o 20 8 0 201.60 234.02 31.25 o 1 9 0 4978.73 4787.71 96.17 o 2 9 0 3.81 24.67 9.21 o 3 9 0 42190.42 41908.18 801.15 o 4 9 0 697.61 702.51 32.78 o 5 9 0 22.92 22.77 9.47 o 6 9 0 395.34 343.15 13.31 o 7 9 0 492.26 500.55 16.84 o 8 9 0 20.89 16.71 8.23 o 9 9 0 1349.50 1140.00 36.40 o 10 9 0 94.97 101.42 10.86 o 11 9 0 289.32 237.74 15.05 o 12 9 0 165.37 169.34 15.36 o 13 9 0 152.88 188.79 19.36 o 14 9 0 0.83 5.79 14.53 o 15 9 0 4177.32 4324.91 130.17 o 16 9 0 53.23 77.71 18.09 o 17 9 0 2428.76 2589.58 85.03 o 18 9 0 237.06 235.59 24.56 o 19 9 0 569.43 634.22 35.92 o 0 10 0 23210.90 21652.04 723.64 o 1 10 0 199.74 179.75 11.25 o 2 10 0 2594.88 2575.45 55.18 o 3 10 0 121.71 127.45 9.96 o 4 10 0 1739.96 1925.20 47.20 o 5 10 0 131.17 121.77 9.99 o 6 10 0 409.36 404.56 14.92 o 7 10 0 0.01 -7.51 7.51 o 8 10 0 554.63 545.25 23.50 o 9 10 0 66.09 70.01 15.01 o 10 10 0 6237.56 6465.78 185.61 o 11 10 0 128.01 133.06 17.87 o 12 10 0 3789.98 3794.54 115.00 o 13 10 0 0.06 -8.03 14.91 o 14 10 0 2374.57 2459.83 80.60 o 15 10 0 136.76 208.82 22.79 o 16 10 0 15.02 7.01 17.67 o 17 10 0 40.12 30.60 19.15 o 1 11 0 86.71 123.43 10.32 o 2 11 0 0.03 4.60 8.03 o 3 11 0 74.72 59.58 10.28 o 4 11 0 0.79 7.87 8.96 o 5 11 0 20.15 14.86 9.41 o 6 11 0 38.91 45.43 12.47 o 7 11 0 3410.31 3771.92 161.26 o 8 11 0 2.74 13.65 13.78 o 9 11 0 121.99 87.96 16.39 o 10 11 0 47.13 32.86 15.07 o 11 11 0 131.07 119.23 18.65 o 12 11 0 8.56 38.09 16.78 o 13 11 0 4733.57 5253.68 156.01 o 14 11 0 21.72 6.59 18.38 o 15 11 0 1212.33 1334.49 54.72 o 16 11 0 7.00 -1.35 18.41 o 0 12 0 7252.65 7128.50 248.70 o 1 12 0 47.12 29.48 12.28 o 2 12 0 1678.48 1759.51 60.27 o 3 12 0 65.44 120.46 15.10 o 4 12 0 220.45 316.46 20.05 o 5 12 0 7.97 44.69 13.83 o 6 12 0 4296.37 4656.35 137.72 o 7 12 0 170.70 203.86 20.86 o 8 12 0 629.03 657.44 32.29 o 9 12 0 2.91 -5.48 14.98 o 10 12 0 659.56 715.31 35.05 o 11 12 0 66.52 133.87 20.78 o 12 12 0 68.56 112.20 20.66 o 13 12 0 74.09 86.77 20.66 o 14 12 0 107.48 136.09 22.81 o 1 13 0 715.02 688.73 44.77 o 2 13 0 98.38 96.84 26.08 o 3 13 0 1908.99 2008.62 68.90 o 4 13 0 120.81 149.76 21.28 o 5 13 0 553.75 648.14 40.77 o 6 13 0 40.32 29.63 21.51 o 7 13 0 127.91 165.69 27.35 o 8 13 0 141.49 171.69 27.10 o 9 13 0 2137.47 2406.65 98.96 o 10 13 0 10.02 1.72 21.84 o 11 13 0 14.16 -14.63 18.52 o 0 14 0 34.55 143.85 43.23 o 1 14 0 9.24 122.77 29.16 o 2 14 0 210.84 202.25 33.38 o 3 14 0 5.76 -24.88 24.88 o 4 14 0 463.04 448.00 59.30 o 5 14 0 0.43 -35.96 35.96 o 6 14 0 636.66 714.65 71.54 o 7 14 0 135.82 229.55 49.35 o -24 1 1 250.28 245.39 23.22 o -23 1 1 242.17 249.51 21.69 o -22 1 1 684.80 713.09 30.56 o -21 1 1 140.38 208.10 18.38 o -20 1 1 6623.08 6783.86 169.10 o -19 1 1 543.17 635.74 26.05 o -18 1 1 1965.98 1921.91 54.70 o -17 1 1 1547.99 1570.10 46.00 o -16 1 1 4515.00 4481.34 112.76 o -15 1 1 1108.22 1030.25 32.47 o -14 1 1 1070.69 998.21 26.85 o -13 1 1 180.82 156.39 9.59 o -12 1 1 4123.45 3946.81 104.92 o -10 1 1 10615.36 11261.15 266.55 o -9 1 1 2371.15 2422.55 54.05 o -8 1 1 21370.68 22846.45 479.16 o -7 1 1 309.53 342.39 10.21 o -6 1 1 5375.48 5480.82 116.48 o -5 1 1 168.82 158.37 34.81 o -3 1 1 4675.65 4862.62 102.72 o -2 1 1 12454.38 12942.59 229.80 o -1 1 1 2636.87 2637.76 50.99 o 0 1 1 534.72 499.47 17.58 o 1 1 1 2554.77 2494.23 52.94 o 2 1 1 11109.34 11337.07 216.99 o 3 1 1 1920.94 1794.10 61.27 o 4 1 1 27987.29 29739.84 621.51 o 5 1 1 1134.26 1205.65 30.01 o 6 1 1 1348.77 1186.92 155.71 o 7 1 1 942.35 887.40 21.30 o 8 1 1 8442.69 8358.12 397.50 o 9 1 1 3310.96 3242.02 71.06 o 10 1 1 26006.31 27522.40 576.92 o 11 1 1 9482.21 9809.09 208.69 o 12 1 1 11667.39 11962.16 253.93 o 13 1 1 29.28 19.94 6.59 o 14 1 1 302.31 248.14 11.89 o 15 1 1 868.35 867.89 28.69 o 16 1 1 1027.88 878.74 59.25 o 17 1 1 424.16 397.45 33.85 o 18 1 1 288.63 242.94 28.94 o 19 1 1 79.83 64.25 15.52 o 20 1 1 982.36 1024.82 74.22 o 21 1 1 40.26 67.95 14.90 o 22 1 1 1411.61 1374.05 45.23 o 23 1 1 63.43 68.20 17.50 o 24 1 1 1042.39 1249.38 44.99 o -24 2 1 497.49 538.70 33.28 o -23 2 1 783.53 805.43 33.69 o -22 2 1 185.91 202.37 19.51 o -21 2 1 291.90 285.59 19.93 o -20 2 1 364.28 362.38 20.25 o -19 2 1 45.32 49.72 12.80 o -18 2 1 584.04 567.50 23.79 o -17 2 1 1953.57 1868.00 52.79 o -16 2 1 646.15 645.59 24.38 o -15 2 1 4631.88 4684.84 103.90 o -14 2 1 67.10 61.99 8.80 o -13 2 1 510.72 487.74 17.37 o -12 2 1 585.46 518.88 16.25 o -11 2 1 113.91 106.27 13.51 o -10 2 1 109.59 122.17 7.82 o -9 2 1 2046.57 1795.11 47.55 o -8 2 1 1456.91 1490.91 102.89 o -7 2 1 9591.00 11941.70 564.30 o -6 2 1 1662.71 1858.32 54.83 o -5 2 1 24892.07 26557.38 555.50 o -4 2 1 911.15 880.97 20.49 o -3 2 1 8264.72 8590.87 164.88 o -2 2 1 1452.53 1476.20 32.23 o -1 2 1 4478.84 5044.16 157.28 o 0 2 1 3031.73 3149.90 61.04 o 1 2 1 21912.40 23563.67 449.42 o 2 2 1 4012.89 4180.26 80.77 o 3 2 1 7544.21 7766.85 149.21 o 4 2 1 235.99 218.61 9.98 o 5 2 1 4504.84 5414.20 258.24 o 6 2 1 5106.65 5430.17 115.66 o 7 2 1 52384.46 57610.77 1202.99 o 8 2 1 6477.48 7114.94 151.55 o 9 2 1 4832.30 5037.90 108.64 o 10 2 1 236.28 196.68 9.09 o 11 2 1 771.57 715.22 19.76 o 12 2 1 193.80 169.76 9.90 o 13 2 1 75.73 50.83 8.38 o 14 2 1 428.80 409.44 15.51 o 15 2 1 3698.26 3588.12 81.07 o 16 2 1 124.91 100.37 17.34 o 17 2 1 1918.33 1820.62 51.74 o 18 2 1 159.27 151.17 14.71 o 19 2 1 25.22 39.30 12.48 o 20 2 1 210.95 200.61 17.16 o 21 2 1 311.63 343.84 21.10 o 22 2 1 197.06 218.00 19.79 o 23 2 1 336.52 309.00 23.18 o 24 2 1 305.09 282.45 33.41 o -23 3 1 13.31 27.37 16.34 o -22 3 1 245.50 227.06 20.76 o -21 3 1 297.09 288.39 20.21 o -20 3 1 709.68 663.74 34.52 o -19 3 1 2.56 4.84 11.51 o -18 3 1 4585.72 4672.83 118.74 o -17 3 1 556.61 510.55 21.88 o -16 3 1 4711.72 4554.57 114.82 o -15 3 1 276.94 235.47 19.84 o -14 3 1 2301.16 2066.18 51.31 o -13 3 1 1816.08 1668.82 40.70 o -12 3 1 18355.15 18107.95 381.98 o -11 3 1 1595.60 1506.25 36.36 o -10 3 1 2283.26 1990.57 46.02 o -9 3 1 923.23 811.36 21.61 o -8 3 1 6556.22 7190.37 153.30 o -7 3 1 1508.52 1467.67 34.04 o -6 3 1 7220.36 6703.51 142.62 o -5 3 1 1716.92 1629.15 33.25 o -4 3 1 2863.82 3544.52 220.94 o -3 3 1 1340.65 1298.53 26.86 o -2 3 1 1320.77 1309.71 29.25 o -1 3 1 1968.96 1985.06 39.36 o 0 3 1 1265.83 1318.29 26.70 o 1 3 1 613.11 619.61 13.50 o 2 3 1 5778.24 5792.28 111.72 o 3 3 1 1338.90 1319.35 26.99 o 4 3 1 19165.27 20123.00 384.81 o 5 3 1 497.10 468.01 20.36 o 6 3 1 1591.20 1424.96 50.36 o 7 3 1 620.25 573.23 22.51 o 8 3 1 1801.12 1985.61 77.69 o 9 3 1 572.67 573.50 19.24 o 10 3 1 1206.32 1148.58 28.56 o 11 3 1 584.14 476.39 32.93 o 12 3 1 2741.77 2935.50 150.35 o 13 3 1 284.81 243.15 62.17 o 14 3 1 4342.94 4201.50 93.61 o 15 3 1 1819.11 1708.70 42.58 o 16 3 1 6826.68 6684.63 146.37 o 17 3 1 368.49 384.67 20.71 o 18 3 1 826.75 753.13 58.29 o 19 3 1 15.91 30.95 12.32 o 20 3 1 2382.85 2488.44 69.43 o 21 3 1 1814.86 1915.63 57.09 o 22 3 1 1641.08 1867.55 56.89 o 23 3 1 11.37 14.38 16.42 o -23 4 1 5.70 -11.79 16.28 o -22 4 1 28.82 23.63 15.76 o -21 4 1 6.12 3.40 13.39 o -20 4 1 28.92 32.74 13.70 o -19 4 1 109.58 86.36 14.17 o -18 4 1 40.48 70.90 13.41 o 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