#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:15:04 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180988 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/68/2206859.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206859_Fobs loop_ _publ_author_name 'Grigoriev, Mikhail S.' 'Moisy, Philippe' 'Den Auwer, Christophe' 'Charushnikova, Iraida A.' _publ_section_title ; Hydrazinium nitrate ; _journal_coeditor_code BR6216 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i216 _journal_page_last i217 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.340 _cell_angle_gamma 90.000 _cell_length_a 7.9649 _cell_length_b 5.6569 _cell_length_c 8.1221 _exptl_crystal_F_000 200.00 _reflns_d_resolution_high 0.7712 _cod_data_source_file br6216Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hydnit in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 46.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 353.10 376.14 12.30 o 4 0 0 5.12 3.08 0.28 o 6 0 0 314.39 310.83 8.72 o 8 0 0 212.33 227.50 8.19 o 10 0 0 0.56 0.45 0.41 o 1 1 0 40.01 47.10 1.23 o 3 1 0 474.06 457.23 14.72 o 4 1 0 56.12 66.57 1.64 o 5 1 0 69.72 70.20 1.87 o 6 1 0 14.34 13.45 0.38 o 7 1 0 132.60 132.38 5.66 o 8 1 0 228.92 229.24 11.65 o 9 1 0 50.09 51.47 2.36 o 10 1 0 22.49 18.89 1.18 o 0 2 0 1355.03 1319.99 53.55 o 2 2 0 279.17 301.65 6.59 o 3 2 0 669.75 706.64 19.54 o 4 2 0 10.99 13.17 0.41 o 5 2 0 374.08 368.94 7.95 o 6 2 0 16.06 15.48 0.53 o 7 2 0 314.85 329.33 8.47 o 8 2 0 0.79 0.58 0.13 o 9 2 0 1.08 1.09 0.80 o 1 3 0 34.78 36.09 1.06 o 2 3 0 69.73 69.66 2.01 o 3 3 0 263.31 266.60 7.48 o 4 3 0 139.06 150.26 3.19 o 5 3 0 57.20 63.28 1.49 o 6 3 0 56.83 56.86 1.49 o 7 3 0 301.77 314.08 10.25 o 8 3 0 4.92 3.80 0.31 o 9 3 0 61.53 61.14 2.80 o 0 4 0 1018.79 1038.45 32.19 o 1 4 0 40.70 41.16 0.89 o 2 4 0 597.39 622.11 16.09 o 3 4 0 1.53 1.71 0.17 o 4 4 0 96.40 98.07 2.49 o 5 4 0 50.96 54.90 1.40 o 6 4 0 13.88 13.66 0.46 o 7 4 0 22.53 20.59 1.62 o 8 4 0 60.85 64.43 2.65 o 1 5 0 10.95 10.15 0.34 o 2 5 0 138.61 143.44 3.39 o 3 5 0 23.87 24.10 0.96 o 4 5 0 9.84 9.72 0.45 o 5 5 0 0.00 0.22 0.23 o 6 5 0 99.14 96.70 6.70 o 7 5 0 0.96 1.05 0.43 o 0 6 0 44.45 44.95 2.34 o 1 6 0 105.52 107.96 4.07 o 2 6 0 20.10 20.84 1.00 o 3 6 0 74.29 73.65 2.97 o 4 6 0 78.33 83.53 4.50 o 5 6 0 46.72 48.51 4.22 o 1 7 0 10.36 10.35 0.78 o 2 7 0 2.08 2.79 1.27 o 3 7 0 38.45 38.27 2.24 o -9 0 1 26.92 25.98 1.21 o -7 0 1 101.22 106.59 7.02 o -5 0 1 4.48 3.81 0.15 o -1 0 1 29.86 34.88 1.37 o 1 0 1 829.28 917.96 31.59 o 5 0 1 42.78 42.09 1.35 o 7 0 1 616.15 677.85 29.94 o 9 0 1 74.85 81.44 3.56 o -10 1 1 87.56 95.72 4.84 o -9 1 1 9.65 10.44 0.60 o -8 1 1 1.11 1.63 0.26 o -7 1 1 163.75 173.47 3.75 o -6 1 1 47.63 44.04 1.26 o -5 1 1 1067.93 1141.15 28.78 o -4 1 1 216.13 216.87 4.72 o -2 1 1 1069.42 936.12 28.15 o -1 1 1 249.38 260.14 6.29 o 0 1 1 237.40 229.44 5.11 o 1 1 1 737.70 674.26 15.74 o 2 1 1 77.00 64.88 1.53 o 4 1 1 5.30 6.86 0.36 o 5 1 1 33.98 32.87 1.11 o 6 1 1 69.74 69.09 1.84 o 7 1 1 74.30 77.87 1.92 o 8 1 1 28.14 28.43 0.91 o 9 1 1 7.42 7.23 0.50 o 10 1 1 10.89 11.86 0.74 o -9 2 1 32.15 30.58 1.34 o -8 2 1 43.73 45.40 1.08 o -7 2 1 13.46 14.15 0.56 o -6 2 1 24.96 23.36 0.76 o -5 2 1 2.56 2.08 0.12 o -4 2 1 220.55 208.77 7.70 o -3 2 1 141.06 145.79 3.61 o -2 2 1 384.33 376.99 10.75 o -1 2 1 494.38 458.47 10.42 o 0 2 1 2147.30 1979.16 89.67 o 1 2 1 234.10 226.29 4.52 o 3 2 1 184.20 195.93 4.40 o 4 2 1 79.08 88.24 1.84 o 5 2 1 96.21 97.43 1.96 o 6 2 1 34.79 34.34 2.22 o 7 2 1 24.81 24.24 0.58 o 8 2 1 362.37 363.85 16.54 o 9 2 1 0.77 1.06 0.27 o -9 3 1 41.48 41.82 2.63 o -8 3 1 4.77 3.95 0.24 o -7 3 1 34.92 32.77 0.98 o -6 3 1 22.81 21.10 0.74 o -5 3 1 3.15 2.23 0.13 o -4 3 1 10.64 11.64 0.55 o -3 3 1 685.70 690.24 15.26 o -2 3 1 338.41 315.45 7.14 o -1 3 1 28.97 27.78 0.76 o 0 3 1 259.39 252.11 5.03 o 1 3 1 164.80 160.94 3.90 o 2 3 1 7.61 7.52 0.22 o 3 3 1 7.45 6.74 0.20 o 4 3 1 177.59 186.96 3.85 o 5 3 1 123.56 127.13 3.08 o 6 3 1 89.06 88.51 2.07 o 7 3 1 12.49 10.86 0.45 o 8 3 1 56.14 60.25 2.61 o 9 3 1 20.38 18.04 1.28 o -8 4 1 0.09 0.59 0.26 o -7 4 1 2.94 2.57 0.25 o -6 4 1 1.08 1.38 0.14 o -5 4 1 2.76 2.55 0.22 o -4 4 1 4.99 4.73 0.41 o -3 4 1 257.73 245.89 8.21 o -2 4 1 66.06 66.08 1.49 o -1 4 1 328.07 328.31 6.69 o 0 4 1 3.64 3.59 0.19 o 1 4 1 36.87 35.71 0.94 o 2 4 1 36.99 37.01 1.00 o 3 4 1 217.19 219.04 6.54 o 4 4 1 0.35 0.37 0.14 o 5 4 1 215.90 226.27 6.82 o 6 4 1 43.06 41.23 3.16 o 7 4 1 76.44 74.98 3.25 o 8 4 1 24.50 21.21 1.40 o -7 5 1 4.18 3.73 0.41 o -6 5 1 11.52 9.46 0.81 o -5 5 1 10.44 8.90 0.48 o -4 5 1 27.18 28.27 1.47 o -3 5 1 126.08 130.94 3.11 o -2 5 1 65.03 67.82 1.63 o -1 5 1 13.53 12.41 0.40 o 0 5 1 1.01 1.48 0.23 o 1 5 1 239.52 244.27 5.33 o 2 5 1 0.46 0.57 0.21 o 3 5 1 31.75 29.28 1.60 o 4 5 1 33.88 32.95 1.83 o 5 5 1 63.55 60.63 2.42 o 6 5 1 1.40 0.89 0.35 o 7 5 1 3.63 2.77 0.51 o -5 6 1 3.81 2.64 0.36 o -4 6 1 3.03 2.44 0.37 o -3 6 1 3.30 3.73 0.40 o -2 6 1 49.59 48.21 1.93 o -1 6 1 3.26 2.96 0.45 o 0 6 1 36.07 37.10 1.43 o 1 6 1 80.93 81.26 3.20 o 2 6 1 0.19 0.61 0.26 o 3 6 1 74.76 75.38 5.08 o 4 6 1 10.03 10.49 1.36 o 5 6 1 4.22 4.12 0.55 o -2 7 1 53.56 53.57 4.20 o -1 7 1 17.78 17.63 1.61 o 0 7 1 3.82 2.85 0.38 o 1 7 1 10.12 10.23 0.80 o 2 7 1 18.30 17.52 1.13 o -10 0 2 0.08 0.64 0.36 o -8 0 2 127.93 129.15 5.14 o -6 0 2 6.84 5.04 0.20 o -4 0 2 324.06 326.78 9.01 o -2 0 2 1266.03 1072.83 57.14 o 0 0 2 661.47 531.88 31.58 o 2 0 2 798.37 773.45 33.50 o 4 0 2 631.95 695.64 23.76 o 6 0 2 3.26 3.13 0.24 o 8 0 2 448.54 470.44 27.08 o 10 0 2 1.28 1.94 0.59 o -10 1 2 0.00 0.59 0.37 o -9 1 2 11.74 10.59 0.48 o -8 1 2 61.46 65.97 1.76 o -7 1 2 1.52 1.30 0.12 o -6 1 2 56.10 59.38 1.22 o -5 1 2 165.36 172.22 3.51 o -4 1 2 203.84 220.99 4.57 o -3 1 2 430.34 428.90 11.63 o -2 1 2 675.58 589.80 15.25 o -1 1 2 341.32 311.93 6.20 o 1 1 2 412.81 362.01 7.47 o 2 1 2 1072.25 1150.90 26.24 o 3 1 2 760.91 800.89 17.59 o 4 1 2 267.71 297.16 6.31 o 5 1 2 579.12 626.59 13.50 o 6 1 2 316.35 326.66 7.82 o 7 1 2 35.87 36.23 1.04 o 8 1 2 94.29 94.04 4.00 o 9 1 2 1.50 2.21 1.01 o -9 2 2 118.65 120.70 4.19 o -8 2 2 81.44 84.84 2.28 o -7 2 2 23.60 21.29 0.52 o -6 2 2 0.50 0.50 0.10 o -5 2 2 142.12 150.21 3.06 o -4 2 2 40.85 38.32 1.37 o -3 2 2 12.66 10.96 0.31 o -2 2 2 206.80 193.79 4.70 o -1 2 2 382.89 324.91 6.93 o 0 2 2 169.49 169.12 3.50 o 1 2 2 115.26 119.71 2.37 o 2 2 2 263.56 273.24 5.86 o 3 2 2 253.77 262.79 5.45 o 4 2 2 48.85 51.94 1.65 o 5 2 2 283.69 298.73 8.22 o 6 2 2 104.79 103.45 4.10 o 7 2 2 274.90 292.88 7.07 o 8 2 2 49.80 51.49 2.23 o 9 2 2 2.15 1.57 0.32 o -9 3 2 23.40 21.54 0.94 o -8 3 2 3.13 2.20 0.29 o -7 3 2 70.87 72.25 1.65 o -6 3 2 159.33 158.70 3.83 o -5 3 2 16.95 17.17 0.67 o -4 3 2 4.14 4.08 0.17 o -3 3 2 193.37 189.85 4.36 o -2 3 2 852.50 832.03 16.08 o -1 3 2 299.03 287.63 5.73 o 0 3 2 47.55 45.01 2.07 o 1 3 2 678.79 692.85 16.28 o 2 3 2 99.34 99.43 3.59 o 3 3 2 347.37 361.17 10.28 o 4 3 2 217.93 230.43 8.42 o 5 3 2 528.26 559.60 12.96 o 6 3 2 87.30 91.54 2.33 o 7 3 2 34.94 33.25 2.07 o 8 3 2 0.00 0.55 0.30 o 9 3 2 2.27 2.50 0.45 o -8 4 2 0.63 1.08 0.31 o -7 4 2 45.84 43.71 2.07 o -6 4 2 79.93 76.22 2.29 o -5 4 2 73.06 74.97 2.81 o -4 4 2 126.91 132.41 5.01 o -3 4 2 40.40 40.82 1.43 o -2 4 2 145.84 142.31 2.96 o -1 4 2 313.35 312.46 6.61 o 0 4 2 210.01 205.98 4.07 o 1 4 2 11.78 11.88 0.56 o 2 4 2 31.70 30.95 1.04 o 3 4 2 93.18 96.86 3.52 o 4 4 2 0.74 1.30 0.14 o 5 4 2 0.51 0.52 0.18 o 6 4 2 125.62 121.20 4.22 o 7 4 2 7.30 6.93 0.65 o 8 4 2 31.01 30.13 1.39 o -7 5 2 41.02 41.63 2.12 o -6 5 2 0.44 0.13 0.31 o -5 5 2 69.07 71.13 3.07 o -4 5 2 92.55 95.35 2.99 o -3 5 2 70.04 67.52 1.71 o -2 5 2 559.83 588.94 15.41 o -1 5 2 0.99 1.09 0.16 o 0 5 2 76.80 82.70 1.86 o 1 5 2 66.66 67.18 1.61 o 2 5 2 0.32 1.58 1.25 o 3 5 2 22.67 20.46 1.43 o 4 5 2 65.66 62.46 2.68 o 5 5 2 53.01 50.34 2.69 o 6 5 2 137.85 144.22 5.66 o 7 5 2 0.72 -0.01 0.34 o -5 6 2 0.59 0.86 0.37 o -4 6 2 128.73 136.80 6.11 o -3 6 2 9.44 8.70 0.76 o -2 6 2 194.79 208.61 7.93 o -1 6 2 0.46 0.85 0.65 o 0 6 2 6.76 6.98 0.47 o 1 6 2 9.19 9.54 1.09 o 2 6 2 0.11 -0.04 0.26 o 3 6 2 14.86 13.95 1.42 o 4 6 2 46.47 46.96 2.44 o 5 6 2 45.61 46.96 2.68 o -2 7 2 11.21 11.95 1.00 o -1 7 2 37.90 38.52 1.83 o 0 7 2 5.99 5.99 0.80 o 1 7 2 54.51 59.98 3.18 o 2 7 2 32.40 33.54 1.77 o -9 0 3 4.25 3.26 0.47 o -7 0 3 17.05 18.54 0.58 o -5 0 3 667.70 700.54 18.54 o -3 0 3 311.35 328.78 8.35 o 1 0 3 350.61 350.68 10.64 o 3 0 3 435.64 410.58 26.19 o 5 0 3 48.85 44.79 1.66 o 7 0 3 177.05 174.51 9.27 o 9 0 3 3.77 2.25 0.53 o -9 1 3 17.02 14.19 0.56 o -8 1 3 43.78 42.33 1.06 o -7 1 3 0.01 0.09 0.08 o -6 1 3 54.69 49.65 1.13 o -5 1 3 62.87 59.65 1.05 o -4 1 3 37.38 33.71 0.70 o -3 1 3 296.48 282.81 8.00 o -2 1 3 34.51 27.10 0.49 o -1 1 3 1991.36 2036.77 81.55 o 0 1 3 531.87 560.82 13.22 o 2 1 3 987.75 1058.61 32.42 o 3 1 3 729.91 768.88 19.02 o 4 1 3 44.32 47.40 1.38 o 5 1 3 19.51 23.93 0.67 o 6 1 3 19.49 20.08 0.59 o 7 1 3 2.78 3.01 0.22 o 8 1 3 22.27 22.07 0.84 o 9 1 3 20.89 18.21 1.16 o -9 2 3 0.86 0.32 0.16 o -8 2 3 66.66 67.03 1.71 o -7 2 3 36.89 35.32 0.94 o -6 2 3 8.33 9.20 0.25 o -5 2 3 160.98 165.07 5.40 o -4 2 3 170.89 170.06 4.83 o -3 2 3 44.53 45.54 1.01 o -2 2 3 5.05 3.76 0.14 o -1 2 3 171.52 160.28 3.34 o 0 2 3 133.79 131.89 2.46 o 1 2 3 35.02 35.05 1.45 o 2 2 3 69.67 78.71 2.37 o 3 2 3 102.61 113.24 2.62 o 4 2 3 9.32 9.72 0.55 o 5 2 3 17.42 17.88 1.24 o 6 2 3 200.08 204.28 5.36 o 7 2 3 108.61 108.40 3.98 o 8 2 3 6.09 5.40 0.71 o 9 2 3 7.00 6.15 0.48 o -9 3 3 1.65 1.93 0.33 o -8 3 3 34.25 31.07 1.65 o -7 3 3 15.55 14.52 0.53 o -6 3 3 3.13 2.88 0.15 o -5 3 3 190.25 183.92 7.09 o -4 3 3 1.72 2.42 0.23 o -3 3 3 6.63 7.95 0.26 o -2 3 3 2.19 2.51 0.23 o -1 3 3 0.98 1.08 0.11 o 0 3 3 149.22 151.28 3.22 o 1 3 3 656.61 665.48 13.45 o 2 3 3 232.82 247.42 5.80 o 3 3 3 25.14 27.03 0.94 o 4 3 3 4.61 4.15 0.20 o 5 3 3 156.13 164.16 4.98 o 6 3 3 3.18 3.62 0.72 o 7 3 3 1.68 1.38 0.45 o 8 3 3 101.65 100.92 5.15 o -8 4 3 0.54 0.05 0.23 o -7 4 3 133.62 139.27 5.77 o -6 4 3 6.85 5.84 0.36 o -5 4 3 14.35 14.06 0.46 o -4 4 3 66.25 65.65 1.48 o -3 4 3 0.15 0.29 0.34 o -2 4 3 31.34 30.56 0.85 o -1 4 3 0.02 0.11 0.12 o 0 4 3 58.32 58.71 1.68 o 1 4 3 17.02 15.97 0.43 o 2 4 3 1.83 1.84 0.19 o 3 4 3 0.15 0.33 0.16 o 4 4 3 0.69 0.58 0.17 o 5 4 3 31.16 29.35 1.66 o 6 4 3 150.47 148.29 5.85 o 7 4 3 0.63 0.57 0.30 o 8 4 3 6.24 5.63 0.68 o -7 5 3 14.49 14.48 1.09 o -6 5 3 65.81 62.90 3.30 o -5 5 3 52.88 53.16 1.99 o -4 5 3 11.59 10.58 0.66 o -3 5 3 19.16 19.81 0.63 o -2 5 3 1.22 1.78 0.26 o -1 5 3 24.57 23.53 0.62 o 0 5 3 47.14 48.37 1.20 o 1 5 3 36.97 34.39 1.18 o 2 5 3 151.18 149.22 4.92 o 3 5 3 8.20 6.47 0.46 o 4 5 3 30.82 30.55 2.35 o 5 5 3 38.24 34.27 1.78 o 6 5 3 14.61 14.39 0.85 o -5 6 3 3.16 2.75 0.45 o -4 6 3 1.58 2.60 1.06 o -3 6 3 12.27 11.47 0.87 o -2 6 3 21.34 21.18 0.93 o -1 6 3 48.52 48.13 2.17 o 0 6 3 30.02 29.65 1.49 o 1 6 3 33.27 33.82 1.44 o 2 6 3 29.52 30.75 2.28 o 3 6 3 2.70 2.59 0.35 o 4 6 3 0.40 0.67 0.31 o 5 6 3 64.91 63.91 2.92 o -1 7 3 13.64 12.37 0.77 o 0 7 3 9.31 9.59 1.08 o -8 0 4 134.73 143.55 4.73 o -6 0 4 439.80 450.22 11.29 o -4 0 4 26.22 27.69 1.42 o -2 0 4 88.46 86.72 4.06 o 2 0 4 202.49 220.73 7.69 o 4 0 4 256.09 297.63 9.14 o 6 0 4 43.20 39.85 1.68 o 8 0 4 2.67 4.09 0.52 o -9 1 4 30.73 29.17 2.40 o -8 1 4 175.42 186.20 4.63 o -7 1 4 4.27 3.71 0.14 o -6 1 4 4.14 4.45 0.21 o -5 1 4 2.03 1.91 0.16 o -4 1 4 612.64 597.86 15.10 o -3 1 4 223.10 197.72 4.00 o -2 1 4 65.77 57.26 1.00 o -1 1 4 653.85 621.98 17.66 o 0 1 4 443.48 449.69 8.25 o 1 1 4 11.73 10.27 0.23 o 2 1 4 132.02 135.45 3.47 o 3 1 4 4.77 5.34 0.22 o 4 1 4 7.74 7.50 0.34 o 5 1 4 23.81 27.02 1.08 o 6 1 4 24.08 23.05 0.62 o 7 1 4 20.96 20.97 0.87 o 8 1 4 16.40 17.02 0.79 o 9 1 4 16.24 16.30 1.00 o -9 2 4 13.91 12.70 1.31 o -8 2 4 9.87 9.96 0.50 o -7 2 4 0.04 0.05 0.12 o -6 2 4 165.48 173.04 5.37 o -5 2 4 25.66 23.94 0.85 o -4 2 4 107.55 106.70 2.80 o -3 2 4 155.63 146.30 2.65 o -2 2 4 1.00 1.18 0.11 o -1 2 4 11.06 9.99 0.24 o 0 2 4 195.53 203.15 3.98 o 1 2 4 1.51 1.39 0.09 o 2 2 4 0.11 0.08 0.08 o 3 2 4 783.82 830.51 23.49 o 4 2 4 77.28 80.22 2.02 o 5 2 4 26.44 28.35 0.71 o 6 2 4 4.56 4.92 0.25 o 7 2 4 1.25 1.88 0.28 o 8 2 4 16.02 14.49 0.87 o 9 2 4 2.16 2.82 0.73 o -8 3 4 3.21 2.12 0.37 o -7 3 4 0.46 0.30 0.14 o -6 3 4 12.85 11.90 0.91 o -5 3 4 59.37 60.10 1.43 o -4 3 4 5.10 4.07 0.16 o -3 3 4 290.32 289.03 7.45 o -2 3 4 129.77 119.34 2.29 o -1 3 4 409.80 427.05 9.24 o 0 3 4 0.73 0.73 0.14 o 1 3 4 167.52 169.43 3.55 o 2 3 4 446.83 451.38 14.57 o 3 3 4 52.28 55.41 1.84 o 4 3 4 31.20 30.36 1.17 o 5 3 4 23.74 21.72 0.81 o 6 3 4 15.32 14.21 0.57 o 7 3 4 12.55 11.12 0.66 o 8 3 4 25.52 24.15 1.44 o -7 4 4 21.83 20.35 1.33 o -6 4 4 7.34 7.42 0.47 o -5 4 4 6.73 6.76 0.32 o -4 4 4 70.09 70.31 2.10 o -3 4 4 11.31 11.19 0.31 o -2 4 4 77.98 75.49 2.10 o -1 4 4 128.79 128.84 2.84 o 0 4 4 137.85 142.45 4.97 o 1 4 4 88.93 95.97 2.37 o 2 4 4 19.70 17.20 0.65 o 3 4 4 144.37 141.59 3.76 o 4 4 4 31.57 33.90 1.10 o 5 4 4 31.05 30.73 1.19 o 6 4 4 108.14 97.09 8.67 o 7 4 4 14.98 15.46 0.94 o -6 5 4 2.64 2.76 0.32 o -5 5 4 28.66 29.37 1.16 o -4 5 4 293.34 303.49 14.42 o -3 5 4 0.84 0.61 0.23 o -2 5 4 103.16 103.99 3.04 o -1 5 4 8.57 8.69 0.42 o 0 5 4 29.50 27.06 0.75 o 1 5 4 84.73 82.63 4.14 o 2 5 4 1.79 1.97 0.30 o 3 5 4 47.29 48.32 2.03 o 4 5 4 160.09 164.14 8.31 o 5 5 4 1.16 1.57 0.36 o 6 5 4 20.41 20.37 1.29 o -4 6 4 3.99 3.79 0.42 o -3 6 4 23.92 26.91 1.31 o -2 6 4 192.96 201.65 10.43 o -1 6 4 3.43 4.77 0.99 o 0 6 4 13.64 12.94 0.82 o 1 6 4 16.18 14.88 0.86 o 2 6 4 0.78 0.67 0.59 o 3 6 4 33.34 34.78 1.60 o 4 6 4 41.26 41.42 2.27 o -9 0 5 9.20 10.60 1.39 o -7 0 5 7.52 6.58 0.23 o -5 0 5 237.50 240.16 10.65 o -3 0 5 400.06 387.22 19.41 o -1 0 5 1396.77 1454.46 73.26 o 1 0 5 88.47 84.88 2.35 o 3 0 5 0.00 -0.03 0.09 o 5 0 5 326.65 334.18 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