#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/68/2206891.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206891_Fobs loop_ _publ_author_name 'Klausmeyer, Kevin K.' 'Adrian, Rafael A.' _publ_section_title ; Tris(tetraethylammonium) \m-3-hydroxypropanolato-di-\m-methoxo-bis[tricarbonyltungsten(0)] ; _journal_coeditor_code BV6028 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2039 _journal_page_last m2041 _journal_volume 61 _journal_year 2005 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.9476 _cell_length_b 24.1286 _cell_length_c 10.2457 _exptl_crystal_F_000 2120.00 _reflns_d_resolution_high 0.7500 _[local]_cod_data_source_file bv6028Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kk28a in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 663.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 440001.66 443915.78 15176.15 o 6 0 0 5332.65 4423.45 175.96 o 8 0 0 290588.03 285820.09 6481.49 o 10 0 0 21866.62 20009.05 470.55 o 12 0 0 114805.28 117176.87 2674.34 o 14 0 0 4919.85 4735.48 341.70 o 2 1 0 308918.25 326283.94 16251.23 o 4 1 0 1324.27 1620.46 49.80 o 6 1 0 188785.41 194108.11 4696.33 o 8 1 0 2828.63 2678.04 56.91 o 10 1 0 106620.04 105608.09 1699.54 o 12 1 0 9097.55 9099.49 218.38 o 14 1 0 61770.30 58919.90 1135.26 o 16 1 0 13086.66 13680.48 461.67 o 2 2 0 1692.14 1221.62 124.64 o 4 2 0 143812.36 151848.83 3670.79 o 6 2 0 417.54 607.08 24.56 o 8 2 0 28177.99 26749.90 618.45 o 10 2 0 3373.69 2843.60 79.44 o 12 2 0 37000.26 36961.43 715.74 o 14 2 0 7008.01 6632.11 154.41 o 16 2 0 16081.65 16297.67 537.66 o 18 2 0 2706.27 2718.06 151.08 o 2 3 0 7255.55 7297.91 185.38 o 4 3 0 7937.51 8881.81 260.39 o 6 3 0 18099.04 18396.64 356.73 o 8 3 0 1675.86 1584.35 45.24 o 10 3 0 5955.09 6064.14 132.81 o 12 3 0 5416.69 5155.60 121.96 o 14 3 0 5589.50 5528.07 134.59 o 16 3 0 1084.71 970.89 92.87 o 18 3 0 2471.33 2659.40 148.86 o 0 4 0 18977.51 17173.83 419.46 o 4 4 0 7485.03 7263.43 187.11 o 6 4 0 1222.92 1082.34 31.17 o 8 4 0 8347.60 8754.80 170.81 o 10 4 0 1212.90 1016.41 38.73 o 12 4 0 319.20 190.54 33.13 o 14 4 0 4409.28 4388.01 113.96 o 16 4 0 2305.17 2295.48 125.31 o 18 4 0 82.11 10.22 79.54 o 20 4 0 11.26 -101.75 101.75 o 2 5 0 52123.98 65058.63 1576.65 o 4 5 0 13.01 9.48 36.88 o 6 5 0 45470.11 47321.09 748.02 o 8 5 0 1624.57 1289.68 40.88 o 10 5 0 54458.54 51581.29 944.67 o 12 5 0 2654.83 2332.11 70.16 o 14 5 0 19248.14 17715.96 360.10 o 16 5 0 3130.04 3233.05 161.74 o 18 5 0 9110.90 8608.29 322.59 o 20 5 0 1854.79 1904.02 146.19 o 0 6 0 108569.01 126005.43 3049.77 o 2 6 0 202.74 250.50 17.42 o 4 6 0 115568.32 125180.03 3138.18 o 6 6 0 15108.26 13963.43 281.77 o 8 6 0 67695.90 67616.22 1067.21 o 10 6 0 11823.08 11084.31 216.05 o 12 6 0 63445.51 63380.88 1162.92 o 14 6 0 6169.33 6276.63 150.12 o 16 6 0 22969.00 24270.99 774.94 o 18 6 0 4868.84 4583.41 214.17 o 20 6 0 15698.25 16367.43 559.87 o 22 6 0 3914.82 4007.99 217.73 o 2 7 0 89388.60 102904.59 2496.31 o 4 7 0 9877.24 9192.35 157.49 o 6 7 0 194474.70 202332.94 2818.39 o 8 7 0 11069.02 9889.62 166.25 o 10 7 0 124292.84 119899.66 2176.99 o 12 7 0 18530.68 17233.16 330.23 o 14 7 0 54550.41 53524.80 989.93 o 16 7 0 8412.94 8274.59 299.93 o 18 7 0 30751.02 31098.35 989.11 o 20 7 0 10828.98 11428.54 416.35 o 22 7 0 12378.42 12688.20 426.79 o 0 8 0 7582.89 8274.77 215.85 o 2 8 0 4183.11 3549.49 60.92 o 4 8 0 227530.44 239864.34 5790.03 o 6 8 0 7829.07 6955.17 107.55 o 8 8 0 98434.48 100249.53 1578.77 o 10 8 0 11897.60 11347.73 192.61 o 12 8 0 59351.48 59483.88 1093.49 o 14 8 0 19685.56 19422.62 375.23 o 16 8 0 31356.21 32029.25 1008.66 o 18 8 0 11284.45 11814.23 414.57 o 20 8 0 14546.30 14845.46 439.24 o 2 9 0 59022.34 63814.83 930.27 o 4 9 0 1030.75 771.66 29.27 o 6 9 0 132000.78 138826.55 1932.13 o 8 9 0 7023.61 6564.21 104.29 o 10 9 0 69965.66 70417.47 1130.39 o 12 9 0 4820.06 4680.78 158.06 o 14 9 0 22749.48 21921.96 405.73 o 16 9 0 7930.86 8044.11 215.63 o 18 9 0 18421.35 18963.11 708.95 o 20 9 0 5645.91 6448.33 203.15 o 0 10 0 71132.76 79449.89 1506.71 o 2 10 0 7.63 -10.34 10.97 o 4 10 0 14760.75 15155.75 244.89 o 6 10 0 29.10 53.89 17.98 o 8 10 0 49070.95 50395.68 710.27 o 10 10 0 505.13 467.84 27.35 o 12 10 0 7657.37 7755.65 143.12 o 14 10 0 51.73 62.67 41.18 o 16 10 0 8273.11 8686.80 187.60 o 18 10 0 1695.49 1740.21 144.63 o 20 10 0 5184.94 5507.71 251.94 o 2 11 0 104.86 119.48 36.35 o 4 11 0 22.14 50.32 18.28 o 6 11 0 1296.48 1497.56 42.00 o 8 11 0 16.77 -18.44 19.97 o 10 11 0 1256.84 1174.05 42.07 o 12 11 0 114.65 60.26 31.33 o 14 11 0 42.94 66.32 41.02 o 16 11 0 7.28 -18.54 47.45 o 18 11 0 372.87 422.43 76.31 o 20 11 0 197.71 117.78 84.23 o 0 12 0 72033.20 71536.30 1627.86 o 2 12 0 463.61 603.27 28.22 o 4 12 0 20503.49 19224.88 276.75 o 6 12 0 56.85 73.24 17.81 o 8 12 0 15787.34 16092.02 236.63 o 10 12 0 6081.89 5740.74 98.30 o 12 12 0 6584.13 6015.74 144.43 o 14 12 0 125.15 242.64 46.29 o 16 12 0 3500.15 3204.94 191.32 o 18 12 0 1960.61 1788.27 99.46 o 20 12 0 2718.26 2614.94 165.52 o 2 13 0 103995.37 110317.98 1453.06 o 4 13 0 363.73 373.33 33.96 o 6 13 0 79831.56 78835.98 1102.71 o 8 13 0 3382.77 3301.84 75.30 o 10 13 0 31744.93 32192.60 516.74 o 12 13 0 2110.54 2236.73 62.45 o 14 13 0 23183.48 22503.25 509.15 o 16 13 0 6325.46 6276.03 182.32 o 18 13 0 7815.38 7589.02 284.15 o 20 13 0 4334.71 4654.58 277.49 o 0 14 0 212494.89 227186.91 6945.99 o 2 14 0 359.62 573.59 35.76 o 4 14 0 146117.00 152488.64 2374.16 o 6 14 0 5131.34 5136.39 99.90 o 8 14 0 114808.39 116321.02 1816.35 o 10 14 0 5850.75 5579.23 125.85 o 12 14 0 43366.47 44007.87 788.92 o 14 14 0 11736.31 12193.48 243.90 o 16 14 0 27137.97 26979.05 500.13 o 18 14 0 7843.43 8398.07 193.71 o 20 14 0 8881.22 8783.28 256.32 o 2 15 0 167428.91 176326.56 2337.22 o 4 15 0 2289.06 2441.35 61.25 o 6 15 0 101377.05 102565.37 1603.41 o 8 15 0 6039.17 5490.32 108.15 o 10 15 0 71112.84 71979.55 1132.29 o 12 15 0 6481.19 6494.47 147.21 o 14 15 0 38817.05 39028.22 706.06 o 16 15 0 9856.82 10288.31 218.78 o 18 15 0 15181.38 15556.10 380.32 o 0 16 0 172598.05 179174.39 3256.07 o 2 16 0 7.27 102.72 40.15 o 4 16 0 96866.20 101159.73 1580.37 o 6 16 0 6373.05 6110.03 116.69 o 8 16 0 61307.65 63758.97 1002.20 o 10 16 0 3650.03 3457.54 84.79 o 12 16 0 52179.53 52241.42 933.78 o 14 16 0 3976.18 4223.46 121.06 o 16 16 0 18912.04 19117.39 490.97 o 18 16 0 3803.31 4027.87 124.26 o 2 17 0 66828.39 69657.09 1093.13 o 4 17 0 1672.54 1727.40 49.64 o 6 17 0 28009.54 27861.41 449.19 o 8 17 0 1287.24 1200.67 47.06 o 10 17 0 18974.76 20317.96 421.06 o 12 17 0 4792.39 4966.37 203.38 o 14 17 0 18440.24 19172.10 366.91 o 16 17 0 1485.18 1513.08 82.16 o 18 17 0 3620.88 3502.73 115.84 o 0 18 0 550.89 601.87 69.76 o 2 18 0 68.90 139.50 28.61 o 4 18 0 3087.84 3294.38 76.84 o 6 18 0 517.78 551.59 37.87 o 8 18 0 62.60 43.00 35.15 o 10 18 0 3.39 -11.14 63.16 o 12 18 0 2742.15 2798.48 93.42 o 14 18 0 223.15 198.69 56.44 o 16 18 0 564.77 553.92 68.57 o 18 18 0 46.99 17.62 71.07 o 2 19 0 1509.55 1592.53 49.14 o 4 19 0 679.05 631.13 45.73 o 6 19 0 5349.62 5160.76 106.99 o 8 19 0 77.05 66.53 38.94 o 10 19 0 5644.67 5357.21 131.47 o 12 19 0 256.83 265.00 70.00 o 14 19 0 827.70 777.71 103.61 o 16 19 0 299.36 230.88 69.18 o 18 19 0 1736.50 1935.71 99.50 o 0 20 0 3039.92 3267.27 154.19 o 2 20 0 145.04 161.15 34.08 o 4 20 0 20727.57 20827.94 342.80 o 6 20 0 1576.40 1634.58 54.85 o 8 20 0 11900.06 11460.33 230.34 o 10 20 0 394.01 440.56 79.96 o 12 20 0 9537.85 9629.92 208.50 o 14 20 0 4679.88 5008.28 142.72 o 16 20 0 4295.79 4686.05 138.46 o 2 21 0 54917.88 56132.54 1032.11 o 4 21 0 715.85 713.39 53.60 o 6 21 0 43283.90 43619.16 783.45 o 8 21 0 981.82 1056.43 72.00 o 10 21 0 38930.63 38756.47 703.74 o 12 21 0 4288.19 4283.45 160.86 o 14 21 0 19128.20 19605.38 586.50 o 16 21 0 3117.73 3158.60 164.49 o 0 22 0 89465.47 91458.12 2782.93 o 2 22 0 1582.75 1529.52 80.10 o 4 22 0 69353.00 70051.10 1241.35 o 6 22 0 702.60 726.91 56.12 o 8 22 0 52209.05 52334.32 938.31 o 10 22 0 6311.36 6151.37 170.47 o 12 22 0 31393.39 31744.24 587.55 o 14 22 0 3304.52 3343.42 113.97 o 16 22 0 15482.20 16319.44 403.42 o 2 23 0 60415.04 60458.91 1312.25 o 4 23 0 124.93 193.02 60.92 o 6 23 0 46259.50 46209.49 968.65 o 8 23 0 2207.63 2199.01 84.31 o 10 23 0 29690.24 29468.74 547.44 o 12 23 0 3157.40 3190.95 115.02 o 14 23 0 19301.37 19387.39 492.39 o 0 24 0 15258.21 15152.60 507.44 o 2 24 0 74.96 187.27 60.48 o 4 24 0 25858.65 25510.89 578.42 o 6 24 0 349.67 397.63 75.62 o 8 24 0 25091.74 25056.94 575.90 o 10 24 0 1239.23 1103.53 76.41 o 12 24 0 9738.35 10020.36 225.93 o 14 24 0 2814.22 3430.60 119.49 o 2 25 0 3697.62 3718.65 141.45 o 4 25 0 4.73 -23.03 63.52 o 6 25 0 4591.73 4472.25 491.89 o 8 25 0 907.35 1075.82 92.44 o 10 25 0 4561.12 4499.90 163.93 o 12 25 0 269.70 162.15 99.28 o 14 25 0 1207.37 1292.11 124.31 o 0 26 0 3040.13 2999.33 167.52 o 2 26 0 104.68 87.68 68.26 o 4 26 0 669.23 764.52 85.57 o 6 26 0 298.35 396.99 83.36 o 8 26 0 3.42 -53.93 79.43 o 10 26 0 163.73 120.07 93.72 o 12 26 0 361.76 235.78 104.63 o 2 27 0 11508.57 11970.65 405.24 o 4 27 0 26.21 34.23 77.04 o 6 27 0 6764.15 6795.78 211.74 o 8 27 0 573.59 587.61 101.00 o 10 27 0 4507.13 4287.93 387.25 o 12 27 0 854.33 734.50 179.07 o 0 28 0 40384.05 42114.54 1324.59 o 2 28 0 18.22 196.74 79.03 o 4 28 0 21157.17 20307.59 480.16 o 6 28 0 1032.34 1082.23 172.85 o 8 28 0 16378.02 16516.23 412.26 o 10 28 0 2149.49 1797.10 128.96 o 2 29 0 31727.26 31610.02 717.46 o 4 29 0 656.00 813.84 231.73 o 6 29 0 25647.83 26694.41 657.18 o 8 29 0 2668.43 3042.06 182.40 o 0 30 0 24109.08 24148.79 797.60 o 2 30 0 3.71 286.70 204.84 o 4 30 0 27320.02 28571.62 660.65 o 6 30 0 1860.65 1749.89 196.18 o 8 30 0 20010.46 21746.38 1097.09 o 2 31 0 18165.52 18963.00 462.81 o 4 31 0 528.90 512.58 108.22 o 6 31 0 15124.43 15805.00 761.61 o 0 32 0 9094.11 9096.18 376.36 o 2 32 0 230.83 363.72 107.93 o 1 0 1 156405.22 176058.22 6038.20 o 2 0 1 88173.87 88308.37 2136.40 o 3 0 1 51631.76 57859.17 1401.96 o 4 0 1 400.79 754.31 35.99 o 5 0 1 21444.35 19378.91 455.20 o 6 0 1 28815.25 28540.44 555.08 o 7 0 1 11646.25 12332.90 243.79 o 8 0 1 2084.75 2450.14 53.02 o 9 0 1 93040.86 94522.54 1534.57 o 10 0 1 25614.04 25702.29 438.11 o 11 0 1 11085.90 11299.16 197.29 o 12 0 1 2559.35 2408.74 63.80 o 13 0 1 48301.79 47133.88 771.96 o 14 0 1 16664.23 15629.21 272.34 o 15 0 1 5303.75 4826.42 182.63 o 0 1 1 102689.29 105743.19 2446.13 o 1 1 1 81641.53 87064.17 1336.87 o 2 1 1 985.37 723.21 23.56 o 3 1 1 65368.42 69853.81 1196.06 o 4 1 1 51258.66 53335.84 914.85 o 5 1 1 19688.69 21194.56 291.65 o 6 1 1 824.93 721.22 24.17 o 7 1 1 93431.30 89706.08 1087.83 o 8 1 1 42915.52 39899.07 457.58 o 9 1 1 17687.81 16842.30 199.35 o 10 1 1 2762.30 2769.77 49.57 o 11 1 1 62088.25 60410.41 693.27 o 12 1 1 30973.96 29420.30 370.08 o 13 1 1 7224.81 7175.17 125.49 o 14 1 1 3174.01 3157.55 67.39 o 15 1 1 42551.12 43516.00 651.24 o 16 1 1 12207.02 11872.02 320.15 o 1 2 1 73239.91 80090.66 1064.56 o 2 2 1 193701.45 186968.19 3704.54 o 3 2 1 100004.41 99359.98 1698.95 o 4 2 1 4466.73 4844.23 102.02 o 5 2 1 97687.69 102827.02 1383.88 o 6 2 1 43570.50 43333.87 637.10 o 7 2 1 22674.26 23063.18 309.28 o 8 2 1 7844.58 7099.27 93.80 o 9 2 1 36282.16 34851.16 463.95 o 10 2 1 15780.92 15809.05 222.10 o 11 2 1 8834.99 8584.51 127.97 o 12 2 1 902.73 785.40 38.02 o 13 2 1 43282.14 41852.28 574.39 o 14 2 1 19665.75 20271.55 287.85 o 15 2 1 2945.28 3017.38 92.74 o 16 2 1 1362.34 1400.52 73.50 o 17 2 1 12165.45 12350.56 301.41 o 18 2 1 3952.69 4063.98 192.85 o 0 3 1 4323.14 4415.43 80.84 o 1 3 1 870.70 1355.59 20.35 o 2 3 1 302.25 161.30 7.68 o 3 3 1 12076.02 12692.25 220.62 o 4 3 1 3713.04 4063.89 100.69 o 5 3 1 12506.75 13707.54 188.99 o 6 3 1 2495.70 2472.66 34.84 o 7 3 1 6165.59 5779.87 81.39 o 8 3 1 1587.35 1393.83 33.42 o 9 3 1 1328.79 1053.17 29.08 o 10 3 1 2463.98 2571.79 63.59 o 11 3 1 10496.84 10649.53 151.92 o 12 3 1 2312.05 2168.46 49.61 o 13 3 1 1026.38 780.19 32.14 o 14 3 1 800.53 737.41 35.62 o 15 3 1 1761.36 1828.29 65.62 o 16 3 1 1567.19 1615.07 74.83 o 17 3 1 49.12 -18.62 55.48 o 18 3 1 690.61 610.11 70.43 o 19 3 1 2695.96 2662.92 111.10 o 1 4 1 5439.79 5479.78 72.92 o 2 4 1 8224.47 10171.98 164.84 o 3 4 1 1008.48 1201.47 36.46 o 4 4 1 13.08 9.50 10.26 o 5 4 1 5595.19 6161.13 98.16 o 6 4 1 7822.83 9385.88 118.88 o 7 4 1 2334.77 2133.11 33.80 o 8 4 1 466.50 529.90 18.70 o 9 4 1 710.27 681.38 19.92 o 10 4 1 738.25 616.09 20.95 o 11 4 1 98.35 54.40 19.03 o 12 4 1 188.90 180.81 22.17 o 13 4 1 550.13 509.96 29.17 o 14 4 1 121.49 122.40 28.30 o 15 4 1 45.54 -6.31 42.56 o 16 4 1 93.98 54.15 48.17 o 17 4 1 894.67 830.59 118.42 o 18 4 1 7.03 -27.16 57.41 o 19 4 1 33.24 -64.80 66.77 o 20 4 1 2.66 -59.54 74.08 o 0 5 1 15853.55 19161.97 331.09 o 1 5 1 38735.21 40597.10 514.76 o 2 5 1 273.84 156.89 6.97 o 3 5 1 35242.07 36797.37 585.41 o 4 5 1 47926.52 49492.29 663.99 o 5 5 1 8208.26 8675.87 112.23 o 6 5 1 65.60 86.78 20.21 o 7 5 1 20458.87 19320.84 235.01 o 8 5 1 26248.46 26608.02 320.91 o 9 5 1 8984.64 9359.83 119.74 o 10 5 1 146.36 112.82 17.52 o 11 5 1 13355.15 12570.69 190.76 o 12 5 1 10566.28 10079.01 145.94 o 13 5 1 1615.52 1504.56 40.21 o 14 5 1 825.95 760.52 34.64 o 15 5 1 10188.33 9421.62 317.48 o 16 5 1 3767.04 3539.61 118.06 o 17 5 1 992.03 894.88 68.45 o 18 5 1 502.26 465.90 107.09 o 19 5 1 4040.80 4167.49 145.45 o 20 5 1 1998.51 1906.40 102.95 o 21 5 1 151.30 -68.38 81.49 o 1 6 1 72594.19 77057.52 1024.14 o 2 6 1 49974.52 54472.85 810.50 o 3 6 1 91236.45 97568.15 1669.90 o 4 6 1 5342.56 4678.28 56.96 o 5 6 1 49340.27 51254.94 689.24 o 6 6 1 47837.20 49083.46 584.83 o 7 6 1 17826.36 17813.75 217.23 o 8 6 1 5195.85 4875.57 62.91 o 9 6 1 33853.45 33005.09 397.48 o 10 6 1 38175.80 36498.01 440.08 o 11 6 1 11993.34 11702.52 149.77 o 12 6 1 7385.12 7144.70 117.47 o 13 6 1 31140.74 30533.32 412.72 o 14 6 1 8189.25 8067.04 124.92 o 15 6 1 2172.05 2058.15 103.09 o 16 6 1 3964.25 3779.11 122.15 o 17 6 1 16218.16 15976.87 518.33 o 18 6 1 7692.78 7391.53 236.17 o 19 6 1 543.82 609.19 74.12 o 20 6 1 2329.84 2677.51 116.39 o 21 6 1 11366.91 12010.11 256.15 o 22 6 1 1589.34 1677.93 98.35 o 0 7 1 19582.80 22569.23 400.68 o 1 7 1 38750.24 39590.79 525.28 o 2 7 1 13.55 76.93 12.16 o 3 7 1 141116.06 152459.34 1939.00 o 4 7 1 72507.86 78513.23 865.51 o 5 7 1 74698.65 78936.25 831.22 o 6 7 1 4717.60 4558.36 54.98 o 7 7 1 69888.33 69861.44 775.08 o 8 7 1 67549.93 68814.15 821.23 o 9 7 1 21747.27 21962.29 249.98 o 10 7 1 3305.51 2932.80 46.66 o 11 7 1 51340.32 49429.06 553.36 o 12 7 1 26290.75 25558.61 312.88 o 13 7 1 6261.47 6046.69 109.09 o 14 7 1 6889.68 6581.20 107.49 o 15 7 1 24914.74 23957.39 474.26 o 16 7 1 14986.81 14770.02 346.54 o 17 7 1 2695.77 2432.00 94.47 o 18 7 1 2646.77 2713.89 102.57 o 19 7 1 21402.61 21785.22 413.94 o 20 7 1 6041.11 6486.04 202.23 o 21 7 1 276.37 456.90 72.36 o 1 8 1 35381.61 39622.66 582.12 o 2 8 1 89307.94 96508.98 1087.43 o 3 8 1 65262.81 69811.20 767.93 o 4 8 1 1978.60 1786.65 25.61 o 5 8 1 72818.43 74789.63 801.61 o 6 8 1 61972.82 65061.52 678.78 o 7 8 1 44731.55 45614.80 509.61 o 8 8 1 10675.36 10420.87 123.67 o 9 8 1 46911.19 46602.68 521.29 o 10 8 1 32871.85 32426.19 366.74 o 11 8 1 11467.86 11718.75 140.94 o 12 8 1 2439.96 2176.93 42.09 o 13 8 1 31797.63 31807.78 388.29 o 14 8 1 15667.54 15596.56 233.34 o 15 8 1 4856.69 5060.03 106.80 o 16 8 1 1934.19 2043.47 71.91 o 17 8 1 20759.23 20703.54 389.99 o 18 8 1 8765.22 8632.23 188.08 o 19 8 1 673.88 876.95 70.11 o 20 8 1 2248.83 2254.77 146.90 o 21 8 1 14229.74 14978.78 304.88 o 0 9 1 31299.86 34768.70 522.57 o 1 9 1 18948.99 20129.15 312.25 o 2 9 1 81.00 95.39 9.09 o 3 9 1 44559.49 44911.16 475.65 o 4 9 1 58354.14 61105.76 685.52 o 5 9 1 32141.74 32575.52 406.57 o 6 9 1 954.87 884.64 25.62 o 7 9 1 61445.89 61257.37 639.97 o 8 9 1 41128.12 41563.16 436.93 o 9 9 1 13512.98 14018.27 154.90 o 10 9 1 1844.02 1701.82 31.79 o 11 9 1 20697.48 20431.04 236.13 o 12 9 1 13064.18 12670.94 152.69 o 13 9 1 3778.10 3650.93 63.78 o 14 9 1 2714.60 2657.00 104.09 o 15 9 1 16497.90 16172.17 267.15 o 16 9 1 6619.20 6417.87 127.47 o 17 9 1 1136.69 1193.67 63.27 o 18 9 1 1555.39 1594.81 74.30 o 19 9 1 12946.01 13879.88 279.47 o 20 9 1 4145.73 4151.26 131.99 o 21 9 1 585.81 625.87 69.43 o 1 10 1 24163.37 24596.65 308.29 o 2 10 1 5000.39 4753.38 54.97 o 3 10 1 2176.48 2137.31 30.98 o 4 10 1 4.42 63.73 11.63 o 5 10 1 7251.77 7234.26 79.66 o 6 10 1 8256.30 9238.57 100.41 o 7 10 1 6673.66 7434.26 88.23 o 8 10 1 10.19 53.04 14.66 o 9 10 1 20789.42 21198.28 229.02 o 10 10 1 6096.39 6226.37 77.38 o 11 10 1 1476.61 1644.13 46.97 o 12 10 1 1346.60 1206.28 42.44 o 13 10 1 2090.98 1970.63 41.33 o 14 10 1 539.94 494.13 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265.78 o 10 8 2 1113.21 1068.03 26.04 o 11 8 2 51938.29 51556.68 578.03 o 12 8 2 13124.94 12629.53 152.09 o 13 8 2 3527.14 3523.49 59.55 o 14 8 2 233.95 274.24 28.46 o 15 8 2 44033.51 42351.52 658.67 o 16 8 2 4783.54 5190.85 124.29 o 17 8 2 2270.26 2222.79 117.36 o 18 8 2 1103.00 1170.06 76.33 o 19 8 2 20873.34 20871.31 398.70 o 20 8 2 2541.55 2812.18 179.29 o 21 8 2 24.21 214.21 74.71 o 1 9 2 59400.16 62591.11 893.81 o 2 9 2 7663.08 7750.74 87.42 o 3 9 2 51279.36 51908.59 547.63 o 4 9 2 538.38 509.88 16.56 o 5 9 2 72490.26 74537.30 773.44 o 6 9 2 12359.98 11044.54 115.01 o 7 9 2 29003.03 30843.27 316.45 o 8 9 2 999.76 936.38 21.15 o 9 9 2 63721.75 63380.78 706.43 o 10 9 2 4860.37 4689.80 65.10 o 11 9 2 8908.85 9224.40 114.44 o 12 9 2 93.16 99.76 21.40 o 13 9 2 25267.07 24662.96 284.90 o 14 9 2 4511.29 4461.02 79.73 o 15 9 2 2241.28 2120.01 75.23 o 16 9 2 459.95 494.94 45.60 o 17 9 2 18873.63 18714.14 308.66 o 18 9 2 1608.09 1708.07 76.54 o 19 9 2 803.79 891.81 68.26 o 20 9 2 295.94 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5027.13 4929.04 91.07 o 3 13 2 17738.15 18893.66 203.39 o 4 13 2 834.26 783.01 26.38 o 5 13 2 38474.38 37399.88 394.24 o 6 13 2 18530.89 18777.45 203.03 o 7 13 2 8462.19 8340.72 97.51 o 8 13 2 2572.02 2500.29 56.26 o 9 13 2 32095.02 32208.43 343.19 o 10 13 2 5238.01 5119.55 69.10 o 11 13 2 3298.45 3348.59 65.50 o 12 13 2 328.07 291.40 26.41 o 13 13 2 29234.13 28715.21 344.36 o 14 13 2 731.47 724.93 35.67 o 15 13 2 3355.22 3458.04 69.00 o 16 13 2 650.83 545.36 59.25 o 17 13 2 13669.31 13398.19 211.28 o 18 13 2 1286.17 1172.85 59.26 o 19 13 2 252.38 303.63 53.62 o 20 13 2 274.37 255.34 64.32 o 0 14 2 23671.03 24413.45 390.06 o 1 14 2 43340.58 44194.42 476.78 o 2 14 2 25.91 22.07 13.00 o 3 14 2 77862.65 78982.17 799.82 o 4 14 2 7864.73 7750.18 86.12 o 5 14 2 34937.76 36360.36 363.62 o 6 14 2 620.78 591.08 21.08 o 7 14 2 60295.19 59138.13 619.67 o 8 14 2 15873.57 15853.12 175.49 o 9 14 2 12888.08 13072.29 148.15 o 10 14 2 708.11 668.24 27.87 o 11 14 2 54528.54 53907.94 597.07 o 12 14 2 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