#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/68/2206893.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206893_Fobs loop_ _publ_author_name 'Lund, Clinton L.' 'Schachner, J\"org A.' 'Quail, J. Wilson' 'M\"uller, Jens' _publ_section_title ; A monomeric fourfold-coordinated indium dihalide with an unusual coordination geometry ; _journal_coeditor_code BV6030 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2063 _journal_page_last m2065 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 116.972 _cell_angle_gamma 90.000 _cell_length_a 9.9492 _cell_length_b 13.6254 _cell_length_c 18.9012 _exptl_crystal_F_000 1264.00 _reflns_d_resolution_high 0.6701 _[local]_cod_data_source_file bv6030IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound 231' _shelx_refln_list_code 4 _shelx_f_calc_maximum 471.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 33962.17 34009.36 429.24 o 3 0 0 8145.16 8832.89 126.71 o 4 0 0 13265.39 12146.07 188.94 o 5 0 0 22228.45 20351.79 296.90 o 6 0 0 5216.38 4736.22 101.22 o 7 0 0 1894.71 2003.35 65.60 o 8 0 0 23714.13 25108.24 446.11 o 9 0 0 2422.20 2381.23 107.59 o 10 0 0 2397.40 2702.12 165.32 o 11 0 0 1302.86 1521.26 200.56 o 12 0 0 132.76 89.97 116.21 o 13 0 0 4.37 89.97 168.32 o 2 1 0 6456.43 5661.73 70.85 o 3 1 0 55920.59 52747.36 590.62 o 4 1 0 68029.02 65302.75 630.25 o 5 1 0 19357.40 19742.42 377.88 o 6 1 0 6555.17 5615.71 119.40 o 7 1 0 1012.02 967.56 26.48 o 8 1 0 127.18 152.34 14.50 o 9 1 0 306.15 293.77 23.86 o 10 1 0 202.28 216.52 123.15 o 11 1 0 6565.34 6607.03 404.24 o 12 1 0 5517.89 6181.07 407.84 o 13 1 0 863.49 586.98 121.40 o 0 2 0 77905.07 69881.49 1508.33 o 1 2 0 2.87 81.24 8.08 o 2 2 0 25232.93 22018.72 272.54 o 3 2 0 19623.08 15168.66 177.53 o 4 2 0 13537.46 13363.82 166.63 o 5 2 0 612.13 770.10 20.45 o 6 2 0 3849.41 4106.39 65.22 o 7 2 0 21916.89 22428.16 281.33 o 8 2 0 35791.35 37800.89 501.83 o 9 2 0 4430.50 4655.36 272.16 o 10 2 0 139.26 135.30 45.00 o 11 2 0 4.05 -18.53 68.89 o 12 2 0 10.47 -89.97 89.97 o 13 2 0 213.41 220.56 189.31 o 1 3 0 17029.98 14617.41 155.91 o 2 3 0 608.19 527.20 36.18 o 3 3 0 34946.66 33371.43 362.84 o 4 3 0 69016.39 68223.18 815.17 o 5 3 0 13715.10 14031.69 167.17 o 6 3 0 501.99 425.67 18.72 o 7 3 0 600.72 591.76 25.99 o 8 3 0 30.07 60.84 39.36 o 9 3 0 1652.48 1667.90 174.51 o 10 3 0 1019.91 1012.79 111.71 o 11 3 0 3994.57 3974.14 206.85 o 12 3 0 2882.74 2820.70 273.29 o 13 3 0 139.45 37.89 95.59 o 0 4 0 93253.14 85925.15 1160.10 o 1 4 0 22554.21 21344.66 210.58 o 2 4 0 6088.86 5676.38 71.70 o 3 4 0 6988.61 6362.88 86.61 o 4 4 0 96.85 168.45 16.63 o 5 4 0 8413.27 7511.76 109.71 o 6 4 0 2513.58 2499.72 83.41 o 7 4 0 9202.01 9000.71 569.82 o 8 4 0 10463.91 10355.78 347.89 o 9 4 0 101.02 86.48 46.67 o 10 4 0 603.45 624.84 140.02 o 11 4 0 467.85 455.16 71.83 o 12 4 0 59.97 37.88 198.31 o 1 5 0 4908.74 3580.31 58.48 o 2 5 0 5584.97 4816.67 62.96 o 3 5 0 3822.21 3538.53 106.28 o 4 5 0 24970.55 24349.12 353.51 o 5 5 0 101.84 125.02 16.28 o 6 5 0 3238.07 3048.73 48.38 o 7 5 0 1767.78 1674.27 54.71 o 8 5 0 89.57 82.80 16.80 o 9 5 0 1177.29 1146.24 197.56 o 10 5 0 96.12 186.77 57.66 o 11 5 0 885.73 903.90 95.97 o 12 5 0 1996.99 2055.52 245.36 o 0 6 0 45159.60 42778.98 620.05 o 1 6 0 13983.48 13108.94 167.95 o 2 6 0 8384.72 8437.20 174.51 o 3 6 0 43.02 151.39 10.59 o 4 6 0 3885.43 3742.08 76.68 o 5 6 0 8081.33 7681.87 126.28 o 6 6 0 16135.75 16325.30 258.38 o 7 6 0 15.97 42.37 17.88 o 8 6 0 1437.79 1288.46 48.54 o 9 6 0 0.73 17.74 48.84 o 10 6 0 2433.22 2543.79 145.21 o 11 6 0 796.72 811.09 104.97 o 12 6 0 41.16 256.40 137.39 o 1 7 0 6480.19 5795.77 75.93 o 2 7 0 17254.72 17291.69 189.59 o 3 7 0 2766.30 3506.18 53.73 o 4 7 0 20451.61 18983.39 261.29 o 5 7 0 1652.91 1632.01 154.45 o 6 7 0 8567.70 8585.84 192.96 o 7 7 0 1569.67 1564.44 88.66 o 8 7 0 519.81 503.68 65.60 o 9 7 0 2767.87 2983.99 265.23 o 10 7 0 609.13 670.97 84.72 o 11 7 0 53.25 85.66 140.20 o 12 7 0 427.15 376.22 98.21 o 0 8 0 2627.75 3081.21 68.86 o 1 8 0 10687.00 10892.60 166.63 o 2 8 0 82898.02 82519.56 818.71 o 3 8 0 18995.39 17848.95 211.92 o 4 8 0 4168.82 3986.79 73.60 o 5 8 0 284.38 277.18 25.68 o 6 8 0 2711.96 2737.98 86.41 o 7 8 0 979.85 897.97 56.23 o 8 8 0 3046.74 2957.63 243.48 o 9 8 0 211.70 282.61 66.06 o 10 8 0 1080.38 1064.07 282.28 o 11 8 0 174.56 186.61 95.59 o 12 8 0 555.64 718.74 119.92 o 1 9 0 3833.27 3527.82 169.07 o 2 9 0 11790.71 11765.93 354.45 o 3 9 0 1155.01 1398.98 33.93 o 4 9 0 3685.50 3585.98 124.83 o 5 9 0 1987.62 2036.24 84.92 o 6 9 0 2895.36 3077.58 171.51 o 7 9 0 719.65 701.78 44.86 o 8 9 0 259.70 262.99 62.35 o 9 9 0 3470.29 3675.65 214.98 o 10 9 0 1766.19 1931.64 159.63 o 11 9 0 634.16 384.74 72.34 o 0 10 0 5426.73 4537.18 225.49 o 1 10 0 868.65 782.75 28.42 o 2 10 0 886.97 995.93 37.05 o 3 10 0 28.33 8.73 33.55 o 4 10 0 4631.14 4619.51 124.64 o 5 10 0 14412.58 14310.78 477.60 o 6 10 0 17311.34 18624.04 594.93 o 7 10 0 1933.70 2037.02 134.02 o 8 10 0 848.96 789.10 92.60 o 9 10 0 2757.52 2962.31 268.23 o 10 10 0 2613.90 2595.30 237.11 o 11 10 0 437.12 591.48 256.42 o 1 11 0 12104.95 12353.96 167.66 o 2 11 0 15588.81 15806.06 232.67 o 3 11 0 2001.46 2117.54 75.35 o 4 11 0 203.69 219.77 39.74 o 5 11 0 3609.27 3644.47 131.33 o 6 11 0 6221.64 6713.54 214.21 o 7 11 0 2455.96 2305.33 105.93 o 8 11 0 315.83 77.63 65.23 o 9 11 0 2273.83 2156.78 178.66 o 10 11 0 2073.68 2142.43 198.38 o 11 11 0 54.48 -8.14 72.44 o 0 12 0 1744.06 1824.20 262.98 o 1 12 0 5965.28 6464.53 116.68 o 2 12 0 9926.05 9991.35 179.60 o 3 12 0 6014.69 6015.75 128.28 o 4 12 0 29.48 18.46 26.24 o 5 12 0 1164.84 1119.02 380.13 o 6 12 0 3247.02 3388.86 133.74 o 7 12 0 277.74 160.02 48.92 o 8 12 0 48.81 120.98 62.18 o 9 12 0 998.47 855.50 118.35 o 10 12 0 454.86 398.07 93.72 o 1 13 0 803.55 794.89 95.97 o 2 13 0 7413.89 7770.11 397.93 o 3 13 0 1200.20 1207.09 259.60 o 4 13 0 31.75 71.77 42.74 o 5 13 0 1090.60 983.96 71.36 o 6 13 0 3213.68 3617.34 380.69 o 7 13 0 207.81 94.18 171.88 o 8 13 0 104.09 41.87 65.96 o 9 13 0 620.94 622.57 170.94 o 10 13 0 1598.23 1424.08 168.68 o 0 14 0 1393.55 1282.46 167.57 o 1 14 0 3868.35 3821.97 113.23 o 2 14 0 7193.38 7656.87 183.69 o 3 14 0 1459.38 1295.12 84.54 o 4 14 0 5.44 23.12 32.97 o 5 14 0 796.60 783.82 95.03 o 6 14 0 1834.21 1883.62 120.32 o 7 14 0 1308.11 973.22 476.47 o 8 14 0 232.44 182.28 73.23 o 9 14 0 235.54 141.61 99.34 o 1 15 0 64.92 32.44 44.80 o 2 15 0 6555.00 6394.27 334.77 o 3 15 0 332.12 329.15 48.21 o 4 15 0 16.18 102.90 233.55 o 5 15 0 208.40 194.94 49.48 o 6 15 0 2771.92 2588.91 180.69 o 7 15 0 155.47 67.48 112.46 o 8 15 0 147.89 201.68 119.96 o 0 16 0 1879.26 1992.10 120.34 o 1 16 0 100.23 100.84 45.36 o 2 16 0 62.27 78.72 44.61 o 3 16 0 166.53 82.10 48.73 o 4 16 0 612.26 549.95 63.35 o 5 16 0 938.09 881.71 87.35 o 6 16 0 1606.40 1628.10 247.04 o 7 16 0 971.45 845.73 188.56 o 8 16 0 68.37 74.60 112.09 o 1 17 0 475.55 483.22 56.61 o 2 17 0 917.23 1089.02 84.72 o 3 17 0 55.09 97.09 56.61 o 4 17 0 45.89 74.60 70.85 o 5 17 0 125.07 168.32 71.60 o 6 17 0 523.56 15.00 100.47 o 7 17 0 216.79 -164.20 164.20 o 0 18 0 345.70 221.18 74.60 o 1 18 0 368.83 291.66 62.60 o 2 18 0 1631.36 1603.36 127.46 o 3 18 0 1191.08 1196.61 110.21 o 4 18 0 770.23 693.15 86.97 o 5 18 0 10.70 -7.50 64.10 o 6 18 0 6.81 -55.86 127.08 o 1 19 0 51.24 18.74 56.61 o 2 19 0 0.82 -11.25 64.10 o 3 19 0 129.68 206.93 67.10 o 4 19 0 549.18 491.09 86.97 o 0 20 0 1014.51 742.26 126.71 o 1 20 0 546.99 611.80 78.72 o 2 20 0 32.80 78.72 59.98 o -13 1 1 53.97 -12.82 86.84 o -12 1 1 251.96 278.12 135.33 o -11 1 1 12.43 11.22 78.15 o -10 1 1 330.48 359.00 45.06 o -9 1 1 505.15 545.75 94.28 o -8 1 1 660.52 690.90 125.58 o -7 1 1 76.07 109.11 12.06 o -6 1 1 789.28 740.64 18.82 o -5 1 1 11163.34 10821.35 223.43 o -4 1 1 908.76 698.48 80.79 o -3 1 1 34675.11 35073.64 330.14 o -2 1 1 22521.58 21473.95 278.75 o 1 1 1 30184.54 28153.81 318.73 o 2 1 1 43370.73 42313.61 592.12 o 3 1 1 15224.71 14327.10 198.12 o 4 1 1 4184.52 3778.96 53.28 o 5 1 1 6149.29 5527.81 177.32 o 6 1 1 110.94 130.02 11.71 o 7 1 1 769.51 750.26 88.28 o 8 1 1 487.06 439.37 24.38 o 9 1 1 675.93 730.61 40.86 o 10 1 1 104.06 63.35 36.55 o 11 1 1 144.87 241.58 83.88 o 12 1 1 242.24 119.12 164.95 o -13 2 1 148.24 200.18 198.69 o -12 2 1 1018.49 1014.11 125.06 o -11 2 1 1787.29 2031.73 167.30 o -10 2 1 25.87 -8.77 134.77 o -9 2 1 1746.29 1858.22 333.08 o -8 2 1 1069.93 1108.60 70.10 o -7 2 1 2073.52 2071.43 41.26 o -6 2 1 1620.41 1832.29 144.52 o -5 2 1 107.43 104.22 7.10 o -4 2 1 302.11 565.77 20.62 o -3 2 1 4068.83 4993.64 319.02 o -2 2 1 7236.31 7506.70 99.35 o -1 2 1 726.90 816.01 18.04 o 0 2 1 1559.47 1648.70 95.03 o 1 2 1 294.70 512.04 20.81 o 2 2 1 7611.80 7564.43 105.37 o 3 2 1 24842.81 25412.86 302.68 o 4 2 1 1914.18 1751.64 46.30 o 5 2 1 8342.60 8478.22 121.92 o 6 2 1 1070.10 1119.02 80.22 o 7 2 1 23.65 91.14 14.81 o 8 2 1 9.50 4.32 13.26 o 9 2 1 32.48 77.62 84.35 o 10 2 1 19.55 11.90 35.56 o 11 2 1 1358.67 1443.01 154.53 o 12 2 1 17.54 27.98 70.47 o -13 3 1 22.83 18.74 83.48 o -12 3 1 138.19 258.93 96.48 o -11 3 1 343.45 408.64 156.70 o -10 3 1 397.21 362.51 54.91 o -9 3 1 2214.82 2123.71 71.46 o -8 3 1 6823.10 6893.98 334.20 o -7 3 1 5132.69 5238.42 160.26 o -6 3 1 7705.98 7669.30 112.97 o -5 3 1 215.41 243.03 11.62 o -4 3 1 11585.12 12046.42 208.99 o -3 3 1 32.21 83.37 18.42 o -2 3 1 797.98 841.21 21.05 o -1 3 1 2348.62 2839.20 52.30 o 0 3 1 2964.85 3489.61 50.52 o 1 3 1 738.50 669.19 15.64 o 2 3 1 2909.83 2797.57 49.69 o 3 3 1 10443.37 10251.59 135.71 o 4 3 1 2022.47 2192.78 42.44 o 5 3 1 4331.08 4436.79 80.10 o 6 3 1 9194.28 9415.25 150.51 o 7 3 1 8966.09 9473.69 168.89 o 8 3 1 5599.54 5729.45 124.78 o 9 3 1 140.18 180.79 39.17 o 10 3 1 1063.32 1129.29 141.52 o 11 3 1 36.73 107.19 78.70 o 12 3 1 9.21 26.02 82.09 o -13 4 1 260.33 171.98 94.45 o -12 4 1 615.55 322.66 101.73 o -11 4 1 1130.25 986.44 281.91 o -10 4 1 0.00 33.65 85.85 o -9 4 1 7.00 9.34 21.70 o -8 4 1 3059.10 3193.57 67.82 o -7 4 1 3431.56 3299.69 219.49 o -6 4 1 10572.54 10933.44 141.63 o -5 4 1 31374.63 30650.76 328.82 o -4 4 1 38424.65 38746.77 1489.20 o -3 4 1 49534.49 49907.55 1387.43 o -2 4 1 19199.15 19235.39 203.08 o -1 4 1 35791.10 35681.25 377.92 o 0 4 1 68.80 256.77 40.86 o 1 4 1 5763.68 5588.87 71.17 o 2 4 1 1293.03 1789.92 46.48 o 3 4 1 1417.53 1628.19 40.28 o 4 4 1 1045.42 1124.17 26.60 o 5 4 1 2238.06 2322.77 49.46 o 6 4 1 778.44 779.35 27.11 o 7 4 1 42.19 102.64 16.68 o 8 4 1 935.71 1009.23 41.67 o 9 4 1 2345.61 2030.26 110.03 o 10 4 1 1385.64 1649.93 107.62 o 11 4 1 1895.69 1715.17 117.43 o 12 4 1 317.77 534.10 113.96 o -13 5 1 75.00 39.43 88.76 o -12 5 1 5.38 17.95 123.71 o -11 5 1 73.91 132.78 55.66 o -10 5 1 269.41 307.96 58.86 o -9 5 1 5349.20 5215.08 159.42 o -8 5 1 5390.24 5577.91 125.02 o -7 5 1 1641.78 1783.02 69.91 o -6 5 1 6413.90 6544.73 87.94 o -5 5 1 734.60 709.38 27.58 o -4 5 1 1108.26 1158.39 106.84 o -3 5 1 3227.47 3459.19 111.90 o -2 5 1 927.53 962.61 24.74 o -1 5 1 18281.55 18382.90 307.59 o 0 5 1 24755.02 25222.41 260.21 o 1 5 1 371.34 444.78 41.05 o 2 5 1 938.98 1144.32 23.33 o 3 5 1 10.79 52.74 15.77 o 4 5 1 33.62 33.34 15.95 o 5 5 1 7404.32 7745.19 116.49 o 6 5 1 6248.79 6289.15 109.20 o 7 5 1 5250.67 5298.26 126.91 o 8 5 1 10810.29 10870.52 548.82 o 9 5 1 622.68 626.78 66.20 o 10 5 1 212.04 181.48 49.70 o 11 5 1 22.83 82.25 58.04 o 12 5 1 15.17 -87.99 176.19 o -12 6 1 2207.77 2202.35 202.53 o -11 6 1 2644.89 2643.56 189.69 o -10 6 1 1557.73 1665.53 274.41 o -9 6 1 1410.92 1441.21 75.31 o -8 6 1 39.90 46.52 16.87 o -7 6 1 1273.90 1265.13 36.25 o -6 6 1 0.78 24.37 10.60 o -5 6 1 3418.82 3708.77 108.34 o -4 6 1 11801.78 12940.85 188.38 o -3 6 1 75.87 178.89 35.24 o -2 6 1 1719.63 1574.88 72.54 o -1 6 1 185.42 124.91 12.73 o 0 6 1 18964.62 19313.95 208.23 o 1 6 1 9395.00 9206.42 437.48 o 2 6 1 17805.67 18116.03 445.92 o 3 6 1 40681.95 41142.48 769.44 o 4 6 1 26256.74 27601.29 366.64 o 5 6 1 15324.32 16206.15 351.64 o 6 6 1 82.40 73.69 11.09 o 7 6 1 1854.89 1754.56 107.22 o 8 6 1 245.14 190.43 76.66 o 9 6 1 1495.63 1267.52 169.45 o 10 6 1 1049.67 1054.74 86.03 o 11 6 1 1775.48 1819.92 132.16 o 12 6 1 824.43 621.65 131.14 o -12 7 1 0.84 -22.12 115.46 o -11 7 1 31.10 6.06 168.70 o -10 7 1 273.18 135.85 51.97 o -9 7 1 2872.49 2915.84 210.49 o -8 7 1 3517.46 3572.09 89.25 o -7 7 1 2551.19 2571.37 107.96 o -6 7 1 96.34 129.87 22.68 o -5 7 1 863.37 787.62 36.13 o -4 7 1 2503.27 2624.51 69.35 o -3 7 1 12202.95 12682.40 158.25 o -2 7 1 24248.48 25016.40 349.76 o -1 7 1 55235.45 54405.14 532.58 o 0 7 1 55691.00 55326.02 1023.61 o 1 7 1 23021.42 23303.21 255.46 o 2 7 1 8708.61 8895.99 110.09 o 3 7 1 5488.87 5245.06 78.20 o 4 7 1 3612.13 3482.46 119.02 o 5 7 1 64.76 49.02 16.91 o 6 7 1 801.85 840.08 76.85 o 7 7 1 2153.31 2207.99 84.32 o 8 7 1 2301.21 2083.36 82.73 o 9 7 1 1.23 9.25 50.16 o 10 7 1 26.58 242.46 68.10 o 11 7 1 181.71 181.00 63.35 o 12 7 1 142.59 151.18 88.50 o -12 8 1 1450.20 1391.99 150.02 o -11 8 1 1421.73 1361.93 121.46 o -10 8 1 172.75 102.68 65.42 o -9 8 1 15.13 34.53 47.65 o -8 8 1 278.10 330.04 21.47 o -7 8 1 1350.77 1430.34 61.21 o -6 8 1 3795.57 3973.76 224.74 o -5 8 1 8514.79 9024.87 214.43 o -4 8 1 15954.45 16271.46 227.00 o -3 8 1 10483.19 10882.82 143.97 o -2 8 1 3143.09 3358.08 126.33 o -1 8 1 120.75 154.27 17.06 o 0 8 1 498.85 418.23 24.93 o 1 8 1 171.52 254.43 37.49 o 2 8 1 6436.85 7129.03 101.46 o 3 8 1 7547.68 8018.28 116.37 o 4 8 1 4026.34 4218.85 341.70 o 5 8 1 948.62 845.46 36.83 o 6 8 1 25.54 72.62 50.61 o 7 8 1 467.86 397.83 42.92 o 8 8 1 1033.12 986.78 73.16 o 9 8 1 682.11 567.64 85.08 o 10 8 1 2310.22 1964.31 165.87 o 11 8 1 1972.19 1826.55 145.67 o -12 9 1 95.73 174.68 101.80 o -11 9 1 194.77 160.45 70.33 o -10 9 1 1507.71 1395.64 210.31 o -9 9 1 1694.72 1663.95 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