#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/69/2206934.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206934_Fobs loop_ _publ_author_name 'Chen, Y.-C.' 'Ren, X.-M.' _publ_section_title ; \b-Phase of 1-(4-bromobenzyl)pyridinium bis(1,2-dicyanoethene-1,2-dithiolato-\k^2^S,S')platinate(III) ; _journal_coeditor_code CV6579 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2176 _journal_page_last m2178 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.739 _cell_angle_gamma 90.000 _cell_length_a 7.3814 _cell_length_b 26.1802 _cell_length_c 12.6488 _exptl_crystal_F_000 1372.00 _reflns_d_resolution_high 0.7965 _[local]_cod_data_source_file cv6579Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 0605Bm in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 569.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2562.51 2921.36 174.26 o 2 0 0 191019.92 233667.72 2439.59 o 3 0 0 8124.08 7639.10 481.77 o 4 0 0 14970.08 15859.90 802.09 o 5 0 0 11631.82 12710.47 820.03 o 6 0 0 219.40 36.61 198.36 o 7 0 0 11089.58 13123.05 1053.23 o 1 1 0 4214.55 4687.86 320.52 o 2 1 0 30904.32 38881.43 650.90 o 3 1 0 26.44 15.03 94.50 o 4 1 0 3350.48 3607.21 295.98 o 5 1 0 571.25 664.60 161.73 o 6 1 0 367.91 560.07 190.22 o 7 1 0 102.55 71.66 267.77 o 8 1 0 121.36 502.27 420.27 o 0 2 0 181164.11 83350.99 948.16 o 1 2 0 8536.66 8526.25 252.03 o 2 2 0 163824.72 194026.11 12909.09 o 3 2 0 10802.33 11159.02 751.04 o 4 2 0 17068.41 17618.06 835.29 o 5 2 0 18458.76 18848.07 790.61 o 6 2 0 66.23 105.73 167.82 o 7 2 0 11796.50 12528.42 728.00 o 8 2 0 600.47 878.97 445.89 o 1 3 0 1399.53 1427.56 88.67 o 2 3 0 52406.01 62741.43 3711.31 o 3 3 0 289.78 467.30 104.52 o 4 3 0 15027.44 15954.67 466.07 o 5 3 0 4169.38 4456.07 297.47 o 6 3 0 6435.42 6366.83 560.21 o 7 3 0 205.45 196.44 292.14 o 8 3 0 713.30 1173.67 486.89 o 0 4 0 28865.05 15706.15 440.77 o 1 4 0 413.84 553.08 77.30 o 2 4 0 36207.87 40773.65 1284.64 o 3 4 0 13418.70 14575.80 683.80 o 4 4 0 4718.17 5336.24 283.14 o 5 4 0 18762.23 19259.33 864.67 o 6 4 0 425.51 636.55 193.86 o 7 4 0 6547.34 6533.82 557.02 o 8 4 0 54.16 499.71 425.39 o 1 5 0 4484.91 4393.70 170.52 o 2 5 0 22381.39 24246.79 811.37 o 3 5 0 5605.46 6017.73 228.71 o 4 5 0 10450.87 10336.31 511.94 o 5 5 0 3898.83 4067.09 290.22 o 6 5 0 5852.38 5301.10 362.79 o 7 5 0 13.15 39.20 196.96 o 8 5 0 1181.02 1565.75 522.77 o 0 6 0 4350.58 3195.56 261.38 o 1 6 0 680.69 654.60 95.60 o 2 6 0 2957.07 3297.44 183.97 o 3 6 0 12505.01 13560.30 345.56 o 4 6 0 3522.29 3536.56 210.54 o 5 6 0 9425.00 8575.00 350.62 o 6 6 0 89.29 67.60 142.92 o 7 6 0 2347.12 1925.53 287.18 o 8 6 0 50.30 466.39 433.08 o 1 7 0 29025.43 27927.28 470.36 o 2 7 0 1149.91 1133.47 127.52 o 3 7 0 13156.63 13601.12 801.25 o 4 7 0 6611.60 6755.54 286.98 o 5 7 0 2384.62 2318.09 210.60 o 6 7 0 1573.62 1530.01 206.21 o 7 7 0 71.26 169.05 224.67 o 8 7 0 933.37 1411.99 502.27 o 0 8 0 2534.55 2052.64 256.26 o 1 8 0 25.20 29.74 41.66 o 2 8 0 1082.15 1199.45 137.99 o 3 8 0 6919.06 7761.14 325.06 o 4 8 0 1143.54 1364.37 180.89 o 5 8 0 4511.40 4166.75 267.01 o 6 8 0 208.54 277.72 163.83 o 7 8 0 940.37 841.27 248.28 o 8 8 0 58.28 0.00 381.83 o 1 9 0 39288.15 35476.72 551.49 o 2 9 0 2484.49 2390.23 183.82 o 3 9 0 16300.77 17163.28 570.42 o 4 9 0 3566.53 3612.38 268.49 o 5 9 0 884.25 900.54 187.98 o 6 9 0 2782.30 2444.07 247.07 o 7 9 0 175.23 200.77 209.78 o 8 9 0 1083.31 1160.86 504.83 o 0 10 0 6853.64 4499.92 394.64 o 1 10 0 1028.06 1031.64 105.79 o 2 10 0 7731.23 7765.77 423.76 o 3 10 0 305.89 420.04 132.01 o 4 10 0 1347.61 1596.91 196.43 o 5 10 0 62.47 202.44 166.62 o 6 10 0 306.47 249.99 238.25 o 7 10 0 48.63 0.00 257.90 o 8 10 0 31.71 0.00 379.26 o 1 11 0 42096.13 34515.29 1115.84 o 2 11 0 2453.60 2458.55 203.55 o 3 11 0 34790.52 35689.94 740.93 o 4 11 0 9524.17 10557.53 446.27 o 5 11 0 1907.61 1967.57 250.01 o 6 11 0 4672.69 4371.87 527.92 o 7 11 0 109.86 400.64 278.11 o 8 11 0 1630.93 2475.47 632.96 o 0 12 0 6628.59 4933.00 451.02 o 1 12 0 353.98 441.64 77.51 o 2 12 0 3166.18 3361.96 239.13 o 3 12 0 4919.05 5261.23 312.30 o 4 12 0 660.15 647.92 179.40 o 5 12 0 2093.15 2152.04 267.61 o 6 12 0 24.41 184.55 208.02 o 7 12 0 232.90 361.84 280.71 o 8 12 0 36.17 533.02 468.96 o 1 13 0 27556.46 21001.75 976.98 o 2 13 0 8104.09 7913.34 357.54 o 3 13 0 21657.91 23206.31 776.63 o 4 13 0 21066.30 22638.99 674.79 o 5 13 0 3515.96 3651.46 329.11 o 6 13 0 6600.53 6644.80 450.77 o 7 13 0 1.62 64.80 251.75 o 8 13 0 1968.09 2444.72 650.90 o 0 14 0 13.25 58.94 184.51 o 1 14 0 85.57 20.68 83.40 o 2 14 0 2150.68 1842.27 204.31 o 3 14 0 3366.18 3475.20 283.46 o 4 14 0 395.96 497.18 191.09 o 5 14 0 4309.50 4092.27 353.18 o 6 14 0 118.53 198.21 217.96 o 7 14 0 794.24 1048.10 458.70 o 8 14 0 43.87 597.08 461.27 o 1 15 0 8454.93 6827.17 449.48 o 2 15 0 17516.84 16213.65 538.49 o 3 15 0 7476.41 7859.45 408.47 o 4 15 0 17536.53 19264.71 794.57 o 5 15 0 2664.56 3144.51 331.37 o 6 15 0 5958.26 6632.25 470.57 o 7 15 0 33.34 0.00 389.51 o 0 16 0 13373.97 11923.76 794.40 o 1 16 0 172.03 216.49 97.90 o 2 16 0 9674.91 8602.15 740.03 o 3 16 0 1661.13 1641.14 231.70 o 4 16 0 713.50 755.16 222.67 o 5 16 0 4088.06 4459.58 380.70 o 6 16 0 133.90 595.34 250.09 o 7 16 0 1240.72 1291.55 517.64 o 1 17 0 5150.62 4488.33 255.98 o 2 17 0 7174.24 5943.43 365.22 o 3 17 0 1326.83 1531.41 238.67 o 4 17 0 4445.94 4847.63 372.80 o 5 17 0 1188.54 1078.93 258.38 o 6 17 0 2713.18 3299.20 421.26 o 7 17 0 24.39 333.14 445.89 o 0 18 0 26611.66 23687.52 741.92 o 1 18 0 7.59 16.64 176.94 o 2 18 0 13776.85 11062.73 866.16 o 3 18 0 242.95 292.72 184.58 o 4 18 0 599.01 527.99 210.32 o 5 18 0 848.83 749.99 247.12 o 6 18 0 77.17 294.21 240.83 o 7 18 0 1095.23 1181.36 520.21 o 1 19 0 3034.01 2903.40 355.85 o 2 19 0 449.80 484.07 236.05 o 3 19 0 607.90 550.63 201.37 o 4 19 0 89.80 0.00 196.45 o 5 19 0 206.70 317.05 226.48 o 6 19 0 650.58 804.72 269.05 o 7 19 0 1.98 240.88 435.64 o 0 20 0 18591.57 17659.52 1113.45 o 1 20 0 15.13 121.83 220.71 o 2 20 0 5472.55 4353.94 433.98 o 3 20 0 47.90 0.00 178.91 o 4 20 0 477.49 798.82 237.95 o 5 20 0 894.79 1346.07 278.53 o 6 20 0 1.43 377.39 259.60 o 7 20 0 865.00 1511.93 545.83 o 1 21 0 2303.99 2182.42 347.90 o 2 21 0 478.49 85.12 222.21 o 3 21 0 391.12 235.39 199.66 o 4 21 0 84.91 92.80 206.69 o 5 21 0 18.64 282.11 228.77 o 6 21 0 21.74 96.39 244.47 o 0 22 0 3376.80 3410.81 579.15 o 1 22 0 366.30 256.27 165.48 o 2 22 0 1400.24 1067.34 299.79 o 3 22 0 785.39 703.04 344.67 o 4 22 0 599.64 583.82 238.96 o 5 22 0 1228.85 1184.02 289.84 o 6 22 0 13.34 176.32 253.66 o 1 23 0 801.63 1131.77 232.83 o 2 23 0 352.44 364.85 263.65 o 3 23 0 44.49 46.13 235.56 o 4 23 0 169.60 133.80 213.74 o 5 23 0 3.93 465.87 254.90 o 6 23 0 57.49 272.58 263.65 o 0 24 0 2460.84 3046.93 604.77 o 1 24 0 367.68 462.34 203.97 o 2 24 0 1267.43 1487.35 344.76 o 3 24 0 1557.57 1399.49 336.98 o 4 24 0 246.48 540.50 279.74 o 5 24 0 1147.85 1261.35 307.53 o 6 24 0 54.93 300.62 336.12 o 1 25 0 341.38 332.70 278.89 o 2 25 0 376.65 396.69 262.26 o 3 25 0 2.75 0.00 249.98 o 4 25 0 190.44 232.12 279.03 o 5 25 0 14.29 67.76 241.61 o 0 26 0 1329.57 2198.71 556.08 o 1 26 0 216.31 113.05 286.23 o 2 26 0 1332.42 1465.84 306.22 o 3 26 0 812.89 1172.53 276.38 o 4 26 0 491.06 708.13 267.06 o 5 26 0 1094.37 1326.62 320.32 o 1 27 0 1504.77 1800.08 400.26 o 2 27 0 292.85 486.63 250.66 o 3 27 0 424.38 522.70 252.30 o 4 27 0 258.70 516.27 260.32 o 5 27 0 40.82 251.27 256.97 o 0 28 0 909.97 1737.44 584.27 o 1 28 0 16.88 0.00 295.57 o 2 28 0 703.05 1378.27 400.35 o 3 28 0 346.81 846.48 278.60 o 4 28 0 372.20 446.67 273.72 o 1 29 0 1779.64 2312.41 453.59 o 2 29 0 203.88 303.77 348.81 o 3 29 0 663.77 1023.56 299.75 o 4 29 0 253.44 423.23 277.58 o 0 30 0 490.07 863.59 520.21 o 1 30 0 54.57 322.24 316.86 o 2 30 0 430.89 670.20 368.66 o 3 30 0 2.52 332.85 346.50 o 1 31 0 613.50 1149.82 394.82 o 2 31 0 161.02 266.70 361.09 o 0 32 0 62.24 622.71 512.52 o 1 32 0 0.42 186.19 342.24 o 2 32 0 119.98 0.00 341.31 o -8 1 1 62.38 274.20 275.43 o -7 1 1 17454.67 18226.86 1069.88 o -6 1 1 1568.33 1800.64 235.18 o -5 1 1 23670.36 22982.31 965.59 o -4 1 1 6020.93 6255.76 342.97 o -3 1 1 26033.98 29342.63 682.01 o -2 1 1 42357.22 45836.94 2600.31 o -1 1 1 6094.39 6721.90 190.12 o 0 1 1 77372.48 90104.30 4013.85 o 1 1 1 14918.76 18637.79 1680.73 o 2 1 1 7841.63 9016.97 288.11 o 3 1 1 28995.32 32734.43 678.52 o 4 1 1 5127.03 5498.32 375.42 o 5 1 1 36275.09 38356.88 2542.29 o 6 1 1 123.26 375.02 182.89 o 7 1 1 11069.26 11080.35 1208.55 o -8 2 1 285.21 469.85 294.54 o -7 2 1 15.37 0.00 390.80 o -6 2 1 36.45 148.23 161.05 o -5 2 1 374.56 464.30 148.68 o -4 2 1 208.18 243.93 109.89 o -3 2 1 1748.52 1690.54 145.05 o -2 2 1 29987.13 34862.00 1466.57 o -1 2 1 11656.87 13154.10 432.14 o 0 2 1 776.69 762.19 45.29 o 1 2 1 3216.38 3392.98 84.95 o 2 2 1 4073.58 4210.41 286.28 o 3 2 1 3864.78 3759.18 223.52 o 4 2 1 185.86 156.06 106.96 o 5 2 1 1630.48 1636.77 217.92 o 6 2 1 504.07 520.78 188.57 o 7 2 1 38.52 18.96 325.45 o -8 3 1 347.82 420.20 286.48 o -7 3 1 7977.57 8427.23 780.31 o -6 3 1 331.00 340.55 171.62 o -5 3 1 12137.20 12356.75 459.37 o -4 3 1 10388.94 11211.04 699.52 o -3 3 1 8725.44 9608.91 401.86 o -2 3 1 69592.66 76255.73 3118.82 o -1 3 1 1777.74 1842.80 72.38 o 0 3 1 60989.29 57320.80 4149.29 o 1 3 1 2866.96 3018.47 167.92 o 2 3 1 11792.33 11984.62 836.30 o 3 3 1 19287.37 21219.79 1290.42 o 4 3 1 2828.61 2930.78 215.00 o 5 3 1 24034.49 25702.83 1630.83 o 6 3 1 1.98 58.35 162.93 o 7 3 1 6821.94 7024.10 803.37 o -8 4 1 619.42 622.72 257.51 o -7 4 1 74.22 0.00 257.29 o -6 4 1 223.58 425.10 176.69 o -5 4 1 1262.24 1210.14 181.16 o -4 4 1 361.13 496.27 126.01 o -3 4 1 6558.31 7468.59 353.07 o -2 4 1 298.53 301.83 55.54 o -1 4 1 26448.68 30749.22 1436.24 o 0 4 1 1715.06 1307.47 91.80 o 1 4 1 41881.77 47421.86 881.61 o 2 4 1 23.85 50.98 47.48 o 3 4 1 26808.01 27491.70 1480.67 o 4 4 1 566.18 691.26 136.78 o 5 4 1 4719.43 4400.53 301.39 o 6 4 1 1470.13 1565.06 238.00 o 7 4 1 267.63 37.50 248.75 o -8 5 1 348.88 269.85 237.88 o -7 5 1 2521.48 2148.44 298.36 o -6 5 1 260.57 241.53 168.17 o -5 5 1 2954.65 3049.12 249.87 o -4 5 1 10678.94 11222.53 395.72 o -3 5 1 192.51 226.40 85.17 o -2 5 1 35241.72 36585.52 817.66 o -1 5 1 7384.04 8237.04 530.52 o 0 5 1 28602.29 21408.33 2515.92 o 1 5 1 3666.04 3341.61 153.37 o 2 5 1 33323.34 34802.71 1218.01 o 3 5 1 12059.19 11955.30 384.21 o 4 5 1 242.79 344.49 87.17 o 5 5 1 5719.20 6017.04 296.30 o 6 5 1 585.58 589.43 164.37 o 7 5 1 3061.04 3000.02 430.52 o -8 6 1 932.11 812.47 258.54 o -7 6 1 74.86 48.40 192.01 o -6 6 1 2814.60 2756.88 315.88 o -5 6 1 1114.50 1076.27 154.31 o -4 6 1 8360.65 8426.73 488.98 o -3 6 1 1544.42 1688.82 140.76 o -2 6 1 4085.38 4065.62 142.59 o -1 6 1 30409.54 33082.80 1390.10 o 0 6 1 90.67 146.73 53.72 o 1 6 1 9969.79 9752.82 266.28 o 2 6 1 5817.84 6064.50 300.52 o 3 6 1 10886.31 11797.84 338.41 o 4 6 1 4506.31 4577.42 190.06 o 5 6 1 1681.41 1606.85 202.70 o 6 6 1 2807.22 2775.49 290.35 o 7 6 1 224.93 337.09 268.11 o -8 7 1 436.52 298.24 246.40 o -7 7 1 466.80 234.94 208.77 o -6 7 1 328.57 283.29 155.29 o -5 7 1 875.54 849.35 149.42 o -4 7 1 4848.60 4455.70 241.56 o -3 7 1 530.06 534.68 103.73 o -2 7 1 20119.27 20772.45 436.81 o -1 7 1 6806.35 6780.34 290.46 o 0 7 1 54559.12 39383.10 4425.23 o 1 7 1 1990.34 2190.36 147.79 o 2 7 1 17080.90 16843.22 407.53 o 3 7 1 1281.76 1326.68 160.06 o 4 7 1 641.43 651.35 127.92 o 5 7 1 1538.51 1614.94 183.19 o 6 7 1 75.94 80.49 155.81 o 7 7 1 919.64 772.24 298.04 o 8 7 1 174.02 328.01 440.77 o -8 8 1 1295.76 1304.57 300.44 o -7 8 1 110.68 138.97 213.12 o -6 8 1 8768.04 7889.93 387.35 o -5 8 1 2775.67 2667.74 227.17 o -4 8 1 19428.87 19007.80 481.58 o -3 8 1 7493.33 8134.24 328.21 o -2 8 1 15513.45 17135.68 444.59 o -1 8 1 354.54 502.55 80.86 o 0 8 1 6870.90 5331.29 467.16 o 1 8 1 9111.63 8499.11 428.61 o 2 8 1 18304.52 18892.43 448.79 o 3 8 1 8705.36 9651.91 627.29 o 4 8 1 18942.05 21720.20 953.65 o 5 8 1 735.09 861.98 153.98 o 6 8 1 5072.12 4809.71 313.53 o 7 8 1 139.82 278.04 260.93 o 8 8 1 1516.83 1027.60 533.02 o -8 9 1 77.62 182.24 237.68 o -7 9 1 263.20 217.78 214.55 o -6 9 1 20.53 210.03 162.91 o -5 9 1 681.56 631.65 156.35 o -4 9 1 749.87 773.88 170.01 o -3 9 1 190.23 194.98 115.86 o -2 9 1 3964.99 4219.29 193.44 o -1 9 1 4386.85 4590.30 191.50 o 0 9 1 4374.23 3488.76 243.75 o 1 9 1 932.51 946.46 125.90 o 2 9 1 6796.36 7174.36 295.78 o 3 9 1 1167.13 1213.31 161.17 o 4 9 1 1359.33 1367.76 190.58 o 5 9 1 68.05 121.50 170.78 o 6 9 1 167.91 186.38 201.17 o 7 9 1 309.42 688.99 292.64 o 8 9 1 23.54 176.82 463.83 o -8 10 1 1709.37 2147.30 443.60 o -7 10 1 212.88 207.46 233.77 o -6 10 1 12141.09 11602.45 892.96 o -5 10 1 3188.03 3453.39 301.54 o -4 10 1 26710.06 29065.01 733.86 o -3 10 1 6862.21 7276.16 331.65 o -2 10 1 4788.58 5190.13 173.59 o -1 10 1 11401.28 11097.38 305.64 o 0 10 1 597.80 513.66 92.92 o 1 10 1 29475.01 24432.62 1833.37 o 2 10 1 31332.60 34086.27 651.77 o 3 10 1 9383.85 10079.13 390.48 o 4 10 1 22577.99 24278.43 651.12 o 5 10 1 1271.28 1442.58 226.99 o 6 10 1 5987.01 5824.23 410.96 o 7 10 1 37.01 198.86 268.07 o 8 10 1 1531.00 1363.30 589.40 o -8 11 1 172.82 494.31 323.81 o -7 11 1 168.27 194.76 280.18 o -6 11 1 86.92 218.15 206.64 o -5 11 1 1948.93 2077.67 257.49 o -4 11 1 238.94 431.03 159.28 o -3 11 1 1762.16 1820.85 197.03 o -2 11 1 4857.55 5138.56 181.36 o -1 11 1 1423.21 1374.33 129.90 o 0 11 1 5993.15 4966.71 232.36 o 1 11 1 1378.82 1225.97 148.96 o 2 11 1 13.12 61.79 105.45 o 3 11 1 76.70 150.94 124.04 o 4 11 1 305.27 345.31 157.70 o 5 11 1 153.11 369.46 183.42 o 6 11 1 980.59 1063.36 242.52 o 7 11 1 55.17 106.75 276.76 o 8 11 1 216.49 156.32 481.77 o -8 12 1 2132.78 2882.92 661.15 o -7 12 1 72.61 73.99 268.90 o -6 12 1 10262.66 10492.21 535.39 o -5 12 1 4621.36 4926.31 358.44 o -4 12 1 21940.75 23513.14 1117.29 o -3 12 1 19822.67 21040.03 946.82 o -2 12 1 9128.40 9099.08 367.97 o -1 12 1 13233.17 10506.35 335.76 o 0 12 1 390.01 349.91 90.46 o 1 12 1 24678.71 18340.37 2745.19 o 2 12 1 18306.01 18216.25 514.47 o 3 12 1 18512.58 19821.73 573.09 o 4 12 1 13589.76 12388.72 1142.45 o 5 12 1 770.45 990.87 217.89 o 6 12 1 5308.74 5417.90 431.73 o 7 12 1 16.50 23.65 261.46 o 8 12 1 1981.17 1283.86 571.46 o -8 13 1 299.37 638.09 481.77 o -7 13 1 20.88 173.59 267.28 o -6 13 1 131.60 363.02 223.61 o -5 13 1 115.40 416.78 202.13 o -4 13 1 1692.13 2041.58 249.40 o -3 13 1 843.48 853.96 173.25 o -2 13 1 12751.74 12996.19 478.67 o -1 13 1 125.32 0.00 81.77 o 0 13 1 15606.56 12696.21 676.15 o 1 13 1 125.31 0.00 103.71 o 2 13 1 5076.43 5382.88 303.69 o 3 13 1 756.95 846.10 172.90 o 4 13 1 214.31 235.77 171.69 o 5 13 1 169.87 234.46 191.90 o 6 13 1 553.53 751.68 238.54 o 7 13 1 90.86 40.54 257.98 o 8 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