#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:15:20 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180989 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/69/2206952.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206952_Fobs loop_ _publ_author_name 'Wang, Zi-Liang' 'Wei, Lin-Heng' 'Niu, Jing-Yang' _publ_section_title ; Diaquabis[malonato(1--)-\k^2^O,O']cobalt(II) ; _journal_coeditor_code HB6253 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1907 _journal_page_last m1908 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.018 _cell_angle_gamma 90.000 _cell_length_a 4.9331 _cell_length_b 11.2760 _cell_length_c 9.6819 _exptl_crystal_F_000 306.00 _reflns_d_resolution_high 0.7840 _cod_data_source_file hb6253Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' t in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 117.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1467.69 1716.32 13.69 o 3 0 0 1380.07 1439.34 15.37 o 4 0 0 1203.11 1276.96 17.04 o 5 0 0 584.83 562.57 42.27 o 1 1 0 0.29 1.75 0.46 o 2 1 0 356.16 368.28 14.24 o 3 1 0 11.33 7.05 2.92 o 4 1 0 34.59 28.85 1.86 o 5 1 0 44.01 41.98 2.11 o 6 1 0 8.04 8.94 1.84 o 0 2 0 465.87 495.31 43.68 o 1 2 0 786.62 900.50 18.06 o 2 2 0 1332.65 1302.55 58.98 o 3 2 0 971.07 999.80 35.55 o 4 2 0 833.35 837.29 40.88 o 5 2 0 4.90 5.73 1.04 o 6 2 0 1.14 2.92 1.72 o 1 3 0 44.32 45.05 2.54 o 2 3 0 411.03 389.95 61.85 o 3 3 0 114.49 111.34 7.43 o 4 3 0 21.70 21.05 1.74 o 5 3 0 18.84 17.22 1.97 o 6 3 0 5.11 4.40 1.96 o 0 4 0 3555.58 3570.86 131.79 o 1 4 0 1192.35 1190.12 25.58 o 2 4 0 1525.95 1595.81 49.21 o 3 4 0 1291.54 1250.83 25.50 o 4 4 0 219.77 193.73 10.17 o 5 4 0 177.51 169.44 5.42 o 6 4 0 172.91 176.21 9.10 o 1 5 0 1855.65 2013.58 27.56 o 2 5 0 417.72 445.77 12.12 o 3 5 0 56.13 36.01 13.84 o 4 5 0 41.31 44.60 5.03 o 5 5 0 4.70 6.08 1.49 o 0 6 0 1923.40 1914.70 97.78 o 1 6 0 1123.62 1101.89 30.04 o 2 6 0 491.36 488.10 13.59 o 3 6 0 647.32 330.25 232.78 o 4 6 0 425.71 439.21 14.35 o 5 6 0 59.47 57.99 3.46 o 1 7 0 363.15 373.20 15.13 o 2 7 0 138.17 138.20 5.49 o 3 7 0 3.88 5.36 0.94 o 4 7 0 2.81 2.12 1.08 o 5 7 0 0.20 0.12 0.98 o 0 8 0 2365.85 2515.38 144.12 o 1 8 0 362.03 382.54 12.05 o 2 8 0 29.97 34.01 1.72 o 3 8 0 341.67 335.13 11.03 o 4 8 0 181.38 166.09 5.58 o 5 8 0 66.95 63.93 3.93 o 1 9 0 57.16 52.15 2.38 o 2 9 0 181.85 191.06 9.59 o 3 9 0 22.36 22.89 1.81 o 4 9 0 91.04 81.64 4.15 o 0 10 0 243.57 232.13 8.28 o 1 10 0 652.88 635.64 21.11 o 2 10 0 431.21 428.55 7.01 o 3 10 0 252.95 238.69 5.89 o 4 10 0 474.31 476.63 14.43 o 1 11 0 498.92 472.08 25.32 o 2 11 0 54.62 51.22 2.49 o 3 11 0 139.07 139.84 4.26 o 4 11 0 25.06 25.50 5.70 o 0 12 0 567.90 544.96 14.22 o 1 12 0 85.96 77.91 3.89 o 2 12 0 30.97 34.93 2.75 o 3 12 0 120.09 120.10 4.15 o 1 13 0 5.41 4.85 1.28 o 2 13 0 33.58 37.33 3.01 o 0 14 0 106.37 105.56 7.04 o 1 14 0 187.55 202.15 6.89 o -6 1 1 8.73 8.96 1.50 o -5 1 1 316.15 201.93 69.48 o -4 1 1 1606.09 1125.25 382.90 o -3 1 1 394.64 335.16 34.14 o -2 1 1 32.77 37.94 1.26 o -1 1 1 3295.00 3232.00 61.25 o 0 1 1 6714.33 5577.14 612.80 o 1 1 1 1682.25 1897.39 7.94 o 2 1 1 832.17 658.12 113.76 o 3 1 1 324.53 313.51 17.03 o 4 1 1 336.07 335.21 18.88 o 5 1 1 261.12 247.20 6.63 o -6 2 1 20.54 22.09 2.60 o -5 2 1 9.32 8.51 1.27 o -4 2 1 167.94 168.09 6.55 o -3 2 1 99.62 115.02 3.24 o -2 2 1 1357.66 1515.15 32.47 o -1 2 1 184.88 199.87 6.04 o 0 2 1 145.34 152.18 2.44 o 1 2 1 1133.85 1185.19 28.12 o 2 2 1 16.96 15.20 1.05 o 3 2 1 64.62 58.33 2.30 o 4 2 1 12.54 17.05 1.65 o 5 2 1 5.81 5.41 1.96 o 6 2 1 0.92 2.63 1.53 o -6 3 1 149.56 151.04 5.77 o -5 3 1 116.49 118.92 3.78 o -4 3 1 250.54 230.25 12.88 o -3 3 1 1511.03 1591.89 50.16 o -2 3 1 2938.20 3134.98 73.18 o -1 3 1 4211.60 3905.43 233.00 o 0 3 1 3995.46 3770.78 108.82 o 1 3 1 3.60 9.27 2.44 o 2 3 1 1220.08 1281.28 24.14 o 3 3 1 4251.69 4351.78 181.15 o 4 3 1 505.62 503.25 29.61 o 5 3 1 3.62 3.23 1.02 o 6 3 1 84.47 97.27 6.70 o -6 4 1 1.92 1.80 1.17 o -5 4 1 31.44 34.61 3.83 o -4 4 1 14.23 14.48 1.68 o -3 4 1 39.98 36.00 1.61 o -2 4 1 497.23 517.61 11.16 o -1 4 1 234.98 273.54 7.01 o 0 4 1 1.22 1.28 0.24 o 1 4 1 43.42 35.04 0.93 o 2 4 1 0.26 13.16 7.91 o 3 4 1 12.46 15.47 0.97 o 4 4 1 13.99 13.08 1.65 o 5 4 1 0.02 0.08 0.70 o 6 4 1 0.05 -0.38 1.15 o -5 5 1 207.67 199.24 8.95 o -4 5 1 434.88 423.15 21.88 o -3 5 1 152.48 161.13 7.25 o -2 5 1 265.46 263.30 4.49 o -1 5 1 2107.96 2124.47 38.60 o 0 5 1 671.51 642.01 16.41 o 1 5 1 163.66 141.32 4.62 o 2 5 1 1091.97 1073.31 25.32 o 3 5 1 609.82 595.21 10.08 o 4 5 1 84.21 83.95 3.62 o 5 5 1 37.90 39.72 2.85 o -5 6 1 0.68 2.01 1.53 o -4 6 1 79.24 73.91 3.47 o -3 6 1 105.05 102.02 2.80 o -2 6 1 56.71 54.21 3.92 o -1 6 1 6.82 7.92 0.78 o 0 6 1 158.04 158.73 5.46 o 1 6 1 16.45 20.23 0.83 o 2 6 1 28.38 24.74 1.55 o 3 6 1 92.45 90.09 6.51 o 4 6 1 0.01 0.29 0.51 o 5 6 1 18.01 17.44 2.30 o -5 7 1 327.94 327.53 12.06 o -4 7 1 428.85 413.76 15.13 o -3 7 1 82.06 74.12 2.86 o -2 7 1 655.92 650.89 27.79 o -1 7 1 2667.79 2636.04 90.51 o 0 7 1 1485.80 1607.91 37.51 o 1 7 1 649.73 636.62 15.84 o 2 7 1 767.47 745.44 18.69 o 3 7 1 571.81 560.11 20.29 o 4 7 1 240.50 236.68 8.32 o 5 7 1 114.70 112.93 5.22 o -5 8 1 10.66 12.25 2.21 o -4 8 1 38.77 32.14 4.07 o -3 8 1 167.65 157.06 3.85 o -2 8 1 0.87 0.62 0.50 o -1 8 1 100.94 100.39 4.12 o 0 8 1 147.30 158.14 4.19 o 1 8 1 19.49 23.20 1.36 o 2 8 1 855.30 884.43 28.13 o 3 8 1 11.74 12.49 1.39 o 4 8 1 254.19 250.64 7.69 o 5 8 1 0.32 0.31 1.08 o -4 9 1 283.79 264.81 7.27 o -3 9 1 644.09 536.89 99.62 o -2 9 1 93.93 86.40 3.43 o -1 9 1 128.82 114.83 3.56 o 0 9 1 898.39 872.08 13.60 o 1 9 1 311.53 325.32 13.42 o 2 9 1 136.79 136.65 5.81 o 3 9 1 301.39 298.26 9.66 o 4 9 1 166.49 160.66 10.54 o -4 10 1 5.23 2.00 1.32 o -3 10 1 99.92 88.86 6.77 o -2 10 1 14.91 14.55 1.44 o -1 10 1 72.00 67.26 2.55 o 0 10 1 9.28 8.61 1.45 o 1 10 1 17.47 19.20 2.00 o 2 10 1 27.18 30.04 1.88 o 3 10 1 1.81 2.75 0.92 o 4 10 1 4.34 3.74 1.49 o -4 11 1 154.81 161.09 12.37 o -3 11 1 157.77 160.77 5.72 o -2 11 1 177.49 177.03 4.65 o -1 11 1 321.14 333.15 9.17 o 0 11 1 454.75 417.40 8.32 o 1 11 1 270.64 248.00 6.55 o 2 11 1 130.23 120.64 4.72 o 3 11 1 182.75 179.85 4.87 o 4 11 1 104.24 105.64 7.78 o -3 12 1 55.82 59.92 3.77 o -2 12 1 2.06 2.13 1.01 o -1 12 1 27.56 24.67 2.39 o 0 12 1 0.22 1.08 0.82 o 1 12 1 21.04 17.66 2.22 o 2 12 1 2.66 0.52 0.76 o 3 12 1 1.56 2.09 1.11 o -2 13 1 131.53 128.28 5.31 o -1 13 1 363.91 358.54 13.19 o 0 13 1 131.10 130.32 6.85 o 1 13 1 136.74 138.49 5.46 o 2 13 1 247.47 251.51 7.51 o -1 14 1 8.78 11.72 2.05 o 0 14 1 8.06 9.45 1.91 o 1 14 1 1.55 4.04 1.28 o -6 0 2 47.56 44.38 4.55 o -5 0 2 367.45 409.16 7.78 o -4 0 2 1420.74 1525.04 13.17 o -3 0 2 740.53 780.22 8.12 o -2 0 2 286.90 288.31 8.29 o -1 0 2 561.10 568.11 12.69 o 0 0 2 3812.64 2828.91 316.45 o 1 0 2 13802.69 12069.49 101.97 o 2 0 2 2532.34 2451.32 94.43 o 3 0 2 2.57 6.38 1.82 o 4 0 2 38.30 28.29 2.44 o 6 0 2 381.53 419.21 13.26 o -6 1 2 56.94 56.13 4.09 o -5 1 2 230.05 226.17 12.65 o -4 1 2 263.22 236.71 23.85 o -3 1 2 30.45 29.23 0.98 o -2 1 2 322.75 388.92 6.26 o -1 1 2 1749.46 1878.52 38.52 o 0 1 2 95.09 76.24 6.50 o 1 1 2 7645.57 7301.75 159.90 o 2 1 2 4.63 6.48 0.81 o 3 1 2 40.43 34.86 1.86 o 4 1 2 21.67 23.40 1.43 o 5 1 2 1.27 1.55 1.04 o 6 1 2 1.49 2.25 2.11 o -6 2 2 83.19 84.42 4.76 o -5 2 2 257.49 246.83 11.00 o -4 2 2 237.66 236.71 7.05 o -3 2 2 817.58 863.14 9.97 o -2 2 2 1803.14 1857.49 78.69 o -1 2 2 4221.04 3889.08 78.56 o 0 2 2 951.07 880.33 79.99 o 1 2 2 222.63 254.45 5.58 o 2 2 2 1843.24 1858.48 9.52 o 3 2 2 1986.01 2140.43 20.03 o 4 2 2 212.97 233.31 5.60 o 5 2 2 99.36 106.87 4.26 o 6 2 2 36.48 35.23 4.12 o -6 3 2 0.12 -0.32 0.75 o -5 3 2 61.17 53.86 2.63 o -4 3 2 14.96 14.27 1.14 o -3 3 2 5.92 6.16 0.57 o -2 3 2 180.17 202.13 4.65 o -1 3 2 251.21 257.22 3.58 o 0 3 2 26.94 24.89 0.70 o 1 3 2 995.04 1035.35 33.40 o 2 3 2 28.18 29.76 1.24 o 3 3 2 50.17 52.82 2.54 o 4 3 2 6.45 7.43 1.31 o 5 3 2 10.36 9.25 1.68 o 6 3 2 22.97 18.96 3.30 o -5 4 2 474.32 488.41 23.31 o -4 4 2 616.55 587.05 9.34 o -3 4 2 32.45 38.54 1.33 o -2 4 2 1926.03 2090.63 56.48 o -1 4 2 9955.48 9552.99 45.69 o 0 4 2 5.22 3.87 0.33 o 1 4 2 110.99 100.53 2.81 o 2 4 2 2705.79 2771.28 58.47 o 3 4 2 662.81 649.00 31.14 o 4 4 2 144.30 129.13 8.62 o 5 4 2 85.26 80.16 3.92 o -5 5 2 49.15 42.38 3.06 o -4 5 2 1.16 2.80 0.96 o -3 5 2 41.57 42.48 2.24 o -2 5 2 0.01 0.17 0.30 o -1 5 2 32.08 26.65 1.16 o 0 5 2 191.56 217.08 5.19 o 1 5 2 50.23 66.70 2.23 o 2 5 2 41.25 42.69 1.35 o 3 5 2 0.40 0.88 0.54 o 4 5 2 0.26 2.57 0.97 o 5 5 2 0.82 0.80 0.78 o -5 6 2 337.57 314.14 24.99 o -4 6 2 173.12 161.79 5.00 o -3 6 2 671.86 708.94 9.40 o -2 6 2 567.97 547.12 14.03 o -1 6 2 539.88 512.69 6.61 o 0 6 2 2634.64 2662.56 23.82 o 1 6 2 302.23 297.03 9.06 o 2 6 2 409.44 380.06 7.92 o 3 6 2 1251.54 1278.67 25.41 o 4 6 2 125.86 124.42 6.36 o 5 6 2 35.10 35.86 2.89 o -5 7 2 8.03 6.05 1.57 o -4 7 2 47.04 44.11 2.87 o -3 7 2 20.92 22.59 1.92 o -2 7 2 274.91 270.21 4.35 o -1 7 2 45.43 39.70 1.63 o 0 7 2 439.32 519.49 7.75 o 1 7 2 0.05 0.41 0.27 o 2 7 2 313.60 310.41 9.79 o 3 7 2 21.29 22.84 1.83 o 4 7 2 13.93 12.28 1.52 o 5 7 2 18.24 19.27 3.35 o -5 8 2 187.46 203.40 10.01 o -4 8 2 348.99 328.17 10.12 o -3 8 2 44.77 45.41 2.76 o -2 8 2 298.32 286.17 4.90 o -1 8 2 1237.64 1227.64 13.58 o 0 8 2 430.98 394.14 5.09 o 1 8 2 841.32 866.07 28.53 o 2 8 2 489.76 495.46 11.88 o 3 8 2 32.72 31.16 1.91 o 4 8 2 108.29 107.21 4.08 o 5 8 2 118.59 114.95 7.97 o -4 9 2 55.00 55.86 3.48 o -3 9 2 0.08 0.81 0.83 o -2 9 2 171.93 163.79 5.82 o -1 9 2 426.49 414.75 6.12 o 0 9 2 517.29 483.35 10.56 o 1 9 2 104.21 105.87 3.42 o 2 9 2 56.73 60.85 2.47 o 3 9 2 8.55 7.29 1.27 o 4 9 2 34.94 33.64 2.31 o -4 10 2 144.55 144.45 5.66 o -3 10 2 610.71 606.66 17.78 o -2 10 2 623.27 556.22 64.07 o -1 10 2 279.40 270.18 11.62 o 0 10 2 101.55 102.56 3.95 o 1 10 2 161.05 148.83 4.86 o 2 10 2 703.65 752.13 39.00 o 3 10 2 372.51 391.15 17.30 o 4 10 2 42.05 42.46 2.61 o -3 11 2 1.42 2.24 1.29 o -2 11 2 48.53 52.32 2.51 o -1 11 2 238.31 219.89 6.08 o 0 11 2 266.02 250.12 13.57 o 1 11 2 26.73 26.10 2.37 o 2 11 2 17.72 19.51 2.26 o 3 11 2 7.52 7.96 1.42 o -3 12 2 7.21 6.45 1.79 o -2 12 2 91.86 85.45 6.18 o -1 12 2 313.14 298.79 11.23 o 0 12 2 317.26 308.56 7.64 o 1 12 2 241.08 239.24 6.85 o 2 12 2 62.72 60.64 3.60 o 3 12 2 35.85 36.47 3.00 o -2 13 2 5.54 3.88 2.25 o -1 13 2 63.94 60.65 3.66 o 0 13 2 54.44 51.57 3.36 o 1 13 2 11.40 12.52 2.78 o 2 13 2 1.41 1.82 1.03 o -1 14 2 82.60 78.97 6.39 o 0 14 2 134.29 142.17 5.79 o 1 14 2 68.73 75.54 4.28 o -6 1 3 123.49 113.98 7.37 o -5 1 3 269.29 282.95 6.85 o -4 1 3 485.86 514.17 5.57 o -3 1 3 877.99 917.94 15.11 o -2 1 3 2484.83 2617.43 28.21 o -1 1 3 1619.18 1660.74 37.17 o 0 1 3 7.76 9.65 1.14 o 1 1 3 3172.54 3318.44 70.72 o 2 1 3 4312.20 4513.76 62.16 o 3 1 3 132.99 131.19 3.04 o 4 1 3 8.08 10.15 1.54 o 5 1 3 237.37 244.12 6.56 o 6 1 3 139.67 149.31 8.57 o -6 2 3 49.04 48.01 2.81 o -5 2 3 137.30 134.80 10.54 o -4 2 3 71.88 70.29 2.70 o -3 2 3 609.98 630.02 21.98 o -2 2 3 660.29 775.89 7.31 o -1 2 3 2278.60 2395.64 55.10 o 0 2 3 75.06 46.56 17.70 o 1 2 3 24.25 23.79 1.00 o 2 2 3 10.55 10.97 0.90 o 3 2 3 2.86 16.33 9.86 o 4 2 3 14.10 19.00 2.59 o 5 2 3 0.50 0.93 1.01 o 6 2 3 0.18 -0.29 1.77 o -5 3 3 406.83 393.01 13.45 o -4 3 3 25.15 27.28 1.75 o -3 3 3 251.32 257.59 7.30 o -2 3 3 2665.17 2745.86 37.07 o -1 3 3 2061.85 2077.10 49.55 o 0 3 3 719.98 719.13 14.23 o 1 3 3 790.29 723.35 15.82 o 2 3 3 328.46 303.12 10.87 o 3 3 3 558.99 580.68 10.29 o 4 3 3 470.33 481.01 10.72 o -5 4 3 47.31 47.14 2.61 o -4 4 3 0.06 1.33 0.66 o -3 4 3 33.22 37.44 1.29 o -2 4 3 132.51 156.84 1.74 o -1 4 3 232.33 234.43 6.20 o 0 4 3 122.07 133.09 3.19 o 1 4 3 420.63 460.15 10.17 o 2 4 3 53.36 53.03 2.06 o 3 4 3 54.21 55.01 3.26 o 4 4 3 120.91 117.51 11.32 o 5 4 3 24.62 14.31 2.82 o -5 5 3 342.00 339.74 8.36 o -4 5 3 383.31 350.57 12.69 o -3 5 3 323.07 323.71 4.17 o -2 5 3 1379.61 1330.62 30.74 o -1 5 3 2344.35 2230.31 62.42 o 0 5 3 620.21 602.13 17.67 o 1 5 3 551.51 474.62 26.83 o 2 5 3 1294.56 1261.92 52.77 o 3 5 3 620.66 638.66 21.71 o 4 5 3 139.88 136.69 4.86 o 5 5 3 64.26 59.79 5.07 o -5 6 3 0.50 0.84 0.96 o -4 6 3 90.02 82.11 3.89 o -3 6 3 29.45 26.23 1.63 o -2 6 3 2.02 2.65 0.50 o -1 6 3 116.20 117.65 2.25 o 0 6 3 131.15 146.94 3.08 o 1 6 3 0.07 0.08 0.39 o 2 6 3 2.04 2.39 0.53 o 3 6 3 109.16 110.31 4.57 o 4 6 3 28.79 27.15 1.95 o 5 6 3 0.66 1.34 1.72 o -5 7 3 334.49 317.69 8.58 o -4 7 3 474.28 442.84 13.57 o -3 7 3 72.21 76.18 3.40 o -2 7 3 110.22 106.28 3.64 o -1 7 3 1073.66 1062.00 8.30 o 0 7 3 660.54 690.59 12.97 o 1 7 3 770.18 773.05 26.23 o 2 7 3 720.95 725.29 28.65 o 3 7 3 27.94 28.28 1.81 o 4 7 3 39.38 39.12 2.30 o 5 7 3 185.95 193.72 6.73 o -5 8 3 6.88 8.04 1.93 o -4 8 3 9.07 8.53 1.82 o -3 8 3 113.27 105.57 7.11 o -2 8 3 91.45 89.18 3.54 o -1 8 3 0.13 -0.08 0.29 o 0 8 3 26.74 24.12 1.14 o 1 8 3 15.37 12.02 2.21 o 2 8 3 70.91 67.67 3.73 o 3 8 3 127.77 123.51 5.06 o 4 8 3 2.41 2.42 0.95 o 5 8 3 17.96 17.82 2.66 o -4 9 3 9.07 7.75 1.39 o -3 9 3 602.44 587.77 10.03 o -2 9 3 1540.24 1533.19 15.04 o -1 9 3 159.70 156.65 3.65 o 0 9 3 63.98 59.19 2.22 o 1 9 3 500.44 494.55 21.92 o 2 9 3 467.47 487.69 21.59 o 3 9 3 295.21 295.53 10.73 o 4 9 3 82.35 86.40 4.24 o -4 10 3 5.25 5.55 1.21 o -3 10 3 0.03 0.24 0.94 o -2 10 3 1.00 2.37 1.10 o -1 10 3 41.12 41.11 2.05 o 0 10 3 0.14 0.96 0.71 o 1 10 3 29.44 28.99 2.25 o 2 10 3 21.93 24.13 1.90 o 3 10 3 62.62 59.23 2.82 o 4 10 3 1.49 1.98 0.98 o -3 11 3 169.25 175.47 6.07 o -2 11 3 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2 9 0.51 0.38 0.74 o 2 2 9 19.80 23.21 2.40 o 3 2 9 0.30 1.12 0.98 o 4 2 9 7.64 7.72 2.03 o -4 3 9 293.23 310.48 15.96 o -3 3 9 13.68 19.41 2.07 o -2 3 9 290.59 302.07 33.27 o -1 3 9 642.57 617.90 28.50 o 0 3 9 234.69 224.63 11.05 o 1 3 9 272.14 264.57 6.61 o 2 3 9 198.15 202.97 7.40 o 3 3 9 22.82 27.31 2.75 o 4 3 9 17.36 21.99 2.79 o -3 4 9 0.58 0.09 0.49 o -2 4 9 29.73 29.18 2.43 o -1 4 9 0.63 0.62 0.44 o 0 4 9 2.97 2.67 0.81 o 1 4 9 25.48 24.33 2.31 o 2 4 9 0.43 0.33 0.80 o 3 4 9 0.61 0.70 0.98 o -3 5 9 122.46 118.21 4.07 o -2 5 9 461.43 466.10 32.77 o -1 5 9 223.70 229.64 15.99 o 0 5 9 1.14 1.29 0.59 o 1 5 9 28.97 31.74 3.00 o 2 5 9 240.50 240.07 10.58 o 3 5 9 81.86 76.97 3.35 o -3 6 9 49.85 52.13 3.50 o -2 6 9 0.16 0.57 0.93 o -1 6 9 52.24 53.92 3.26 o 0 6 9 0.78 0.50 0.89 o 1 6 9 74.33 74.21 3.02 o 2 6 9 10.65 10.92 1.32 o 3 6 9 14.67 16.11 1.84 o -3 7 9 187.60 206.11 11.80 o -2 7 9 280.29 308.37 17.26 o -1 7 9 230.21 235.58 19.99 o 0 7 9 222.11 236.54 19.22 o 1 7 9 112.91 120.03 11.01 o 2 7 9 75.17 84.89 3.17 o 3 7 9 64.32 75.18 4.20 o -2 8 9 47.03 49.57 3.45 o -1 8 9 4.10 4.02 2.20 o 0 8 9 18.57 20.53 2.44 o 1 8 9 1.11 1.32 1.15 o 2 8 9 2.81 3.51 1.13 o -1 9 9 104.43 104.89 7.08 o 0 9 9 38.14 41.72 4.05 o 1 9 9 83.17 91.41 4.57 o -3 0 10 187.30 204.18 6.77 o -2 0 10 522.55 511.72 24.70 o -1 0 10 436.97 415.29 21.88 o 0 0 10 27.16 25.28 3.11 o 1 0 10 253.81 221.21 9.05 o 2 0 10 265.30 256.01 10.15 o 3 0 10 32.10 31.93 4.45 o -3 1 10 3.46 4.70 1.24 o -2 1 10 0.32 0.52 0.54 o -1 1 10 12.42 11.25 1.45 o 0 1 10 0.68 1.34 0.74 o 1 1 10 1.06 2.40 1.03 o 2 1 10 0.41 1.28 1.72 o 3 1 10 2.99 2.03 1.24 o -3 2 10 284.75 283.88 14.26 o -2 2 10 200.46 192.03 10.11 o -1 2 10 7.33 7.94 1.27 o 0 2 10 133.92 106.97 20.82 o 1 2 10 165.61 166.81 5.62 o 2 2 10 31.17 33.40 2.75 o 3 2 10 8.11 9.49 1.96 o -3 3 10 16.70 22.22 2.17 o -2 3 10 104.63 106.39 7.32 o -1 3 10 49.26 44.97 2.36 o 0 3 10 116.45 113.78 4.47 o 1 3 10 15.47 17.77 2.20 o 2 3 10 52.93 54.19 3.47 o 3 3 10 4.64 4.11 1.53 o -3 4 10 65.61 66.96 5.91 o -2 4 10 172.92 168.02 15.01 o -1 4 10 212.41 206.78 13.33 o 0 4 10 121.03 121.04 3.81 o 1 4 10 240.99 235.95 6.75 o 2 4 10 135.02 128.49 5.23 o 3 4 10 17.76 19.89 4.93 o -2 5 10 56.64 61.82 6.97 o -1 5 10 128.83 125.14 12.02 o 0 5 10 75.55 76.21 3.87 o 1 5 10 45.38 45.83 3.13 o 2 5 10 15.51 13.54 2.15 o -2 6 10 428.89 465.17 42.25 o -1 6 10 239.37 255.37 17.11 o 0 6 10 33.08 36.67 4.31 o 1 6 10 13.95 16.61 1.83 o 2 6 10 54.34 59.47 3.69 o -2 7 10 5.86 8.27 1.91 o -1 7 10 3.56 3.78 2.06 o 0 7 10 5.23 8.19 2.73 o 1 7 10 6.02 7.78 1.86 o 2 7 10 3.26 3.27 1.13 o -1 8 10 36.74 40.83 4.69 o 0 8 10 56.21 53.90 5.22 o 1 8 10 147.54 163.12 6.14 o -2 1 11 262.21 262.42 6.11 o -1 1 11 36.97 37.22 2.28 o 0 1 11 76.13 73.28 3.85 o 1 1 11 119.37 104.77 6.77 o 2 1 11 27.25 24.76 2.78 o -2 2 11 4.34 4.75 1.37 o -1 2 11 0.22 0.39 0.58 o 0 2 11 2.93 2.09 0.93 o 1 2 11 0.24 1.19 0.76 o 2 2 11 7.59 9.98 1.96 o -2 3 11 52.88 54.69 3.57 o -1 3 11 81.87 75.34 3.20 o 0 3 11 138.82 135.07 5.23 o 1 3 11 206.74 205.56 8.90 o 2 3 11 83.76 83.95 4.46 o -2 4 11 17.50 16.67 3.04 o -1 4 11 6.66 5.34 1.45 o 0 4 11 14.72 16.16 2.27 o 1 4 11 5.05 4.49 1.40 o 2 4 11 0.66 0.94 1.00 o -1 5 11 105.33 117.79 7.87 o 0 5 11 100.15 117.14 7.52 o 1 5 11 18.96 22.94 2.63 o -1 6 11 3.00 4.08 1.47 o 0 6 11 15.97 16.80 3.64 o 1 6 11 17.88 17.76 3.69 o -1 0 12 94.94 94.07 6.51 o 0 0 12 199.43 192.20 9.33 o 1 0 12 60.83 62.38 5.46 o -1 1 12 2.59 3.93 1.20 o 0 1 12 11.49 12.84 2.59 o 1 1 12 1.37 1.78 0.94 o -1 2 12 65.16 70.66 3.98 o 0 2 12 22.09 26.22 2.79 o 1 2 12 32.10 35.19 6.22 o 0 3 12 3.23 4.02 1.23 o