#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:15:39 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180990 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/70/2207079.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207079_Fobs loop_ _publ_author_name 'Duan, Xue-Min' 'Huang, Peng-Mian' 'Zheng, Peng-Wu' 'Li, Jiang-Sheng' _publ_section_title ; 9-Benzyl-3,6-dibromo-9H-carbazole ; _journal_coeditor_code TK6261 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3361 _journal_page_last o3363 _journal_volume 61 _journal_year 2005 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 116.449 _cell_angle_gamma 90.000 _cell_length_a 39.1126 _cell_length_b 4.5063 _cell_length_c 20.4690 _exptl_crystal_F_000 1632.00 _reflns_d_resolution_high 0.7983 _cod_data_source_file tk6261Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50710C in Cc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 513.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 9 1 -24 761.14 282.54 406.32 o 11 1 -24 96.31 -248.06 360.43 o 13 1 -24 1649.06 2183.16 418.23 o 3 1 -23 5.58 -263.19 407.81 o 5 1 -23 0.81 -348.77 348.77 o 7 1 -23 4.96 297.17 405.08 o 9 1 -23 10.11 -262.45 323.47 o 11 1 -23 62.66 607.74 337.11 o 13 1 -23 44.66 -311.81 311.81 o 15 1 -23 5.68 -179.35 296.18 o 8 2 -23 141.76 -403.84 403.84 o 10 2 -23 41.52 -197.70 347.53 o 12 2 -23 166.87 -117.58 355.22 o 14 2 -23 285.29 -146.11 341.82 o 16 2 -23 28.89 -297.67 297.67 o 26 2 -23 41.99 -20.84 525.63 o 28 2 -23 404.56 -306.10 646.69 o 30 2 -23 402.13 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