#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/70/2207082.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207082_Fobs loop_ _publ_author_name 'Salloum, D.' 'Gougeon, P.' 'Potel, M.' _publ_section_title ; Ag~1.91~Cs~1.16~Mo~9~S~11~: a novel quaternary reduced molybdenum sulfide containing Mo~9~ clusters ; _journal_coeditor_code WM6090 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i213 _journal_page_last i215 _journal_volume 61 _journal_year 2005 _space_group_IT_number 176 _symmetry_space_group_name_Hall '-P 6c' _symmetry_space_group_name_H-M 'P 63/m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 9.6366 _cell_length_b 9.6366 _cell_length_c 11.6119 _exptl_crystal_F_000 1415.69 _reflns_d_resolution_high 0.5556 _[local]_cod_data_source_file wm6090Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' agcs_0m in P 63/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 661.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y, x-y, z' '-x+y, -x, z' 'x-y, x, z+1/2' 'y, -x+y, z+1/2' '-x, -y, -z' 'x, y, -z-1/2' 'y, -x+y, -z' 'x-y, x, -z' '-x+y, -x, -z-1/2' '-y, x-y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 2 0 29364.11 31210.39 550.62 o 0 2 0 2168.53 2064.64 42.03 o -2 3 0 20197.62 21039.60 374.66 o -1 3 0 113638.59 114042.15 2380.00 o 0 3 0 5063.12 5372.78 119.86 o -3 4 0 76683.18 76286.80 1351.32 o -2 4 0 35452.99 37553.08 640.45 o -1 4 0 3605.69 3788.58 103.92 o 0 4 0 323.60 316.03 18.20 o -4 5 0 14190.62 14130.12 179.33 o -3 5 0 1914.49 2261.86 57.82 o -2 5 0 50255.16 49888.28 690.75 o -1 5 0 13546.11 13967.62 240.10 o 0 5 0 44.81 107.40 14.15 o -5 6 0 1010.52 986.20 22.66 o -4 6 0 5656.47 5540.16 72.47 o -3 6 0 3153.64 3201.60 62.45 o -2 6 0 15469.21 15174.35 219.85 o -1 6 0 19887.52 20318.37 325.54 o 0 6 0 225294.84 231141.13 3411.09 o -6 7 0 5862.25 5936.98 98.87 o -5 7 0 5858.62 6130.85 115.04 o -4 7 0 4215.50 4317.71 64.66 o -3 7 0 6201.28 6126.67 85.59 o -2 7 0 48627.24 48804.87 668.76 o -1 7 0 25800.13 25978.37 354.85 o 0 7 0 9988.62 10401.34 144.49 o -7 8 0 7550.30 7906.30 114.62 o -6 8 0 22500.61 22149.78 272.13 o -5 8 0 4906.38 4893.32 72.80 o -4 8 0 15494.63 15979.26 201.17 o -3 8 0 4369.58 4309.31 78.18 o -2 8 0 2685.66 2814.19 75.60 o -1 8 0 92694.69 92143.54 1221.49 o 0 8 0 311.31 361.76 24.08 o -8 9 0 3952.54 3900.61 87.06 o -7 9 0 1580.10 1603.32 51.56 o -6 9 0 1710.71 1714.15 40.11 o -5 9 0 44938.50 44256.50 501.53 o -4 9 0 9863.89 9752.18 139.99 o -3 9 0 503.94 506.90 28.30 o -2 9 0 1557.24 1567.53 48.44 o -1 9 0 2639.23 2786.90 62.64 o 0 9 0 6536.56 6479.72 110.69 o -9 10 0 47046.36 46675.13 690.28 o -8 10 0 209.66 233.79 26.93 o -7 10 0 427.68 459.61 30.10 o -6 10 0 224.75 307.79 27.29 o -5 10 0 195.60 368.27 38.64 o -4 10 0 1704.20 1717.60 47.66 o -3 10 0 10650.79 10762.57 180.46 o -2 10 0 5505.43 5589.32 109.43 o -1 10 0 5023.25 5056.26 103.46 o 0 10 0 2059.50 2102.11 84.64 o -10 11 0 4387.71 4394.01 196.94 o -9 11 0 1822.05 1898.74 73.53 o -8 11 0 183.15 227.48 37.68 o -7 11 0 28173.48 27902.17 389.52 o -6 11 0 178.85 207.30 28.51 o -5 11 0 962.51 1044.94 38.98 o -4 11 0 1100.99 1245.23 47.41 o -3 11 0 25.43 71.90 33.11 o -2 11 0 16468.98 15841.64 256.99 o -1 11 0 12880.97 12617.77 237.49 o 0 11 0 278.65 408.01 57.63 o -11 12 0 110.71 175.02 76.74 o -10 12 0 4509.33 4315.87 147.54 o -9 12 0 944.35 975.94 62.28 o -8 12 0 1549.69 1491.30 63.61 o -7 12 0 2495.99 2608.41 98.48 o -6 12 0 34081.47 34155.70 475.94 o -5 12 0 562.01 547.81 36.84 o -4 12 0 20075.19 19947.82 292.80 o -3 12 0 5829.09 6080.32 151.20 o -2 12 0 394.07 417.18 51.15 o -1 12 0 2621.28 2320.23 99.00 o 0 12 0 29447.46 29499.36 765.63 o -12 13 0 709.36 556.32 107.61 o -11 13 0 831.50 801.46 94.85 o -10 13 0 4997.75 5150.41 169.80 o -9 13 0 99.32 119.44 52.65 o -8 13 0 43587.00 43290.62 703.19 o -7 13 0 12170.96 12069.13 227.41 o -6 13 0 3453.31 3324.31 113.47 o -5 13 0 2505.08 2495.18 78.69 o -4 13 0 6.40 18.06 43.57 o -3 13 0 1085.88 1033.19 67.63 o -2 13 0 16481.42 16024.79 345.41 o -1 13 0 10145.46 9419.18 389.90 o 0 13 0 3082.12 3272.58 167.69 o -13 14 0 1334.67 1559.67 128.20 o -12 14 0 5935.97 5583.19 221.78 o -11 14 0 30.35 53.39 81.83 o -10 14 0 1128.85 1162.77 118.46 o -9 14 0 545.53 562.51 71.79 o -8 14 0 1060.19 1020.40 72.88 o -7 14 0 14025.32 13743.29 325.56 o -6 14 0 1425.65 1423.38 94.47 o -5 14 0 24.70 16.40 67.27 o -4 14 0 48.80 78.39 56.55 o -3 14 0 697.53 756.04 84.66 o -2 14 0 4304.81 4490.92 201.66 o -1 14 0 34843.91 35754.00 929.32 o 0 14 0 37.04 222.08 113.86 o -14 15 0 276.67 303.58 109.28 o -13 15 0 703.48 717.86 113.91 o -12 15 0 5088.54 5004.87 216.24 o -11 15 0 5410.13 5194.96 234.00 o -10 15 0 2439.57 2546.00 148.66 o -9 15 0 332.45 388.75 78.36 o -8 15 0 1105.63 1117.99 98.88 o -7 15 0 327.42 368.21 83.81 o -6 15 0 2395.20 2434.25 122.69 o -5 15 0 8306.67 8347.24 235.20 o -4 15 0 1302.18 1106.26 148.74 o -3 15 0 195.62 102.29 82.39 o -2 15 0 119.77 138.98 85.83 o -1 15 0 230.19 524.07 101.21 o 0 15 0 1993.46 1753.08 151.34 o -13 16 0 2668.40 2539.68 235.62 o -12 16 0 626.26 389.08 110.12 o -11 16 0 1378.85 1860.51 230.37 o -10 16 0 57.74 -21.62 163.67 o -9 16 0 4498.37 4732.01 216.45 o -8 16 0 1870.79 2020.63 144.92 o -7 16 0 3404.68 3632.27 164.52 o -6 16 0 8.98 3.31 87.39 o -5 16 0 2690.72 2833.23 258.94 o -4 16 0 1198.25 1225.95 206.52 o -3 16 0 964.76 1111.14 179.10 o -11 17 0 348.63 368.74 202.03 o -9 17 0 441.15 493.65 131.37 o -8 17 0 87.12 94.24 101.17 o -7 17 0 3274.96 3507.34 382.87 o -6 17 0 143.70 227.84 121.69 o 0 1 1 21938.00 23992.92 654.28 o -1 2 1 3332.95 3567.43 47.05 o 0 2 1 1453.82 1499.01 28.57 o -2 3 1 9016.21 9652.32 122.38 o -1 3 1 14559.75 14922.58 189.50 o 0 3 1 7905.84 7924.36 101.76 o -3 4 1 32199.54 32625.76 388.93 o -2 4 1 9569.06 9799.75 132.00 o -1 4 1 2184.71 2331.10 78.66 o 0 4 1 2.75 43.44 8.57 o -4 5 1 122.35 185.04 10.61 o -3 5 1 47086.48 47324.25 447.51 o -2 5 1 16976.59 17482.69 175.82 o -1 5 1 3103.59 3308.08 49.82 o 0 5 1 2979.25 3153.09 38.82 o -5 6 1 1543.38 1593.93 33.44 o -4 6 1 7511.81 7413.45 71.66 o -3 6 1 74.34 111.58 9.15 o -2 6 1 444.45 488.68 16.12 o -1 6 1 40530.82 39993.83 371.60 o 0 6 1 50.85 103.14 9.92 o -6 7 1 17602.94 17748.49 161.19 o -5 7 1 1002.46 1065.16 23.25 o -4 7 1 120.26 218.07 14.42 o -3 7 1 62.19 104.82 11.63 o -2 7 1 2394.34 2390.41 32.33 o -1 7 1 34546.04 34779.77 335.73 o 0 7 1 26880.77 26425.75 248.35 o -7 8 1 987.06 931.76 21.62 o -6 8 1 2793.49 2825.65 36.44 o -5 8 1 7895.35 7943.28 71.48 o -4 8 1 496.59 591.71 23.98 o -3 8 1 3447.75 3411.17 44.24 o -2 8 1 316.94 384.63 17.12 o -1 8 1 260.71 301.21 19.68 o 0 8 1 132.05 169.53 14.49 o -8 9 1 1859.74 1984.78 36.84 o -7 9 1 3667.33 3482.48 46.73 o -6 9 1 580.52 641.76 19.08 o -5 9 1 7399.07 7638.08 73.58 o -4 9 1 3595.91 3534.11 44.41 o -3 9 1 87.11 102.03 16.52 o -2 9 1 7924.84 7663.74 99.47 o -1 9 1 5104.02 5373.72 69.23 o 0 9 1 1247.72 1344.79 33.68 o -9 10 1 8316.29 8175.35 109.60 o -8 10 1 1169.40 1332.12 34.08 o -7 10 1 858.13 953.75 28.63 o -6 10 1 2146.33 2050.45 34.45 o -5 10 1 461.95 534.87 23.99 o -4 10 1 86.85 141.73 18.96 o -3 10 1 7003.20 6896.16 89.29 o -2 10 1 2056.06 2003.60 41.96 o -1 10 1 444.57 429.36 26.07 o 0 10 1 233.80 147.41 25.39 o -10 11 1 174.16 220.95 34.50 o -9 11 1 4745.70 4950.46 73.26 o -8 11 1 2017.39 1921.98 42.34 o -7 11 1 157.49 155.75 23.44 o -6 11 1 2517.42 2446.74 42.00 o -5 11 1 5864.19 5744.90 70.75 o -4 11 1 388.14 519.83 38.05 o -3 11 1 3563.51 3492.24 87.70 o -2 11 1 2940.70 2970.10 59.45 o -1 11 1 48.58 54.76 28.74 o 0 11 1 160.18 255.38 40.26 o -11 12 1 217.79 232.30 45.14 o -10 12 1 247.16 292.40 38.29 o -9 12 1 663.72 602.15 37.77 o -8 12 1 419.26 366.53 30.04 o -7 12 1 8313.45 8249.87 111.33 o -6 12 1 6.58 48.12 24.36 o -5 12 1 369.95 380.89 27.13 o -4 12 1 2796.80 2873.97 57.83 o -3 12 1 953.14 913.14 36.72 o -2 12 1 780.66 894.97 42.22 o -1 12 1 2529.14 2174.20 67.69 o 0 12 1 3.49 44.24 47.61 o -12 13 1 439.96 465.92 63.74 o -11 13 1 867.67 684.31 64.30 o -10 13 1 1328.19 1356.60 54.89 o -9 13 1 77.55 110.10 35.37 o -8 13 1 284.64 295.28 37.00 o -7 13 1 20296.15 20243.87 262.42 o -6 13 1 2691.18 2719.73 60.00 o -5 13 1 718.41 728.48 39.73 o -4 13 1 1344.58 1314.19 42.48 o -3 13 1 262.78 258.45 38.69 o -2 13 1 368.64 395.39 50.79 o -1 13 1 4660.15 4927.14 133.84 o 0 13 1 2119.59 1851.72 92.15 o -13 14 1 486.33 527.10 73.15 o -12 14 1 144.93 187.27 63.25 o -11 14 1 156.64 130.06 58.41 o -10 14 1 922.88 835.17 57.96 o -9 14 1 64.74 92.54 42.37 o -8 14 1 3329.71 3253.94 110.56 o -7 14 1 30.10 74.56 43.03 o -6 14 1 2345.23 2205.50 77.56 o -5 14 1 1600.18 1652.86 62.28 o -4 14 1 878.87 936.21 67.01 o -3 14 1 11.90 33.31 52.95 o -2 14 1 2808.19 2696.05 108.37 o -1 14 1 326.36 260.10 69.33 o 0 14 1 369.06 488.38 94.48 o -14 15 1 175.83 197.47 76.12 o -13 15 1 2546.99 2422.91 126.12 o -12 15 1 139.84 201.05 68.47 o -11 15 1 4596.56 4402.97 140.96 o -10 15 1 3605.81 3483.68 112.61 o -9 15 1 427.17 410.71 57.57 o -8 15 1 138.28 151.01 54.19 o -7 15 1 1856.35 1894.69 79.07 o -6 15 1 160.40 141.96 55.10 o -5 15 1 2412.90 2448.13 139.61 o -4 15 1 379.46 376.62 64.92 o -3 15 1 59.32 41.62 62.37 o -2 15 1 481.39 477.03 66.18 o -1 15 1 47.78 79.34 68.65 o 0 15 1 1.58 44.29 72.61 o -13 16 1 92.02 104.59 92.43 o -12 16 1 163.95 187.94 88.82 o -11 16 1 89.28 86.59 89.44 o -10 16 1 682.57 690.63 88.65 o -9 16 1 1768.59 1844.06 121.61 o -8 16 1 4.09 -1.22 66.88 o -7 16 1 320.59 287.30 66.23 o -6 16 1 1385.16 1418.04 87.52 o -5 16 1 10.92 45.24 71.02 o -4 16 1 1016.00 1068.47 92.92 o -3 16 1 2385.81 2446.12 118.14 o -11 17 1 301.33 299.49 138.32 o -10 17 1 32.75 36.93 111.84 o -9 17 1 792.51 783.92 102.38 o -8 17 1 31.60 18.67 77.84 o -7 17 1 444.15 381.01 81.39 o -6 17 1 943.47 999.48 136.07 o 0 1 2 2767.95 3211.76 59.68 o -1 2 2 754.27 885.92 32.16 o 0 2 2 103.11 215.48 13.28 o -2 3 2 46457.71 47730.18 575.24 o -1 3 2 1852.25 1998.47 75.94 o 0 3 2 276.31 321.31 16.65 o -3 4 2 109848.41 109540.92 1429.01 o -2 4 2 4476.44 4732.23 67.43 o -1 4 2 35511.43 37282.21 510.98 o 0 4 2 4116.90 4217.84 87.07 o -4 5 2 15751.76 15611.70 154.88 o -3 5 2 66147.15 65673.75 636.75 o -2 5 2 53725.41 52894.83 513.52 o -1 5 2 1894.97 1885.18 29.74 o 0 5 2 5600.14 5667.09 68.19 o -5 6 2 669.16 742.28 22.92 o -4 6 2 1362.20 1375.22 28.95 o -3 6 2 2213.24 2311.63 36.01 o -2 6 2 4384.06 4380.42 50.95 o -1 6 2 1340.95 1440.04 34.37 o 0 6 2 4118.39 4171.06 60.63 o -6 7 2 790.53 806.97 21.97 o -5 7 2 175.02 329.33 20.54 o -4 7 2 23325.04 23642.11 219.20 o -3 7 2 18618.79 19168.98 178.30 o -2 7 2 2925.99 2967.13 39.27 o -1 7 2 4954.62 5035.05 73.34 o 0 7 2 8774.48 8720.44 97.28 o -7 8 2 1419.25 1496.02 33.90 o -6 8 2 746.52 802.17 20.17 o -5 8 2 57553.54 57024.69 466.32 o -4 8 2 120.74 354.17 41.29 o -3 8 2 2994.99 2867.36 44.87 o -2 8 2 1105.70 1115.65 28.96 o -1 8 2 237.96 338.84 23.78 o 0 8 2 94.22 122.84 18.57 o -8 9 2 8911.21 8700.25 107.37 o -7 9 2 3657.43 3651.43 58.77 o -6 9 2 2156.61 2243.15 35.59 o -5 9 2 71370.89 70475.66 591.74 o -4 9 2 23882.70 23858.32 244.95 o -3 9 2 976.12 993.55 29.43 o -2 9 2 1606.83 1603.92 33.06 o -1 9 2 578.68 496.31 23.91 o 0 9 2 132.24 161.51 21.42 o -9 10 2 18331.90 17972.70 219.65 o -8 10 2 232.43 303.07 31.93 o -7 10 2 909.23 977.29 29.62 o -6 10 2 5006.33 4958.27 80.27 o -5 10 2 11.46 68.96 17.27 o -4 10 2 4511.45 4555.52 83.28 o -3 10 2 19889.44 19419.41 215.20 o -2 10 2 527.34 570.85 32.96 o -1 10 2 3217.81 3211.14 62.71 o 0 10 2 2715.84 2631.53 79.99 o -10 11 2 779.75 845.04 37.87 o -9 11 2 25070.03 24848.33 285.49 o -8 11 2 8372.86 8243.08 105.35 o -7 11 2 884.99 909.59 30.65 o -6 11 2 1702.15 1726.73 42.63 o -5 11 2 2479.37 2584.67 48.17 o -4 11 2 439.84 429.59 26.88 o -3 11 2 25704.82 25599.46 280.36 o -2 11 2 8878.77 8476.45 121.78 o -1 11 2 30.06 24.28 26.91 o 0 11 2 761.56 857.35 49.12 o -11 12 2 69.70 136.87 39.29 o -10 12 2 3027.22 2915.64 70.25 o -9 12 2 23.40 30.80 29.28 o -8 12 2 295.04 352.26 30.54 o -7 12 2 369.07 353.28 28.72 o -6 12 2 697.20 726.69 39.51 o -5 12 2 348.26 395.99 31.78 o -4 12 2 6250.36 6167.31 89.28 o -3 12 2 10.56 45.17 27.86 o -2 12 2 565.93 538.30 35.75 o -1 12 2 19.37 47.47 35.46 o 0 12 2 880.91 923.70 60.96 o -12 13 2 1212.03 1225.65 70.30 o -11 13 2 158.41 179.62 49.41 o -10 13 2 1766.38 1646.18 94.18 o -9 13 2 5515.22 5191.55 95.82 o -8 13 2 4850.37 4758.31 85.53 o -7 13 2 285.45 241.07 35.64 o -6 13 2 1291.53 1289.40 45.58 o -5 13 2 913.76 905.65 42.04 o -4 13 2 1666.23 1626.87 49.95 o -3 13 2 2413.60 2425.29 69.47 o -2 13 2 814.12 820.94 50.85 o -1 13 2 77.67 142.84 57.24 o 0 13 2 44.49 47.62 54.10 o -13 14 2 50.33 92.77 67.21 o -12 14 2 3861.87 4106.06 122.46 o -11 14 2 9955.12 9528.13 195.88 o -10 14 2 71.81 51.40 52.65 o -9 14 2 298.78 231.69 54.84 o -8 14 2 830.73 842.05 66.56 o -7 14 2 348.69 391.95 52.09 o -6 14 2 2105.22 2036.60 66.31 o -5 14 2 7768.75 7642.62 131.71 o -4 14 2 59.54 40.51 44.88 o -3 14 2 392.06 344.16 55.47 o -2 14 2 290.99 272.46 60.39 o -1 14 2 1143.62 1177.07 90.56 o 0 14 2 1230.20 1219.23 81.32 o -14 15 2 2641.08 2330.06 118.89 o -13 15 2 404.01 481.48 93.07 o -12 15 2 114.69 135.67 74.72 o -11 15 2 9045.46 9288.71 308.29 o -10 15 2 547.44 514.89 69.48 o -9 15 2 247.61 250.09 61.19 o -8 15 2 4010.45 3864.21 105.72 o -7 15 2 1116.85 1102.67 75.08 o -6 15 2 615.26 529.87 61.44 o -5 15 2 14409.34 14692.26 250.53 o -4 15 2 1471.66 1484.20 84.34 o -3 15 2 644.22 583.22 70.86 o -2 15 2 2177.99 2158.36 119.40 o -1 15 2 737.74 674.65 80.05 o -13 16 2 820.74 819.77 110.25 o -12 16 2 2470.05 2148.42 129.15 o -11 16 2 572.10 556.70 87.75 o -10 16 2 1186.35 1150.17 115.56 o -9 16 2 4271.06 4358.19 133.22 o -8 16 2 189.27 214.08 69.99 o -7 16 2 361.21 280.85 71.07 o -6 16 2 7781.84 7816.87 225.51 o -5 16 2 41.11 56.36 68.72 o -4 16 2 1003.56 841.71 91.54 o -3 16 2 3757.54 3734.77 128.96 o -11 17 2 1515.86 1486.87 112.42 o -10 17 2 161.45 123.25 92.31 o -9 17 2 8378.40 8979.86 245.60 o -8 17 2 2010.30 1906.21 133.72 o -7 17 2 155.85 56.66 85.56 o -6 17 2 1802.69 1794.36 111.58 o 0 1 3 19479.06 20026.97 372.68 o -1 2 3 298.22 304.30 55.27 o 0 2 3 12145.71 12444.90 243.50 o -2 3 3 51307.13 52101.19 741.72 o -1 3 3 3136.76 3282.45 56.39 o 0 3 3 139.33 141.33 34.27 o -3 4 3 21489.53 21764.18 230.31 o -2 4 3 296423.19 302815.06 4292.91 o -1 4 3 40611.87 40401.92 406.38 o 0 4 3 3163.68 3244.64 54.17 o -4 5 3 13830.01 13838.20 138.35 o -3 5 3 43916.93 43339.73 426.27 o -2 5 3 5286.74 5395.52 58.85 o -1 5 3 1636.43 1732.33 29.35 o 0 5 3 135.83 196.83 11.94 o -5 6 3 2174.40 2245.71 35.53 o -4 6 3 1073.83 1070.76 20.16 o -3 6 3 4271.51 4182.19 46.46 o -2 6 3 43.89 91.56 10.75 o -1 6 3 2496.44 2489.31 36.20 o 0 6 3 1039.72 1081.59 25.93 o -6 7 3 2727.00 2758.74 41.27 o -5 7 3 11694.56 12043.27 108.20 o -4 7 3 1740.19 1913.13 30.03 o -3 7 3 9011.36 8952.29 92.09 o -2 7 3 4530.34 4630.72 57.52 o -1 7 3 11976.95 11718.99 125.00 o 0 7 3 3166.48 3177.06 50.48 o -7 8 3 576.35 701.45 25.39 o -6 8 3 1577.44 1468.16 27.99 o -5 8 3 34509.30 34621.05 313.28 o -4 8 3 42613.82 43555.06 408.75 o -3 8 3 1852.08 1834.26 43.61 o -2 8 3 8811.81 8769.85 94.74 o -1 8 3 385.25 454.18 26.76 o 0 8 3 155.47 196.33 20.25 o -8 9 3 9730.22 9465.28 115.81 o -7 9 3 411.59 408.83 20.30 o -6 9 3 19439.84 18879.05 183.07 o -5 9 3 4042.91 4238.45 55.98 o -4 9 3 14969.86 14838.04 174.51 o -3 9 3 3492.31 3457.22 50.77 o -2 9 3 22.63 73.40 17.51 o -1 9 3 462.90 509.47 25.49 o 0 9 3 7806.90 7904.48 115.27 o -9 10 3 3098.08 3003.70 57.18 o -8 10 3 33632.04 33898.54 360.05 o -7 10 3 223.37 281.24 22.01 o -6 10 3 4991.57 5059.56 68.89 o -5 10 3 14921.79 14488.91 171.79 o -4 10 3 1273.19 1343.65 33.43 o -3 10 3 2480.48 2493.15 47.43 o -2 10 3 25269.04 24463.98 255.18 o -1 10 3 1505.44 1549.62 40.47 o 0 10 3 15154.02 14462.17 176.70 o -10 11 3 35433.02 35460.61 398.11 o -9 11 3 18999.16 18455.66 219.27 o -8 11 3 4501.09 4288.35 75.34 o -7 11 3 2667.71 2688.37 49.89 o -6 11 3 1077.81 1058.12 34.23 o -5 11 3 1192.96 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