#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2207122.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207122_Fobs loop_ _publ_author_name 'Venkatraman, Ramaiyer' 'Swesi, Abdurazak T.' 'Yamin, Bohari M.' _publ_section_title ; Acetone 4-phenylthiosemicarbazone ; _journal_coeditor_code AC6214 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3914 _journal_page_last o3916 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.660 _cell_angle_gamma 90.000 _cell_length_a 12.2248 _cell_length_b 7.6184 _cell_length_c 11.6389 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.7967 _[local]_cod_data_source_file ac6214Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' test1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 140.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1527.20 1370.14 21.16 o 3 0 0 7319.29 6061.07 64.26 o 4 0 0 271.84 282.83 4.73 o 5 0 0 1622.74 1623.23 17.07 o 6 0 0 7389.14 7139.07 60.56 o 7 0 0 51.01 36.27 0.60 o 8 0 0 214.60 239.09 4.75 o 9 0 0 48.28 38.76 1.59 o 10 0 0 217.93 191.65 4.35 o 11 0 0 56.91 64.66 2.34 o 12 0 0 16.47 17.48 1.34 o 13 0 0 4.48 3.78 0.88 o 14 0 0 6.44 5.57 0.93 o 1 1 0 2806.49 2570.97 17.48 o 2 1 0 202.93 203.73 1.50 o 3 1 0 13.30 9.36 0.19 o 4 1 0 8.48 6.85 0.18 o 5 1 0 1727.86 1920.45 12.79 o 6 1 0 702.79 766.61 5.35 o 7 1 0 441.12 456.40 3.37 o 8 1 0 396.86 414.14 5.16 o 9 1 0 21.18 20.72 0.67 o 10 1 0 109.44 99.04 1.62 o 11 1 0 0.25 0.36 0.43 o 12 1 0 54.82 46.07 1.47 o 13 1 0 85.37 75.22 1.98 o 14 1 0 16.92 19.53 1.06 o 0 2 0 1253.51 1476.05 22.37 o 1 2 0 792.17 843.78 9.17 o 2 2 0 134.78 131.74 1.11 o 3 2 0 150.85 141.19 1.66 o 4 2 0 1.13 1.00 0.38 o 5 2 0 1.15 1.78 0.18 o 6 2 0 1.04 0.43 0.43 o 7 2 0 152.07 156.43 1.65 o 8 2 0 19.61 21.32 1.02 o 9 2 0 11.94 9.98 0.53 o 10 2 0 46.82 42.08 1.28 o 11 2 0 10.34 7.74 0.68 o 12 2 0 28.21 26.98 1.14 o 13 2 0 5.12 7.21 0.71 o 14 2 0 0.03 0.22 0.49 o 1 3 0 540.19 597.91 6.81 o 2 3 0 456.81 495.09 4.65 o 3 3 0 25.57 23.99 0.42 o 4 3 0 566.13 554.06 4.03 o 5 3 0 308.14 283.39 2.29 o 6 3 0 52.21 45.47 0.66 o 7 3 0 717.91 747.24 6.38 o 8 3 0 342.33 374.65 3.42 o 9 3 0 27.58 26.92 1.03 o 10 3 0 116.91 119.67 2.35 o 11 3 0 71.57 72.95 1.83 o 12 3 0 1.85 1.75 0.67 o 13 3 0 61.22 63.34 1.85 o 14 3 0 26.23 28.72 1.29 o 0 4 0 6085.97 5890.96 88.46 o 1 4 0 3287.20 3418.93 36.17 o 2 4 0 10.67 8.23 0.43 o 3 4 0 451.69 454.07 4.48 o 4 4 0 184.62 188.48 1.72 o 5 4 0 213.65 209.35 1.89 o 6 4 0 689.37 708.65 5.66 o 7 4 0 633.47 663.82 5.58 o 8 4 0 4.83 5.02 0.40 o 9 4 0 80.04 86.21 1.92 o 10 4 0 8.42 6.18 0.65 o 11 4 0 43.74 41.05 1.40 o 12 4 0 8.67 9.34 0.81 o 13 4 0 3.86 4.25 0.79 o 1 5 0 15.25 13.84 0.72 o 2 5 0 199.15 195.27 3.04 o 3 5 0 225.32 251.24 4.05 o 4 5 0 8.48 9.03 0.48 o 5 5 0 56.38 57.64 0.98 o 6 5 0 0.01 0.54 0.28 o 7 5 0 160.06 162.58 1.95 o 8 5 0 55.50 55.21 1.24 o 9 5 0 4.17 4.36 0.52 o 10 5 0 36.78 35.33 1.33 o 11 5 0 30.44 29.31 1.25 o 12 5 0 4.19 6.72 0.78 o 0 6 0 99.61 100.16 2.91 o 2 6 0 161.49 160.16 2.21 o 3 6 0 3.13 3.74 0.55 o 4 6 0 0.47 0.82 0.34 o 5 6 0 16.12 19.05 0.75 o 6 6 0 95.33 103.03 2.21 o 7 6 0 0.02 0.67 0.43 o 8 6 0 222.39 210.59 2.87 o 9 6 0 257.26 270.17 3.47 o 10 6 0 1.18 1.17 1.55 o 11 6 0 4.01 8.47 1.10 o 1 7 0 51.61 49.02 1.49 o 2 7 0 20.80 20.93 0.85 o 3 7 0 18.90 18.67 1.02 o 4 7 0 148.89 138.34 2.17 o 5 7 0 19.20 21.88 0.84 o 6 7 0 18.22 18.33 1.00 o 7 7 0 38.37 40.75 1.45 o 8 7 0 78.25 77.43 2.05 o 9 7 0 22.20 22.19 1.19 o 10 7 0 55.31 52.05 2.51 o 0 8 0 164.06 162.45 4.48 o 1 8 0 106.97 105.20 2.45 o 2 8 0 11.20 10.05 0.70 o 3 8 0 32.63 31.05 1.05 o 4 8 0 35.15 33.29 1.64 o 5 8 0 0.01 0.64 0.46 o 6 8 0 15.77 17.93 1.98 o 7 8 0 36.68 40.57 1.53 o 8 8 0 46.90 44.43 1.65 o 1 9 0 0.65 1.08 0.62 o 2 9 0 0.12 1.46 0.60 o 3 9 0 0.20 1.13 1.48 o 4 9 0 0.08 1.56 0.57 o 5 9 0 0.52 1.89 0.96 o -15 1 1 47.26 47.78 4.11 o -14 1 1 6.14 8.36 0.75 o -13 1 1 16.94 16.26 0.95 o -12 1 1 156.39 153.31 3.30 o -11 1 1 8.50 4.52 0.48 o -10 1 1 124.79 128.03 1.91 o -9 1 1 552.43 563.06 5.58 o -8 1 1 235.35 269.00 3.00 o -7 1 1 40.64 27.66 0.52 o -6 1 1 260.66 264.00 2.34 o -5 1 1 719.83 842.19 6.48 o -4 1 1 290.63 318.35 3.72 o -3 1 1 1138.96 1219.50 8.19 o -2 1 1 338.09 336.74 2.37 o -1 1 1 87.78 88.93 0.97 o 0 1 1 2782.50 2566.34 19.84 o 1 1 1 101.51 107.58 0.88 o 2 1 1 1349.74 1460.05 8.83 o 3 1 1 624.97 615.30 3.86 o 4 1 1 134.44 161.24 1.21 o 5 1 1 167.27 165.82 1.27 o 6 1 1 1738.06 1834.50 11.15 o 7 1 1 141.72 147.07 1.23 o 8 1 1 133.35 117.69 1.20 o 9 1 1 67.57 74.40 1.66 o 10 1 1 22.59 23.12 0.99 o 11 1 1 132.02 118.44 2.40 o 12 1 1 20.67 24.08 1.09 o 13 1 1 8.91 9.12 0.76 o 14 1 1 31.20 25.48 1.23 o -14 2 1 23.15 26.55 1.21 o -13 2 1 44.29 44.45 1.95 o -12 2 1 56.24 50.40 1.52 o -11 2 1 0.61 0.11 0.47 o -10 2 1 233.69 233.13 3.99 o -9 2 1 594.81 610.45 6.01 o -8 2 1 1148.19 1177.44 9.17 o -7 2 1 291.49 263.64 2.45 o -6 2 1 304.84 323.86 2.49 o -5 2 1 743.44 776.67 5.42 o -4 2 1 13.37 8.72 0.28 o -3 2 1 346.66 386.78 2.80 o -2 2 1 12904.61 9860.78 117.35 o -1 2 1 11327.46 8422.02 100.20 o 0 2 1 19683.98 12208.50 182.59 o 1 2 1 2654.62 2813.66 24.43 o 2 2 1 2986.02 3003.05 22.23 o 3 2 1 6.37 4.99 0.22 o 4 2 1 1396.79 1521.32 10.23 o 5 2 1 3305.57 3432.09 22.71 o 6 2 1 622.39 710.47 5.17 o 7 2 1 348.97 343.85 4.03 o 8 2 1 56.48 50.97 1.07 o 9 2 1 255.12 263.34 3.98 o 10 2 1 355.34 354.78 4.93 o 11 2 1 14.98 15.76 0.87 o 12 2 1 46.54 40.41 1.40 o 13 2 1 135.49 139.38 2.90 o 14 2 1 0.24 1.00 0.52 o -14 3 1 0.22 1.68 0.56 o -13 3 1 5.95 5.16 0.66 o -12 3 1 43.03 43.01 1.45 o -11 3 1 0.19 0.24 0.46 o -10 3 1 212.93 206.85 2.70 o -9 3 1 9.02 7.48 0.50 o -8 3 1 264.11 260.16 3.63 o -7 3 1 2.46 1.84 0.29 o -6 3 1 108.27 111.49 1.14 o -5 3 1 200.83 221.32 1.87 o -4 3 1 149.07 154.27 1.39 o -3 3 1 0.59 0.25 0.24 o -2 3 1 79.89 71.15 1.04 o -1 3 1 11.13 19.99 0.63 o 0 3 1 963.16 901.74 14.09 o 1 3 1 21.49 14.82 0.43 o 2 3 1 150.28 128.73 1.33 o 3 3 1 597.25 588.29 4.73 o 4 3 1 94.94 83.22 0.92 o 5 3 1 47.72 32.00 0.54 o 6 3 1 386.92 421.81 3.26 o 7 3 1 216.83 246.82 4.75 o 8 3 1 95.67 80.67 1.52 o 9 3 1 5.68 6.24 0.68 o 10 3 1 0.58 0.37 0.46 o 11 3 1 10.02 8.20 0.73 o 12 3 1 0.43 0.74 0.54 o 13 3 1 11.50 15.04 0.95 o -13 4 1 16.74 16.67 1.02 o -12 4 1 18.04 20.13 1.05 o -11 4 1 15.30 18.22 0.97 o -10 4 1 61.20 59.37 1.64 o -9 4 1 8.01 8.84 0.59 o -8 4 1 692.54 693.49 10.29 o -7 4 1 20.00 19.10 0.59 o -6 4 1 2.71 3.75 0.32 o -5 4 1 38.45 30.92 0.56 o -4 4 1 40.53 57.70 0.79 o -3 4 1 599.58 574.24 4.78 o -2 4 1 829.66 832.79 17.64 o -1 4 1 0.59 4.77 2.48 o 0 4 1 36.74 43.12 4.02 o 1 4 1 173.55 131.01 2.12 o 2 4 1 487.45 574.73 5.47 o 3 4 1 37.56 24.87 0.99 o 4 4 1 244.43 235.64 2.30 o 5 4 1 2.45 1.15 0.23 o 6 4 1 0.86 1.68 0.25 o 7 4 1 15.78 16.48 0.64 o 8 4 1 175.43 171.23 2.32 o 9 4 1 151.11 143.99 3.06 o 10 4 1 43.90 44.95 1.43 o 11 4 1 12.21 13.65 0.87 o 12 4 1 1.49 1.00 0.54 o 13 4 1 0.28 0.40 0.55 o -12 5 1 32.60 37.78 1.43 o -11 5 1 0.02 0.79 0.57 o -10 5 1 15.32 18.72 2.37 o -9 5 1 501.42 528.77 5.55 o -8 5 1 26.57 26.00 0.74 o -7 5 1 26.65 28.02 0.73 o -6 5 1 143.48 140.36 1.52 o -5 5 1 52.96 43.45 0.73 o -4 5 1 30.51 30.20 0.80 o -3 5 1 506.48 475.05 13.17 o -2 5 1 3.02 4.13 0.52 o -1 5 1 115.57 115.68 2.08 o 0 5 1 290.83 303.37 9.30 o 1 5 1 3.99 6.67 0.56 o 2 5 1 189.69 196.13 2.87 o 3 5 1 85.21 84.30 1.37 o 4 5 1 28.31 26.93 0.76 o 5 5 1 239.71 255.45 2.85 o 6 5 1 400.18 408.67 3.78 o 7 5 1 6.05 4.44 0.46 o 8 5 1 4.42 4.41 0.49 o 9 5 1 57.19 61.06 1.79 o 10 5 1 28.01 26.03 1.17 o 11 5 1 54.05 55.26 1.72 o 12 5 1 42.74 46.08 1.61 o -11 6 1 0.01 -0.04 0.98 o -10 6 1 2.14 0.92 0.92 o -9 6 1 196.89 215.35 3.67 o -8 6 1 237.29 236.39 3.24 o -7 6 1 76.16 83.47 1.36 o -6 6 1 21.18 19.41 0.96 o -5 6 1 165.29 169.46 2.34 o -4 6 1 43.27 45.01 1.07 o -3 6 1 190.15 194.83 2.56 o -2 6 1 767.28 818.04 9.75 o -1 6 1 885.31 921.05 22.01 o 0 6 1 127.76 123.80 2.86 o 1 6 1 26.59 25.23 1.51 o 2 6 1 102.23 99.02 1.62 o 3 6 1 2.84 3.60 0.45 o 4 6 1 65.45 61.58 1.26 o 5 6 1 157.15 164.27 2.32 o 6 6 1 12.46 13.72 0.66 o 7 6 1 2.23 2.81 0.46 o 8 6 1 0.10 0.26 0.46 o 9 6 1 11.39 13.30 0.97 o 10 6 1 14.32 15.25 1.41 o 11 6 1 1.18 1.43 1.41 o -10 7 1 28.40 27.48 1.95 o -9 7 1 0.07 0.87 1.55 o -8 7 1 10.69 9.89 1.28 o -7 7 1 0.18 0.05 1.08 o -6 7 1 2.31 2.87 0.62 o -5 7 1 10.21 10.34 0.63 o -4 7 1 5.86 6.04 0.55 o -3 7 1 11.76 11.00 0.66 o -2 7 1 2.72 3.31 0.63 o -1 7 1 0.20 -0.29 0.51 o 0 7 1 14.51 14.79 0.88 o 1 7 1 2.93 4.26 0.53 o 2 7 1 1.48 1.76 0.44 o 3 7 1 15.81 15.14 0.71 o 4 7 1 0.20 0.62 0.39 o 5 7 1 0.03 0.69 0.39 o 6 7 1 5.32 4.74 0.67 o 7 7 1 25.12 25.76 2.38 o 8 7 1 3.64 4.28 0.73 o 9 7 1 0.02 0.37 0.94 o -8 8 1 75.22 75.17 2.13 o -7 8 1 19.78 23.23 1.21 o -6 8 1 0.01 1.67 0.69 o -5 8 1 0.34 0.83 0.47 o -4 8 1 5.78 7.37 0.72 o -3 8 1 29.52 26.30 1.13 o -2 8 1 96.51 90.95 1.80 o -1 8 1 10.78 10.21 0.90 o 0 8 1 10.63 10.33 0.92 o 1 8 1 3.31 3.23 0.82 o 2 8 1 2.10 0.65 0.61 o 3 8 1 12.50 12.67 0.96 o 4 8 1 57.74 56.05 1.85 o 5 8 1 5.53 5.61 0.74 o 6 8 1 0.80 1.35 0.67 o 7 8 1 8.30 9.12 1.14 o -5 9 1 0.09 1.10 0.74 o -4 9 1 0.44 1.78 0.66 o -3 9 1 19.62 20.37 0.92 o -2 9 1 4.48 6.80 0.79 o -1 9 1 43.73 50.43 1.74 o 0 9 1 0.67 1.32 0.62 o 1 9 1 0.74 0.85 0.62 o 2 9 1 5.45 7.05 0.82 o 3 9 1 11.79 13.02 1.79 o 4 9 1 1.42 2.17 0.61 o -15 0 2 101.52 106.81 3.60 o -14 0 2 6.50 5.01 0.94 o -13 0 2 25.98 23.88 1.54 o -12 0 2 137.28 122.89 3.34 o -11 0 2 837.64 825.47 13.72 o -10 0 2 2007.05 2055.46 30.94 o -9 0 2 1269.64 1260.35 19.47 o -8 0 2 4.76 7.25 0.73 o -7 0 2 1183.13 1236.36 18.73 o -6 0 2 7.03 15.82 0.79 o -5 0 2 184.38 214.38 3.80 o -4 0 2 8673.74 7211.87 105.51 o -3 0 2 7363.68 6288.14 92.20 o -2 0 2 1567.46 1597.78 23.56 o -1 0 2 5215.18 4244.37 64.58 o 0 0 2 50.90 30.91 0.43 o 1 0 2 2601.52 2483.51 56.48 o 2 0 2 13.87 6.36 0.63 o 3 0 2 2798.33 2804.40 29.66 o 4 0 2 608.97 707.48 7.79 o 5 0 2 767.67 1067.94 11.55 o 6 0 2 467.80 395.48 4.75 o 7 0 2 43.61 41.71 1.14 o 8 0 2 238.05 197.54 4.26 o 9 0 2 643.50 613.25 10.52 o 10 0 2 18.28 20.90 1.32 o 11 0 2 460.09 407.46 8.00 o 12 0 2 106.33 99.82 3.27 o 13 0 2 21.23 17.81 1.47 o 14 0 2 114.92 116.71 3.83 o -15 1 2 5.99 5.18 0.73 o -14 1 2 27.94 32.56 1.33 o -13 1 2 37.33 32.98 1.27 o -12 1 2 73.61 68.17 1.43 o -11 1 2 208.22 206.39 2.73 o -10 1 2 160.63 158.24 2.20 o -9 1 2 1.78 2.38 0.37 o -8 1 2 116.41 118.37 3.36 o -7 1 2 12.15 23.21 0.46 o -6 1 2 273.63 314.61 2.70 o -5 1 2 263.51 283.21 2.42 o -4 1 2 157.66 172.31 1.36 o -3 1 2 87.64 89.28 0.78 o -2 1 2 1393.70 1490.11 10.13 o -1 1 2 647.27 682.70 9.07 o 0 1 2 3120.79 2860.24 25.27 o 1 1 2 3826.95 3599.53 26.95 o 2 1 2 0.84 0.29 0.14 o 3 1 2 344.25 342.24 2.51 o 4 1 2 651.16 703.56 4.90 o 5 1 2 273.65 365.30 2.74 o 6 1 2 2.26 11.18 0.34 o 7 1 2 85.56 98.71 1.21 o 8 1 2 71.77 81.18 1.11 o 9 1 2 52.54 50.51 1.38 o 10 1 2 179.77 165.15 2.89 o 11 1 2 3.58 1.94 0.49 o 12 1 2 65.02 55.00 1.67 o 13 1 2 39.38 33.27 1.34 o 14 1 2 10.63 8.90 0.79 o -14 2 2 16.04 19.68 1.06 o -13 2 2 0.18 0.04 0.47 o -12 2 2 3.81 1.67 0.52 o -11 2 2 40.90 38.98 1.06 o -10 2 2 20.19 21.14 0.77 o -9 2 2 3.87 3.51 0.80 o -8 2 2 588.57 566.04 5.53 o -7 2 2 115.40 149.05 1.67 o -6 2 2 41.11 44.78 0.57 o -5 2 2 0.27 0.44 0.22 o -4 2 2 41.10 48.22 0.57 o -3 2 2 407.73 464.55 3.32 o -2 2 2 2025.41 2060.55 26.84 o -1 2 2 5099.92 4691.06 41.16 o 0 2 2 613.87 663.82 6.59 o 1 2 2 474.27 452.75 3.22 o 2 2 2 1760.28 1847.81 12.20 o 3 2 2 45.81 43.26 0.57 o 4 2 2 25.28 44.95 0.54 o 5 2 2 503.91 492.79 3.38 o 6 2 2 116.76 100.64 0.97 o 7 2 2 33.94 48.23 0.80 o 8 2 2 376.92 387.79 4.10 o 9 2 2 123.39 100.78 2.07 o 10 2 2 7.02 7.30 1.16 o 11 2 2 0.08 0.15 0.50 o 12 2 2 2.53 3.31 0.61 o 13 2 2 5.57 4.98 0.81 o 14 2 2 2.07 4.42 0.77 o -14 3 2 38.31 37.01 1.44 o -13 3 2 12.58 14.71 0.92 o -12 3 2 6.44 7.06 0.72 o -11 3 2 476.95 480.81 5.18 o -10 3 2 59.80 60.97 1.29 o -9 3 2 22.21 23.64 0.76 o -8 3 2 167.39 162.59 2.42 o -7 3 2 300.79 307.27 3.17 o -6 3 2 167.02 166.63 1.52 o -5 3 2 197.33 190.41 1.65 o -4 3 2 27.02 14.84 0.35 o -3 3 2 54.52 57.05 0.75 o -2 3 2 2430.20 2463.80 28.86 o -1 3 2 8.89 3.18 0.38 o 0 3 2 165.28 164.87 2.34 o 1 3 2 89.71 85.89 1.14 o 2 3 2 523.39 635.45 6.72 o 3 3 2 720.49 796.81 6.28 o 4 3 2 915.95 940.23 7.36 o 5 3 2 43.71 41.08 0.92 o 6 3 2 13.71 10.09 0.34 o 7 3 2 304.95 308.10 2.93 o 8 3 2 55.47 46.74 1.05 o 9 3 2 187.23 175.46 4.34 o 10 3 2 5.73 6.31 0.66 o 11 3 2 61.41 56.91 1.68 o 12 3 2 69.83 58.52 1.77 o 13 3 2 93.41 96.62 2.41 o -13 4 2 8.89 7.74 1.16 o -12 4 2 5.56 7.71 2.39 o -11 4 2 99.60 102.58 2.24 o -10 4 2 1142.90 1188.34 11.08 o -9 4 2 189.62 200.56 2.63 o -8 4 2 96.20 100.37 1.39 o -7 4 2 472.84 467.53 10.77 o -6 4 2 80.95 91.92 1.18 o -5 4 2 27.83 16.43 0.42 o -4 4 2 1822.03 1870.96 14.87 o -3 4 2 1232.30 1360.91 12.24 o -2 4 2 1769.18 2037.88 18.53 o -1 4 2 19.17 21.77 0.78 o 0 4 2 83.73 83.37 1.59 o 1 4 2 353.83 417.41 4.13 o 2 4 2 57.21 54.00 0.96 o 3 4 2 504.55 530.80 4.82 o 4 4 2 44.38 46.47 0.82 o 5 4 2 3.63 7.36 0.55 o 6 4 2 0.24 0.43 0.25 o 7 4 2 83.72 85.22 1.48 o 8 4 2 357.54 369.60 4.11 o 9 4 2 41.98 43.71 1.10 o 10 4 2 0.76 1.69 0.52 o 11 4 2 124.61 126.79 2.67 o 12 4 2 48.91 48.77 1.63 o -13 5 2 3.10 3.06 1.11 o -12 5 2 9.95 8.83 1.23 o -11 5 2 18.28 14.41 1.40 o -10 5 2 73.16 65.94 1.80 o -9 5 2 85.48 88.46 2.07 o -8 5 2 61.45 64.58 1.41 o -7 5 2 51.58 49.23 0.95 o -6 5 2 0.74 0.17 0.26 o -5 5 2 4.84 4.49 0.35 o -4 5 2 0.10 0.96 0.28 o -3 5 2 15.99 16.12 1.18 o -2 5 2 5.40 3.92 0.67 o -1 5 2 3.76 1.93 0.47 o 0 5 2 7.72 5.14 0.73 o 1 5 2 0.80 0.55 0.56 o 2 5 2 125.00 116.69 1.67 o 3 5 2 17.29 21.60 0.68 o 4 5 2 33.87 33.52 1.25 o 5 5 2 18.73 16.16 0.79 o 6 5 2 5.46 5.91 0.41 o 7 5 2 31.51 37.18 0.99 o 8 5 2 77.74 77.50 1.52 o 9 5 2 71.59 68.03 1.45 o 10 5 2 4.64 6.38 0.73 o 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