#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:16:00 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180991 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/71/2207157.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207157_Fobs loop_ _publ_author_name 'Lis, Tadeusz' 'Kinzhybalo, Vasyl' 'Zieba, Krzysztof' _publ_section_title ; A trinuclear mixed-valence manganese carboxylate: tris(acetic acid-\kO)-\m~3~-oxo-hexakis(\m~2~-trichloroacetato-\k^2^O:O')trimanganese(II,III,III) ; _journal_coeditor_code BT6762 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2382 _journal_page_last m2384 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 88.010 _cell_angle_beta 79.450 _cell_angle_gamma 65.940 _cell_length_a 10.1210 _cell_length_b 10.4240 _cell_length_c 22.8910 _exptl_crystal_F_000 1306.00 _reflns_d_resolution_high 0.7671 _cod_data_source_file bt6762Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ziebabs in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 306.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 39102.93 41677.79 112.34 o 3 0 0 14472.85 13719.38 105.22 o 4 0 0 6718.32 6309.55 90.82 o 5 0 0 4000.11 3972.56 122.47 o 6 0 0 1452.69 1399.81 30.68 o 7 0 0 1653.37 1682.79 32.84 o 8 0 0 207.68 303.28 28.26 o 9 0 0 650.02 698.05 29.62 o 10 0 0 32.60 100.65 42.31 o 11 0 0 1900.47 1852.43 80.06 o -11 1 0 2063.60 1866.86 65.80 o -10 1 0 89.88 175.66 47.90 o -9 1 0 5.60 48.44 33.93 o -8 1 0 2251.32 2093.14 68.78 o -7 1 0 1601.78 1790.08 127.68 o -6 1 0 4157.10 3820.53 57.27 o -5 1 0 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