#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/71/2207159.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207159_Fobs loop_ _publ_author_name 'Nichol, Gary S.' 'Clegg, William' _publ_section_title ; Violuric acid monohydrate: a definitive redetermination at 150 K ; _journal_coeditor_code BT6764 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3788 _journal_page_last o3790 _journal_volume 61 _journal_year 2005 _space_group_IT_number 36 _symmetry_space_group_name_Hall 'C 2c -2' _symmetry_space_group_name_H-M 'C m c 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.0754 _cell_length_b 14.3430 _cell_length_c 7.5288 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7491 _[local]_cod_data_source_file bt6764Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gsn66 in Cmc2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 246.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 60711.88 57758.27 896.09 o 4 0 0 12861.99 12857.04 206.06 o 6 0 0 2812.88 2742.82 48.90 o 8 0 0 722.43 681.85 16.05 o 1 1 0 414.94 424.75 3.83 o 3 1 0 124.62 150.76 2.87 o 5 1 0 57.75 60.09 1.08 o 7 1 0 32.36 29.46 1.41 o 0 2 0 1981.16 1940.95 57.37 o 2 2 0 775.69 920.00 8.93 o 4 2 0 140.16 167.67 2.01 o 6 2 0 37.45 36.78 1.14 o 8 2 0 12.56 11.21 2.39 o 1 3 0 102.59 127.69 2.60 o 3 3 0 43.06 42.56 1.08 o 5 3 0 6.58 6.55 0.49 o 7 3 0 0.48 -1.36 2.08 o 0 4 0 206.17 248.91 3.34 o 2 4 0 95.54 123.28 1.70 o 4 4 0 17.21 22.28 0.89 o 6 4 0 2.77 1.69 0.60 o 1 5 0 1306.48 1369.40 12.06 o 3 5 0 486.04 505.20 6.73 o 5 5 0 108.19 109.50 1.62 o 7 5 0 20.51 22.60 3.06 o 0 6 0 8796.71 9330.36 115.62 o 2 6 0 4940.49 5273.85 46.11 o 4 6 0 1320.02 1311.82 12.91 o 6 6 0 303.07 292.99 4.61 o 1 7 0 510.39 609.52 5.54 o 3 7 0 181.26 173.15 2.07 o 5 7 0 22.00 23.30 1.57 o 7 7 0 0.26 -0.37 1.14 o 0 8 0 3530.31 3880.46 47.98 o 2 8 0 2195.50 2304.16 20.27 o 4 8 0 697.51 703.12 8.23 o 6 8 0 177.84 172.73 3.24 o 1 9 0 591.21 691.17 6.33 o 3 9 0 322.75 345.70 4.35 o 5 9 0 133.90 131.02 2.61 o 0 10 0 0.91 0.33 0.38 o 2 10 0 0.01 -0.38 0.38 o 4 10 0 1.34 2.26 0.59 o 6 10 0 2.33 1.22 0.94 o 1 11 0 107.50 108.05 1.58 o 3 11 0 58.59 57.20 1.31 o 5 11 0 21.40 20.55 1.77 o 0 12 0 337.12 341.07 4.83 o 2 12 0 201.86 208.86 2.95 o 4 12 0 42.77 45.56 1.52 o 6 12 0 1.55 -0.46 1.23 o 1 13 0 549.38 492.01 5.98 o 3 13 0 310.58 295.58 4.03 o 5 13 0 118.27 127.19 2.84 o 0 14 0 164.84 130.55 3.09 o 2 14 0 158.99 135.14 2.26 o 4 14 0 133.11 132.09 2.81 o 1 15 0 250.38 206.05 3.65 o 3 15 0 169.23 158.74 3.10 o 2 16 0 16.67 16.18 1.18 o 4 16 0 5.00 5.75 1.43 o 1 17 0 178.23 184.99 6.05 o 3 17 0 120.82 127.66 3.74 o 2 18 0 67.82 74.33 2.86 o 1 19 0 173.23 177.50 6.78 o 1 1 1 2762.09 2748.34 17.23 o 3 1 1 828.91 939.83 5.94 o 5 1 1 288.06 305.24 2.40 o 7 1 1 125.38 128.62 1.85 o 0 2 1 1013.26 943.91 9.09 o 2 2 1 477.39 460.17 2.96 o 4 2 1 107.63 105.09 0.95 o 6 2 1 27.45 27.88 0.81 o 8 2 1 8.51 8.86 1.54 o 1 3 1 516.26 499.22 3.35 o 3 3 1 152.60 149.76 1.25 o 5 3 1 23.74 25.91 0.55 o 7 3 1 2.92 2.79 0.68 o 0 4 1 530.39 503.80 4.54 o 2 4 1 284.71 272.48 1.92 o 4 4 1 83.92 83.53 1.00 o 6 4 1 27.54 28.77 0.73 o 1 5 1 902.04 1029.42 6.72 o 3 5 1 307.62 302.22 2.18 o 5 5 1 46.09 44.08 1.22 o 7 5 1 3.86 4.91 0.87 o 0 6 1 70.70 73.93 0.88 o 2 6 1 38.47 36.11 0.50 o 4 6 1 8.17 7.60 0.38 o 6 6 1 1.08 1.64 0.45 o 1 7 1 358.55 452.34 3.23 o 3 7 1 197.70 224.53 1.94 o 5 7 1 91.71 99.24 1.28 o 7 7 1 39.96 42.51 1.30 o 0 8 1 1346.47 1314.42 11.67 o 2 8 1 874.04 860.62 6.09 o 4 8 1 315.15 307.30 2.79 o 6 8 1 95.58 94.36 1.76 o 1 9 1 66.35 58.49 0.64 o 3 9 1 26.41 23.77 0.56 o 5 9 1 5.78 5.96 0.55 o 7 9 1 1.06 1.85 1.09 o 0 10 1 261.37 244.15 2.50 o 2 10 1 192.97 182.78 1.69 o 4 10 1 93.19 93.74 1.35 o 6 10 1 38.01 41.91 1.18 o 1 11 1 30.78 27.00 0.55 o 3 11 1 10.42 9.06 0.51 o 5 11 1 1.56 0.94 0.53 o 0 12 1 74.95 71.52 1.22 o 2 12 1 55.03 54.01 0.89 o 4 12 1 25.02 23.93 0.81 o 6 12 1 9.07 7.73 1.21 o 1 13 1 711.62 688.54 6.21 o 3 13 1 448.19 445.13 4.26 o 5 13 1 208.08 215.33 2.80 o 0 14 1 341.89 298.85 5.87 o 2 14 1 271.74 242.47 2.99 o 4 14 1 149.01 143.89 1.95 o 1 15 1 16.80 15.57 0.70 o 3 15 1 9.81 9.74 0.76 o 0 16 1 12.49 12.77 1.44 o 2 16 1 8.74 8.83 0.71 o 4 16 1 3.14 2.65 1.30 o 1 17 1 112.14 110.89 2.31 o 3 17 1 67.85 69.45 1.92 o 0 18 1 18.53 18.29 2.79 o 2 18 1 14.92 15.78 1.23 o 0 0 2 2287.12 2295.97 53.80 o 2 0 2 1299.05 1283.18 11.31 o 4 0 2 397.83 417.20 4.56 o 6 0 2 123.28 130.39 5.25 o 1 1 2 679.87 643.84 4.24 o 3 1 2 194.10 175.08 1.28 o 5 1 2 28.31 27.89 0.60 o 7 1 2 2.86 2.90 0.71 o 0 2 2 6466.54 6769.58 104.38 o 2 2 2 3489.74 3605.34 22.30 o 4 2 2 842.79 824.77 6.68 o 6 2 2 167.73 150.26 1.94 o 1 3 2 3628.54 3770.86 24.55 o 3 3 2 1357.44 1412.34 8.85 o 5 3 2 399.88 394.48 3.48 o 7 3 2 127.79 121.99 2.03 o 0 4 2 427.17 410.54 3.76 o 2 4 2 215.32 215.45 1.50 o 4 4 2 36.44 38.94 0.59 o 6 4 2 2.55 1.97 0.48 o 1 5 2 1267.25 1336.13 8.77 o 3 5 2 458.57 432.97 3.02 o 5 5 2 83.12 75.51 1.05 o 7 5 2 11.59 12.52 1.07 o 0 6 2 824.38 832.27 7.46 o 2 6 2 480.78 463.35 3.22 o 4 6 2 122.23 109.72 1.27 o 6 6 2 22.79 21.53 0.74 o 1 7 2 462.11 498.40 3.43 o 3 7 2 208.59 202.82 2.06 o 5 7 2 61.58 57.17 0.95 o 7 7 2 15.25 13.99 0.96 o 0 8 2 393.18 405.69 3.84 o 2 8 2 240.04 242.26 2.05 o 4 8 2 68.55 66.41 0.99 o 6 8 2 13.39 13.39 0.70 o 1 9 2 141.22 136.93 1.23 o 3 9 2 102.64 104.81 1.60 o 5 9 2 67.31 70.50 1.13 o 0 10 2 129.02 128.23 1.73 o 2 10 2 77.27 74.40 0.93 o 4 10 2 19.95 17.50 0.63 o 6 10 2 6.04 6.64 0.70 o 1 11 2 574.50 574.60 4.25 o 3 11 2 363.30 364.04 3.54 o 5 11 2 181.09 188.70 2.30 o 0 12 2 369.96 329.95 3.98 o 2 12 2 296.78 275.33 2.58 o 4 12 2 169.70 167.87 2.06 o 1 13 2 21.05 20.50 0.73 o 3 13 2 14.19 14.92 0.74 o 5 13 2 7.17 8.74 0.75 o 0 14 2 515.19 492.74 7.85 o 2 14 2 393.06 379.08 4.51 o 4 14 2 189.97 200.60 2.45 o 1 15 2 4.22 4.88 0.65 o 3 15 2 5.50 4.94 0.69 o 0 16 2 39.71 37.83 2.88 o 2 16 2 27.87 29.31 1.06 o 4 16 2 10.22 12.71 2.61 o 1 17 2 104.04 97.36 2.53 o 3 17 2 61.83 63.19 1.71 o 0 18 2 85.48 92.46 4.65 o 2 18 2 72.10 91.19 3.75 o 1 1 3 23.21 24.02 0.38 o 3 1 3 6.99 7.01 0.31 o 5 1 3 9.12 9.86 0.46 o 7 1 3 8.32 10.24 0.94 o 0 2 3 795.80 808.48 10.52 o 2 2 3 477.04 491.33 3.34 o 4 2 3 178.47 176.77 1.53 o 6 2 3 70.59 65.24 1.24 o 1 3 3 4316.19 4776.54 36.32 o 3 3 3 1515.84 1506.93 9.85 o 5 3 3 274.52 252.91 2.56 o 7 3 3 35.14 34.73 1.21 o 0 4 3 3320.39 3730.83 32.58 o 2 4 3 2067.89 2277.90 14.72 o 4 4 3 744.66 789.23 6.35 o 6 4 3 252.49 253.53 2.90 o 1 5 3 519.24 600.55 4.26 o 3 5 3 192.29 211.78 1.86 o 5 5 3 45.87 46.98 0.93 o 7 5 3 10.82 10.03 0.89 o 0 6 3 1.33 2.47 0.52 o 2 6 3 0.59 0.40 0.20 o 4 6 3 0.03 -0.32 0.32 o 6 6 3 0.28 -0.22 0.50 o 1 7 3 69.06 65.96 0.69 o 3 7 3 18.56 21.04 0.53 o 5 7 3 1.12 1.69 0.43 o 7 7 3 0.44 1.64 0.91 o 0 8 3 90.33 92.14 1.61 o 2 8 3 54.86 53.44 0.74 o 4 8 3 14.84 13.92 0.56 o 6 8 3 5.48 5.08 0.62 o 1 9 3 949.72 868.04 6.17 o 3 9 3 427.38 400.26 3.51 o 5 9 3 113.67 109.47 1.47 o 0 10 3 4683.71 4699.16 45.52 o 2 10 3 3553.63 3515.17 25.22 o 4 10 3 1788.48 1774.11 13.89 o 6 10 3 731.76 743.30 6.89 o 1 11 3 1992.35 1984.12 17.90 o 3 11 3 1201.65 1216.89 9.69 o 5 11 3 531.44 536.87 5.15 o 0 12 3 146.25 136.43 1.94 o 2 12 3 112.87 110.62 1.50 o 4 12 3 57.87 57.02 1.15 o 1 13 3 75.27 74.31 1.19 o 3 13 3 41.52 42.72 1.03 o 5 13 3 14.80 15.64 0.89 o 0 14 3 22.46 21.39 1.21 o 2 14 3 16.80 17.23 0.74 o 4 14 3 7.56 8.47 0.82 o 1 15 3 329.06 329.83 3.95 o 3 15 3 185.71 188.94 3.69 o 0 16 3 100.84 100.27 2.91 o 2 16 3 81.43 88.00 1.81 o 1 17 3 59.76 72.21 1.91 o 0 0 4 256.29 237.66 3.31 o 2 0 4 174.77 164.16 1.75 o 4 0 4 76.13 74.91 1.23 o 6 0 4 31.69 30.96 1.71 o 1 1 4 32.35 25.50 0.39 o 3 1 4 12.62 13.78 0.42 o 5 1 4 3.46 2.83 0.57 o 7 1 4 1.20 0.96 0.79 o 0 2 4 579.53 571.21 5.57 o 2 2 4 374.23 378.96 2.82 o 4 2 4 132.93 136.53 1.49 o 6 2 4 39.92 37.43 1.12 o 1 3 4 1614.75 1792.65 11.19 o 3 3 4 807.01 868.82 6.17 o 5 3 4 306.96 308.06 3.05 o 7 3 4 110.51 111.69 2.31 o 0 4 4 612.18 700.87 6.38 o 2 4 4 417.47 449.61 3.53 o 4 4 4 167.70 158.37 1.67 o 6 4 4 56.77 52.31 1.18 o 1 5 4 31.51 27.88 0.49 o 3 5 4 13.65 12.91 0.46 o 5 5 4 2.50 3.03 0.49 o 7 5 4 0.22 0.55 1.05 o 0 6 4 117.52 110.75 1.30 o 2 6 4 77.19 73.08 0.83 o 4 6 4 24.97 25.72 0.68 o 6 6 4 5.51 6.13 0.68 o 1 7 4 149.72 145.84 1.41 o 3 7 4 73.85 70.36 0.93 o 5 7 4 24.02 22.83 0.79 o 0 8 4 148.52 157.28 2.27 o 2 8 4 109.21 113.85 1.23 o 4 8 4 51.79 49.08 0.92 o 6 8 4 20.41 19.53 0.88 o 1 9 4 169.84 159.32 1.57 o 3 9 4 129.55 128.06 1.50 o 5 9 4 82.80 86.53 1.43 o 0 10 4 202.83 170.27 2.50 o 2 10 4 160.99 141.38 1.60 o 4 10 4 89.41 85.44 1.27 o 6 10 4 40.04 41.43 1.82 o 1 11 4 713.51 701.92 5.85 o 3 11 4 472.03 473.74 4.53 o 5 11 4 236.05 258.60 3.35 o 0 12 4 299.35 293.92 3.92 o 2 12 4 248.15 247.84 2.88 o 4 12 4 150.46 157.71 2.09 o 1 13 4 27.39 27.66 0.87 o 3 13 4 15.07 16.40 0.78 o 0 14 4 223.03 224.76 3.90 o 2 14 4 181.87 184.63 3.68 o 4 14 4 104.07 111.42 3.27 o 1 15 4 36.70 35.88 1.26 o 3 15 4 24.14 25.26 1.13 o 0 16 4 5.44 5.90 1.46 o 2 16 4 4.21 4.01 0.86 o 1 17 4 61.83 77.19 2.82 o 1 1 5 154.43 159.39 1.30 o 3 1 5 71.15 60.65 0.83 o 5 1 5 45.65 39.60 1.00 o 0 2 5 858.75 839.95 9.89 o 2 2 5 592.26 588.15 4.51 o 4 2 5 237.57 236.08 2.49 o 6 2 5 75.33 78.69 1.64 o 1 3 5 220.70 215.01 1.67 o 3 3 5 107.71 105.40 1.26 o 5 3 5 37.90 40.98 0.96 o 0 4 5 342.18 355.91 4.97 o 2 4 5 242.79 252.35 2.06 o 4 4 5 104.06 109.81 1.93 o 6 4 5 35.79 37.83 1.23 o 1 5 5 571.91 588.79 4.30 o 3 5 5 217.63 221.90 2.15 o 5 5 5 35.10 36.14 0.93 o 0 6 5 59.40 62.21 1.28 o 2 6 5 44.55 47.50 0.76 o 4 6 5 22.43 22.14 0.70 o 6 6 5 9.62 10.18 1.26 o 1 7 5 134.24 167.77 1.78 o 3 7 5 49.12 57.29 0.88 o 5 7 5 7.41 8.04 0.65 o 0 8 5 923.47 873.33 10.44 o 2 8 5 685.63 659.14 5.95 o 4 8 5 315.59 315.70 3.21 o 6 8 5 109.46 115.51 2.33 o 1 9 5 20.01 19.99 0.68 o 3 9 5 7.79 8.78 0.65 o 5 9 5 2.23 1.13 0.62 o 0 10 5 354.32 333.07 4.31 o 2 10 5 281.52 267.58 2.79 o 4 10 5 153.09 159.52 2.07 o 1 11 5 79.07 81.21 1.28 o 3 11 5 34.47 36.55 1.06 o 5 11 5 7.10 7.61 1.27 o 0 12 5 70.06 73.37 1.93 o 2 12 5 54.95 55.91 1.34 o 4 12 5 28.37 27.13 1.05 o 1 13 5 920.20 943.95 8.34 o 3 13 5 589.31 615.57 7.00 o 0 14 5 21.38 19.29 1.36 o 2 14 5 15.30 15.70 0.92 o 1 15 5 105.58 100.71 1.99 o 0 16 5 25.53 27.46 2.09 o 0 0 6 5833.42 5382.33 66.31 o 2 0 6 4376.80 4242.38 40.34 o 4 0 6 2142.59 2128.03 27.02 o 6 0 6 849.20 827.38 11.45 o 1 1 6 516.63 542.96 3.97 o 3 1 6 321.40 340.45 3.09 o 5 1 6 153.39 156.36 2.15 o 0 2 6 408.93 386.34 4.16 o 2 2 6 296.61 285.20 2.46 o 4 2 6 134.34 130.29 1.70 o 6 2 6 48.75 44.78 1.38 o 1 3 6 37.06 34.06 0.64 o 3 3 6 21.82 22.32 0.72 o 5 3 6 9.81 10.04 0.73 o 0 4 6 349.62 330.00 4.17 o 2 4 6 248.46 247.50 2.21 o 4 4 6 102.90 95.73 1.54 o 6 4 6 31.63 30.28 1.99 o 1 5 6 37.23 35.15 0.71 o 3 5 6 20.95 20.21 0.67 o 5 5 6 7.84 7.72 0.70 o 0 6 6 608.55 467.27 7.10 o 2 6 6 458.84 366.81 3.55 o 4 6 6 221.04 192.28 2.09 o 1 7 6 33.93 42.08 0.82 o 3 7 6 15.98 16.23 0.90 o 5 7 6 5.94 4.54 0.64 o 0 8 6 596.15 535.11 6.49 o 2 8 6 450.69 417.06 4.02 o 4 8 6 214.53 207.12 2.64 o 1 9 6 265.26 240.81 2.71 o 3 9 6 176.07 170.68 2.11 o 5 9 6 86.33 87.25 2.10 o 0 10 6 22.54 22.00 1.02 o 2 10 6 14.63 14.17 0.69 o 4 10 6 4.76 5.46 0.74 o 1 11 6 14.17 15.41 1.06 o 3 11 6 10.43 9.16 0.86 o 0 12 6 1.56 -0.32 0.82 o 2 12 6 0.21 0.05 0.57 o 1 13 6 108.62 108.77 1.67 o 3 13 6 70.82 73.29 2.71 o 0 14 6 84.26 97.04 3.12 o 2 14 6 80.47 92.21 2.51 o 1 1 7 716.00 672.86 6.16 o 3 1 7 466.18 455.80 4.04 o 5 1 7 228.12 234.43 2.95 o 0 2 7 454.44 440.76 7.50 o 2 2 7 360.83 352.21 3.01 o 4 2 7 197.67 197.82 2.54 o 1 3 7 110.68 104.94 1.41 o 3 3 7 63.19 63.92 1.08 o 5 3 7 24.23 24.35 1.05 o 0 4 7 122.95 120.08 2.34 o 2 4 7 94.59 91.81 1.24 o 4 4 7 47.52 47.74 1.10 o 1 5 7 1.42 1.26 0.44 o 3 5 7 1.08 0.83 0.49 o 5 5 7 1.34 0.43 0.78 o 0 6 7 151.30 142.22 2.33 o 2 6 7 119.97 118.11 1.74 o 4 6 7 64.38 63.40 1.26 o 1 7 7 421.72 328.63 3.58 o 3 7 7 276.32 242.89 3.40 o 5 7 7 132.35 121.22 5.05 o 0 8 7 67.20 54.06 1.52 o 2 8 7 56.10 52.00 1.19 o 4 8 7 34.11 34.74 1.29 o 1 9 7 26.56 23.38 0.93 o 3 9 7 14.92 15.67 0.87 o 0 10 7 73.50 74.91 3.73 o 2 10 7 55.95 55.70 1.30 o 1 11 7 6.20 7.10 0.69 o 3 11 7 3.42 2.72 1.37 o 0 12 7 25.59 25.32 1.57 o 2 12 7 23.91 24.82 1.20 o 1 13 7 102.99 123.28 3.66 o 0 0 8 68.53 59.63 2.92 o 2 0 8 64.07 62.49 2.12 o 4 0 8 50.90 56.42 2.01 o 1 1 8 17.44 17.82 0.78 o 3 1 8 13.79 15.06 0.75 o 0 2 8 743.52 761.10 10.23 o 2 2 8 567.22 609.93 5.59 o 4 2 8 269.79 298.51 3.53 o 1 3 8 149.57 151.82 2.03 o 3 3 8 108.07 117.24 3.06 o 0 4 8 278.93 251.70 4.14 o 2 4 8 205.54 189.81 2.44 o 4 4 8 87.87 82.99 1.64 o 1 5 8 15.46 18.24 0.83 o 3 5 8 7.00 7.49 0.82 o 0 6 8 31.48 30.65 1.41 o 2 6 8 24.37 24.94 0.97 o 4 6 8 13.81 14.95 1.64 o 1 7 8 217.32 225.96 2.80 o 3 7 8 148.63 158.45 2.56 o 0 8 8 113.50 115.69 2.53 o 2 8 8 83.79 88.21 1.63 o 1 9 8 41.90 44.48 1.24 o 3 9 8 36.17 34.20 3.15 o 0 10 8 137.83 134.75 3.01 o 2 10 8 101.12 101.53 2.66 o 1 11 8 51.62 46.09 1.88 o 1 1 9 34.81 35.60 1.20 o 3 1 9 26.65 26.31 1.68 o 0 2 9 156.99 176.12 5.29 o 2 2 9 132.24 149.64 2.71 o 1 3 9 31.02 29.53 1.15 o 3 3 9 16.01 16.24 1.72 o 0 4 9 95.59 113.36 5.87 o 2 4 9 84.89 96.63 2.16 o 1 5 9 113.73 134.23 3.10 o 0 6 9 6.63 7.05 1.12 o 2 6 9 6.08 7.93 1.53 o 1 7 9 24.25 28.48 1.63 o