#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:16:00 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180991 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/71/2207177.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207177_Fobs loop_ _publ_author_name 'Wu, Yong-Fei' 'Li, Fen-Fang' 'Jin, Long-Fei' _publ_section_title ; 5-Methyl L-glutamate ; _journal_coeditor_code CI6645 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3752 _journal_page_last o3753 _journal_volume 61 _journal_year 2005 _space_group_IT_number 5 _symmetry_space_group_name_Hall 'C 2y' _symmetry_space_group_name_H-M 'C 1 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.995 _cell_angle_gamma 90.000 _cell_length_a 10.2865 _cell_length_b 4.6163 _cell_length_c 17.1114 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.7829 _cod_data_source_file ci6645Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 050727AM in C2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 129.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 313.26 416.24 14.61 o 4 0 0 678.38 761.94 26.68 o 6 0 0 1655.49 1765.21 60.91 o 8 0 0 0.13 -0.74 0.76 o 10 0 0 9.40 7.65 1.90 o 12 0 0 1.41 0.29 1.41 o 1 1 0 2489.57 2769.85 45.66 o 3 1 0 878.09 985.15 15.84 o 5 1 0 1553.13 1790.39 33.83 o 7 1 0 35.79 43.15 2.13 o 9 1 0 286.33 264.23 7.99 o 11 1 0 64.09 62.55 3.21 o 0 2 0 2191.52 2390.61 46.23 o 2 2 0 134.16 126.49 2.51 o 4 2 0 297.37 291.90 5.17 o 6 2 0 206.51 211.51 4.05 o 8 2 0 31.93 29.10 2.00 o 10 2 0 27.15 30.39 2.24 o 1 3 0 62.15 69.21 1.73 o 3 3 0 23.62 23.81 0.99 o 5 3 0 56.24 74.36 3.02 o 7 3 0 23.70 30.45 2.13 o 9 3 0 180.65 167.94 6.12 o 0 4 0 41.37 58.21 3.86 o 2 4 0 164.59 172.79 4.45 o 4 4 0 88.64 79.91 2.74 o 6 4 0 69.37 72.70 2.62 o 8 4 0 10.80 13.54 2.64 o 1 5 0 28.07 37.75 2.74 o 3 5 0 2.49 4.30 1.52 o 5 5 0 82.44 94.25 4.16 o -12 0 1 1.06 2.97 1.62 o -10 0 1 415.98 383.07 15.69 o -8 0 1 328.40 325.01 13.14 o -6 0 1 10.80 11.43 1.52 o -4 0 1 306.84 277.85 6.69 o -2 0 1 146.57 181.66 5.74 o 0 0 1 1311.52 -0.02 0.04 o 2 0 1 399.44 585.82 20.48 o 4 0 1 42.86 63.02 3.19 o 6 0 1 48.45 46.75 2.97 o 8 0 1 35.70 40.11 3.04 o 10 0 1 16.57 21.20 2.64 o 12 0 1 100.26 90.47 5.84 o -11 1 1 9.93 10.16 1.54 o -9 1 1 17.47 13.58 1.54 o -7 1 1 166.00 143.05 3.46 o -5 1 1 744.01 816.92 13.37 o -3 1 1 1359.35 1655.23 29.99 o -1 1 1 163.88 161.55 2.85 o 1 1 1 1197.06 1279.73 30.50 o 3 1 1 1195.61 1316.30 21.15 o 5 1 1 116.55 156.95 3.54 o 7 1 1 325.51 302.74 8.54 o 9 1 1 582.84 574.46 15.42 o 11 1 1 47.12 46.25 2.72 o -12 2 1 55.37 55.40 3.19 o -10 2 1 83.23 82.57 3.67 o -8 2 1 32.39 23.81 1.84 o -6 2 1 152.62 153.38 3.08 o -4 2 1 760.59 811.48 25.43 o -2 2 1 554.10 639.77 10.78 o 0 2 1 1454.05 1578.97 23.77 o 2 2 1 669.11 833.03 13.96 o 4 2 1 758.20 856.04 12.97 o 6 2 1 39.71 43.59 1.65 o 8 2 1 69.14 74.87 3.12 o 10 2 1 34.65 32.92 2.28 o -11 3 1 5.60 8.88 2.42 o -9 3 1 132.51 125.73 6.73 o -7 3 1 20.19 24.51 1.48 o -5 3 1 124.45 123.79 2.81 o -3 3 1 2.98 5.57 0.55 o -1 3 1 151.40 166.46 3.02 o 1 3 1 102.07 101.12 2.30 o 3 3 1 354.09 331.69 6.12 o 5 3 1 154.41 152.35 3.31 o 7 3 1 1.82 2.45 1.03 o 9 3 1 93.02 88.47 4.13 o -8 4 1 3.24 4.01 2.00 o -6 4 1 13.93 16.39 1.37 o -4 4 1 19.58 16.85 1.71 o -2 4 1 75.77 64.91 2.91 o 0 4 1 22.66 26.51 1.56 o 2 4 1 128.75 166.86 4.36 o 4 4 1 457.64 467.70 9.95 o 6 4 1 5.19 6.83 1.48 o 8 4 1 10.45 10.57 2.61 o -5 5 1 60.76 58.75 3.31 o -3 5 1 39.11 50.13 3.04 o -1 5 1 12.03 13.05 1.94 o 1 5 1 32.36 31.95 2.49 o 3 5 1 17.80 19.63 2.19 o 5 5 1 26.74 25.77 2.40 o -12 0 2 16.08 17.71 2.93 o -10 0 2 345.58 314.32 13.43 o -8 0 2 372.24 381.72 15.10 o -6 0 2 221.87 234.01 5.95 o -4 0 2 1353.10 1435.37 32.58 o -2 0 2 3346.99 3691.14 110.64 o 2 0 2 159.07 265.87 9.62 o 4 0 2 3669.76 4085.57 138.12 o 6 0 2 0.01 -0.21 0.63 o 8 0 2 170.43 130.59 6.35 o 10 0 2 163.57 143.01 7.30 o 12 0 2 57.99 63.69 4.81 o -11 1 2 7.82 5.63 1.33 o -9 1 2 2.89 1.83 0.86 o -7 1 2 284.06 289.73 5.21 o -5 1 2 224.98 272.50 5.38 o -3 1 2 894.64 478.31 14.91 o -1 1 2 16807.79 18182.89 292.07 o 1 1 2 4135.49 4652.46 77.57 o 3 1 2 1463.21 1793.38 28.68 o 5 1 2 239.41 297.53 8.06 o 7 1 2 174.47 186.43 5.74 o 9 1 2 90.94 81.70 3.44 o 11 1 2 24.42 24.89 2.13 o -12 2 2 81.71 86.02 4.13 o -10 2 2 53.38 43.21 2.59 o -8 2 2 97.91 80.44 3.35 o -6 2 2 258.75 283.42 5.82 o -4 2 2 112.50 102.47 2.47 o -2 2 2 296.30 328.13 5.76 o 0 2 2 565.43 608.18 9.38 o 2 2 2 21.74 30.41 0.93 o 4 2 2 129.09 134.61 2.47 o 6 2 2 116.05 107.83 2.83 o 8 2 2 95.04 82.50 3.33 o 10 2 2 12.11 10.95 1.56 o -11 3 2 87.95 76.58 5.34 o -9 3 2 11.76 10.06 2.09 o -7 3 2 213.56 211.23 3.94 o -5 3 2 96.10 109.56 2.55 o -3 3 2 203.53 227.81 4.55 o -1 3 2 579.78 656.22 10.33 o 1 3 2 273.92 325.35 5.97 o 3 3 2 137.10 136.51 2.99 o 5 3 2 102.77 101.50 2.47 o 7 3 2 24.00 30.41 2.23 o 9 3 2 18.93 23.60 2.34 o -6 4 2 212.51 240.99 6.77 o -4 4 2 1.06 0.40 1.06 o -2 4 2 37.32 32.08 2.13 o 0 4 2 4.91 3.04 0.91 o 2 4 2 135.43 114.52 3.40 o 4 4 2 161.10 185.78 4.75 o 6 4 2 99.86 98.63 4.07 o 8 4 2 2.09 3.73 2.24 o -5 5 2 3.43 3.37 1.58 o -3 5 2 70.67 63.39 3.37 o -1 5 2 107.95 107.77 4.34 o 1 5 2 27.70 31.66 2.59 o 3 5 2 30.32 34.86 2.61 o 5 5 2 16.68 18.88 3.37 o -12 0 3 31.19 36.70 3.92 o -10 0 3 48.38 56.62 4.24 o -8 0 3 721.96 716.28 26.47 o -6 0 3 336.17 415.57 10.08 o -4 0 3 233.62 334.75 10.63 o -2 0 3 6.74 18.69 1.03 o 0 0 3 101.77 53.82 2.49 o 2 0 3 454.59 513.89 17.90 o 4 0 3 1123.27 1465.53 50.38 o 6 0 3 273.06 293.73 11.54 o 8 0 3 1242.99 1305.54 46.08 o 10 0 3 190.22 191.98 9.05 o 12 0 3 61.87 64.60 4.74 o -11 1 3 76.65 77.97 3.75 o -9 1 3 192.32 168.23 5.76 o -7 1 3 73.09 74.04 1.81 o -5 1 3 346.95 356.83 6.92 o -3 1 3 3398.89 3588.43 76.18 o -1 1 3 542.10 542.48 9.09 o 1 1 3 596.28 618.34 10.52 o 3 1 3 3773.27 4461.20 83.18 o 5 1 3 16.37 14.30 1.08 o 7 1 3 25.74 22.25 1.56 o 9 1 3 27.81 30.98 2.03 o 11 1 3 67.77 67.91 3.35 o -12 2 3 80.54 85.54 4.11 o -10 2 3 79.82 84.19 3.75 o -8 2 3 32.75 27.86 1.48 o -6 2 3 333.01 353.92 7.09 o -4 2 3 78.72 101.23 2.45 o -2 2 3 329.02 295.21 5.21 o 0 2 3 342.30 404.26 8.04 o 2 2 3 192.77 190.96 4.30 o 4 2 3 1081.27 1132.46 17.00 o 6 2 3 254.08 244.85 5.97 o 8 2 3 62.02 67.28 2.95 o 10 2 3 62.09 52.11 4.15 o -11 3 3 75.04 61.98 4.72 o -9 3 3 30.19 22.82 2.72 o -5 3 3 177.18 181.75 3.73 o -3 3 3 50.22 48.67 1.71 o -1 3 3 278.67 257.56 4.43 o 1 3 3 378.78 383.58 6.94 o 3 3 3 654.17 629.39 13.33 o 5 3 3 5.66 9.62 0.84 o 7 3 3 28.44 37.24 2.45 o 9 3 3 0.04 0.86 1.22 o -6 4 3 171.64 161.04 5.06 o -4 4 3 50.46 62.89 2.83 o -2 4 3 96.71 109.54 3.90 o 0 4 3 68.12 77.69 2.64 o 2 4 3 329.96 311.09 7.02 o 4 4 3 55.59 67.36 2.55 o 6 4 3 59.99 60.65 4.62 o 8 4 3 78.60 78.05 3.90 o -5 5 3 31.00 33.89 2.59 o -3 5 3 128.54 127.34 4.79 o -1 5 3 74.89 64.85 3.29 o 1 5 3 25.17 31.85 2.59 o 3 5 3 144.62 145.71 5.25 o 5 5 3 8.64 9.93 2.80 o -12 0 4 0.06 2.02 1.71 o -10 0 4 54.76 55.87 4.16 o -8 0 4 238.67 244.01 6.52 o -6 0 4 228.15 270.66 6.87 o -4 0 4 442.36 483.01 15.10 o -2 0 4 7426.96 6984.27 209.00 o 2 0 4 109.54 125.97 5.00 o 4 0 4 1414.77 1559.99 53.52 o 6 0 4 126.48 107.96 5.21 o 8 0 4 65.27 63.31 4.03 o 10 0 4 31.19 25.65 2.81 o -11 1 4 24.19 26.19 2.28 o -9 1 4 427.93 428.12 12.10 o -7 1 4 477.51 432.57 7.53 o -5 1 4 386.02 428.18 8.25 o -3 1 4 439.31 391.86 8.79 o -1 1 4 2758.50 3015.54 48.70 o 1 1 4 355.31 363.06 5.55 o 3 1 4 909.58 1014.17 17.27 o 5 1 4 217.97 231.35 6.50 o 7 1 4 66.33 68.63 2.85 o 9 1 4 26.93 18.41 1.71 o 11 1 4 1.15 0.27 1.03 o -12 2 4 87.37 81.01 4.01 o -10 2 4 11.88 12.53 1.65 o -8 2 4 50.42 44.90 1.86 o -6 2 4 147.90 130.18 3.33 o -4 2 4 72.92 93.64 2.32 o -2 2 4 448.85 468.84 8.37 o 0 2 4 335.67 391.78 6.87 o 2 2 4 428.70 454.92 9.41 o 4 2 4 220.52 230.34 3.90 o 6 2 4 153.35 171.65 4.51 o 8 2 4 146.23 138.83 4.11 o 10 2 4 8.37 3.94 1.94 o -11 3 4 1.02 -1.43 1.48 o -9 3 4 64.29 58.21 2.97 o -7 3 4 151.72 179.53 4.26 o -5 3 4 235.81 218.68 4.96 o -3 3 4 8.81 12.76 0.89 o -1 3 4 172.37 178.16 3.65 o 1 3 4 188.20 137.33 3.23 o 3 3 4 167.13 165.81 4.45 o 5 3 4 1.60 2.53 0.76 o 7 3 4 7.22 8.73 1.48 o 9 3 4 16.11 15.78 2.17 o -8 4 4 83.53 73.45 4.87 o -6 4 4 41.32 40.70 2.38 o -4 4 4 57.08 53.14 2.59 o -2 4 4 163.50 160.05 4.98 o 0 4 4 23.70 27.73 1.64 o 2 4 4 6.50 12.72 1.26 o 4 4 4 101.48 94.27 3.06 o 6 4 4 31.18 36.93 2.49 o 8 4 4 56.46 55.00 3.35 o -5 5 4 34.82 38.05 2.74 o -3 5 4 107.62 117.83 4.93 o -1 5 4 27.68 30.01 2.47 o 1 5 4 1.02 0.25 1.41 o 3 5 4 41.42 41.25 2.28 o 5 5 4 51.44 55.49 3.42 o -12 0 5 5.05 8.10 2.21 o -10 0 5 0.26 0.30 1.26 o -8 0 5 49.96 49.88 2.09 o -6 0 5 836.94 766.05 23.77 o -4 0 5 1790.35 1745.32 52.87 o -2 0 5 1050.51 983.61 29.97 o 0 0 5 1391.42 1267.54 44.79 o 2 0 5 1592.90 1693.95 57.59 o 4 0 5 224.65 207.81 8.20 o 6 0 5 382.19 394.29 15.00 o 8 0 5 27.68 33.55 2.83 o 10 0 5 42.76 40.09 3.42 o -11 1 5 47.55 49.48 2.97 o -9 1 5 189.62 210.30 6.83 o -7 1 5 202.98 181.54 4.01 o -5 1 5 542.75 612.18 11.58 o -3 1 5 8.63 14.26 0.82 o -1 1 5 136.66 161.59 2.99 o 1 1 5 2645.59 2793.25 40.81 o 3 1 5 488.82 554.04 9.70 o 5 1 5 161.27 187.06 5.46 o 7 1 5 563.10 569.71 14.95 o 9 1 5 131.09 120.04 4.41 o 11 1 5 4.73 9.68 1.60 o -12 2 5 73.14 78.26 3.92 o -10 2 5 54.13 41.57 2.61 o -8 2 5 303.33 297.04 6.28 o -6 2 5 96.12 105.30 4.49 o -4 2 5 286.25 288.90 5.86 o -2 2 5 605.51 608.98 9.32 o 0 2 5 770.20 887.91 14.89 o 2 2 5 945.11 1002.42 16.77 o 4 2 5 208.49 201.28 3.46 o 6 2 5 31.01 36.11 1.69 o 8 2 5 34.47 31.46 2.45 o 10 2 5 25.31 21.62 2.32 o -11 3 5 14.52 11.79 2.53 o -9 3 5 122.45 120.55 4.58 o -7 3 5 44.79 52.03 2.34 o -5 3 5 170.31 165.85 4.75 o -3 3 5 118.76 98.95 3.25 o -1 3 5 30.49 25.67 1.06 o 1 3 5 268.26 249.62 4.85 o 3 3 5 356.17 309.44 7.00 o 5 3 5 48.82 46.56 2.49 o 7 3 5 70.07 68.39 3.42 o 9 3 5 42.49 45.45 3.18 o -8 4 5 66.19 69.28 4.77 o -6 4 5 7.85 10.16 1.52 o -4 4 5 82.13 94.82 3.58 o -2 4 5 49.44 45.00 2.38 o 0 4 5 1.59 2.19 0.87 o 2 4 5 285.46 293.80 5.86 o 4 4 5 59.75 61.66 2.42 o 6 4 5 56.80 60.97 3.19 o 8 4 5 7.36 9.01 1.81 o -5 5 5 21.07 14.62 1.94 o -3 5 5 28.30 31.87 2.55 o -1 5 5 11.82 17.06 2.05 o 1 5 5 70.39 67.00 2.87 o 3 5 5 20.41 23.52 1.88 o 5 5 5 39.85 33.97 4.03 o -12 0 6 37.90 40.37 4.24 o -10 0 6 83.82 89.25 5.69 o -8 0 6 1028.81 1056.64 24.86 o -6 0 6 358.97 409.05 13.22 o -4 0 6 563.53 698.36 21.72 o -2 0 6 364.19 302.13 9.74 o 0 0 6 2747.21 2776.40 69.66 o 2 0 6 428.67 427.57 15.21 o 4 0 6 16.48 29.42 2.13 o 6 0 6 69.62 64.74 3.77 o 8 0 6 92.63 99.06 5.42 o 10 0 6 2.33 3.58 1.62 o -11 1 6 16.64 20.06 2.11 o -9 1 6 122.22 122.99 3.44 o -7 1 6 104.90 113.46 2.81 o -5 1 6 282.06 298.27 7.06 o -3 1 6 1280.10 1353.86 29.23 o -1 1 6 290.09 313.37 5.48 o 1 1 6 2931.77 3051.77 44.60 o 3 1 6 563.20 563.02 9.89 o 5 1 6 28.90 19.17 1.16 o 7 1 6 695.86 690.24 17.90 o 9 1 6 14.70 16.72 1.73 o 11 1 6 34.24 35.68 2.62 o -12 2 6 18.72 20.50 2.24 o -10 2 6 20.73 21.60 2.05 o -8 2 6 757.49 708.50 13.69 o -6 2 6 203.30 193.10 5.04 o -4 2 6 220.45 247.38 5.15 o -2 2 6 1940.25 2141.06 35.09 o 0 2 6 49.31 50.15 1.39 o 2 2 6 40.24 39.40 1.03 o 4 2 6 105.94 98.30 2.32 o 6 2 6 91.60 82.95 3.61 o 8 2 6 24.98 28.64 2.55 o 10 2 6 1.98 1.79 1.35 o -11 3 6 11.82 14.03 2.68 o -9 3 6 64.98 72.57 4.39 o -7 3 6 21.50 18.69 1.52 o -5 3 6 4.08 4.47 0.97 o -3 3 6 149.56 136.45 4.09 o -1 3 6 44.96 47.75 1.52 o 1 3 6 102.99 102.33 2.49 o 3 3 6 301.10 274.39 5.32 o 5 3 6 128.42 98.38 3.97 o 7 3 6 35.23 40.96 2.80 o 9 3 6 9.91 13.16 2.15 o -8 4 6 9.83 12.42 1.60 o -6 4 6 61.38 61.46 2.89 o -4 4 6 8.00 8.48 1.39 o -2 4 6 78.57 78.47 3.19 o 0 4 6 12.37 11.05 0.99 o 2 4 6 161.88 147.56 4.07 o 4 4 6 44.62 46.92 2.19 o 6 4 6 27.31 29.38 2.40 o -5 5 6 4.08 5.29 1.48 o -3 5 6 59.48 47.89 2.95 o -1 5 6 3.04 3.69 1.33 o 1 5 6 21.16 19.04 1.79 o 3 5 6 53.26 49.85 2.53 o -12 0 7 17.03 14.49 2.76 o -10 0 7 60.35 59.98 4.53 o -8 0 7 112.92 111.96 3.63 o -6 0 7 1081.16 1078.72 33.30 o -4 0 7 995.88 950.14 29.33 o -2 0 7 5.29 5.90 0.59 o 0 0 7 1283.63 1262.50 32.06 o 2 0 7 552.02 519.28 12.06 o 4 0 7 372.30 417.07 15.40 o 6 0 7 1292.38 1371.62 47.94 o 8 0 7 35.16 39.96 3.27 o 10 0 7 4.66 4.83 1.75 o -11 1 7 5.79 6.10 1.48 o -9 1 7 266.62 251.64 5.55 o -7 1 7 85.74 96.31 2.57 o -5 1 7 352.37 343.97 8.08 o -3 1 7 205.52 193.64 4.81 o -1 1 7 277.61 314.53 4.98 o 1 1 7 2294.12 2371.38 39.90 o 3 1 7 99.73 98.42 2.64 o 5 1 7 374.72 388.81 8.82 o 7 1 7 271.98 281.29 6.96 o 9 1 7 24.79 25.90 2.05 o -12 2 7 44.43 39.50 2.95 o -10 2 7 9.82 13.58 1.73 o -8 2 7 28.46 27.20 1.39 o -6 2 7 191.66 171.82 3.94 o -4 2 7 226.39 195.65 4.26 o -2 2 7 34.49 36.49 1.20 o 0 2 7 35.72 43.13 1.29 o 2 2 7 55.27 54.12 1.50 o 4 2 7 133.38 130.25 3.39 o 6 2 7 91.55 80.58 3.59 o 8 2 7 52.00 53.50 3.14 o 10 2 7 49.61 51.92 3.94 o -11 3 7 23.70 24.99 3.33 o -9 3 7 3.68 2.42 1.79 o -7 3 7 27.35 32.88 2.81 o -5 3 7 125.94 119.15 3.80 o -3 3 7 58.90 50.59 2.23 o -1 3 7 65.56 60.95 1.79 o 1 3 7 377.32 373.81 6.90 o 3 3 7 229.11 216.44 4.43 o 5 3 7 115.24 101.29 4.15 o 7 3 7 17.59 20.52 2.19 o 9 3 7 4.83 7.72 1.96 o -8 4 7 16.85 13.60 2.61 o -6 4 7 46.22 40.43 2.40 o -4 4 7 96.55 93.87 3.58 o -2 4 7 83.66 68.84 2.17 o 0 4 7 261.57 254.57 6.07 o 2 4 7 15.41 16.47 1.18 o 4 4 7 1.04 2.93 0.97 o 6 4 7 40.88 42.10 2.89 o -5 5 7 13.17 16.58 2.05 o -3 5 7 33.65 25.81 2.26 o -1 5 7 22.22 18.85 1.81 o 1 5 7 12.02 13.64 1.64 o 3 5 7 15.44 16.09 2.13 o -12 0 8 0.32 -0.17 1.50 o -10 0 8 55.93 53.71 4.32 o -8 0 8 1.52 0.63 0.87 o -6 0 8 2.09 2.72 0.84 o -4 0 8 618.97 585.13 18.52 o -2 0 8 80.74 66.09 2.13 o 0 0 8 859.55 918.59 23.60 o 2 0 8 331.04 280.00 6.79 o 4 0 8 1471.74 1463.40 37.50 o 6 0 8 642.47 637.85 23.43 o 8 0 8 42.03 38.76 3.23 o 10 0 8 83.64 82.54 5.36 o -11 1 8 0.17 0.97 1.08 o -9 1 8 786.45 753.99 14.64 o 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