#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2207305.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207305_Fobs loop_ _publ_author_name 'Hu, Mao-Lin' 'Cai, Xiao-Qing' 'Jin, Zhi-Min' _publ_section_title ; Diaquadibenzimidazolebis(5-fluoro-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-1-acetato)cadmium(II) ; _journal_coeditor_code LH6530 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2411 _journal_page_last m2413 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 88.287 _cell_angle_beta 89.114 _cell_angle_gamma 68.041 _cell_length_a 7.5216 _cell_length_b 8.3323 _cell_length_c 12.2228 _exptl_crystal_F_000 382.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file lh6530Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' m27m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2819.89 2507.27 58.43 o 2 0 0 4133.45 4000.79 56.60 o 3 0 0 670.27 661.71 9.95 o 4 0 0 2.28 5.02 2.21 o 5 0 0 337.66 343.59 6.74 o 6 0 0 770.50 770.05 16.33 o 7 0 0 276.03 274.39 12.48 o 8 0 0 48.74 54.73 6.28 o -7 1 0 185.15 189.13 7.22 o -6 1 0 95.39 93.21 5.40 o -5 1 0 5.09 5.13 1.80 o -4 1 0 240.21 237.84 4.95 o -3 1 0 4490.62 4392.58 57.21 o -2 1 0 1645.28 1638.41 21.96 o -1 1 0 4599.25 3900.90 64.60 o 0 1 0 3308.08 2773.61 47.22 o 1 1 0 422.62 430.60 10.41 o 2 1 0 4845.78 4372.67 91.80 o 3 1 0 1.64 2.75 1.18 o 4 1 0 105.83 89.48 2.68 o 5 1 0 1282.70 1371.68 19.95 o 6 1 0 356.14 363.09 9.06 o 7 1 0 274.87 271.00 12.27 o 8 1 0 132.99 145.77 9.11 o -7 2 0 58.25 60.99 4.31 o -6 2 0 238.08 246.32 8.26 o -5 2 0 173.91 179.35 6.33 o -4 2 0 438.40 446.45 11.36 o -3 2 0 577.89 605.31 9.59 o -2 2 0 723.57 728.12 10.78 o -1 2 0 3061.87 3078.23 40.17 o 0 2 0 484.83 476.62 7.15 o 1 2 0 1712.66 1688.92 27.16 o 2 2 0 3958.97 3874.60 56.51 o 3 2 0 1095.06 1104.20 15.48 o 4 2 0 540.93 572.54 11.19 o 5 2 0 549.87 558.51 9.42 o 6 2 0 510.82 501.68 9.21 o 7 2 0 106.33 108.20 8.20 o 8 2 0 111.54 105.22 7.56 o -6 3 0 110.57 113.02 5.67 o -5 3 0 298.10 304.66 9.23 o -4 3 0 291.74 284.69 8.28 o -3 3 0 43.22 33.63 2.52 o -2 3 0 771.56 839.13 12.51 o -1 3 0 854.47 834.09 12.30 o 0 3 0 362.34 364.71 6.12 o 1 3 0 3455.43 3459.03 45.10 o 2 3 0 2963.23 3119.06 40.91 o 3 3 0 2161.94 2395.47 38.84 o 4 3 0 705.20 703.82 16.55 o 5 3 0 33.14 30.89 1.99 o 6 3 0 275.08 289.33 8.07 o 7 3 0 338.02 316.61 9.14 o 8 3 0 152.79 152.80 6.38 o -6 4 0 222.54 227.60 18.95 o -5 4 0 165.49 170.57 7.01 o -4 4 0 40.61 40.91 5.01 o -3 4 0 175.02 174.83 6.12 o -2 4 0 419.90 383.30 39.12 o -1 4 0 326.75 332.24 6.23 o 0 4 0 3347.85 3473.25 45.97 o 1 4 0 2203.20 2224.77 30.12 o 2 4 0 107.75 103.27 2.79 o 3 4 0 1448.36 1615.40 22.54 o 4 4 0 773.28 814.38 12.58 o 5 4 0 32.70 25.82 1.60 o 6 4 0 271.96 278.29 7.99 o 7 4 0 426.41 426.41 11.13 o 8 4 0 190.72 199.66 7.47 o -5 5 0 312.21 308.98 10.35 o -4 5 0 280.98 273.15 9.06 o -3 5 0 0.46 1.31 1.13 o -2 5 0 122.71 120.54 6.84 o -1 5 0 576.99 619.26 13.50 o 0 5 0 1616.47 1659.44 23.62 o 1 5 0 1622.64 1789.27 25.20 o 2 5 0 77.31 71.42 2.55 o 3 5 0 10.97 18.45 1.42 o 4 5 0 467.19 485.07 10.19 o 5 5 0 1148.73 1236.09 18.66 o 6 5 0 572.46 605.20 13.74 o 7 5 0 267.21 288.07 8.82 o 8 5 0 241.92 237.83 8.30 o -4 6 0 79.34 88.15 5.16 o -3 6 0 568.78 570.74 20.89 o -2 6 0 623.98 601.86 14.37 o -1 6 0 67.45 63.48 5.83 o 0 6 0 4.38 6.00 1.15 o 1 6 0 859.40 881.94 14.20 o 2 6 0 457.78 484.25 8.87 o 3 6 0 637.67 642.09 11.00 o 4 6 0 614.39 650.15 11.15 o 5 6 0 357.96 347.22 9.22 o 6 6 0 450.68 482.47 11.92 o 7 6 0 258.96 262.29 9.78 o 8 6 0 85.92 82.59 7.31 o -3 7 0 14.05 12.14 2.39 o -2 7 0 153.75 159.05 6.69 o -1 7 0 44.75 46.97 3.51 o 0 7 0 146.42 141.66 11.53 o 1 7 0 634.07 614.67 13.54 o 2 7 0 312.31 312.30 6.95 o 3 7 0 92.24 87.27 3.34 o 4 7 0 258.07 234.95 15.28 o 5 7 0 425.06 418.33 16.11 o 6 7 0 246.12 249.50 12.21 o 7 7 0 201.61 196.32 11.21 o 8 7 0 86.19 80.19 7.36 o -2 8 0 168.04 164.96 7.19 o -1 8 0 83.79 84.93 9.10 o 0 8 0 64.44 69.30 4.21 o 1 8 0 41.14 59.20 6.10 o 2 8 0 42.23 44.84 6.51 o 3 8 0 167.47 160.94 7.09 o 4 8 0 446.20 449.43 11.64 o 5 8 0 197.16 209.77 10.93 o 6 8 0 159.50 153.95 9.66 o 7 8 0 172.52 171.13 10.52 o 0 9 0 30.09 28.76 5.45 o 1 9 0 84.28 84.82 7.49 o 2 9 0 18.74 19.63 4.18 o 3 9 0 91.79 91.35 5.96 o 4 9 0 329.71 331.81 14.69 o 5 9 0 78.27 92.27 7.39 o 6 9 0 127.47 128.59 9.06 o -5 -9 1 8.23 8.57 3.16 o -4 -9 1 133.76 133.64 6.15 o -3 -9 1 81.51 77.45 5.28 o -2 -9 1 30.41 40.33 5.45 o -1 -9 1 113.96 101.93 8.34 o 0 -9 1 161.68 176.11 11.39 o -7 -8 1 176.43 197.49 11.58 o -6 -8 1 67.55 64.32 6.14 o -5 -8 1 148.98 154.98 9.35 o -4 -8 1 163.38 156.56 6.27 o -3 -8 1 144.07 150.36 7.82 o -2 -8 1 609.62 591.37 14.25 o -1 -8 1 83.84 81.04 6.93 o 0 -8 1 12.68 16.68 4.06 o 1 -8 1 58.43 50.63 6.41 o 2 -8 1 23.78 27.18 5.50 o -8 -7 1 76.38 77.57 7.33 o -7 -7 1 12.46 15.10 3.84 o -6 -7 1 269.34 263.01 12.59 o -5 -7 1 933.02 960.25 15.99 o -4 -7 1 292.61 297.12 8.51 o -3 -7 1 796.42 824.80 20.75 o -2 -7 1 22.11 25.03 3.32 o -1 -7 1 559.56 523.98 20.56 o 0 -7 1 593.79 619.58 14.28 o 1 -7 1 957.25 934.88 19.92 o 2 -7 1 141.69 142.86 6.25 o 3 -7 1 171.74 181.32 7.47 o -8 -6 1 264.13 268.14 13.45 o -7 -6 1 260.46 248.29 12.32 o -6 -6 1 459.25 444.67 16.96 o -5 -6 1 279.43 289.30 10.94 o -4 -6 1 16.48 20.76 1.66 o -3 -6 1 558.45 572.91 15.66 o -2 -6 1 424.58 427.95 8.10 o -1 -6 1 437.67 448.02 8.49 o 0 -6 1 483.21 496.35 9.24 o 1 -6 1 66.80 65.26 3.65 o 2 -6 1 444.01 452.64 11.78 o 3 -6 1 316.27 315.26 9.81 o 4 -6 1 24.18 27.69 3.25 o -8 -5 1 174.63 174.50 6.91 o -7 -5 1 354.62 373.20 11.51 o -6 -5 1 509.19 536.71 20.77 o -5 -5 1 37.96 35.53 1.96 o -4 -5 1 320.08 324.92 6.46 o -3 -5 1 1589.28 1648.72 23.36 o -2 -5 1 428.57 464.52 8.22 o -1 -5 1 1161.10 1222.71 18.00 o 0 -5 1 1594.50 1582.18 22.78 o 1 -5 1 15.01 15.57 1.47 o 2 -5 1 20.75 24.43 2.47 o 3 -5 1 609.39 595.18 15.33 o 4 -5 1 275.25 294.24 9.89 o 5 -5 1 4.20 8.27 2.02 o -8 -4 1 189.87 202.64 8.02 o -7 -4 1 294.88 303.43 10.53 o -6 -4 1 163.79 179.09 4.70 o -5 -4 1 139.86 141.70 3.80 o -4 -4 1 1278.90 1309.48 18.97 o -3 -4 1 1621.23 1733.26 24.01 o -2 -4 1 1935.47 2002.50 27.25 o -1 -4 1 1192.35 1281.99 18.26 o 0 -4 1 324.22 323.25 6.03 o 1 -4 1 248.67 228.92 6.67 o 2 -4 1 42.33 35.98 1.84 o 3 -4 1 167.34 184.95 16.27 o 4 -4 1 647.17 650.66 22.82 o 5 -4 1 288.20 275.11 9.15 o 6 -4 1 34.28 42.64 7.29 o -8 -3 1 68.18 83.65 5.15 o -7 -3 1 69.40 64.42 3.70 o -6 -3 1 370.55 370.60 7.73 o -5 -3 1 575.34 610.32 11.24 o -4 -3 1 707.59 747.04 13.16 o -3 -3 1 1649.74 1796.33 24.52 o -2 -3 1 4408.69 4203.21 54.53 o -1 -3 1 1130.77 1208.45 16.79 o 0 -3 1 16.63 13.28 0.97 o 1 -3 1 762.48 708.70 10.74 o 2 -3 1 452.24 459.25 11.61 o 3 -3 1 471.59 485.07 14.92 o 4 -3 1 597.16 596.97 13.63 o 5 -3 1 301.96 307.15 11.34 o 6 -3 1 197.22 201.20 13.83 o -8 -2 1 160.77 159.53 9.27 o -7 -2 1 66.18 70.71 5.30 o -6 -2 1 2.84 5.03 1.52 o -5 -2 1 989.60 1026.46 15.51 o -4 -2 1 4389.25 4458.12 58.24 o -3 -2 1 156.49 144.74 3.95 o -2 -2 1 1483.67 1518.52 20.43 o -1 -2 1 3830.32 3503.05 50.84 o 0 -2 1 6.82 8.72 0.67 o 1 -2 1 4612.31 4537.17 58.55 o 2 -2 1 3458.95 3379.85 44.39 o 3 -2 1 109.62 89.39 2.63 o 4 -2 1 33.22 27.86 2.38 o 5 -2 1 266.93 280.95 8.37 o 6 -2 1 305.15 304.37 12.89 o 7 -2 1 67.79 75.93 6.62 o -8 -1 1 182.50 188.27 10.75 o -7 -1 1 236.19 227.79 10.83 o -6 -1 1 114.49 107.33 3.52 o -5 -1 1 271.35 273.83 5.70 o -4 -1 1 10.38 13.41 1.87 o -3 -1 1 2330.35 2312.44 30.72 o -2 -1 1 30583.40 15195.07 552.68 o -1 -1 1 2605.75 2440.34 39.32 o 0 -1 1 1.45 2.98 0.41 o 1 -1 1 1635.23 1682.08 22.24 o 2 -1 1 449.56 490.96 7.57 o 3 -1 1 831.49 835.71 12.45 o 4 -1 1 1605.44 1733.17 24.41 o 5 -1 1 134.63 133.93 5.03 o 6 -1 1 135.25 133.88 5.44 o 7 -1 1 358.46 338.27 14.80 o -8 0 1 95.30 92.90 7.45 o -7 0 1 145.88 155.22 9.25 o -6 0 1 74.02 75.00 3.82 o -5 0 1 915.92 926.64 14.84 o -4 0 1 805.06 812.91 12.42 o -3 0 1 2002.34 2019.25 27.11 o -2 0 1 5556.77 4787.53 62.15 o -1 0 1 422.78 438.78 8.86 o 1 0 1 848.55 822.50 18.25 o 2 0 1 542.90 552.21 8.07 o 3 0 1 844.80 828.36 12.07 o 4 0 1 886.56 895.43 13.48 o 5 0 1 547.27 526.17 9.27 o 6 0 1 117.81 123.69 8.54 o 7 0 1 383.65 384.14 15.62 o 8 0 1 261.33 258.08 13.25 o -7 1 1 93.79 99.23 5.35 o -6 1 1 572.53 573.29 18.19 o -5 1 1 173.76 180.85 6.05 o -4 1 1 1.30 3.31 1.29 o -3 1 1 1559.41 1523.08 30.01 o -2 1 1 1792.71 1711.43 22.95 o -1 1 1 3466.33 3201.81 123.88 o 0 1 1 12339.66 7036.86 132.35 o 1 1 1 1365.94 1368.30 22.08 o 2 1 1 86.63 107.93 4.14 o 3 1 1 2.71 0.37 1.09 o 4 1 1 1712.03 1799.39 25.84 o 5 1 1 1156.55 1245.09 22.38 o 6 1 1 410.56 426.54 22.69 o 7 1 1 250.03 237.46 11.13 o 8 1 1 51.88 60.05 6.28 o -7 2 1 56.60 51.14 6.70 o -6 2 1 80.05 82.86 5.46 o -5 2 1 56.82 58.27 3.49 o -4 2 1 578.91 551.93 52.67 o -3 2 1 327.40 343.05 5.93 o -2 2 1 2454.87 2360.82 39.11 o -1 2 1 8052.38 6624.59 146.87 o 0 2 1 12.28 4.43 1.49 o 1 2 1 1546.71 1654.77 21.95 o 2 2 1 2785.25 2795.57 41.24 o 3 2 1 19.32 38.79 1.60 o 4 2 1 669.93 672.50 13.20 o 5 2 1 1249.69 1344.45 19.62 o 6 2 1 718.03 751.86 22.19 o 7 2 1 148.87 146.13 7.93 o 8 2 1 93.30 91.99 7.28 o -6 3 1 8.82 11.68 2.25 o -5 3 1 220.95 219.18 7.62 o -4 3 1 542.58 535.70 14.53 o -3 3 1 380.33 327.05 8.54 o -2 3 1 2862.68 2883.18 47.90 o -1 3 1 1297.83 1272.13 21.11 o 0 3 1 3.92 5.77 0.71 o 1 3 1 1776.90 1864.28 25.09 o 2 3 1 373.64 396.19 6.59 o 3 3 1 1263.64 1352.58 18.80 o 4 3 1 1751.11 1833.71 25.24 o 5 3 1 519.24 506.53 8.71 o 6 3 1 177.61 166.54 5.85 o 7 3 1 102.87 105.53 5.08 o 8 3 1 398.85 401.48 11.48 o -6 4 1 68.04 79.32 5.05 o -5 4 1 3.00 4.58 1.59 o -4 4 1 260.12 264.66 8.39 o -3 4 1 684.27 659.58 15.20 o -2 4 1 410.80 423.04 10.17 o -1 4 1 396.37 401.60 7.02 o 0 4 1 812.74 835.71 15.93 o 1 4 1 22.47 10.73 1.04 o 2 4 1 834.91 898.01 13.39 o 3 4 1 3673.11 3927.90 51.62 o 4 4 1 877.08 878.30 13.33 o 5 4 1 324.91 311.37 8.16 o 6 4 1 285.01 294.23 8.32 o 7 4 1 448.33 443.09 11.58 o 8 4 1 154.29 163.49 6.69 o -5 5 1 111.60 113.66 5.94 o -4 5 1 116.34 119.81 8.06 o -3 5 1 146.84 144.73 13.23 o -2 5 1 0.55 1.46 1.15 o -1 5 1 215.43 227.09 8.24 o 0 5 1 1307.83 1354.10 19.78 o 1 5 1 795.87 791.01 12.49 o 2 5 1 1888.17 1954.43 27.27 o 3 5 1 863.40 932.49 14.31 o 4 5 1 325.00 328.19 6.45 o 5 5 1 385.24 388.46 9.78 o 6 5 1 91.93 89.36 4.27 o 7 5 1 236.17 244.81 10.92 o 8 5 1 207.07 199.19 11.10 o -4 6 1 93.48 83.29 5.01 o -3 6 1 35.55 33.23 4.50 o -2 6 1 50.71 44.14 3.51 o -1 6 1 2324.31 2300.97 40.72 o 0 6 1 453.00 453.89 15.89 o 1 6 1 26.24 27.14 2.44 o 2 6 1 785.21 823.38 13.41 o 3 6 1 1.92 2.09 1.68 o 4 6 1 179.91 208.63 5.11 o 5 6 1 1545.48 1643.18 47.01 o 6 6 1 496.68 519.85 12.73 o 7 6 1 63.96 62.70 4.04 o 8 6 1 62.64 68.50 4.40 o -3 7 1 62.03 61.73 5.68 o -2 7 1 211.45 195.56 7.52 o -1 7 1 151.38 134.69 5.87 o 0 7 1 25.83 27.91 3.85 o 1 7 1 91.55 89.88 4.42 o 2 7 1 765.12 792.45 13.46 o 3 7 1 355.39 332.52 18.49 o 4 7 1 377.92 396.37 14.03 o 5 7 1 483.34 472.85 17.38 o 6 7 1 288.22 280.41 8.69 o 7 7 1 112.34 104.50 5.25 o 8 7 1 24.55 37.24 5.64 o -2 8 1 19.69 21.71 3.13 o -1 8 1 56.27 56.28 4.16 o 0 8 1 41.56 45.38 3.69 o 1 8 1 66.27 60.04 3.82 o 2 8 1 182.21 187.93 5.77 o 3 8 1 422.95 414.29 8.76 o 4 8 1 732.46 760.66 24.22 o 5 8 1 252.80 264.00 12.49 o 6 8 1 29.23 28.41 4.78 o 7 8 1 56.85 59.31 6.57 o 0 9 1 35.02 27.26 5.26 o 1 9 1 173.82 166.60 10.55 o 2 9 1 170.71 186.67 10.90 o 3 9 1 127.48 143.88 6.46 o 4 9 1 124.77 131.64 8.37 o 5 9 1 149.59 155.59 9.60 o 6 9 1 187.92 197.05 11.37 o -6 -9 2 23.92 27.46 5.12 o -5 -9 2 0.63 2.38 2.46 o -4 -9 2 387.83 387.36 11.51 o -3 -9 2 136.61 132.43 6.20 o -2 -9 2 24.13 24.27 4.78 o -1 -9 2 148.93 129.35 9.40 o 0 -9 2 15.41 21.63 5.16 o -7 -8 2 218.52 228.83 12.89 o -5 -8 2 279.15 291.31 9.21 o -4 -8 2 51.40 49.06 3.77 o -3 -8 2 79.60 68.95 5.16 o -2 -8 2 526.28 530.74 13.44 o -1 -8 2 476.02 446.88 18.05 o 0 -8 2 69.56 80.28 7.33 o 1 -8 2 365.24 359.46 16.83 o 2 -8 2 55.00 64.24 7.42 o -8 -7 2 119.49 118.01 8.94 o -7 -7 2 69.58 69.80 6.65 o -6 -7 2 22.44 25.09 4.44 o -5 -7 2 684.51 707.32 15.97 o -4 -7 2 191.68 177.48 9.27 o -3 -7 2 31.27 29.50 6.64 o -2 -7 2 916.42 915.88 19.22 o -1 -7 2 394.94 387.99 10.42 o 0 -7 2 47.21 38.70 5.13 o 1 -7 2 147.98 140.13 9.40 o 2 -7 2 198.62 197.33 7.38 o 3 -7 2 60.53 65.34 5.68 o -8 -6 2 149.78 148.49 9.70 o -7 -6 2 0.45 1.91 2.13 o -6 -6 2 375.18 365.16 15.02 o -5 -6 2 1328.60 1322.40 25.31 o -4 -6 2 303.67 320.56 20.09 o -3 -6 2 715.91 580.60 18.35 o -2 -6 2 96.29 86.42 12.59 o -1 -6 2 5.56 7.80 1.20 o 0 -6 2 633.63 614.81 11.23 o 1 -6 2 1099.86 1135.00 22.31 o 2 -6 2 161.47 170.92 6.47 o 3 -6 2 4.38 7.39 1.73 o 4 -6 2 79.61 84.35 5.00 o -8 -5 2 112.30 106.91 7.91 o -7 -5 2 355.79 355.80 14.88 o -6 -5 2 661.76 695.50 22.63 o -5 -5 2 203.61 200.05 4.91 o -4 -5 2 976.64 993.24 15.26 o -3 -5 2 719.43 728.35 13.82 o -2 -5 2 3.45 4.03 0.84 o -1 -5 2 621.26 612.73 10.16 o 0 -5 2 317.82 298.52 9.50 o 1 -5 2 378.44 391.70 7.62 o 2 -5 2 973.77 997.16 19.95 o 3 -5 2 216.84 221.55 7.50 o 4 -5 2 44.60 48.47 3.81 o 5 -5 2 39.86 41.16 3.93 o -8 -4 2 179.61 179.11 6.87 o -7 -4 2 510.96 491.26 12.08 o -6 -4 2 386.99 392.74 7.87 o -5 -4 2 103.88 109.03 3.35 o -4 -4 2 862.31 875.37 13.47 o -3 -4 2 651.76 682.59 10.66 o -2 -4 2 897.37 929.04 13.70 o -1 -4 2 1175.99 1209.16 17.28 o 0 -4 2 364.64 309.02 8.80 o 1 -4 2 1019.71 1073.82 16.02 o 2 -4 2 407.80 418.34 7.77 o 3 -4 2 193.78 199.97 6.63 o 4 -4 2 393.31 387.64 19.12 o 5 -4 2 174.90 198.27 7.63 o 6 -4 2 62.00 62.62 4.72 o -8 -3 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9.10 o -2 -4 13 9.41 7.91 2.12 o -1 -4 13 54.94 62.35 4.62 o -3 -3 13 95.68 103.99 5.76 o -2 -3 13 62.97 70.70 4.63 o -1 -3 13 191.40 193.10 7.78 o 0 -3 13 71.09 79.72 4.83 o 1 -3 13 117.44 127.41 9.46 o -3 -2 13 153.90 169.44 12.55 o -2 -2 13 333.61 346.26 10.79 o -1 -2 13 123.25 133.57 6.23 o 0 -2 13 100.73 114.75 5.69 o 1 -2 13 210.11 216.17 11.89 o 2 -2 13 103.99 98.38 8.01 o -3 -1 13 167.83 191.57 7.64 o -2 -1 13 395.96 432.46 15.95 o -1 -1 13 300.10 292.62 9.70 o 0 -1 13 168.49 170.26 9.20 o 1 -1 13 151.73 187.24 10.82 o 2 -1 13 47.10 50.88 6.00 o 3 -1 13 140.88 144.74 9.92 o -3 0 13 220.33 261.65 13.12 o -2 0 13 568.95 591.91 15.63 o -1 0 13 286.36 298.09 9.75 o 0 0 13 68.23 71.05 6.27 o 1 0 13 26.88 32.31 4.80 o 2 0 13 87.11 79.38 6.74 o 3 0 13 252.50 243.27 12.82 o -3 1 13 159.29 161.61 9.85 o -2 1 13 51.59 56.06 5.48 o -1 1 13 48.03 54.40 3.72 o 0 1 13 207.96 210.37 10.66 o 1 1 13 199.42 194.63 10.44 o 2 1 13 249.49 234.17 11.95 o 3 1 13 212.31 215.68 11.86 o 4 1 13 192.80 192.72 11.58 o -2 2 13 269.68 269.35 13.01 o 0 2 13 145.33 143.10 8.43 o 1 2 13 381.62 348.52 14.61 o 2 2 13 185.87 195.36 7.70 o 3 2 13 3.50 6.97 2.79 o 4 2 13 192.14 185.42 7.65 o -1 3 13 322.70 333.67 14.80 o 0 3 13 27.26 32.21 4.90 o 1 3 13 135.95 138.36 6.29 o 2 3 13 112.53 115.13 5.74 o 3 3 13 59.59 55.13 9.75 o 0 4 13 67.78 80.85 7.26 o 1 4 13 60.05 67.73 6.93 o 2 4 13 24.72 33.28 3.50 o 3 4 13 249.53 256.10 9.27 o -1 -2 14 116.70 123.08 6.14 o 0 -2 14 26.23 27.86 4.93 o -2 -1 14 70.56 79.12 5.78 o -1 -1 14 42.10 62.56 8.05 o 0 -1 14 112.50 118.10 8.50 o 1 -1 14 39.05 48.29 6.06 o -2 0 14 8.95 12.93 3.41 o -1 0 14 43.56 54.07 4.19 o 0 0 14 282.58 276.89 13.33 o 1 0 14 212.61 223.46 11.97 o 2 0 14 138.24 133.63 9.25 o 0 1 14 89.59 101.29 7.49 o 1 1 14 32.12 35.36 5.07 o 2 1 14 225.78 221.57 12.08 o 0 2 14 58.15 64.65 5.78 o 1 2 14 104.52 101.70 7.56 o 2 2 14 274.52 292.08 14.07 o