#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/73/2207308.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207308_Fobs loop_ _publ_author_name 'Morawitz, Thorsten' 'Lerner, Hans-Wolfram' 'Bru Roig, Miriam' 'Bolte, Michael' _publ_section_title ; \m-1,2-Ethanediylbis(diphenylphosphine)-\k^2^P:P'-bis{acetato[1,2-ethanediylbis(diphenylphosphine)-\k^2^P,P']copper(I)} diethyl ether disolvate ; _journal_coeditor_code NC6048 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2201 _journal_page_last m2203 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 85.069 _cell_angle_beta 83.287 _cell_angle_gamma 61.629 _cell_length_a 12.6520 _cell_length_b 12.8760 _cell_length_c 14.2907 _exptl_crystal_F_000 834.00 _reflns_d_resolution_high 0.8292 _[local]_cod_data_source_file nc60483sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa484 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 212.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4207.34 3724.45 27.85 o 3 0 0 5945.80 5279.47 104.19 o 4 0 0 272.36 215.59 5.75 o 5 0 0 2414.73 2018.66 48.15 o 6 0 0 1788.32 1712.46 32.22 o 7 0 0 652.50 486.46 11.86 o 8 0 0 233.59 230.69 8.20 o 9 0 0 19.76 21.51 6.82 o 10 0 0 13.10 120.98 7.18 o 11 0 0 424.10 391.80 14.61 o 12 0 0 124.45 172.19 8.17 o 13 0 0 30.73 8.24 7.19 o -12 1 0 0.37 126.24 7.02 o -11 1 0 75.30 568.75 22.03 o -10 1 0 402.39 442.22 19.18 o -9 1 0 1175.55 1033.05 38.99 o -8 1 0 35.69 130.80 6.58 o -7 1 0 241.65 560.11 13.50 o -6 1 0 40.41 299.58 12.55 o -5 1 0 1227.07 1324.85 30.38 o -4 1 0 183.11 329.47 6.74 o -3 1 0 1312.38 2012.92 36.97 o -2 1 0 5608.07 4682.54 66.16 o 3 1 0 865.79 822.12 12.06 o 4 1 0 1172.48 1123.49 28.37 o 5 1 0 1908.57 2415.15 52.93 o 6 1 0 386.20 523.60 11.18 o 7 1 0 130.95 934.53 35.32 o 8 1 0 299.63 717.38 13.91 o 9 1 0 1835.11 1670.41 45.81 o 10 1 0 415.22 1315.60 42.65 o 11 1 0 693.49 1321.26 26.71 o 12 1 0 104.80 471.64 8.36 o 13 1 0 12.86 0.42 7.83 o -12 2 0 164.17 269.11 11.84 o -11 2 0 693.50 605.67 36.77 o -10 2 0 839.82 716.76 35.68 o -9 2 0 16.83 286.92 11.32 o -8 2 0 86.76 234.14 10.64 o -7 2 0 703.68 771.43 21.70 o -6 2 0 3816.93 3598.45 55.08 o -5 2 0 2411.67 2095.57 35.55 o -4 2 0 625.56 1025.62 29.58 o -3 2 0 5080.52 6474.88 109.50 o -2 2 0 445.30 456.96 7.42 o -1 2 0 22830.85 25574.78 508.12 o 0 2 0 2674.66 2174.14 38.03 o 2 2 0 2099.73 1994.40 43.54 o 3 2 0 1061.28 1101.16 21.72 o 4 2 0 824.53 1037.72 29.83 o 5 2 0 391.94 514.54 9.77 o 6 2 0 71.21 56.47 7.47 o 7 2 0 1651.53 1543.30 38.49 o 8 2 0 4888.44 5051.52 106.96 o 9 2 0 3105.61 3498.45 163.10 o 10 2 0 1114.06 1654.89 60.40 o 11 2 0 388.78 645.58 25.52 o 12 2 0 206.65 538.02 16.96 o 13 2 0 282.11 313.65 12.67 o 14 2 0 14.11 14.86 7.80 o -11 3 0 406.20 496.52 24.89 o -10 3 0 27.37 349.57 17.34 o -9 3 0 28.74 385.14 22.15 o -8 3 0 570.69 700.71 23.33 o -7 3 0 848.69 762.27 19.13 o -6 3 0 376.15 693.55 10.72 o -5 3 0 1156.82 1145.44 30.72 o -4 3 0 40.56 388.84 15.00 o -3 3 0 2858.33 2722.07 35.82 o -2 3 0 771.20 666.67 7.22 o -1 3 0 7724.32 8977.68 259.81 o 0 3 0 3819.23 6760.35 125.69 o 1 3 0 5052.19 4556.90 171.60 o 2 3 0 7857.57 8196.84 765.20 o 3 3 0 55.61 45.99 7.78 o 4 3 0 843.54 1772.63 64.69 o 5 3 0 779.54 827.87 27.88 o 6 3 0 6515.55 7296.02 200.22 o 7 3 0 1981.79 2152.91 45.87 o 8 3 0 2986.37 3325.01 130.45 o 9 3 0 1517.20 1822.10 83.93 o 10 3 0 381.41 482.29 14.35 o 11 3 0 1145.89 1413.47 66.02 o 12 3 0 1766.77 1671.05 65.04 o 13 3 0 737.79 629.04 33.44 o 14 3 0 191.82 202.84 11.33 o -11 4 0 4.15 37.06 15.01 o -10 4 0 603.57 581.47 35.53 o -9 4 0 323.54 348.99 15.26 o -8 4 0 146.20 165.79 6.20 o -7 4 0 474.60 405.24 8.16 o -6 4 0 304.34 348.33 7.65 o -5 4 0 109.32 169.23 11.06 o -4 4 0 917.62 2513.32 128.62 o -3 4 0 3497.06 4671.69 159.66 o -2 4 0 2651.69 2344.68 31.01 o -1 4 0 36.27 102.26 6.28 o 0 4 0 149.62 91.51 6.11 o 1 4 0 7977.56 9357.57 406.36 o 2 4 0 4155.24 5673.21 245.60 o 3 4 0 1578.09 2503.40 103.46 o 4 4 0 73.05 183.36 8.94 o 5 4 0 309.01 244.63 8.92 o 6 4 0 57.42 233.47 8.41 o 7 4 0 251.48 507.08 27.90 o 8 4 0 111.25 295.97 21.35 o 9 4 0 719.51 701.15 33.54 o 10 4 0 371.10 377.25 19.52 o 11 4 0 5.78 551.91 27.40 o 12 4 0 85.09 431.02 30.74 o 13 4 0 174.42 176.40 8.29 o 14 4 0 0.12 8.63 7.60 o -10 5 0 212.50 275.34 13.31 o -9 5 0 464.00 528.21 19.01 o -8 5 0 336.33 297.94 13.84 o -7 5 0 331.62 456.61 14.59 o -6 5 0 5.22 25.73 5.60 o -5 5 0 44.23 50.25 5.75 o -4 5 0 1530.88 1518.93 33.30 o -3 5 0 1235.43 1187.67 36.39 o -2 5 0 4372.56 4470.47 89.21 o -1 5 0 64.64 190.10 10.87 o 0 5 0 2839.64 2816.65 41.72 o 1 5 0 7250.35 7398.03 175.01 o 2 5 0 2207.43 2779.55 103.60 o 3 5 0 712.41 1011.36 105.91 o 4 5 0 35.61 22.91 8.11 o 5 5 0 854.51 1239.69 29.11 o 6 5 0 3994.69 4144.01 102.68 o 7 5 0 599.80 763.12 24.66 o 8 5 0 2977.73 3512.84 49.51 o 9 5 0 2839.45 2899.99 135.56 o 10 5 0 40.47 31.94 8.07 o 11 5 0 484.41 594.14 25.47 o 12 5 0 1062.25 870.53 60.41 o 13 5 0 50.59 117.71 7.70 o 14 5 0 15.84 29.22 9.84 o -9 6 0 31.91 104.34 6.93 o -8 6 0 10.94 19.85 6.61 o -7 6 0 41.06 104.65 7.01 o -6 6 0 3.14 17.74 5.49 o -5 6 0 19.93 31.59 6.32 o -4 6 0 51.73 82.50 5.83 o -3 6 0 445.28 494.54 11.47 o -2 6 0 2.31 216.42 15.00 o -1 6 0 2628.32 3780.37 148.12 o 0 6 0 968.97 1024.18 26.83 o 1 6 0 35.37 46.82 7.48 o 2 6 0 9.02 36.74 8.26 o 3 6 0 11.69 53.93 8.70 o 4 6 0 564.08 965.92 31.37 o 5 6 0 1407.50 3280.66 174.85 o 6 6 0 5304.50 6199.57 227.47 o 7 6 0 1183.34 1602.20 81.15 o 8 6 0 316.67 841.12 36.81 o 9 6 0 314.45 625.32 46.16 o 10 6 0 114.80 160.56 9.27 o 11 6 0 897.41 1258.21 53.69 o 12 6 0 153.65 186.45 11.40 o 13 6 0 57.18 52.40 7.65 o 14 6 0 62.25 72.24 8.14 o 15 6 0 54.47 45.49 13.70 o -8 7 0 224.75 335.12 14.19 o -7 7 0 201.54 148.38 6.85 o -6 7 0 80.88 114.01 8.32 o -5 7 0 11.65 53.73 6.04 o -4 7 0 353.96 424.03 10.48 o -3 7 0 23.89 85.48 5.96 o -2 7 0 881.27 1051.12 27.96 o -1 7 0 2663.60 2600.53 57.50 o 0 7 0 588.95 587.52 18.30 o 1 7 0 9.67 45.63 7.36 o 2 7 0 0.50 16.84 7.21 o 3 7 0 108.41 199.71 8.96 o 4 7 0 3310.70 4247.54 119.12 o 5 7 0 771.37 1207.59 42.50 o 6 7 0 2564.97 3070.79 92.40 o 7 7 0 441.08 459.07 14.08 o 8 7 0 1143.99 1184.51 55.36 o 9 7 0 1986.13 1906.60 62.54 o 10 7 0 833.27 848.64 39.58 o 11 7 0 188.88 344.22 14.36 o 12 7 0 179.10 192.93 10.79 o 13 7 0 161.15 174.60 9.39 o 14 7 0 0.06 83.14 8.27 o 15 7 0 145.26 190.77 9.90 o -7 8 0 71.79 188.28 17.42 o -6 8 0 18.71 69.83 6.66 o -5 8 0 1.71 0.04 6.30 o -4 8 0 17.64 34.09 6.53 o -3 8 0 547.10 494.89 15.72 o -2 8 0 61.49 163.57 7.30 o -1 8 0 203.33 243.41 7.32 o 0 8 0 1.27 172.98 12.83 o 1 8 0 460.52 697.52 27.59 o 2 8 0 30.56 161.16 8.22 o 3 8 0 1641.86 1843.05 69.45 o 4 8 0 2633.95 3858.59 102.96 o 5 8 0 150.04 177.81 8.42 o 6 8 0 3295.05 4376.11 96.19 o 7 8 0 1570.01 1810.19 57.61 o 8 8 0 2553.46 3002.11 200.54 o 9 8 0 2461.46 2531.68 46.73 o 10 8 0 326.63 338.73 18.05 o 11 8 0 0.97 145.96 18.02 o 12 8 0 199.72 228.69 22.96 o 13 8 0 2.25 24.42 8.43 o 14 8 0 191.72 185.33 10.15 o 15 8 0 822.42 626.03 21.24 o -6 9 0 390.49 417.60 18.85 o -5 9 0 464.16 484.67 15.76 o -4 9 0 151.85 164.96 7.31 o -3 9 0 491.29 516.17 17.19 o -2 9 0 1879.47 1889.29 85.27 o -1 9 0 4049.32 4299.02 126.97 o 0 9 0 623.79 532.99 18.42 o 1 9 0 238.93 249.64 7.93 o 2 9 0 921.45 1216.51 48.44 o 3 9 0 362.67 403.39 20.15 o 4 9 0 134.12 192.65 9.28 o 5 9 0 36.73 74.55 8.62 o 6 9 0 208.79 326.25 9.50 o 7 9 0 128.91 173.00 9.14 o 8 9 0 440.38 630.48 13.92 o 9 9 0 49.84 78.18 9.94 o 10 9 0 67.49 130.57 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79.95 8.94 o 7 11 0 67.96 79.75 8.87 o 8 11 0 1193.63 1523.46 28.56 o 9 11 0 45.33 108.47 9.08 o 10 11 0 219.49 186.95 9.71 o 11 11 0 1.62 20.23 9.93 o 12 11 0 367.94 387.72 21.61 o 13 11 0 460.34 408.80 29.65 o 14 11 0 76.92 61.12 9.09 o -2 12 0 2.52 9.90 7.18 o -1 12 0 424.62 359.72 14.84 o 0 12 0 368.04 380.08 16.60 o 1 12 0 83.46 137.09 9.07 o 2 12 0 294.64 354.57 12.93 o 3 12 0 1863.74 2011.03 116.18 o 4 12 0 0.02 24.22 8.82 o 5 12 0 3006.84 3489.66 186.42 o 6 12 0 1545.32 1889.74 67.38 o 7 12 0 1606.61 1944.89 124.43 o 8 12 0 1031.10 1169.37 31.36 o 9 12 0 160.87 261.62 9.79 o 10 12 0 1060.81 800.44 45.54 o 11 12 0 281.86 280.62 15.71 o 12 12 0 708.34 601.06 31.61 o 13 12 0 59.48 49.03 10.20 o -1 13 0 6.11 36.88 7.69 o 0 13 0 6.81 14.30 7.90 o 1 13 0 14.04 13.05 7.99 o 2 13 0 178.47 177.97 10.49 o 3 13 0 1.62 4.74 8.79 o 4 13 0 87.63 101.06 8.99 o 5 13 0 1207.27 1225.92 59.98 o 6 13 0 3103.92 3683.68 152.72 o 7 13 0 1578.05 1900.86 63.42 o 8 13 0 324.64 342.50 26.09 o 9 13 0 59.38 46.56 8.70 o 10 13 0 282.79 234.90 10.26 o 11 13 0 74.02 77.06 9.48 o 12 13 0 1130.19 843.58 32.56 o 13 13 0 532.50 499.22 45.06 o 1 14 0 316.33 284.93 18.30 o 2 14 0 8.08 34.01 7.90 o 3 14 0 28.40 152.99 12.58 o 4 14 0 8.72 23.63 9.12 o 5 14 0 326.45 305.73 15.49 o 6 14 0 37.57 65.44 8.59 o 7 14 0 198.38 248.20 9.59 o 8 14 0 53.03 64.02 8.97 o 9 14 0 19.87 30.94 9.15 o 10 14 0 44.35 34.06 8.73 o 11 14 0 1.43 6.40 9.18 o 4 15 0 42.84 38.76 11.45 o 5 15 0 626.67 685.35 19.73 o 6 15 0 246.21 292.77 9.13 o 7 15 0 176.00 166.96 9.95 o 8 15 0 219.84 216.95 10.68 o 9 15 0 111.17 99.26 9.42 o -9 -15 1 3.06 15.03 8.76 o -8 -15 1 421.98 480.29 16.28 o -7 -15 1 1040.44 1101.12 41.31 o -6 -15 1 46.46 67.78 8.33 o -5 -15 1 16.87 25.91 8.46 o -11 -14 1 63.07 64.64 9.25 o -10 -14 1 276.89 206.16 9.83 o -9 -14 1 38.20 55.80 8.83 o -8 -14 1 232.89 196.73 9.30 o -7 -14 1 99.27 108.44 8.24 o -6 -14 1 372.35 367.34 15.26 o -5 -14 1 41.92 51.95 8.82 o -4 -14 1 33.17 31.40 10.43 o -3 -14 1 65.36 86.52 9.17 o -2 -14 1 1.73 -4.14 8.24 o -1 -14 1 166.25 124.31 22.28 o -12 -13 1 393.49 278.35 15.21 o -11 -13 1 549.94 476.42 15.69 o -10 -13 1 695.40 716.98 33.24 o -9 -13 1 24.72 32.85 8.59 o -8 -13 1 1738.33 1963.88 65.35 o -7 -13 1 2008.90 2139.26 40.24 o -6 -13 1 1271.53 1350.71 71.56 o -5 -13 1 113.97 142.57 14.62 o -4 -13 1 114.10 172.06 10.96 o -3 -13 1 19.61 32.14 8.13 o -2 -13 1 9.96 65.72 7.77 o -1 -13 1 118.87 114.10 7.78 o 0 -13 1 229.05 203.26 9.25 o 1 -13 1 312.69 264.56 17.36 o -13 -12 1 199.36 162.07 13.70 o -12 -12 1 87.70 87.59 9.26 o -11 -12 1 78.51 92.07 9.16 o -10 -12 1 9.71 43.67 9.23 o -9 -12 1 1769.93 1908.16 77.76 o -8 -12 1 1180.85 1324.91 63.99 o -7 -12 1 134.28 170.07 9.41 o -6 -12 1 96.72 145.39 8.56 o -5 -12 1 137.21 153.12 9.80 o -4 -12 1 5.27 29.04 11.95 o -3 -12 1 780.56 868.40 48.87 o -2 -12 1 136.23 149.33 7.81 o -1 -12 1 65.01 110.21 9.37 o 0 -12 1 332.11 375.62 15.41 o 1 -12 1 26.22 99.80 7.52 o 2 -12 1 25.91 20.62 7.04 o -14 -11 1 6.27 14.19 9.09 o -13 -11 1 25.08 44.68 9.91 o -12 -11 1 321.02 263.49 16.68 o -11 -11 1 257.72 336.17 32.44 o -10 -11 1 290.26 447.15 47.58 o -9 -11 1 1296.94 1330.14 63.11 o -8 -11 1 1100.86 1186.41 43.97 o -7 -11 1 16.65 50.25 8.61 o -6 -11 1 510.62 680.47 37.41 o -5 -11 1 1991.52 2077.41 125.93 o -4 -11 1 1968.64 2135.05 79.33 o -3 -11 1 380.61 364.66 24.32 o -2 -11 1 153.50 314.22 18.64 o -1 -11 1 42.36 67.90 7.09 o 0 -11 1 752.46 705.52 22.16 o 1 -11 1 1609.15 1440.73 58.79 o 2 -11 1 759.71 637.90 31.98 o 3 -11 1 162.89 178.76 11.81 o 4 -11 1 128.42 284.08 13.49 o -14 -10 1 118.46 84.54 9.73 o -13 -10 1 3.93 2.17 8.74 o -12 -10 1 187.55 184.47 18.46 o -11 -10 1 2.68 23.67 9.16 o -10 -10 1 498.18 484.36 39.10 o -9 -10 1 46.20 45.55 8.21 o -8 -10 1 50.59 81.09 9.50 o -7 -10 1 57.46 73.16 9.01 o -6 -10 1 587.72 704.13 22.43 o -5 -10 1 178.41 212.91 19.57 o -4 -10 1 226.69 278.14 10.42 o -3 -10 1 287.51 386.52 20.81 o -2 -10 1 175.05 172.44 10.34 o -1 -10 1 1426.96 1415.90 37.38 o 0 -10 1 1399.29 1433.69 50.39 o 1 -10 1 4014.66 3982.13 102.51 o 2 -10 1 818.61 843.54 35.68 o 3 -10 1 229.15 389.86 16.89 o 4 -10 1 296.70 236.50 7.88 o 5 -10 1 1108.21 766.81 35.96 o -14 -9 1 463.00 305.09 13.39 o -13 -9 1 13.09 1.21 8.28 o -12 -9 1 12.48 29.71 10.10 o -11 -9 1 524.77 523.63 39.62 o -10 -9 1 1430.97 1473.50 224.74 o -9 -9 1 916.92 1024.66 38.21 o -8 -9 1 3167.29 3095.14 187.32 o -7 -9 1 969.53 1216.76 54.73 o -6 -9 1 574.95 703.98 18.80 o -5 -9 1 53.64 52.48 8.73 o -4 -9 1 105.54 105.45 8.13 o -3 -9 1 563.67 676.05 29.66 o -2 -9 1 47.65 216.71 8.28 o -1 -9 1 217.53 180.00 7.42 o 0 -9 1 967.21 1186.52 50.80 o 1 -9 1 1442.88 2276.97 94.44 o 2 -9 1 106.93 422.80 15.43 o 3 -9 1 1875.50 1650.54 54.64 o 4 -9 1 135.11 106.24 6.36 o 5 -9 1 23.93 66.33 8.68 o 6 -9 1 51.52 112.43 15.99 o -14 -8 1 90.77 64.72 9.05 o -13 -8 1 143.75 125.06 9.27 o -12 -8 1 48.27 99.41 20.22 o -11 -8 1 634.17 561.23 52.87 o -10 -8 1 831.07 612.56 54.53 o -9 -8 1 1260.25 1374.42 89.34 o -8 -8 1 634.07 726.74 17.91 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