#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/73/2207368.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207368_Fobs loop_ _publ_author_name 'Howie, R. Alan' 'de Lima Ferreira, Marcelle' 'de Souza, Marcus V. N.' 'Vasconcelos, Thatyana R. A.' 'Wardell, Solange M. S. V.' 'Wardell, James L.' _publ_section_title ; 8-Methyl-5-oxo-5,6-dihydrodipyrido[1,2-a:3',2'-e]pyrimidin-11-ium chloride trihydrate 120 K ; _journal_coeditor_code WK6062 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3579 _journal_page_last o3581 _journal_volume 61 _journal_year 2005 _space_group_IT_number 176 _symmetry_space_group_name_Hall '-P 6c' _symmetry_space_group_name_H-M 'P 63/m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 19.4419 _cell_length_b 19.4419 _cell_length_c 6.5498 _exptl_crystal_F_000 948.00 _reflns_d_resolution_high 0.7695 _[local]_cod_data_source_file wk6062Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'Me-oxo-dihydrodipyridopyrimidinium chloride trihydrate' _shelx_refln_list_code 4 _shelx_f_calc_maximum 122.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x, y, -z+1/2' '-y, x-y, -z+1/2' '-x+y, -x, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x, -y, z-1/2' 'y, -x+y, z-1/2' 'x-y, x, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -2 3 0 1920.69 1954.68 28.05 o -1 3 0 10.07 0.31 0.48 o 0 3 0 3.66 6.27 0.63 o -3 4 0 70.33 54.44 1.27 o -2 4 0 2969.20 2982.89 39.63 o -1 4 0 5862.73 5814.51 83.39 o 0 4 0 1760.69 1874.30 22.34 o -4 5 0 635.16 708.20 8.74 o -3 5 0 1253.77 1123.39 14.16 o -2 5 0 593.95 624.42 8.89 o -1 5 0 14985.00 13990.32 219.12 o 0 5 0 2566.04 2607.60 33.55 o -5 6 0 7399.85 7188.86 86.93 o -4 6 0 1010.48 961.88 12.93 o -3 6 0 556.41 634.43 14.65 o -2 6 0 3715.72 3708.16 54.01 o -1 6 0 987.36 1091.45 14.89 o 0 6 0 486.74 444.28 6.50 o -6 7 0 25.78 15.90 0.83 o -5 7 0 591.85 535.47 7.10 o -4 7 0 2744.29 2680.99 35.19 o -3 7 0 3070.56 3013.00 46.51 o -2 7 0 2197.37 2196.93 30.26 o -1 7 0 804.08 769.73 10.46 o 0 7 0 3447.34 3378.88 40.50 o -7 8 0 1183.47 906.14 12.33 o -6 8 0 1355.67 1408.00 18.61 o -5 8 0 5233.88 5453.37 70.19 o -4 8 0 7.78 8.49 0.93 o -3 8 0 544.57 536.73 8.13 o -2 8 0 5440.47 5156.27 78.20 o -1 8 0 9.64 18.80 0.94 o 0 8 0 2759.76 2779.25 37.27 o -8 9 0 4673.99 4863.12 58.44 o -7 9 0 3984.22 4399.55 61.16 o -6 9 0 3731.56 4510.77 59.51 o -5 9 0 1826.81 1706.17 22.74 o -4 9 0 1885.19 1775.04 23.96 o -3 9 0 668.47 680.22 10.84 o -2 9 0 1278.99 1370.18 19.48 o -1 9 0 33.27 20.35 1.06 o 0 9 0 903.57 913.63 12.58 o -9 10 0 600.99 748.91 10.14 o -8 10 0 686.16 736.79 9.38 o -7 10 0 159.72 133.15 2.59 o -6 10 0 7981.24 8680.67 127.34 o -5 10 0 0.19 11.50 1.17 o -4 10 0 886.59 847.69 12.55 o -3 10 0 1371.63 1398.48 21.46 o -2 10 0 386.50 314.74 4.66 o -1 10 0 392.70 388.42 5.43 o 0 10 0 216.18 221.81 4.03 o -10 11 0 1993.52 2044.41 26.56 o -9 11 0 1130.09 1286.51 18.16 o -8 11 0 1040.42 1350.62 18.03 o -7 11 0 18.18 19.02 1.15 o -6 11 0 866.21 759.32 10.78 o -5 11 0 71.17 71.94 2.52 o -4 11 0 793.36 792.82 12.05 o -3 11 0 594.58 593.43 8.81 o -2 11 0 129.50 176.80 3.70 o -1 11 0 1008.48 1006.35 13.87 o 0 11 0 1697.74 1631.72 24.44 o -11 12 0 1106.94 1091.40 16.85 o -10 12 0 2687.74 2766.39 40.01 o -9 12 0 1573.09 1601.00 21.52 o -8 12 0 1902.56 1773.59 23.89 o -7 12 0 97.47 79.50 2.13 o -6 12 0 26.36 24.72 2.06 o -5 12 0 0.17 0.63 0.68 o -4 12 0 76.94 91.14 2.30 o -3 12 0 692.38 730.73 11.45 o -2 12 0 47.85 46.97 1.56 o -1 12 0 289.11 314.12 6.18 o 0 12 0 33.49 38.51 1.88 o -12 13 0 529.30 506.71 9.77 o -11 13 0 17.26 22.86 1.41 o -10 13 0 47.53 48.93 2.02 o -9 13 0 369.11 396.41 6.20 o -8 13 0 1475.65 1555.90 21.33 o -7 13 0 1154.69 1015.76 14.86 o -6 13 0 2383.90 2410.06 28.83 o -5 13 0 417.31 406.75 6.46 o -4 13 0 3179.26 3039.96 38.80 o -3 13 0 1660.98 1740.95 22.03 o -2 13 0 104.70 105.96 3.37 o -1 13 0 505.35 521.35 9.07 o 0 13 0 12.66 20.94 2.56 o -13 14 0 564.68 582.28 11.25 o -12 14 0 1108.55 1144.66 21.25 o -11 14 0 3.34 9.77 1.73 o -10 14 0 58.23 41.77 1.73 o -9 14 0 603.40 578.01 9.78 o -8 14 0 190.03 208.85 4.51 o -7 14 0 80.78 77.55 2.26 o -6 14 0 15.51 19.25 1.44 o -5 14 0 1059.34 1063.86 18.31 o -4 14 0 440.16 410.72 6.71 o -3 14 0 4719.61 4695.97 68.12 o -2 14 0 788.93 799.32 13.64 o -1 14 0 219.59 202.51 5.66 o 0 14 0 113.78 105.53 3.44 o -14 15 0 224.18 221.39 8.20 o -13 15 0 36.87 40.19 3.86 o -12 15 0 1.69 7.71 1.59 o -11 15 0 57.64 62.66 2.39 o -10 15 0 290.67 330.52 6.15 o -9 15 0 3.74 5.12 1.16 o -8 15 0 17.77 14.83 1.20 o -7 15 0 799.47 832.87 13.40 o -6 15 0 3868.61 3873.51 55.99 o -5 15 0 640.72 615.97 9.84 o -4 15 0 313.09 335.24 5.93 o -3 15 0 34.83 56.61 6.84 o -2 15 0 1582.00 1533.46 25.04 o -1 15 0 1829.11 1842.62 39.44 o 0 15 0 0.04 7.03 1.32 o -15 16 0 1917.11 1964.27 36.97 o -14 16 0 524.06 566.87 13.97 o -13 16 0 201.93 210.63 5.40 o -12 16 0 2182.53 2082.52 43.23 o -11 16 0 208.05 232.55 5.09 o -10 16 0 14.66 8.29 1.38 o -9 16 0 165.18 152.14 4.11 o -8 16 0 33.53 33.72 1.85 o -7 16 0 451.79 456.60 8.48 o -6 16 0 423.93 422.46 7.68 o -5 16 0 448.22 466.69 8.25 o -4 16 0 2303.41 2340.08 45.64 o -3 16 0 899.88 884.35 20.84 o -2 16 0 272.15 265.30 10.73 o -1 16 0 35.15 32.33 3.30 o 0 16 0 207.84 213.63 9.95 o -16 17 0 250.04 243.53 9.23 o -15 17 0 82.93 93.41 4.53 o -14 17 0 95.59 72.91 3.77 o -13 17 0 67.39 68.32 3.07 o -12 17 0 22.30 10.99 1.42 o -11 17 0 490.29 529.28 15.09 o -10 17 0 588.13 573.53 12.25 o -9 17 0 192.78 187.52 4.48 o -8 17 0 99.17 95.98 3.05 o -7 17 0 402.30 386.83 7.19 o -6 17 0 861.86 836.13 16.60 o -5 17 0 2838.64 2925.66 57.60 o -4 17 0 582.92 575.07 17.16 o -3 17 0 735.57 704.81 21.24 o -2 17 0 835.94 861.58 25.23 o -1 17 0 65.52 82.02 6.72 o 0 17 0 125.43 153.79 9.43 o -17 18 0 79.53 64.18 6.59 o -16 18 0 52.25 47.33 6.46 o -15 18 0 28.54 38.52 4.37 o -14 18 0 238.09 227.34 6.82 o -13 18 0 3894.29 3544.22 72.07 o -12 18 0 460.41 395.79 11.15 o -11 18 0 10.71 6.90 1.57 o -10 18 0 0.50 1.98 1.48 o -9 18 0 543.06 556.88 12.36 o -8 18 0 60.89 54.47 2.07 o -7 18 0 433.24 410.52 11.40 o -6 18 0 168.34 162.76 8.03 o -5 18 0 874.03 911.97 28.82 o -4 18 0 46.85 50.20 5.09 o -3 18 0 94.32 104.32 7.66 o -2 18 0 140.81 151.34 9.89 o -1 18 0 37.66 51.05 11.59 o 0 18 0 468.07 506.36 25.55 o -18 19 0 13.18 1.78 3.53 o -17 19 0 110.03 109.58 7.97 o -16 19 0 205.88 224.35 20.15 o -15 19 0 429.39 381.98 13.01 o -14 19 0 821.03 790.65 23.42 o -13 19 0 30.60 44.90 4.10 o -12 19 0 326.42 312.59 10.23 o -11 19 0 222.36 197.53 6.79 o -10 19 0 10.08 14.43 2.76 o -9 19 0 0.72 3.99 2.48 o -8 19 0 607.82 599.18 13.23 o -7 19 0 24.98 23.86 4.57 o -6 19 0 357.62 378.78 17.20 o -5 19 0 118.86 121.40 7.36 o -4 19 0 121.56 115.01 8.70 o -3 19 0 0.13 0.32 3.95 o -2 19 0 231.55 248.08 11.59 o -1 19 0 9.11 5.43 6.50 o 0 19 0 75.63 81.77 7.57 o -19 20 0 171.31 181.00 11.74 o -18 20 0 45.52 47.60 6.41 o -17 20 0 241.08 278.49 13.71 o -16 20 0 207.66 196.18 17.73 o -15 20 0 420.57 405.11 19.02 o -14 20 0 0.12 3.07 4.70 o -13 20 0 184.34 160.81 7.99 o -12 20 0 466.71 464.55 14.81 o -11 20 0 162.45 147.90 6.38 o -10 20 0 241.40 226.42 8.34 o -9 20 0 3.94 6.14 2.74 o -8 20 0 204.22 211.45 8.42 o -7 20 0 283.67 276.87 13.12 o -6 20 0 769.86 829.04 26.90 o -5 20 0 15.14 13.20 4.55 o -4 20 0 1374.60 1490.27 51.83 o -3 20 0 476.88 476.74 24.32 o -2 20 0 0.29 10.05 8.01 o -1 20 0 96.19 110.40 10.67 o 0 20 0 36.81 28.49 9.17 o -20 21 0 2.63 9.19 9.78 o -19 21 0 170.44 188.59 12.96 o -18 21 0 2.82 1.85 4.34 o -17 21 0 43.56 37.61 6.16 o -16 21 0 39.98 42.21 6.06 o -15 21 0 32.11 27.69 4.96 o -14 21 0 173.88 185.32 9.82 o -13 21 0 26.82 25.10 3.03 o -12 21 0 271.18 273.74 11.11 o -11 21 0 231.87 242.20 9.53 o -10 21 0 77.23 80.14 6.29 o -9 21 0 546.54 566.95 21.73 o -8 21 0 47.74 50.05 5.14 o -7 21 0 67.30 66.93 8.64 o -6 21 0 94.16 112.63 7.07 o -5 21 0 23.69 19.59 4.53 o -4 21 0 269.20 249.03 13.94 o -3 21 0 0.03 4.84 5.54 o -2 21 0 775.52 937.94 46.61 o -1 21 0 23.85 15.09 5.11 o 0 21 0 94.63 92.29 11.64 o -21 22 0 82.57 102.48 10.15 o -20 22 0 605.47 722.48 39.86 o -19 22 0 144.06 152.60 9.72 o -18 22 0 3.20 12.06 5.71 o -17 22 0 30.71 22.15 5.41 o -16 22 0 223.65 209.66 13.54 o -15 22 0 62.05 64.78 7.06 o -14 22 0 72.89 78.89 9.14 o -13 22 0 127.75 126.68 7.00 o -12 22 0 124.81 128.80 8.67 o -11 22 0 98.97 112.74 7.21 o -10 22 0 104.70 111.15 7.20 o -9 22 0 334.94 368.00 14.17 o -8 22 0 20.30 20.99 5.06 o -7 22 0 205.02 160.40 9.42 o -6 22 0 0.94 -1.30 4.07 o -5 22 0 163.63 155.12 11.57 o -4 22 0 33.49 39.39 6.56 o -3 22 0 94.83 113.99 11.07 o -2 22 0 29.69 36.81 6.76 o -1 22 0 12.85 14.23 5.98 o -20 23 0 26.65 19.22 6.26 o -19 23 0 1.05 0.21 5.18 o -18 23 0 3.70 4.76 6.79 o -17 23 0 55.93 44.99 6.77 o -16 23 0 0.32 6.73 9.70 o -15 23 0 19.34 22.45 6.93 o -14 23 0 270.36 306.21 37.54 o -13 23 0 163.74 187.61 10.24 o -12 23 0 79.97 77.84 5.90 o -11 23 0 403.99 408.71 19.58 o -10 23 0 44.92 36.57 5.12 o -9 23 0 210.01 226.26 11.86 o -8 23 0 426.15 453.42 18.80 o -7 23 0 37.76 35.18 4.90 o -6 23 0 153.51 176.58 11.51 o -5 23 0 21.87 15.95 5.51 o -4 23 0 54.12 58.92 9.55 o -3 23 0 411.63 427.94 30.86 o -18 24 0 17.96 19.54 8.80 o -17 24 0 318.14 367.76 20.45 o -16 24 0 5.51 6.57 4.91 o -15 24 0 29.80 40.70 8.85 o -14 24 0 263.03 252.11 17.21 o -13 24 0 30.11 46.64 13.63 o -12 24 0 2.07 5.46 6.53 o -11 24 0 46.49 32.92 10.94 o -10 24 0 373.44 331.04 18.77 o -9 24 0 701.53 838.69 33.83 o -8 24 0 105.53 90.57 7.77 o -7 24 0 38.17 41.01 7.05 o -6 24 0 49.90 44.04 6.20 o -15 25 0 150.74 138.41 14.94 o -14 25 0 263.03 280.01 23.90 o -13 25 0 2.22 0.91 6.11 o -12 25 0 557.45 642.95 30.56 o -11 25 0 299.14 312.39 19.35 o -10 25 0 214.15 228.49 13.01 o 0 1 1 796.75 800.09 9.68 o -1 2 1 7040.26 6408.46 81.21 o 0 2 1 601.74 566.81 7.03 o -2 3 1 595.42 572.51 6.25 o -1 3 1 1982.29 1761.71 20.20 o 0 3 1 3.92 4.68 0.50 o -3 4 1 2238.38 2391.21 25.75 o -2 4 1 3399.18 3468.75 38.37 o -1 4 1 535.56 540.11 6.03 o 0 4 1 11083.45 10948.84 137.26 o -4 5 1 2337.93 2436.88 25.08 o -3 5 1 1291.51 1222.44 12.06 o -2 5 1 2770.87 2718.26 27.81 o -1 5 1 3316.90 3336.34 36.21 o 0 5 1 11.63 15.54 0.77 o -5 6 1 449.81 503.25 4.97 o -4 6 1 7366.12 7656.79 78.25 o -3 6 1 3603.51 3494.80 35.83 o -2 6 1 2393.66 2263.62 23.95 o -1 6 1 3882.46 3927.84 42.51 o 0 6 1 1391.09 1249.16 11.98 o -6 7 1 1245.53 1333.74 12.88 o -5 7 1 9184.68 9192.55 89.87 o -4 7 1 2276.51 2271.40 23.02 o -3 7 1 705.82 660.06 7.00 o -2 7 1 311.16 313.78 3.43 o -1 7 1 2657.10 2670.41 28.32 o 0 7 1 2398.95 2328.91 22.91 o -7 8 1 1552.42 1722.08 15.77 o -6 8 1 2335.04 2504.01 23.01 o -5 8 1 321.56 349.87 3.68 o -4 8 1 463.71 507.20 5.39 o -3 8 1 212.16 233.56 2.88 o -2 8 1 18.81 20.39 1.12 o -1 8 1 721.00 680.98 6.82 o 0 8 1 401.19 351.37 3.88 o -8 9 1 26.42 26.88 0.80 o -7 9 1 4623.04 5347.20 53.92 o -6 9 1 8553.17 9217.15 105.79 o -5 9 1 7003.15 7345.39 75.29 o -4 9 1 858.14 827.96 8.60 o -3 9 1 820.05 826.84 8.82 o -2 9 1 451.73 441.96 4.90 o -1 9 1 2269.67 2263.47 21.84 o 0 9 1 1874.35 1957.52 20.15 o -9 10 1 9.58 15.89 0.74 o -8 10 1 5079.57 5247.41 49.52 o -7 10 1 0.12 1.98 0.67 o -6 10 1 427.41 381.31 4.21 o -5 10 1 120.39 123.73 1.85 o -4 10 1 162.21 226.27 3.06 o -3 10 1 637.07 668.44 7.05 o -2 10 1 0.44 2.56 0.69 o -1 10 1 710.98 761.68 8.31 o 0 10 1 527.95 554.16 6.70 o -10 11 1 243.95 229.71 3.19 o -9 11 1 1958.07 1989.22 19.02 o -8 11 1 1711.06 1944.84 18.90 o -7 11 1 2.21 7.64 0.80 o -6 11 1 4170.65 4182.11 44.61 o -5 11 1 45.08 45.47 1.31 o -4 11 1 5.74 4.63 0.76 o -3 11 1 23.78 21.04 1.21 o -2 11 1 157.21 152.12 3.47 o -1 11 1 1265.02 1174.83 12.82 o 0 11 1 112.95 116.71 2.29 o -11 12 1 12.19 9.41 1.00 o -10 12 1 39.20 44.68 1.26 o -9 12 1 488.65 411.24 4.70 o -8 12 1 346.52 352.43 4.02 o -7 12 1 313.25 353.14 4.16 o -6 12 1 7.68 10.38 0.80 o -5 12 1 1306.25 1339.59 13.91 o -4 12 1 411.98 396.49 5.48 o -3 12 1 1940.69 1886.65 19.69 o -2 12 1 95.77 91.23 2.75 o -1 12 1 487.06 476.76 5.74 o 0 12 1 135.48 126.87 2.51 o -12 13 1 95.73 102.09 2.13 o -11 13 1 221.02 205.80 3.10 o -10 13 1 28.73 26.50 1.20 o -9 13 1 46.89 40.98 1.19 o -8 13 1 551.70 545.51 6.07 o -7 13 1 7.09 5.74 0.91 o -6 13 1 72.77 80.22 1.69 o -5 13 1 155.31 154.49 2.52 o -4 13 1 161.45 154.88 2.50 o -3 13 1 1514.18 1457.36 15.25 o -2 13 1 46.07 46.60 1.60 o -1 13 1 216.34 225.03 3.49 o 0 13 1 2120.35 2059.99 27.66 o -13 14 1 5.68 3.21 0.98 o -12 14 1 24.93 27.77 1.55 o -11 14 1 555.10 526.01 7.33 o -10 14 1 79.94 72.17 1.72 o -9 14 1 1743.69 1719.08 17.73 o -8 14 1 866.54 887.53 10.02 o -7 14 1 230.50 226.09 3.48 o -6 14 1 465.98 497.46 7.15 o -5 14 1 175.00 169.96 2.81 o -4 14 1 1324.35 1340.48 15.61 o -3 14 1 547.13 559.36 7.08 o -2 14 1 3112.91 3175.98 37.97 o -1 14 1 212.97 211.21 3.86 o 0 14 1 55.41 49.90 2.19 o -14 15 1 178.40 172.93 6.18 o -13 15 1 95.18 102.53 3.08 o -12 15 1 29.09 23.96 1.42 o -11 15 1 83.33 72.59 2.58 o -10 15 1 327.96 320.35 5.00 o -9 15 1 761.48 755.37 10.52 o -8 15 1 861.13 865.14 10.69 o -7 15 1 339.10 328.01 4.62 o -6 15 1 111.01 104.31 2.28 o -5 15 1 3339.66 3384.16 34.51 o -4 15 1 2519.33 2548.85 27.44 o -3 15 1 0.03 1.45 1.23 o -2 15 1 2999.26 3042.90 36.30 o -1 15 1 14.75 14.00 1.37 o 0 15 1 243.68 234.00 5.63 o -15 16 1 21.87 23.59 2.22 o -14 16 1 68.74 57.70 2.62 o -13 16 1 50.75 45.97 1.86 o -12 16 1 32.45 20.06 1.35 o -11 16 1 0.04 -0.02 0.90 o -10 16 1 82.95 71.31 2.16 o -9 16 1 22.18 17.74 1.16 o -8 16 1 894.04 853.70 11.10 o -7 16 1 747.91 749.09 9.36 o -6 16 1 2324.86 2341.54 26.67 o -5 16 1 439.00 413.62 6.48 o -4 16 1 7127.92 7294.36 105.05 o -3 16 1 1405.27 1420.24 21.77 o -2 16 1 367.47 369.26 7.39 o -1 16 1 19.79 18.37 1.71 o 0 16 1 0.09 -0.88 1.23 o -16 17 1 125.63 125.05 4.82 o -15 17 1 31.43 16.44 1.88 o -14 17 1 83.84 120.77 3.65 o -13 17 1 220.88 208.48 4.86 o -12 17 1 555.29 523.65 10.96 o -11 17 1 75.40 55.34 2.25 o -10 17 1 170.33 182.44 3.96 o -9 17 1 37.08 37.94 1.68 o -8 17 1 22.50 18.71 1.51 o -7 17 1 900.49 913.43 13.38 o -6 17 1 229.95 217.40 4.28 o -5 17 1 1265.38 1276.51 19.11 o -4 17 1 1847.29 1902.98 31.57 o -3 17 1 16.75 14.48 1.94 o -2 17 1 21.96 15.81 2.54 o -1 17 1 35.53 26.97 2.59 o 0 17 1 309.65 321.87 12.32 o -17 18 1 9.45 9.87 2.69 o -16 18 1 555.03 567.93 16.05 o -15 18 1 508.33 485.72 11.86 o -14 18 1 6.14 8.79 2.25 o -13 18 1 1223.80 1229.78 20.94 o -12 18 1 24.54 15.89 1.32 o -11 18 1 165.74 179.43 5.07 o -10 18 1 255.78 219.79 4.67 o -9 18 1 21.40 17.23 1.10 o -8 18 1 20.03 14.23 1.27 o -7 18 1 117.68 135.69 3.13 o -6 18 1 181.25 177.33 4.39 o -5 18 1 0.06 0.79 1.52 o -4 18 1 100.73 108.08 3.80 o -3 18 1 116.77 125.34 4.45 o -2 18 1 349.09 401.40 11.08 o -1 18 1 38.59 36.14 3.29 o 0 18 1 473.23 504.76 16.22 o -18 19 1 206.89 210.15 9.49 o -17 19 1 0.56 0.68 2.95 o -16 19 1 0.91 2.10 1.86 o -15 19 1 916.88 804.77 18.32 o -14 19 1 64.07 70.81 4.29 o -13 19 1 556.74 565.22 13.76 o -12 19 1 532.04 410.92 10.29 o -11 19 1 36.67 47.30 2.88 o -10 19 1 325.61 299.59 6.57 o -9 19 1 72.00 64.12 3.09 o -8 19 1 1117.92 1127.23 18.22 o -7 19 1 18.71 18.21 1.71 o -6 19 1 7.56 8.60 1.72 o -5 19 1 473.75 484.23 15.28 o -4 19 1 319.81 329.26 8.86 o -3 19 1 266.10 284.65 11.58 o -2 19 1 449.46 465.23 15.72 o -1 19 1 73.10 71.84 4.85 o 0 19 1 99.83 94.21 6.31 o -19 20 1 462.10 466.68 22.63 o -18 20 1 29.64 34.08 4.69 o -17 20 1 47.27 41.42 5.03 o -16 20 1 161.35 180.06 8.15 o -15 20 1 191.27 185.92 9.48 o -14 20 1 78.77 45.04 3.77 o -13 20 1 172.21 165.07 6.52 o -12 20 1 160.19 152.00 6.14 o -11 20 1 5.34 5.41 2.14 o -10 20 1 603.85 602.46 13.16 o -9 20 1 86.37 87.81 4.64 o -8 20 1 144.91 125.93 4.21 o -7 20 1 74.05 66.75 5.20 o -6 20 1 11.31 9.58 2.42 o -5 20 1 96.79 110.78 5.36 o -4 20 1 14.18 6.51 3.73 o -3 20 1 68.00 74.88 5.37 o -2 20 1 15.90 17.65 5.45 o -1 20 1 0.39 2.23 3.34 o 0 20 1 5.97 10.39 3.73 o -20 21 1 102.40 81.60 7.36 o -19 21 1 0.27 0.85 3.87 o -18 21 1 0.52 1.48 4.47 o -17 21 1 5.66 6.55 4.41 o -16 21 1 0.13 -2.23 3.12 o -15 21 1 2.08 8.60 2.50 o -14 21 1 84.92 64.68 4.40 o -13 21 1 19.50 21.58 3.14 o -12 21 1 27.82 22.78 4.22 o -11 21 1 14.59 23.49 2.65 o -10 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91.72 1.86 o -5 10 3 133.90 142.37 2.55 o -4 10 3 1569.68 1601.28 20.72 o -3 10 3 0.11 2.50 0.75 o -2 10 3 1.25 3.20 0.89 o -1 10 3 34.59 33.56 1.17 o 0 10 3 18.24 15.51 1.03 o -10 11 3 228.32 217.96 3.94 o -9 11 3 481.95 500.44 6.86 o -8 11 3 342.77 409.18 5.06 o -7 11 3 52.87 47.95 1.59 o -6 11 3 2856.66 2843.99 32.70 o -5 11 3 150.38 156.30 3.53 o -4 11 3 372.51 351.64 4.93 o -3 11 3 122.63 108.00 2.41 o -2 11 3 498.05 475.44 5.88 o -1 11 3 49.68 46.61 2.23 o 0 11 3 727.09 721.64 10.20 o -11 12 3 82.71 77.26 2.31 o -10 12 3 178.55 190.80 3.62 o -9 12 3 0.67 7.89 0.95 o -8 12 3 1537.84 1542.65 20.77 o -7 12 3 618.46 626.96 8.83 o -6 12 3 0.10 10.82 1.20 o -5 12 3 442.06 448.76 6.67 o -4 12 3 113.66 114.77 3.52 o -3 12 3 1925.65 1898.83 23.63 o -2 12 3 761.63 733.18 11.57 o -1 12 3 18.13 19.08 1.41 o 0 12 3 609.63 660.01 9.76 o -12 13 3 141.16 140.54 3.25 o -11 13 3 261.22 256.10 5.48 o -10 13 3 426.44 425.99 7.30 o -9 13 3 565.40 570.13 8.85 o -8 13 3 1155.00 1100.76 15.10 o -7 13 3 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