#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2207421.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207421_Fobs loop_ _publ_author_name 'Fan, Zhi' 'Diao, Chun-Hua' 'Guo, Min-Jie' 'Yu, Ming' 'Chen, Xin' _publ_section_title ; 3,3'-Dihydroxy-4,4'-(propane-1,3-diyldioxy)dibenzaldehyde ; _journal_coeditor_code AT6046 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4004 _journal_page_last o4005 _journal_volume 61 _journal_year 2005 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 22.2474 _cell_length_b 31.1755 _cell_length_c 4.8562 _exptl_crystal_F_000 1456.00 _reflns_d_resolution_high 0.8056 _[local]_cod_data_source_file at6046Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50930D in Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 373.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 39348.32 37392.84 658.40 o 8 0 0 759.09 661.76 18.24 o 12 0 0 13313.52 13825.63 195.15 o 16 0 0 38.00 22.70 16.29 o 20 0 0 3.35 -20.55 20.55 o 24 0 0 227.40 179.36 43.88 o 2 2 0 3601.89 3434.80 47.46 o 4 2 0 3444.32 3468.19 50.82 o 6 2 0 24530.54 22400.59 357.36 o 8 2 0 7005.99 6555.36 66.59 o 10 2 0 801.32 791.58 15.82 o 12 2 0 378.18 423.81 13.66 o 14 2 0 737.75 722.80 18.32 o 16 2 0 666.91 708.17 27.12 o 18 2 0 468.74 448.60 27.39 o 20 2 0 111.69 151.45 31.55 o 22 2 0 0.30 -1.77 19.63 o 24 2 0 13.48 9.80 23.58 o 26 2 0 0.04 -10.76 27.48 o 0 4 0 5144.73 4927.70 95.88 o 2 4 0 76907.03 75880.68 936.69 o 4 4 0 3011.82 3007.94 66.14 o 6 4 0 375.69 331.01 9.99 o 8 4 0 3361.27 3167.71 43.25 o 10 4 0 490.17 493.79 12.95 o 12 4 0 2338.07 2384.88 33.78 o 14 4 0 4550.41 4640.57 56.25 o 16 4 0 392.29 402.07 19.39 o 18 4 0 0.76 -2.31 15.29 o 20 4 0 35.23 42.85 18.52 o 22 4 0 24.66 -0.50 20.79 o 24 4 0 971.98 1044.76 46.44 o 26 4 0 151.30 161.04 33.86 o 2 6 0 3523.91 3232.27 39.78 o 4 6 0 72536.62 69321.22 1886.04 o 6 6 0 7973.01 7636.82 92.58 o 8 6 0 2760.21 2679.23 47.23 o 10 6 0 2727.02 2713.62 42.09 o 12 6 0 925.44 864.90 18.84 o 14 6 0 10355.81 10596.52 109.89 o 16 6 0 1105.18 1114.27 24.62 o 18 6 0 531.20 564.81 24.17 o 20 6 0 140.24 161.77 23.64 o 22 6 0 265.37 281.70 53.20 o 24 6 0 93.49 77.89 25.65 o 26 6 0 603.33 778.49 53.15 o 0 8 0 75480.28 71293.72 1538.31 o 2 8 0 571.80 557.75 18.00 o 4 8 0 403.38 398.34 11.76 o 6 8 0 1192.91 1061.39 20.89 o 8 8 0 6019.54 5656.04 291.69 o 10 8 0 2031.28 1997.79 34.49 o 12 8 0 35.00 32.09 14.93 o 14 8 0 493.73 481.58 23.26 o 16 8 0 776.49 805.57 21.45 o 18 8 0 93.05 66.66 16.39 o 20 8 0 92.59 94.29 21.21 o 22 8 0 31.53 19.06 36.66 o 24 8 0 206.98 171.20 30.05 o 26 8 0 712.68 786.36 53.51 o 2 10 0 53.04 74.89 6.02 o 4 10 0 9109.85 9014.56 103.13 o 6 10 0 1715.43 1680.78 29.02 o 8 10 0 4364.02 4007.16 55.31 o 10 10 0 6762.07 6834.07 86.45 o 12 10 0 3541.99 3659.07 55.55 o 14 10 0 3818.12 3824.28 59.56 o 16 10 0 1505.40 1561.11 30.65 o 18 10 0 156.95 129.26 16.72 o 20 10 0 14.30 15.20 21.03 o 22 10 0 10.38 24.68 21.17 o 24 10 0 772.35 834.38 47.50 o 26 10 0 108.61 123.75 48.92 o 0 12 0 49169.05 48003.07 771.89 o 2 12 0 838.79 877.83 17.05 o 4 12 0 1368.54 1263.39 32.18 o 6 12 0 54.10 51.08 7.81 o 8 12 0 1052.31 1044.01 24.01 o 10 12 0 95.45 83.37 10.70 o 12 12 0 3227.10 3468.90 54.85 o 14 12 0 1209.90 1161.12 30.08 o 16 12 0 327.04 372.88 43.70 o 18 12 0 555.48 478.80 24.31 o 20 12 0 214.76 234.21 27.03 o 22 12 0 243.00 294.82 32.02 o 24 12 0 364.55 404.60 57.83 o 26 12 0 74.87 100.35 48.62 o 2 14 0 289.20 250.17 10.56 o 4 14 0 29936.54 30749.68 325.29 o 6 14 0 309.19 247.60 23.04 o 8 14 0 704.48 680.44 20.19 o 10 14 0 794.37 863.07 23.86 o 12 14 0 475.07 471.85 36.50 o 14 14 0 813.18 793.32 25.45 o 16 14 0 1535.94 1469.18 47.06 o 18 14 0 421.84 492.48 34.69 o 20 14 0 63.96 89.57 24.10 o 22 14 0 68.82 34.22 26.46 o 24 14 0 7.78 35.01 28.15 o 0 16 0 260.70 321.78 14.95 o 2 16 0 11133.75 12616.50 126.02 o 4 16 0 3638.02 3763.30 55.82 o 6 16 0 2910.67 3119.71 51.28 o 8 16 0 2781.21 2627.55 45.22 o 10 16 0 2667.20 2516.33 45.33 o 12 16 0 694.80 694.93 24.16 o 14 16 0 1635.82 1637.80 37.92 o 16 16 0 1236.16 1234.73 44.24 o 18 16 0 412.79 431.91 34.38 o 20 16 0 42.67 40.01 22.99 o 22 16 0 107.70 142.37 29.49 o 24 16 0 226.07 216.56 36.92 o 2 18 0 927.33 1003.54 23.95 o 4 18 0 6.20 11.86 8.70 o 6 18 0 198.87 218.49 15.11 o 8 18 0 5730.85 5853.58 81.71 o 10 18 0 44.81 13.57 11.16 o 12 18 0 466.42 461.29 21.55 o 14 18 0 1631.19 1719.05 66.34 o 16 18 0 0.08 -8.76 17.92 o 18 18 0 2127.76 2212.92 64.44 o 20 18 0 7.41 -21.42 21.76 o 22 18 0 31.60 36.50 28.37 o 24 18 0 82.27 21.50 31.61 o 0 20 0 1125.31 975.49 32.08 o 2 20 0 524.61 539.90 17.37 o 4 20 0 359.80 382.66 17.66 o 6 20 0 731.44 740.43 24.34 o 8 20 0 55.12 50.60 11.41 o 10 20 0 1472.85 1471.67 46.44 o 12 20 0 1746.28 1737.40 40.59 o 14 20 0 657.80 610.70 26.35 o 16 20 0 930.74 911.12 56.65 o 18 20 0 2669.05 2785.56 202.93 o 20 20 0 216.15 186.05 29.87 o 22 20 0 392.32 408.40 89.45 o 2 22 0 1128.07 1135.18 26.05 o 4 22 0 59.83 89.82 13.01 o 6 22 0 220.17 175.95 16.02 o 8 22 0 825.73 846.17 28.19 o 10 22 0 4431.34 4474.78 72.44 o 12 22 0 1972.99 1879.49 43.82 o 14 22 0 670.42 650.61 34.15 o 16 22 0 1796.07 1784.16 58.41 o 18 22 0 95.03 105.02 26.50 o 20 22 0 67.10 57.30 37.08 o 22 22 0 86.59 57.90 40.63 o 0 24 0 14.01 15.82 14.12 o 2 24 0 0.07 1.81 11.62 o 4 24 0 1457.29 1523.23 37.35 o 6 24 0 1374.71 1485.60 37.61 o 8 24 0 3327.87 3431.95 72.25 o 10 24 0 4033.35 4118.88 70.80 o 12 24 0 1356.76 1478.99 40.55 o 14 24 0 73.53 52.75 17.58 o 16 24 0 21.55 7.83 23.21 o 18 24 0 6.65 17.27 26.05 o 20 24 0 185.88 255.34 72.31 o 2 26 0 20.07 10.15 13.07 o 4 26 0 142.48 72.44 14.78 o 6 26 0 227.36 217.93 20.05 o 8 26 0 5553.28 5613.63 88.34 o 10 26 0 161.36 140.25 20.29 o 12 26 0 1944.16 1935.76 47.68 o 14 26 0 48.18 96.65 22.58 o 16 26 0 252.14 291.57 52.36 o 18 26 0 4.89 -26.62 26.62 o 20 26 0 57.97 52.26 32.89 o 0 28 0 1383.17 1428.99 47.69 o 2 28 0 869.42 767.05 28.66 o 4 28 0 978.77 871.30 31.00 o 6 28 0 17.01 38.51 16.30 o 8 28 0 216.25 258.00 44.04 o 10 28 0 1357.86 1323.64 40.33 o 12 28 0 11.31 -17.71 17.71 o 14 28 0 283.71 250.64 39.25 o 16 28 0 1.24 34.81 28.17 o 18 28 0 156.02 162.41 33.87 o 2 30 0 40.73 22.06 15.60 o 4 30 0 26.12 14.10 13.66 o 6 30 0 3020.33 2955.11 61.23 o 8 30 0 95.05 78.77 20.05 o 10 30 0 65.12 81.09 28.38 o 12 30 0 182.23 187.24 26.18 o 14 30 0 19.65 18.14 27.70 o 16 30 0 26.82 -25.08 29.68 o 0 32 0 565.61 537.03 46.78 o 2 32 0 682.72 624.74 29.78 o 4 32 0 86.35 102.93 21.51 o 6 32 0 466.76 456.13 40.23 o 8 32 0 0.30 -22.83 22.83 o 10 32 0 28.90 29.96 20.22 o 12 32 0 5.83 9.34 22.53 o 14 32 0 1.09 -13.57 30.02 o 2 34 0 9.73 -0.48 23.67 o 4 34 0 13.87 24.53 18.19 o 6 34 0 0.70 8.02 17.86 o 8 34 0 17.06 -3.04 33.19 o 10 34 0 21.71 31.90 23.59 o 12 34 0 64.23 51.26 26.07 o 0 36 0 64.88 24.40 34.62 o 2 36 0 38.15 53.23 34.14 o 4 36 0 45.52 88.45 22.26 o 6 36 0 124.88 103.65 24.21 o 8 36 0 8.05 17.41 35.07 o 10 36 0 802.78 945.42 42.08 o 2 38 0 38.45 43.69 28.81 o 4 38 0 32.48 4.78 29.76 o 1 1 1 4504.42 4717.17 39.85 o 3 1 1 32797.43 33406.80 225.75 o 5 1 1 139190.86 146125.95 1629.72 o 7 1 1 9595.95 9204.56 64.68 o 9 1 1 4603.54 4696.30 49.40 o 11 1 1 854.93 761.77 12.69 o 13 1 1 1338.60 1281.60 20.57 o 15 1 1 27.65 23.41 7.23 o 17 1 1 1167.48 1197.52 22.76 o 19 1 1 377.54 367.16 16.41 o 21 1 1 318.89 333.15 17.28 o 23 1 1 379.30 404.92 37.95 o 25 1 1 48.90 30.30 19.81 o 27 1 1 15.98 -21.87 21.87 o 1 3 1 905.29 984.63 9.41 o 3 3 1 91376.20 93421.91 1380.13 o 5 3 1 15543.99 15958.28 105.35 o 7 3 1 23262.20 23570.66 164.68 o 9 3 1 2989.29 3035.90 27.46 o 11 3 1 2418.76 2526.07 24.62 o 13 3 1 1777.65 1702.00 21.49 o 15 3 1 578.64 568.62 15.06 o 17 3 1 238.11 237.62 13.86 o 19 3 1 1001.15 981.55 25.86 o 21 3 1 1272.59 1255.66 29.19 o 23 3 1 579.10 614.22 29.56 o 25 3 1 140.31 129.96 21.66 o 27 3 1 41.62 0.23 21.03 o 1 5 1 18256.38 18101.46 131.96 o 3 5 1 1871.27 1627.84 14.86 o 5 5 1 1522.43 1447.82 14.47 o 7 5 1 427.90 386.45 8.10 o 9 5 1 11165.72 11533.34 81.27 o 11 5 1 2096.58 2275.24 25.68 o 13 5 1 1102.97 1136.93 19.59 o 15 5 1 319.25 310.75 19.49 o 17 5 1 549.32 542.03 16.63 o 19 5 1 199.32 185.55 17.34 o 21 5 1 605.27 656.01 22.69 o 23 5 1 641.20 681.21 27.36 o 25 5 1 73.60 99.49 20.78 o 27 5 1 20.36 -21.45 21.45 o 1 7 1 7091.63 6738.29 50.78 o 3 7 1 19934.21 20305.29 132.18 o 5 7 1 3863.01 3836.02 30.52 o 7 7 1 8165.81 8244.91 63.76 o 9 7 1 8768.66 9181.66 66.10 o 11 7 1 2296.82 2424.24 25.73 o 13 7 1 420.70 485.37 13.71 o 15 7 1 495.94 483.71 14.72 o 17 7 1 895.78 927.03 20.87 o 19 7 1 1057.70 1052.69 23.51 o 21 7 1 902.58 937.22 26.47 o 23 7 1 368.61 375.34 28.07 o 25 7 1 52.17 49.44 19.38 o 1 9 1 4747.03 4531.08 34.56 o 3 9 1 903.83 972.89 11.78 o 5 9 1 4988.16 5086.04 36.68 o 7 9 1 12839.04 13827.36 94.47 o 9 9 1 662.97 695.53 11.56 o 11 9 1 2975.19 3089.18 31.10 o 13 9 1 819.32 847.83 17.67 o 15 9 1 610.59 573.64 16.06 o 17 9 1 978.37 959.55 21.31 o 19 9 1 1275.23 1315.21 26.56 o 21 9 1 93.77 78.88 14.72 o 23 9 1 17.52 31.90 18.81 o 25 9 1 76.22 77.51 20.79 o 1 11 1 10930.47 10745.15 74.43 o 3 11 1 1018.28 977.68 13.08 o 5 11 1 17838.41 18720.17 117.47 o 7 11 1 4342.78 4642.35 35.59 o 9 11 1 2841.99 2964.62 29.74 o 11 11 1 1777.81 1712.78 23.80 o 13 11 1 304.24 339.38 17.30 o 15 11 1 123.02 108.33 10.49 o 17 11 1 17.98 19.99 9.48 o 19 11 1 555.40 525.92 18.88 o 21 11 1 341.48 369.63 30.10 o 23 11 1 119.40 156.26 38.67 o 25 11 1 81.08 104.01 22.50 o 1 13 1 3971.83 4009.24 33.06 o 3 13 1 3953.68 4098.74 31.70 o 5 13 1 1822.10 1772.04 17.91 o 7 13 1 86.55 99.84 6.32 o 9 13 1 4805.95 4650.95 42.25 o 11 13 1 526.83 518.73 13.77 o 13 13 1 583.89 620.83 17.72 o 15 13 1 666.42 668.45 18.07 o 17 13 1 1636.93 1667.36 29.33 o 19 13 1 215.22 225.73 22.37 o 21 13 1 71.39 80.51 15.84 o 23 13 1 139.36 142.13 21.69 o 25 13 1 44.92 38.32 24.59 o 1 15 1 1676.26 1694.23 18.36 o 3 15 1 11181.64 11601.42 82.13 o 5 15 1 2827.98 2958.35 26.20 o 7 15 1 746.24 809.12 14.88 o 9 15 1 2552.30 2535.39 28.05 o 11 15 1 674.00 715.77 16.26 o 13 15 1 689.86 666.06 19.11 o 15 15 1 723.95 697.24 21.25 o 17 15 1 472.45 480.89 18.65 o 19 15 1 371.00 438.83 21.18 o 21 15 1 817.95 848.39 27.32 o 23 15 1 21.53 13.58 19.68 o 25 15 1 9.69 20.42 25.71 o 1 17 1 9079.88 9548.76 69.85 o 3 17 1 247.74 215.34 12.15 o 5 17 1 2672.49 2621.46 27.83 o 7 17 1 1709.64 1762.78 23.26 o 9 17 1 728.58 744.87 16.84 o 11 17 1 2512.37 2396.13 44.04 o 13 17 1 336.56 355.69 16.86 o 15 17 1 165.06 153.87 14.14 o 17 17 1 103.41 119.87 14.50 o 19 17 1 196.03 245.00 24.55 o 21 17 1 311.62 379.99 23.13 o 23 17 1 120.81 154.02 38.55 o 1 19 1 1484.88 1549.79 25.55 o 3 19 1 60.43 65.75 7.96 o 5 19 1 556.02 574.28 13.85 o 7 19 1 1014.49 1006.51 17.94 o 9 19 1 1220.19 1296.84 24.26 o 11 19 1 2907.29 2972.33 42.06 o 13 19 1 1528.65 1462.03 37.59 o 15 19 1 754.95 680.73 26.59 o 17 19 1 685.25 627.50 22.68 o 19 19 1 493.48 581.73 24.94 o 21 19 1 741.58 776.50 28.12 o 23 19 1 343.47 394.78 36.06 o 1 21 1 480.17 487.42 14.44 o 3 21 1 125.01 89.11 8.36 o 5 21 1 1273.15 1291.05 21.16 o 7 21 1 4719.84 4704.89 51.19 o 9 21 1 21.72 3.70 11.55 o 11 21 1 1297.02 1294.61 27.53 o 13 21 1 1482.03 1486.50 31.05 o 15 21 1 129.24 123.13 15.49 o 17 21 1 223.79 219.84 18.73 o 19 21 1 91.97 62.33 18.32 o 21 21 1 136.00 148.67 39.33 o 1 23 1 528.60 477.90 15.41 o 3 23 1 2660.59 2655.02 35.53 o 5 23 1 3703.25 3690.32 44.65 o 7 23 1 598.65 587.53 17.44 o 9 23 1 515.89 488.14 17.18 o 11 23 1 490.78 513.28 17.94 o 13 23 1 2008.08 2084.62 38.16 o 15 23 1 1674.90 1710.73 35.58 o 17 23 1 8.07 -10.38 15.04 o 19 23 1 286.83 278.14 24.89 o 21 23 1 109.61 129.65 23.09 o 1 25 1 1143.43 1183.72 23.53 o 3 25 1 1548.11 1535.23 27.25 o 5 25 1 4131.89 4031.45 48.88 o 7 25 1 1864.28 1815.60 30.59 o 9 25 1 651.59 645.50 19.62 o 11 25 1 279.77 249.77 18.02 o 13 25 1 449.82 432.81 25.31 o 15 25 1 923.54 932.74 28.26 o 17 25 1 355.37 427.42 30.78 o 19 25 1 42.54 6.64 24.22 o 1 27 1 8.52 -9.26 9.26 o 3 27 1 339.99 317.30 15.96 o 5 27 1 372.34 381.16 16.16 o 7 27 1 91.81 72.12 13.39 o 9 27 1 156.58 178.53 14.72 o 11 27 1 211.18 251.46 18.61 o 13 27 1 348.77 347.65 22.73 o 15 27 1 496.52 600.88 38.10 o 17 27 1 123.66 86.56 20.76 o 19 27 1 30.76 3.47 25.08 o 1 29 1 1634.60 1527.08 28.97 o 3 29 1 413.04 406.55 23.29 o 5 29 1 406.00 348.08 18.01 o 7 29 1 211.38 195.62 17.57 o 9 29 1 446.46 481.75 28.30 o 11 29 1 878.09 886.90 29.32 o 13 29 1 382.29 436.63 24.70 o 15 29 1 147.08 115.96 20.22 o 17 29 1 36.44 6.32 22.54 o 1 31 1 299.44 251.23 16.50 o 3 31 1 79.96 102.91 12.87 o 5 31 1 747.13 738.23 25.11 o 7 31 1 109.51 84.09 14.31 o 9 31 1 183.16 178.42 19.27 o 11 31 1 476.11 486.04 25.46 o 13 31 1 39.87 -1.35 18.20 o 15 31 1 57.86 52.66 30.41 o 1 33 1 358.16 319.85 18.68 o 3 33 1 144.38 72.58 14.31 o 5 33 1 20.72 -9.39 14.94 o 7 33 1 80.41 65.24 16.92 o 9 33 1 70.40 74.31 24.27 o 11 33 1 45.18 47.11 18.94 o 13 33 1 63.09 72.36 22.37 o 1 35 1 62.38 75.47 15.32 o 3 35 1 72.36 115.03 17.56 o 5 35 1 56.45 50.58 16.36 o 7 35 1 141.94 178.26 21.16 o 9 35 1 44.39 35.75 20.76 o 1 37 1 49.92 29.15 16.23 o 3 37 1 19.11 6.13 17.74 o 5 37 1 239.87 232.29 22.50 o 2 0 2 2832.92 2813.55 29.60 o 6 0 2 2231.31 2150.04 34.03 o 10 0 2 29371.38 28849.61 270.40 o 14 0 2 1989.93 2015.46 35.46 o 18 0 2 1157.98 1167.34 35.14 o 22 0 2 364.69 406.71 61.32 o 26 0 2 72.90 146.89 46.88 o 0 2 2 4159.52 4101.66 54.27 o 2 2 2 527.63 517.91 9.83 o 4 2 2 978.00 954.02 12.28 o 6 2 2 53.50 43.73 3.85 o 8 2 2 16614.74 16393.27 112.29 o 10 2 2 11935.92 12124.00 87.46 o 12 2 2 1499.91 1427.82 19.55 o 14 2 2 920.01 877.58 16.37 o 16 2 2 2620.80 2591.39 31.51 o 18 2 2 1770.98 1752.41 29.87 o 20 2 2 1168.17 1136.72 28.15 o 22 2 2 347.98 297.78 23.31 o 24 2 2 176.51 178.40 23.12 o 26 2 2 1.43 -15.81 31.01 o 2 4 2 1378.74 1245.50 13.31 o 4 4 2 3505.09 3718.47 29.11 o 6 4 2 19220.13 20539.89 128.49 o 8 4 2 5200.53 5423.24 47.55 o 10 4 2 3377.28 3320.68 31.66 o 12 4 2 1297.71 1380.28 19.27 o 14 4 2 1179.48 1134.80 18.45 o 16 4 2 560.49 541.78 14.88 o 18 4 2 1670.86 1693.19 44.73 o 20 4 2 157.02 151.07 16.25 o 22 4 2 77.41 56.03 18.85 o 24 4 2 121.42 141.05 26.47 o 0 6 2 6267.37 6658.84 77.25 o 2 6 2 1581.02 1495.25 15.48 o 4 6 2 12098.56 13101.50 96.42 o 6 6 2 3877.16 3871.21 28.71 o 8 6 2 220.38 187.21 6.82 o 10 6 2 2457.70 2463.23 26.09 o 12 6 2 533.22 594.18 13.27 o 14 6 2 448.43 435.94 12.61 o 16 6 2 2223.48 2240.21 30.61 o 18 6 2 447.03 444.86 22.97 o 20 6 2 112.69 124.58 15.62 o 22 6 2 128.37 109.32 17.50 o 24 6 2 128.59 174.71 27.65 o 2 8 2 12150.89 12554.19 81.63 o 4 8 2 8339.29 8696.75 59.45 o 6 8 2 8251.32 8886.48 61.27 o 8 8 2 3161.38 3200.10 27.96 o 10 8 2 2520.74 2572.42 27.20 o 12 8 2 2203.89 2171.59 25.51 o 14 8 2 374.09 327.58 12.28 o 16 8 2 679.72 649.89 18.54 o 18 8 2 9.33 17.56 12.11 o 20 8 2 189.24 160.40 16.27 o 22 8 2 89.96 91.32 16.97 o 24 8 2 63.88 90.20 40.70 o 0 10 2 1530.34 1521.26 38.97 o 2 10 2 3214.26 3618.20 29.58 o 4 10 2 1946.02 2093.35 21.37 o 6 10 2 322.75 340.68 11.06 o 8 10 2 62.29 57.96 5.64 o 10 10 2 4648.52 4892.54 43.06 o 12 10 2 215.24 219.96 10.62 o 14 10 2 1049.86 1013.78 18.23 o 16 10 2 244.21 249.59 15.50 o 18 10 2 588.22 590.88 22.61 o 20 10 2 113.26 127.19 16.61 o 22 10 2 34.45 43.75 16.41 o 24 10 2 57.40 88.18 30.01 o 2 12 2 1049.61 1080.68 13.98 o 4 12 2 2163.91 2191.13 23.54 o 6 12 2 1143.72 1128.96 15.74 o 8 12 2 79.63 103.38 10.72 o 10 12 2 450.84 422.60 10.50 o 12 12 2 2347.90 2371.27 28.49 o 14 12 2 119.62 94.65 10.24 o 16 12 2 167.07 171.09 20.35 o 18 12 2 256.83 227.25 17.33 o 20 12 2 507.64 539.97 24.69 o 22 12 2 287.27 315.01 36.57 o 24 12 2 345.29 402.17 29.72 o 0 14 2 3255.99 3092.97 41.56 o 2 14 2 4926.27 5109.22 38.18 o 4 14 2 2382.08 2342.36 23.29 o 6 14 2 592.73 645.71 12.58 o 8 14 2 3681.35 3852.40 36.02 o 10 14 2 434.35 404.37 11.61 o 12 14 2 759.60 696.00 16.74 o 14 14 2 512.30 531.01 17.56 o 16 14 2 138.55 127.66 16.97 o 18 14 2 113.48 101.00 17.68 o 20 14 2 23.43 8.29 14.81 o 22 14 2 37.80 46.59 17.57 o 24 14 2 75.39 32.94 21.78 o 2 16 2 2365.83 2346.73 23.76 o 4 16 2 4438.85 4469.53 37.31 o 6 16 2 2818.45 2711.20 28.44 o 8 16 2 1789.69 1811.06 23.30 o 10 16 2 44.45 27.25 8.27 o 12 16 2 1301.92 1260.49 23.98 o 14 16 2 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13 3 3 9076.51 9003.55 87.42 o 15 3 3 114.91 99.34 12.70 o 17 3 3 715.30 684.71 21.99 o 19 3 3 216.92 213.72 16.43 o 21 3 3 90.45 86.66 30.73 o 23 3 3 55.63 43.54 22.54 o 1 5 3 2818.32 2787.78 26.85 o 3 5 3 1531.83 1635.73 18.47 o 5 5 3 654.36 641.74 11.60 o 7 5 3 280.69 307.37 10.06 o 9 5 3 1027.09 984.54 20.76 o 11 5 3 1065.87 1010.12 32.91 o 13 5 3 3352.81 3257.87 48.24 o 15 5 3 392.82 368.80 19.42 o 17 5 3 350.84 351.09 18.04 o 19 5 3 63.20 40.81 13.72 o 21 5 3 77.06 60.00 20.31 o 23 5 3 21.81 -4.28 20.31 o 1 7 3 8979.40 9241.53 66.82 o 3 7 3 1772.84 1949.33 20.90 o 5 7 3 125.50 117.45 7.02 o 7 7 3 81.73 71.07 6.93 o 9 7 3 329.71 362.18 12.64 o 11 7 3 3726.58 3533.95 52.70 o 13 7 3 489.05 499.12 18.47 o 15 7 3 529.07 488.64 19.01 o 17 7 3 54.04 72.59 13.00 o 19 7 3 21.15 -11.72 13.28 o 21 7 3 3.48 -7.34 18.53 o 23 7 3 2.05 -22.47 22.47 o 1 9 3 2811.66 3046.94 31.04 o 3 9 3 1765.98 1673.28 21.32 o 5 9 3 53.21 40.88 6.20 o 7 9 3 1423.19 1367.19 19.55 o 9 9 3 2615.09 2628.87 32.31 o 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-17.81 18.91 o 3 33 3 191.19 175.67 32.56 o 0 0 4 1957.74 1993.77 56.13 o 4 0 4 198.40 179.11 23.89 o 8 0 4 5534.61 5540.11 150.57 o 12 0 4 255.61 237.04 27.96 o 16 0 4 425.19 412.31 35.45 o 20 0 4 1246.39 1160.28 44.60 o 2 2 4 422.17 425.44 15.52 o 4 2 4 488.85 464.76 22.59 o 6 2 4 2258.42 2209.09 44.29 o 8 2 4 1467.59 1504.05 37.11 o 10 2 4 1256.50 1218.87 34.56 o 12 2 4 192.16 162.21 16.11 o 14 2 4 27.80 22.85 13.87 o 16 2 4 51.12 23.71 14.18 o 18 2 4 355.47 308.60 21.24 o 20 2 4 263.90 204.96 20.51 o 0 4 4 998.74 1007.10 27.86 o 2 4 4 121.46 111.55 10.46 o 4 4 4 219.11 236.65 17.87 o 6 4 4 389.74 395.46 24.61 o 8 4 4 935.26 935.99 31.81 o 10 4 4 948.99 978.76 31.11 o 12 4 4 16.27 28.15 13.17 o 14 4 4 41.72 3.16 13.42 o 16 4 4 749.89 760.41 27.46 o 18 4 4 496.45 459.76 25.75 o 20 4 4 307.97 349.53 23.00 o 2 6 4 377.46 415.48 15.52 o 4 6 4 93.25 80.36 13.40 o 6 6 4 3678.31 3642.48 59.55 o 8 6 4 567.81 560.25 28.69 o 10 6 4 377.81 399.13 20.60 o 12 6 4 349.75 432.43 22.12 o 14 6 4 15.14 10.00 14.06 o 16 6 4 624.34 596.38 26.51 o 18 6 4 196.52 172.12 19.77 o 20 6 4 82.64 52.90 18.32 o 0 8 4 482.89 499.40 22.14 o 2 8 4 41.80 29.32 9.50 o 4 8 4 1188.23 1206.43 25.58 o 6 8 4 11.04 16.04 13.13 o 8 8 4 885.67 849.83 24.71 o 10 8 4 523.49 516.65 21.63 o 12 8 4 9.29 8.62 13.53 o 14 8 4 194.27 193.82 18.55 o 16 8 4 222.84 187.11 19.39 o 18 8 4 144.15 123.31 19.84 o 2 10 4 329.71 340.35 15.30 o 4 10 4 1889.23 1951.73 34.54 o 6 10 4 70.94 75.35 15.05 o 8 10 4 306.06 286.65 31.62 o 10 10 4 41.05 20.21 12.40 o 12 10 4 83.76 51.78 14.59 o 14 10 4 21.07 -13.86 13.86 o 16 10 4 152.50 176.27 18.92 o 18 10 4 101.47 84.99 19.56 o 0 12 4 816.55 813.54 26.25 o 2 12 4 175.78 165.81 12.49 o 4 12 4 94.10 68.63 13.55 o 6 12 4 2.86 -1.60 10.91 o 8 12 4 575.02 523.39 21.86 o 10 12 4 555.60 541.75 22.94 o 12 12 4 45.12 20.39 14.79 o 14 12 4 95.74 62.59 16.53 o 16 12 4 83.24 92.07 18.65 o 18 12 4 9.50 -15.95 20.80 o 2 14 4 41.32 35.19 13.30 o 4 14 4 410.99 397.42 18.03 o 6 14 4 751.09 726.72 21.97 o 8 14 4 114.02 117.81 17.79 o 10 14 4 19.49 23.60 14.09 o 12 14 4 417.35 468.31 29.54 o 14 14 4 34.38 22.81 16.02 o 16 14 4 17.94 -17.03 17.03 o 18 14 4 220.27 189.45 29.96 o 0 16 4 256.51 247.39 23.03 o 2 16 4 557.28 567.40 20.27 o 4 16 4 412.99 433.96 17.88 o 6 16 4 41.35 21.63 12.15 o 8 16 4 75.52 102.93 19.13 o 10 16 4 60.01 35.40 16.21 o 12 16 4 28.76 8.13 14.99 o 14 16 4 2.23 -13.44 18.32 o 16 16 4 122.20 95.41 22.32 o 2 18 4 248.23 235.49 20.31 o 4 18 4 668.88 684.48 26.71 o 6 18 4 937.35 893.64 26.85 o 8 18 4 964.86 952.73 31.17 o 10 18 4 88.26 55.19 20.93 o 12 18 4 81.75 62.78 19.35 o 14 18 4 65.05 38.94 20.53 o 16 18 4 486.08 552.87 33.33 o 0 20 4 857.74 807.79 28.02 o 2 20 4 1026.01 1065.85 32.77 o 4 20 4 140.90 168.41 17.60 o 6 20 4 1.98 -8.75 16.83 o 8 20 4 543.33 639.84 28.51 o 10 20 4 420.83 500.44 32.39 o 12 20 4 6.06 -2.01 18.80 o 14 20 4 294.49 348.10 31.04 o 2 22 4 454.51 542.17 24.98 o 4 22 4 501.94 523.04 27.40 o 6 22 4 237.33 181.62 20.90 o 8 22 4 718.59 748.62 38.10 o 10 22 4 597.20 716.63 32.74 o 12 22 4 181.18 216.69 27.61 o 0 24 4 1229.94 1328.41 42.65 o 2 24 4 905.20 912.93 28.61 o 4 24 4 22.69 -6.23 18.07 o 6 24 4 258.99 256.97 33.68 o 8 24 4 151.40 107.82 25.48 o 10 24 4 260.77 260.13 30.53 o 2 26 4 12.07 13.41 21.07 o 4 26 4 77.28 71.99 20.84 o 6 26 4 63.36 43.35 20.99 o 8 26 4 104.49 90.92 27.65 o 0 28 4 146.57 128.18 33.15 o 2 28 4 68.31 83.66 22.10 o 4 28 4 95.57 114.95 34.20 o 1 1 5 51.80 37.90 14.25 o 3 1 5 2872.91 3125.88 48.99 o 5 1 5 277.55 320.93 26.62 o 7 1 5 470.48 514.02 28.58 o 9 1 5 98.39 69.79 19.51 o 11 1 5 22.69 -0.89 18.48 o 13 1 5 0.15 -3.26 18.51 o 15 1 5 63.76 110.98 23.43 o 1 3 5 697.97 692.85 32.67 o 3 3 5 494.11 560.42 25.66 o 5 3 5 650.47 661.73 28.36 o 7 3 5 63.02 36.30 17.89 o 9 3 5 133.06 129.44 27.87 o 11 3 5 3.43 -7.02 18.71 o 13 3 5 51.31 31.72 19.92 o 15 3 5 4.80 -16.33 19.95 o 1 5 5 17.52 27.50 14.21 o 3 5 5 473.87 496.86 26.22 o 5 5 5 187.77 214.79 23.97 o 7 5 5 539.49 585.25 30.30 o 9 5 5 127.16 92.64 20.85 o 11 5 5 387.93 403.47 28.60 o 13 5 5 14.42 14.46 20.22 o 15 5 5 12.26 38.52 21.25 o 1 7 5 363.64 466.94 25.61 o 3 7 5 41.52 12.29 13.83 o 5 7 5 48.22 40.54 16.23 o 7 7 5 151.29 146.90 20.77 o 9 7 5 153.06 81.60 19.69 o 11 7 5 370.93 398.36 28.75 o 13 7 5 7.76 -11.72 19.40 o 1 9 5 13.23 19.87 15.17 o 3 9 5 181.04 180.73 19.36 o 5 9 5 47.13 47.34 16.03 o 7 9 5 302.45 306.88 22.07 o 9 9 5 197.26 189.48 29.79 o 11 9 5 1.17 -15.73 18.77 o 13 9 5 139.02 141.91 22.74 o 1 11 5 59.55 29.72 14.44 o 3 11 5 268.18 304.48 31.34 o 5 11 5 119.30 116.93 23.07 o 7 11 5 11.45 12.36 16.26 o 9 11 5 11.37 -13.62 18.82 o 11 11 5 94.28 123.02 22.45 o 13 11 5 171.40 224.54 31.28 o 1 13 5 10.02 -7.33 16.81 o 3 13 5 117.41 148.20 23.96 o 5 13 5 131.83 108.58 18.79 o 7 13 5 161.33 111.84 28.11 o 9 13 5 203.32 175.39 20.57 o 11 13 5 45.99 98.74 22.06 o 1 15 5 617.59 649.43 24.77 o 3 15 5 240.75 240.56 21.97 o 5 15 5 64.46 30.47 17.80 o 7 15 5 21.49 -3.36 17.67 o 9 15 5 15.58 42.32 21.06 o 11 15 5 239.41 265.45 27.78 o 1 17 5 8.05 2.90 15.80 o 3 17 5 22.10 8.47 17.46 o 5 17 5 150.74 111.43 22.31 o 7 17 5 71.91 84.95 26.12 o 9 17 5 3.40 -18.41 20.61 o 1 19 5 256.99 218.29 30.59 o 3 19 5 33.33 25.58 19.11 o 5 19 5 22.20 7.36 21.19 o 7 19 5 147.94 200.43 51.05 o 1 21 5 3.49 -15.27 24.68 o 3 21 5 46.37 28.76 32.35 o 2 0 6 287.04 369.90 47.00 o 0 2 6 2012.83 1979.32 107.47 o 2 2 6 776.67 825.21 37.77 o