#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2207471.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207471_Fobs loop_ _publ_author_name 'Zhang, Tian-Le' 'Qin, Yu' 'Meng, Xiang-Gao' _publ_section_title ; Dichloro-1\kCl,3\kCl-bis[\m-methylenebis(diphenylphosphine)]-1:2\k^2^P:P';2:3\k^2^P:P'-trigold(I) perchlorate ; _journal_coeditor_code CF6461 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2588 _journal_page_last m2589 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 104.648 _cell_angle_beta 102.068 _cell_angle_gamma 101.456 _cell_length_a 9.8043 _cell_length_b 15.1538 _cell_length_c 18.8497 _exptl_crystal_F_000 1448.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file cf6461Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 050124cm in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 454.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 84976.39 81956.32 2784.95 o 2 0 0 31281.35 29059.00 1039.45 o 3 0 0 44063.47 42882.95 1353.34 o 4 0 0 22815.17 24667.59 799.10 o 5 0 0 192.34 261.72 44.45 o 6 0 0 186.64 339.15 53.96 o 7 0 0 1949.94 1840.22 116.55 o 8 0 0 375.75 216.46 62.15 o 9 0 0 420.74 587.44 110.17 o 10 0 0 184.67 144.57 99.43 o 11 0 0 114.12 93.07 101.02 o -11 1 0 5.28 25.06 92.07 o -10 1 0 375.76 440.28 115.94 o -9 1 0 1291.65 1557.28 157.10 o -8 1 0 16.21 19.82 48.88 o -7 1 0 994.58 586.12 69.13 o -6 1 0 1618.24 2000.77 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