#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/74/2207477.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207477_Fobs loop_ _publ_author_name 'Pu, Shou-Zhi' 'Yang, Tian-She' 'Wang, Ru-Ji' 'Xu, Jing-Kun' _publ_section_title ; 1,2-Bis[5-(2,2-dicyanovinyl)-2-ethyl-3-thienyl]-3,3,4,4,5,5-hexafluorocyclopent-1-ene, a new photochromic diarylethene compound ; _journal_coeditor_code CF6475 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4077 _journal_page_last o4079 _journal_volume 61 _journal_year 2005 _space_group_IT_number 179 _symmetry_space_group_name_Hall 'P 65 2 (0 0 1)' _symmetry_space_group_name_H-M 'P 65 2 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.4786 _cell_length_b 8.4786 _cell_length_c 59.5616 _exptl_crystal_F_000 1668.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file cf6475Iasup2.hkl _[local]_cod_data_source_block Ia #BEGIN Tags that were not found in dictionaries: _shelx_title ' pszjx-13 in P6(5)22' _shelx_refln_list_code 4 _shelx_f_calc_maximum 197.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z+2/3' '-x+y, -x, z+1/3' '-x, -y, z+1/2' 'y, -x+y, z+1/6' 'x-y, x, z+5/6' 'y, x, -z+2/3' 'x-y, -y, -z' '-x, -x+y, -z+1/3' '-y, -x, -z+1/6' '-x+y, y, -z+1/2' 'x, x-y, -z+5/6' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 22307.63 27414.42 546.65 o -1 2 0 5857.53 5143.81 117.46 o 0 2 0 7.70 23.24 5.17 o -1 3 0 6177.63 5746.57 200.41 o 0 3 0 351.41 403.08 20.83 o -2 4 0 17932.74 16956.48 2083.55 o -1 4 0 2484.90 2614.61 88.64 o 0 4 0 72.94 57.14 8.94 o -2 5 0 48.69 456.63 279.95 o -1 5 0 803.62 807.13 27.85 o 0 5 0 895.14 897.18 71.72 o -3 6 0 495.87 467.71 175.79 o -2 6 0 55.30 61.08 11.03 o -1 6 0 427.78 440.28 35.03 o 0 6 0 45.27 22.68 9.81 o -3 7 0 650.64 729.50 95.79 o -2 7 0 0.34 118.75 78.84 o -1 7 0 210.93 192.51 11.08 o 0 7 0 213.73 189.33 48.61 o -4 8 0 1.27 -17.66 34.39 o -3 8 0 21.62 14.76 7.45 o -2 8 0 637.96 685.54 36.87 o -1 8 0 18.13 12.64 7.32 o 0 8 0 246.30 296.27 18.39 o -4 9 0 2.13 29.04 24.79 o -3 9 0 108.93 123.85 13.68 o -2 9 0 23.20 11.85 7.92 o -1 9 0 37.43 6.34 8.11 o -5 10 0 3.96 -7.94 11.40 o -4 10 0 6.24 8.46 9.76 o 0 1 1 2976.62 2937.45 79.85 o -1 2 1 1722.87 1371.80 38.22 o 0 2 1 8093.96 7690.84 191.32 o -2 3 1 171.66 298.64 213.76 o -1 3 1 179.81 323.52 211.93 o 0 3 1 68.96 59.76 5.08 o -3 4 1 443.51 532.36 99.87 o -2 4 1 107.84 175.57 149.96 o -1 4 1 456.15 559.55 85.15 o 0 4 1 775.62 772.78 36.73 o -4 5 1 1270.38 1371.10 60.99 o -3 5 1 1822.81 1852.91 91.77 o -2 5 1 1804.82 1688.36 112.61 o -1 5 1 1260.72 1316.21 34.69 o 0 5 1 36.97 30.12 9.73 o -5 6 1 1739.38 1661.79 57.14 o -4 6 1 89.28 100.83 16.42 o -3 6 1 425.81 380.41 62.89 o -2 6 1 92.78 95.32 14.61 o -1 6 1 1738.16 1757.55 79.05 o 0 6 1 41.71 19.72 7.12 o -6 7 1 42.85 21.54 11.08 o -5 7 1 525.15 549.02 28.36 o -4 7 1 684.19 707.57 82.57 o -3 7 1 701.74 758.08 55.33 o -2 7 1 528.96 513.13 26.72 o -1 7 1 45.16 18.78 8.55 o 0 7 1 354.93 360.73 42.72 o -7 8 1 91.07 92.77 17.16 o -6 8 1 20.78 81.84 46.40 o -5 8 1 47.69 68.05 22.04 o -4 8 1 391.89 429.75 24.06 o -3 8 1 47.68 78.58 21.32 o -2 8 1 20.58 116.90 70.05 o -1 8 1 95.21 112.15 9.94 o 0 8 1 33.60 33.43 11.38 o -8 9 1 77.48 63.51 9.44 o -7 9 1 3.44 -0.79 9.09 o -6 9 1 71.33 78.90 18.35 o -5 9 1 228.80 244.02 14.81 o -4 9 1 230.92 231.83 14.87 o -3 9 1 72.55 106.42 28.81 o -2 9 1 3.34 5.96 6.19 o -1 9 1 79.59 78.71 10.42 o -6 10 1 22.81 4.69 10.47 o -5 10 1 23.95 28.78 9.74 o -4 10 1 23.93 13.63 25.62 o 0 1 2 26074.98 30569.92 274.68 o -1 2 2 6887.64 6611.82 145.96 o 0 2 2 16788.74 16241.08 484.25 o -2 3 2 2623.02 2611.14 82.56 o -1 3 2 2664.96 2649.35 66.02 o 0 3 2 1993.64 1889.82 58.95 o -3 4 2 863.12 866.88 145.73 o -2 4 2 244.14 190.26 11.42 o -1 4 2 878.49 889.72 56.70 o 0 4 2 129.13 137.50 9.86 o -4 5 2 1475.10 1425.05 125.77 o -3 5 2 1286.83 1546.92 59.09 o -2 5 2 1298.45 1360.12 45.74 o -1 5 2 1477.42 1593.68 41.47 o 0 5 2 255.39 257.64 48.76 o -5 6 2 98.38 198.97 67.48 o -4 6 2 326.48 294.25 18.09 o -3 6 2 29.77 -12.92 44.96 o -2 6 2 320.90 382.22 30.71 o -1 6 2 99.55 109.20 11.95 o 0 6 2 176.88 128.69 45.44 o -6 7 2 457.48 434.82 39.59 o -5 7 2 300.83 320.33 33.39 o -4 7 2 198.55 361.73 147.20 o -3 7 2 203.43 158.61 66.61 o -2 7 2 303.17 256.66 36.53 o -1 7 2 449.02 446.54 20.69 o 0 7 2 775.58 786.09 69.42 o -7 8 2 172.68 174.99 15.33 o -6 8 2 26.07 114.55 102.71 o -5 8 2 257.18 249.16 22.83 o -4 8 2 173.27 199.74 21.13 o -3 8 2 261.43 245.42 19.89 o -2 8 2 25.82 -11.36 17.88 o -1 8 2 170.05 157.51 20.89 o 0 8 2 0.38 8.19 7.32 o -8 9 2 6.33 -0.70 6.99 o -7 9 2 23.94 10.95 9.96 o -6 9 2 14.16 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16.61 o 0 7 3 206.59 173.27 36.68 o -7 8 3 153.16 158.33 15.61 o -6 8 3 414.28 403.17 40.28 o -5 8 3 11.41 51.63 44.71 o -4 8 3 96.49 41.75 17.67 o -3 8 3 12.30 -5.16 10.25 o -2 8 3 425.65 464.85 41.68 o -1 8 3 155.06 135.38 16.42 o 0 8 3 6.81 1.75 7.49 o -8 9 3 1.66 -5.72 6.23 o -7 9 3 3.99 31.22 32.20 o -6 9 3 26.40 59.54 39.98 o -5 9 3 59.59 80.17 16.56 o -4 9 3 59.69 50.84 24.15 o -3 9 3 27.82 4.96 17.85 o -2 9 3 3.81 8.41 20.99 o -1 9 3 1.55 -2.13 6.89 o -6 10 3 14.22 -1.09 12.11 o -5 10 3 77.40 84.23 17.49 o -4 10 3 14.20 -2.35 12.55 o 0 1 4 1283.50 1699.99 31.96 o -1 2 4 11091.33 11041.33 381.19 o 0 2 4 6646.67 6179.78 169.42 o -2 3 4 2038.94 2342.62 490.66 o -1 3 4 2090.21 2032.57 75.81 o 0 3 4 152.68 143.00 16.70 o -3 4 4 247.21 429.03 255.77 o -2 4 4 468.92 430.59 16.79 o -1 4 4 253.89 262.61 11.48 o 0 4 4 725.97 621.45 17.56 o -4 5 4 147.92 113.95 30.05 o -3 5 4 2190.29 2285.64 205.51 o -2 5 4 2194.31 2016.53 62.23 o -1 5 4 147.82 124.28 9.57 o 0 5 4 1294.57 1311.24 37.87 o -5 6 4 605.20 561.70 35.83 o -4 6 4 201.94 240.26 16.87 o -3 6 4 771.02 631.79 104.89 o -2 6 4 211.62 200.32 15.81 o -1 6 4 602.98 631.83 21.82 o 0 6 4 748.48 860.35 52.92 o -6 7 4 699.95 692.91 63.56 o -5 7 4 128.29 177.93 15.26 o -4 7 4 91.56 109.70 17.94 o -3 7 4 91.56 102.38 42.43 o -2 7 4 124.70 149.76 16.76 o -1 7 4 687.03 699.62 24.85 o 0 7 4 103.11 78.83 14.16 o -7 8 4 86.67 61.48 13.26 o -6 8 4 39.70 81.21 42.36 o -5 8 4 9.61 11.04 10.21 o -4 8 4 282.12 352.02 41.96 o -3 8 4 9.99 16.05 11.79 o -2 8 4 39.54 23.32 14.26 o -1 8 4 84.92 53.51 13.37 o 0 8 4 2.31 -5.71 8.32 o -8 9 4 10.03 -2.98 9.12 o -7 9 4 100.89 80.07 18.57 o -6 9 4 150.47 141.31 18.50 o -5 9 4 16.23 9.97 29.52 o -4 9 4 15.25 3.86 12.49 o -3 9 4 150.76 145.75 21.64 o -2 9 4 99.75 118.57 21.97 o -1 9 4 10.15 17.46 8.35 o -6 10 4 13.32 8.80 16.35 o -5 10 4 4.77 11.86 11.19 o -4 10 4 12.18 16.58 14.67 o 0 1 5 16267.30 16846.57 309.71 o -1 2 5 3472.74 3259.70 59.25 o 0 2 5 1691.30 1640.19 74.71 o -2 3 5 8180.95 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88.35 86.98 12.09 o -5 6 52 1.28 1.08 6.49 o -4 6 52 71.46 33.50 17.01 o -3 6 52 51.81 52.47 14.75 o -2 6 52 73.12 25.90 12.82 o -1 6 52 1.17 -1.29 5.93 o 0 1 53 671.21 792.01 17.91 o -1 2 53 93.06 101.53 12.07 o 0 2 53 63.26 98.27 16.39 o -2 3 53 63.14 80.17 12.53 o -1 3 53 62.96 74.07 11.44 o 0 3 53 32.42 39.19 10.97 o -3 4 53 35.13 36.00 13.37 o -2 4 53 219.91 229.96 29.95 o -1 4 53 37.53 30.41 10.03 o 0 4 53 156.86 166.88 14.32 o -4 5 53 54.76 47.81 14.40 o -3 5 53 16.47 23.49 10.80 o -2 5 53 16.02 0.93 9.56 o -1 5 53 55.44 65.76 11.50 o 0 5 53 0.18 2.93 5.43 o -5 6 53 103.08 110.27 13.64 o -4 6 53 27.79 5.91 10.29 o -3 6 53 7.29 5.28 6.86 o -2 6 53 27.04 8.10 10.00 o -1 6 53 103.08 113.65 12.58 o 0 0 54 569.47 501.69 38.64 o 0 1 54 1368.22 1446.34 24.78 o -1 2 54 4.76 -0.51 7.92 o 0 2 54 36.33 34.21 10.63 o -2 3 54 338.37 356.93 18.73 o -1 3 54 342.84 315.84 16.91 o 0 3 54 477.67 515.11 20.86 o -3 4 54 209.78 215.97 16.05 o -2 4 54 210.69 172.92 19.95 o -1 4 54 210.54 244.40 15.97 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