#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2207498.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207498_Fobs loop_ _publ_author_name 'You, Zhong-Lu' _publ_section_title ; Bis[4-bromo-2-(cyclopropyliminomethyl)phenolato]zinc(II) ; _journal_coeditor_code CI6696 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2501 _journal_page_last m2502 _journal_volume 61 _journal_year 2005 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 23.2600 _cell_length_b 13.3052 _cell_length_c 13.1186 _exptl_crystal_F_000 2144.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file ci6696Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 473.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1717.16 2023.85 54.73 o 4 0 0 202194.03 174411.47 3394.42 o 6 0 0 66363.22 69524.41 1373.42 o 8 0 0 140780.67 134082.83 2625.04 o 10 0 0 350.65 460.72 60.39 o 12 0 0 52872.07 53639.02 1675.06 o 14 0 0 687.61 860.54 90.29 o 16 0 0 9999.88 10657.00 294.55 o 18 0 0 2287.86 1930.44 217.40 o 20 0 0 55.69 84.20 170.28 o 22 0 0 8373.73 6838.96 388.42 o 24 0 0 360.80 231.92 213.95 o 26 0 0 1639.89 1772.00 290.22 o 28 0 0 1662.86 1722.49 327.62 o 2 1 0 21311.98 22061.95 312.13 o 4 1 0 27223.32 29552.05 419.43 o 6 1 0 29412.04 29323.77 422.23 o 8 1 0 12087.17 13416.77 217.77 o 10 1 0 53575.45 52621.25 753.46 o 12 1 0 86.94 155.03 44.20 o 14 1 0 52181.13 51850.29 756.92 o 16 1 0 828.87 903.96 71.88 o 18 1 0 27988.61 27655.66 445.15 o 20 1 0 1195.95 1257.65 140.20 o 22 1 0 3039.29 2886.88 200.73 o 24 1 0 450.38 529.33 196.51 o 26 1 0 3417.12 3628.20 241.75 o 28 1 0 25.71 49.14 297.32 o 0 2 0 8351.25 8203.20 181.98 o 2 2 0 41332.53 43751.96 717.90 o 4 2 0 17439.33 19405.66 333.16 o 6 2 0 25820.17 26552.07 388.04 o 8 2 0 4898.88 4946.83 100.72 o 10 2 0 2518.02 2408.01 76.18 o 12 2 0 956.00 1053.61 60.35 o 14 2 0 601.85 724.41 63.86 o 16 2 0 4.74 -48.64 54.15 o 18 2 0 136.43 113.58 92.02 o 20 2 0 1917.33 1881.91 123.40 o 22 2 0 241.73 280.79 134.75 o 24 2 0 461.86 566.37 179.69 o 26 2 0 90.38 295.43 254.90 o 28 2 0 121.33 484.67 199.42 o 2 3 0 31370.54 33893.38 482.41 o 4 3 0 67017.05 71296.38 995.89 o 6 3 0 56717.47 56989.67 806.03 o 8 3 0 7121.91 6690.30 129.46 o 10 3 0 123356.52 121234.79 1692.72 o 12 3 0 46431.91 45762.27 670.81 o 14 3 0 44507.35 40883.22 611.24 o 16 3 0 14609.26 13739.23 251.47 o 18 3 0 37661.27 34402.38 1406.04 o 20 3 0 4459.30 4447.81 262.95 o 22 3 0 9443.95 9934.38 272.75 o 24 3 0 1529.45 1730.02 217.09 o 26 3 0 2581.63 2648.58 222.72 o 28 3 0 440.30 298.95 194.52 o 0 4 0 143683.44 134488.09 2629.75 o 2 4 0 42859.38 43812.26 624.04 o 4 4 0 182249.58 168445.20 2322.86 o 6 4 0 4687.53 4728.59 102.17 o 8 4 0 81678.26 78452.43 1253.98 o 10 4 0 3980.48 3899.02 103.50 o 12 4 0 16852.63 14773.24 253.92 o 14 4 0 197.37 261.26 60.22 o 16 4 0 5797.08 5466.52 270.00 o 18 4 0 363.83 162.95 98.05 o 20 4 0 917.18 881.38 113.79 o 22 4 0 1250.03 1213.31 129.40 o 24 4 0 2379.54 2355.95 202.78 o 26 4 0 257.34 22.61 172.54 o 28 4 0 1351.98 1409.60 223.93 o 2 5 0 5254.23 5148.56 123.25 o 4 5 0 117.78 92.11 34.25 o 6 5 0 620.60 581.78 47.18 o 8 5 0 1498.51 1345.95 66.08 o 10 5 0 10.42 269.58 77.85 o 12 5 0 12034.10 11273.53 213.09 o 14 5 0 2435.86 2726.04 159.99 o 16 5 0 12007.20 11644.00 268.28 o 18 5 0 7563.88 7117.93 259.39 o 20 5 0 3663.67 3457.79 165.19 o 22 5 0 3881.23 3997.05 188.80 o 24 5 0 681.35 549.16 130.27 o 26 5 0 1510.17 1625.41 274.44 o 28 5 0 495.30 622.41 195.92 o 0 6 0 8387.53 8432.22 222.86 o 2 6 0 123459.43 121877.75 1943.09 o 4 6 0 9386.72 8688.55 163.21 o 6 6 0 107816.90 107034.63 1503.81 o 8 6 0 4904.68 4636.39 121.43 o 10 6 0 25065.68 24135.87 388.00 o 12 6 0 272.24 326.76 67.20 o 14 6 0 11563.68 11090.68 261.35 o 16 6 0 2959.96 3183.55 174.44 o 18 6 0 286.15 344.87 132.35 o 20 6 0 1842.90 1896.04 145.65 o 22 6 0 34.56 -130.77 112.25 o 24 6 0 1176.41 1197.47 150.74 o 26 6 0 616.88 646.85 191.86 o 28 6 0 433.73 465.30 310.17 o 2 7 0 2709.69 2667.21 90.77 o 4 7 0 1792.13 1939.12 78.37 o 6 7 0 11860.56 12522.61 226.74 o 8 7 0 6361.10 6972.51 212.82 o 10 7 0 16724.21 16815.49 303.13 o 12 7 0 15034.35 15299.91 321.74 o 14 7 0 14866.75 14753.85 322.87 o 16 7 0 14466.23 14144.73 323.67 o 18 7 0 8302.37 8508.65 249.66 o 20 7 0 1917.03 2161.92 155.07 o 22 7 0 6432.08 5963.32 235.95 o 24 7 0 1930.83 2003.58 171.82 o 26 7 0 1286.80 1396.77 177.07 o 0 8 0 6671.08 6114.73 200.39 o 2 8 0 3029.95 3229.24 153.56 o 4 8 0 10166.48 9609.33 191.07 o 6 8 0 3955.08 4159.41 125.21 o 8 8 0 11015.40 10341.59 211.94 o 10 8 0 3189.93 3157.26 120.37 o 12 8 0 12686.90 12396.07 289.64 o 14 8 0 747.14 733.35 179.89 o 16 8 0 78.15 36.54 102.62 o 18 8 0 99.98 5.96 106.60 o 20 8 0 67.73 139.94 122.32 o 22 8 0 2.80 28.87 131.30 o 24 8 0 199.91 197.83 141.79 o 26 8 0 3.12 -184.57 144.14 o 2 9 0 147.84 259.55 64.89 o 4 9 0 6403.71 6321.19 163.94 o 6 9 0 914.75 711.94 77.37 o 8 9 0 19104.49 19141.32 335.57 o 10 9 0 629.93 848.58 88.49 o 12 9 0 21654.50 21397.56 435.73 o 14 9 0 799.12 921.40 120.16 o 16 9 0 5169.89 5080.32 206.62 o 18 9 0 45.95 -2.63 111.26 o 20 9 0 4747.17 4590.59 230.38 o 22 9 0 144.33 198.28 150.11 o 24 9 0 2118.40 2264.37 191.44 o 0 10 0 282.42 287.71 159.00 o 2 10 0 33128.49 31452.57 493.71 o 4 10 0 2826.20 2831.62 113.92 o 6 10 0 25139.57 24339.24 409.27 o 8 10 0 162.36 137.23 80.59 o 10 10 0 8059.42 7865.20 231.43 o 12 10 0 3605.48 2979.82 152.36 o 14 10 0 1559.21 1616.57 141.01 o 16 10 0 0.53 8.60 109.34 o 18 10 0 541.15 649.64 191.09 o 20 10 0 183.02 69.86 131.16 o 22 10 0 166.92 -45.55 198.70 o 24 10 0 65.05 34.14 430.10 o 2 11 0 1.18 60.51 73.06 o 4 11 0 9.38 10.13 74.38 o 6 11 0 189.82 274.69 84.03 o 8 11 0 25.48 180.85 134.24 o 10 11 0 188.06 202.94 132.20 o 12 11 0 3051.40 3551.73 211.00 o 14 11 0 139.44 -16.28 141.24 o 16 11 0 906.83 938.88 171.50 o 18 11 0 280.10 419.12 170.45 o 20 11 0 872.39 1160.13 195.42 o 22 11 0 193.62 -0.24 180.81 o 0 12 0 1621.03 1915.34 239.44 o 2 12 0 3821.67 3639.67 213.43 o 4 12 0 270.44 265.28 136.83 o 6 12 0 1879.50 1924.43 175.91 o 8 12 0 98.06 132.05 212.91 o 10 12 0 698.32 404.50 256.37 o 12 12 0 269.09 521.72 234.64 o 14 12 0 130.09 353.94 224.19 o 16 12 0 188.50 255.74 251.35 o 18 12 0 81.55 477.84 262.84 o 20 12 0 110.83 -81.28 261.59 o 2 13 0 38.34 95.90 196.19 o 4 13 0 1908.16 1899.04 199.02 o 6 13 0 170.95 300.66 237.98 o 8 13 0 3193.26 3324.21 331.17 o 10 13 0 84.43 -219.18 237.77 o 12 13 0 2790.42 3850.10 379.43 o 14 13 0 15.89 302.75 253.86 o 16 13 0 3326.26 3853.66 387.37 o 18 13 0 5.87 -56.41 247.80 o 0 14 0 561.06 375.25 233.59 o 2 14 0 3487.11 3511.83 262.53 o 4 14 0 586.07 1033.62 244.46 o 6 14 0 4472.63 4465.01 392.59 o 8 14 0 22.97 -245.71 235.26 o 10 14 0 2495.91 2062.01 334.93 o 12 14 0 1503.39 1065.79 314.87 o 14 14 0 2081.94 2277.43 358.54 o 16 14 0 17.82 -350.18 234.64 o 2 15 0 7.60 -249.51 203.30 o 4 15 0 8.34 -372.64 248.43 o 6 15 0 422.77 902.61 311.11 o 8 15 0 45.55 83.78 267.02 o 10 15 0 235.66 298.15 304.01 o 12 15 0 23.40 35.31 306.51 o 0 16 0 4.38 -91.51 260.96 o 2 16 0 1248.09 735.88 291.89 o 4 16 0 105.61 13.79 282.90 o 8 16 0 4.37 -155.45 308.18 o 10 16 0 317.47 17.34 302.54 o 2 17 0 3.27 -390.92 272.87 o 4 17 0 0.95 -86.50 302.12 o 1 1 1 687.82 732.67 15.44 o 2 1 1 4240.56 4341.80 54.17 o 3 1 1 439.03 392.54 15.02 o 4 1 1 3544.00 3540.32 46.70 o 5 1 1 590.79 654.86 28.29 o 6 1 1 2204.98 2356.76 40.54 o 7 1 1 35.66 51.09 17.56 o 8 1 1 22.48 46.52 20.26 o 9 1 1 4739.88 5051.24 74.30 o 10 1 1 11871.55 12443.88 146.90 o 11 1 1 65.02 84.07 28.65 o 12 1 1 621.35 576.58 36.86 o 13 1 1 7806.90 7787.79 112.66 o 14 1 1 3222.54 2937.24 71.05 o 15 1 1 3.26 86.29 38.11 o 16 1 1 2604.45 2600.60 71.25 o 17 1 1 4679.02 4592.84 95.05 o 18 1 1 1334.90 1323.16 68.37 o 19 1 1 35.78 15.22 55.67 o 20 1 1 9751.36 9111.67 171.43 o 21 1 1 711.13 867.27 89.21 o 22 1 1 784.62 838.76 91.58 o 23 1 1 190.67 22.44 97.84 o 24 1 1 2059.19 2142.69 257.86 o 25 1 1 254.97 315.82 171.39 o 26 1 1 12.22 152.77 120.59 o 27 1 1 305.04 218.32 125.06 o 28 1 1 1261.29 1406.82 152.61 o 29 1 1 40.78 55.32 136.12 o 0 2 1 52769.09 54266.12 885.84 o 1 2 1 17624.82 18233.94 186.71 o 2 2 1 25252.32 26472.23 266.71 o 3 2 1 69469.55 69265.41 681.48 o 4 2 1 15018.27 15343.92 162.31 o 5 2 1 2213.96 1987.38 37.66 o 6 2 1 19286.58 19449.01 205.91 o 7 2 1 11859.12 12283.21 139.42 o 8 2 1 5879.03 5441.16 76.41 o 9 2 1 10091.03 10456.87 126.48 o 10 2 1 21524.32 22793.96 247.18 o 11 2 1 1720.85 1897.32 52.55 o 12 2 1 6415.89 6787.17 99.12 o 13 2 1 8054.60 7802.84 112.37 o 14 2 1 12854.48 12815.46 162.84 o 15 2 1 2.81 80.89 40.94 o 16 2 1 0.90 22.69 45.78 o 17 2 1 4288.49 3793.92 96.53 o 18 2 1 1271.64 1372.19 69.51 o 19 2 1 18.68 76.02 57.20 o 20 2 1 8.62 -4.19 64.50 o 21 2 1 1316.84 1134.93 92.77 o 22 2 1 1487.86 1418.59 103.78 o 23 2 1 617.98 670.79 98.57 o 24 2 1 244.20 289.55 106.96 o 25 2 1 834.13 774.58 120.65 o 26 2 1 1.98 44.46 118.44 o 27 2 1 352.13 293.83 127.95 o 28 2 1 15.86 -44.34 130.58 o 29 2 1 241.49 112.81 136.41 o 1 3 1 12809.54 13939.85 149.26 o 2 3 1 186.58 182.72 16.65 o 3 3 1 5566.50 5545.48 75.01 o 4 3 1 3542.65 3509.54 51.97 o 5 3 1 8867.90 8623.37 102.82 o 6 3 1 510.93 508.74 26.27 o 7 3 1 16.94 3.62 22.08 o 8 3 1 2896.77 2602.76 62.27 o 9 3 1 5684.76 5387.61 81.04 o 10 3 1 13.27 33.41 27.65 o 11 3 1 23.09 75.68 30.14 o 12 3 1 9714.64 9033.49 122.58 o 13 3 1 663.70 710.07 42.57 o 14 3 1 3615.91 3520.21 76.47 o 15 3 1 6676.43 6435.90 150.10 o 16 3 1 6533.66 6071.40 117.07 o 17 3 1 305.21 391.65 56.40 o 18 3 1 3378.22 3309.58 104.84 o 19 3 1 1044.23 1132.67 78.15 o 20 3 1 595.78 576.36 84.58 o 21 3 1 100.67 115.37 72.48 o 22 3 1 8.98 -64.65 83.38 o 23 3 1 698.61 702.07 99.74 o 24 3 1 641.28 654.90 100.53 o 25 3 1 11.40 -155.30 106.29 o 26 3 1 305.35 396.70 123.80 o 27 3 1 421.06 602.67 134.40 o 28 3 1 326.08 388.79 140.22 o 29 3 1 12.86 -13.38 133.19 o 0 4 1 43532.86 46365.28 752.03 o 1 4 1 9390.03 9448.44 110.78 o 2 4 1 50434.39 50491.38 542.92 o 3 4 1 20641.79 22023.88 232.05 o 4 4 1 383.17 408.95 24.61 o 5 4 1 4018.33 4340.74 66.06 o 6 4 1 252.45 177.12 25.23 o 7 4 1 72.79 59.03 25.53 o 8 4 1 4947.67 5049.73 79.61 o 9 4 1 4127.81 3690.15 69.59 o 10 4 1 1053.69 1352.36 46.00 o 11 4 1 185.72 196.66 35.06 o 12 4 1 685.91 595.39 41.02 o 13 4 1 2073.93 2022.53 78.10 o 14 4 1 94.72 108.42 47.05 o 15 4 1 68.07 103.84 48.64 o 16 4 1 4787.44 4335.21 101.56 o 17 4 1 558.81 557.92 67.62 o 18 4 1 386.87 414.93 69.42 o 19 4 1 1812.12 1876.58 101.02 o 20 4 1 983.04 984.89 96.28 o 21 4 1 4.87 19.87 74.21 o 22 4 1 105.63 31.88 77.95 o 23 4 1 345.09 274.05 92.94 o 24 4 1 598.80 467.19 100.72 o 25 4 1 145.22 -12.42 134.36 o 26 4 1 57.58 108.72 119.27 o 27 4 1 905.23 1016.17 273.38 o 28 4 1 17.72 -24.41 136.80 o 29 4 1 312.70 172.62 223.35 o 1 5 1 6144.14 6288.03 85.93 o 2 5 1 268.10 379.86 28.85 o 3 5 1 164.34 122.34 24.80 o 4 5 1 103.44 104.06 24.39 o 5 5 1 610.17 756.53 44.68 o 6 5 1 5880.27 6111.60 88.77 o 7 5 1 31.93 21.75 28.12 o 8 5 1 2282.14 2421.31 59.74 o 9 5 1 2471.46 2438.84 62.60 o 10 5 1 234.10 242.86 37.51 o 11 5 1 28.38 21.43 37.34 o 12 5 1 124.07 146.78 39.60 o 13 5 1 339.61 300.38 49.45 o 14 5 1 5.57 30.51 49.75 o 15 5 1 659.69 661.82 60.14 o 16 5 1 24.58 51.58 59.72 o 17 5 1 1126.01 1056.59 77.24 o 18 5 1 68.87 136.52 86.39 o 19 5 1 8.08 75.29 71.92 o 20 5 1 1212.95 1215.36 91.43 o 21 5 1 577.39 604.48 84.27 o 22 5 1 144.30 74.98 79.33 o 23 5 1 36.14 53.17 112.14 o 24 5 1 850.95 769.37 108.41 o 25 5 1 85.23 -101.39 98.81 o 26 5 1 111.30 158.26 123.83 o 27 5 1 93.94 208.13 129.53 o 28 5 1 164.14 415.54 141.02 o 0 6 1 23681.02 23864.42 416.88 o 1 6 1 4968.66 4580.68 75.54 o 2 6 1 19554.49 17863.02 215.33 o 3 6 1 576.16 650.52 36.36 o 4 6 1 2665.87 2598.59 79.40 o 5 6 1 3315.24 3290.07 67.18 o 6 6 1 24930.72 24570.69 269.44 o 7 6 1 213.49 299.51 36.60 o 8 6 1 7983.60 8330.42 119.63 o 9 6 1 11267.07 11142.59 184.97 o 10 6 1 6015.18 5780.48 101.02 o 11 6 1 18.19 41.47 41.83 o 12 6 1 1916.89 2132.64 89.00 o 13 6 1 2728.27 2590.99 81.92 o 14 6 1 16.22 -34.89 51.56 o 15 6 1 935.43 841.75 72.97 o 16 6 1 918.41 1063.40 79.66 o 17 6 1 588.89 593.09 76.35 o 18 6 1 112.53 9.70 68.94 o 19 6 1 5.43 -63.40 70.94 o 20 6 1 169.50 7.04 77.03 o 21 6 1 194.05 147.80 81.01 o 22 6 1 24.32 -122.24 81.50 o 23 6 1 106.87 -147.22 98.14 o 24 6 1 42.70 -92.10 87.63 o 25 6 1 0.22 115.48 104.58 o 26 6 1 251.10 445.59 115.34 o 27 6 1 172.82 237.59 136.51 o 28 6 1 11.54 80.14 158.09 o 1 7 1 748.79 807.96 52.62 o 2 7 1 1889.39 2112.83 79.74 o 3 7 1 228.62 177.44 36.93 o 4 7 1 135.26 116.85 34.28 o 5 7 1 351.20 359.71 38.47 o 6 7 1 93.91 103.50 36.91 o 7 7 1 48.99 10.70 38.29 o 8 7 1 18154.81 17963.91 215.22 o 9 7 1 891.60 1030.17 56.10 o 10 7 1 3067.16 3155.60 81.78 o 11 7 1 1939.23 1838.91 97.27 o 12 7 1 13883.66 13374.08 215.96 o 13 7 1 752.68 846.66 65.52 o 14 7 1 468.57 509.44 67.72 o 15 7 1 8620.76 8514.19 167.20 o 16 7 1 2848.61 2860.89 106.00 o 17 7 1 1.78 6.98 90.67 o 18 7 1 2559.65 2568.40 107.62 o 19 7 1 3890.85 3866.90 212.19 o 20 7 1 2746.60 2891.05 121.92 o 21 7 1 5.56 11.88 84.89 o 22 7 1 1935.97 2000.45 139.12 o 23 7 1 1586.02 1531.77 110.67 o 24 7 1 368.13 373.27 98.06 o 25 7 1 83.92 12.51 96.00 o 26 7 1 1224.68 1162.88 130.43 o 27 7 1 363.33 129.62 120.74 o 0 8 1 1719.36 1524.08 117.39 o 1 8 1 2752.25 2757.83 69.09 o 2 8 1 4527.59 4613.01 87.31 o 3 8 1 2517.55 2578.17 99.88 o 4 8 1 3651.38 3486.74 87.90 o 5 8 1 1451.60 1387.82 55.22 o 6 8 1 5176.67 5244.88 97.36 o 7 8 1 1045.44 1125.77 55.59 o 8 8 1 4251.24 3985.71 89.83 o 9 8 1 293.56 285.72 53.36 o 10 8 1 4.36 -7.20 52.38 o 11 8 1 797.56 1035.12 78.10 o 12 8 1 2602.74 2534.48 89.04 o 13 8 1 462.03 513.36 71.02 o 14 8 1 362.76 485.23 74.13 o 15 8 1 164.33 275.35 71.51 o 16 8 1 1436.12 1404.80 91.21 o 17 8 1 245.99 158.74 78.44 o 18 8 1 77.54 119.26 80.60 o 19 8 1 898.11 893.31 96.34 o 20 8 1 1433.97 1368.35 105.00 o 21 8 1 38.02 -19.02 88.84 o 22 8 1 36.34 20.01 89.70 o 23 8 1 380.16 357.74 100.15 o 24 8 1 93.27 -119.74 94.63 o 25 8 1 288.40 117.53 103.11 o 26 8 1 143.68 188.91 115.88 o 1 9 1 3276.00 3392.76 115.02 o 2 9 1 344.77 332.53 45.95 o 3 9 1 1577.38 1689.76 66.89 o 4 9 1 964.17 1082.07 56.01 o 5 9 1 2008.06 2097.70 83.48 o 6 9 1 6.65 23.93 46.36 o 7 9 1 80.28 104.35 48.99 o 8 9 1 2707.23 2884.75 82.73 o 9 9 1 64.26 47.47 56.62 o 10 9 1 385.44 313.36 63.58 o 11 9 1 13.69 55.55 59.87 o 12 9 1 47.65 62.49 66.73 o 13 9 1 261.53 377.11 75.04 o 14 9 1 1038.95 1164.64 88.02 o 15 9 1 5.77 -18.27 73.40 o 16 9 1 782.96 783.31 86.86 o 17 9 1 10.76 7.26 80.55 o 18 9 1 60.01 104.62 85.07 o 19 9 1 194.44 418.63 91.67 o 20 9 1 87.29 -52.04 88.34 o 21 9 1 190.52 176.83 95.35 o 22 9 1 1.52 -106.50 103.40 o 23 9 1 72.11 -57.91 107.74 o 24 9 1 7.46 -54.19 111.59 o 25 9 1 188.72 176.22 118.64 o 0 10 1 4.11 23.11 66.38 o 1 10 1 820.12 949.79 72.62 o 2 10 1 5697.66 5525.67 115.96 o 3 10 1 5.67 76.16 47.98 o 4 10 1 124.91 96.07 48.99 o 5 10 1 3982.65 3830.81 93.62 o 6 10 1 383.03 453.50 57.54 o 7 10 1 200.42 311.47 58.04 o 8 10 1 650.96 522.33 73.84 o 9 10 1 1508.23 1624.87 90.13 o 10 10 1 1112.86 1098.31 82.61 o 11 10 1 1623.24 1779.36 104.62 o 12 10 1 1962.14 1897.92 107.41 o 13 10 1 166.62 244.19 84.67 o 14 10 1 274.18 270.20 86.33 o 15 10 1 3.58 -38.13 86.14 o 16 10 1 380.98 451.19 94.61 o 17 10 1 232.64 294.22 97.21 o 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3891.74 75.23 o 4 5 4 17584.75 18243.74 206.00 o 5 5 4 1981.16 2439.86 55.63 o 6 5 4 1867.88 1800.32 71.22 o 7 5 4 130.30 92.26 32.33 o 8 5 4 5889.02 5442.00 100.48 o 9 5 4 4787.94 4337.22 93.15 o 10 5 4 1279.53 1248.81 59.89 o 11 5 4 5368.77 5083.08 119.70 o 12 5 4 4030.35 3810.07 96.24 o 13 5 4 1205.25 1198.59 74.58 o 14 5 4 409.09 417.96 60.99 o 15 5 4 2297.35 2191.62 85.97 o 16 5 4 1072.55 1182.41 83.40 o 17 5 4 2575.25 2719.55 96.55 o 18 5 4 9.12 31.99 72.32 o 19 5 4 4229.18 4224.19 120.71 o 20 5 4 199.65 327.94 92.27 o 21 5 4 890.72 983.87 106.77 o 22 5 4 1545.44 1547.47 152.93 o 23 5 4 1650.69 1629.89 126.63 o 24 5 4 175.80 123.66 104.58 o 25 5 4 631.24 432.47 114.94 o 26 5 4 621.53 763.37 124.94 o 27 5 4 155.28 249.53 118.30 o 28 5 4 23.02 54.01 160.47 o 0 6 4 49006.12 50113.35 865.75 o 1 6 4 4320.22 4504.48 104.18 o 2 6 4 43540.49 41436.60 477.29 o 3 6 4 5233.13 5109.24 93.32 o 4 6 4 18804.04 18410.34 211.30 o 5 6 4 1166.51 1205.34 45.24 o 6 6 4 29360.40 28585.44 312.60 o 7 6 4 8777.71 8840.71 146.66 o 8 6 4 4820.19 4656.39 97.45 o 9 6 4 1980.06 2011.46 71.24 o 10 6 4 13081.57 12549.08 260.30 o 11 6 4 4957.63 4945.02 109.14 o 12 6 4 254.87 161.30 53.45 o 13 6 4 114.43 92.75 55.13 o 14 6 4 1796.81 1747.46 95.78 o 15 6 4 3068.39 3082.72 99.59 o 16 6 4 685.57 720.20 73.21 o 17 6 4 40.61 -76.07 62.23 o 18 6 4 405.39 368.40 73.55 o 19 6 4 1073.36 1104.30 91.17 o 20 6 4 166.68 178.52 82.56 o 21 6 4 236.67 240.93 99.04 o 22 6 4 204.19 232.63 102.78 o 23 6 4 734.12 604.36 140.19 o 24 6 4 631.33 670.19 114.11 o 25 6 4 413.31 257.89 133.00 o 26 6 4 536.09 486.57 142.05 o 27 6 4 59.93 151.13 288.13 o 1 7 4 3402.93 3494.70 99.03 o 2 7 4 376.37 359.13 57.41 o 3 7 4 2033.47 2313.95 92.55 o 4 7 4 3033.66 2979.34 76.98 o 5 7 4 3696.56 3572.21 84.20 o 6 7 4 733.16 806.05 53.17 o 7 7 4 78.35 91.12 57.54 o 8 7 4 7907.83 7806.72 198.81 o 9 7 4 745.47 708.31 66.58 o 10 7 4 12764.21 12785.69 208.44 o 11 7 4 33.24 -39.97 59.73 o 12 7 4 3467.92 3632.53 114.62 o 13 7 4 275.38 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4 112.26 192.76 179.32 o 14 11 4 521.37 612.45 126.45 o 15 11 4 3.63 23.35 120.47 o 16 11 4 321.09 686.14 132.91 o 17 11 4 106.21 69.76 140.96 o 18 11 4 294.83 374.84 138.16 o 19 11 4 25.86 189.47 134.58 o 20 11 4 1004.65 1377.86 196.21 o 21 11 4 47.66 -92.66 139.90 o 22 11 4 230.14 -149.93 151.89 o 0 12 4 48.64 2.63 128.72 o 1 12 4 228.13 312.41 102.68 o 2 12 4 2821.00 2849.97 137.20 o 3 12 4 23.85 17.86 96.27 o 4 12 4 66.85 -64.41 98.44 o 5 12 4 206.17 204.98 102.09 o 6 12 4 1245.79 1162.45 116.28 o 7 12 4 4.28 139.55 105.52 o 8 12 4 77.13 78.31 120.34 o 9 12 4 73.54 155.58 114.46 o 10 12 4 275.20 304.57 110.77 o 11 12 4 447.26 497.07 116.03 o 12 12 4 108.53 96.37 151.57 o 13 12 4 19.07 90.71 202.65 o 14 12 4 215.09 59.08 145.79 o 15 12 4 91.41 86.73 126.74 o 16 12 4 30.60 198.79 134.87 o 17 12 4 195.70 82.90 129.28 o 18 12 4 0.59 49.27 138.97 o 19 12 4 2.01 -92.67 126.23 o 20 12 4 61.76 151.49 167.95 o 1 13 4 31.00 -47.85 103.66 o 2 13 4 157.03 80.85 104.90 o 3 13 4 234.11 339.72 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5 1378.87 1377.38 92.21 o 15 7 5 680.74 889.63 87.91 o 16 7 5 7175.06 6567.67 187.64 o 17 7 5 2134.32 2071.63 110.50 o 18 7 5 1597.96 1894.76 109.30 o 19 7 5 441.31 447.40 99.58 o 20 7 5 1897.05 1901.02 125.23 o 21 7 5 1570.38 1739.12 167.08 o 22 7 5 964.19 1052.39 139.03 o 23 7 5 4.64 -50.27 122.82 o 24 7 5 217.42 268.11 128.40 o 25 7 5 936.19 977.95 153.02 o 26 7 5 1209.76 536.34 316.33 o 0 8 5 387.15 355.49 109.56 o 1 8 5 100.67 93.08 64.47 o 2 8 5 13047.63 13128.00 215.74 o 3 8 5 453.19 542.12 76.97 o 4 8 5 2307.92 2144.52 92.56 o 5 8 5 292.19 278.37 80.44 o 6 8 5 6797.43 6765.88 246.50 o 7 8 5 71.94 114.70 81.27 o 8 8 5 1802.01 1671.11 107.64 o 9 8 5 1554.70 1713.53 110.92 o 10 8 5 617.38 649.49 97.05 o 11 8 5 34.64 35.06 88.93 o 12 8 5 1322.26 1398.54 125.85 o 13 8 5 134.06 210.82 109.00 o 14 8 5 515.91 498.33 98.62 o 15 8 5 28.66 119.53 96.29 o 16 8 5 717.54 963.93 114.16 o 17 8 5 334.41 295.04 109.77 o 18 8 5 19.75 182.57 110.77 o 19 8 5 5.20 38.29 167.95 o 20 8 5 1887.72 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