#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:17:38 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180996 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/76/2207601.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207601_Fobs loop_ _publ_author_name 'Fu, Yun-Long' 'Ren, Jia-Lin' 'Xu, Zhi-Wei' 'Ng, Seik Weng' _publ_section_title ; catena-Poly[sesqui(1,2-ethanediammonium) [[aqua(sulfato-\kO)cerate(III)]-di-\m-sulfato-\k^3^O,O':O'';\k^4^O,O':O'',O'''] dihydrate] ; _journal_coeditor_code LH6556 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2738 _journal_page_last m2740 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.655 _cell_angle_gamma 90.000 _cell_length_a 6.6287 _cell_length_b 26.6289 _cell_length_c 10.0073 _exptl_crystal_F_000 1144.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file lh6556Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 386.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 56555.99 58330.19 2120.45 o 2 0 0 149149.19 137921.23 3034.08 o 3 0 0 37745.25 38778.07 716.41 o 4 0 0 5047.02 5160.45 248.59 o 5 0 0 33.06 74.27 48.17 o 6 0 0 755.63 838.42 123.03 o 7 0 0 2378.38 2147.02 199.24 o 8 0 0 3985.00 3618.72 282.90 o 1 1 0 1432.55 1400.95 29.24 o 2 1 0 11222.73 11587.88 177.78 o 3 1 0 15734.98 16520.49 253.57 o 4 1 0 17978.60 17455.79 375.18 o 5 1 0 20444.27 20266.28 428.51 o 6 1 0 27480.89 27826.23 578.36 o 7 1 0 5400.43 5673.70 386.31 o 8 1 0 7092.01 7680.15 306.35 o 0 2 0 39986.36 36136.62 1133.41 o 1 2 0 12728.05 13627.34 253.55 o 2 2 0 24302.98 25450.99 409.91 o 3 2 0 4105.38 3975.18 81.05 o 4 2 0 5426.03 5476.93 122.05 o 5 2 0 4621.42 4633.10 146.73 o 6 2 0 1142.50 1048.60 78.41 o 7 2 0 60.73 167.13 61.66 o 8 2 0 655.82 819.83 151.36 o 1 3 0 4988.85 5856.09 101.63 o 2 3 0 6423.50 6364.12 120.31 o 3 3 0 799.14 820.75 38.28 o 4 3 0 5047.41 5108.44 117.24 o 5 3 0 4249.45 4263.44 139.60 o 6 3 0 504.12 420.69 59.07 o 7 3 0 490.06 649.40 72.07 o 8 3 0 1.63 61.23 63.11 o 0 4 0 1197.05 1205.97 83.24 o 1 4 0 3066.96 3413.73 67.16 o 2 4 0 3359.30 3543.24 65.94 o 3 4 0 1607.63 1711.03 75.80 o 4 4 0 870.50 856.39 45.78 o 5 4 0 869.35 775.89 62.92 o 6 4 0 12.49 49.63 39.49 o 7 4 0 1816.22 1888.01 109.39 o 8 4 0 27.77 32.27 59.35 o 1 5 0 6992.73 7524.96 130.21 o 2 5 0 9423.16 9488.19 149.42 o 3 5 0 4338.39 4551.75 102.55 o 4 5 0 11983.94 12007.19 227.59 o 5 5 0 1080.94 1074.74 73.32 o 6 5 0 2792.21 2658.46 115.80 o 7 5 0 15.49 6.17 42.34 o 8 5 0 1599.26 1650.71 283.32 o 0 6 0 24991.73 25478.25 571.49 o 1 6 0 11680.15 12017.67 200.83 o 2 6 0 15676.38 16446.98 274.33 o 3 6 0 916.53 1056.56 49.52 o 4 6 0 3129.54 2998.33 86.90 o 5 6 0 144.46 167.27 45.03 o 6 6 0 191.37 152.28 46.08 o 7 6 0 1464.94 1580.83 120.53 o 8 6 0 3624.00 3713.24 307.43 o 1 7 0 241.27 214.35 19.53 o 2 7 0 13380.69 14264.63 245.00 o 3 7 0 17463.85 18965.06 287.81 o 4 7 0 5970.95 5974.40 136.66 o 5 7 0 7265.74 7175.98 196.99 o 6 7 0 7586.73 7161.94 208.81 o 7 7 0 2591.78 2614.14 128.58 o 8 7 0 3308.18 3662.33 235.86 o 0 8 0 15108.59 15651.81 366.06 o 1 8 0 15194.02 15693.00 260.01 o 2 8 0 9519.34 9545.48 155.04 o 3 8 0 1544.81 1542.53 45.92 o 4 8 0 529.98 579.12 43.66 o 5 8 0 2980.56 2753.25 115.58 o 6 8 0 3391.50 3303.90 147.14 o 7 8 0 1429.57 1458.66 98.94 o 8 8 0 4563.42 4317.67 313.69 o 1 9 0 2078.78 2491.47 59.62 o 2 9 0 6380.43 6968.69 121.46 o 3 9 0 3301.72 3248.84 81.05 o 4 9 0 2698.70 2700.06 86.76 o 5 9 0 5492.07 5189.21 159.36 o 6 9 0 652.25 669.98 67.18 o 7 9 0 2063.26 2229.35 120.73 o 8 9 0 264.20 127.81 123.17 o 0 10 0 7072.75 7120.82 239.52 o 1 10 0 372.45 406.62 24.67 o 2 10 0 299.83 266.22 28.69 o 3 10 0 119.99 46.60 23.22 o 4 10 0 701.31 726.88 49.12 o 5 10 0 971.52 1003.11 73.29 o 6 10 0 573.98 516.69 64.69 o 7 10 0 0.65 13.70 41.79 o 1 11 0 489.02 514.17 27.81 o 2 11 0 2940.95 3122.56 71.20 o 3 11 0 22.51 43.93 19.93 o 4 11 0 5255.91 5146.70 188.68 o 5 11 0 1879.63 1746.36 91.39 o 6 11 0 5870.36 5704.65 183.00 o 7 11 0 1018.43 944.36 86.92 o 0 12 0 8060.04 7853.82 206.67 o 1 12 0 19536.92 19352.44 324.06 o 2 12 0 24979.65 25300.68 419.72 o 3 12 0 1093.10 1046.18 44.45 o 4 12 0 10895.84 9899.26 266.49 o 5 12 0 12.92 8.10 35.41 o 6 12 0 782.97 775.65 74.11 o 7 12 0 74.73 63.91 46.48 o 1 13 0 1976.48 1869.93 55.78 o 2 13 0 11833.84 12005.88 218.45 o 3 13 0 19700.25 19965.19 312.84 o 5 13 0 17319.56 17429.78 386.95 o 6 13 0 8536.77 8197.69 369.90 o 7 13 0 5625.02 5982.78 251.46 o 0 14 0 47874.81 48882.72 1097.30 o 1 14 0 45675.36 45814.74 730.66 o 2 14 0 22800.68 23417.63 394.69 o 3 14 0 21223.70 21763.91 339.68 o 4 14 0 6688.32 6614.40 156.86 o 5 14 0 1091.18 1269.06 87.37 o 6 14 0 25.33 13.39 65.43 o 7 14 0 467.69 522.60 70.92 o 1 15 0 438.99 409.36 29.17 o 2 15 0 2357.57 2373.55 91.69 o 3 15 0 15288.71 15307.92 253.10 o 4 15 0 5149.80 5158.95 135.47 o 5 15 0 15233.29 14921.41 428.73 o 6 15 0 6733.26 6808.24 208.03 o 7 15 0 6664.21 6439.06 311.85 o 0 16 0 16138.62 16500.93 505.96 o 1 16 0 18133.65 18048.10 278.97 o 2 16 0 4109.18 4243.49 103.34 o 3 16 0 12259.44 12343.79 242.28 o 4 16 0 762.31 774.82 55.17 o 5 16 0 57.42 103.67 34.61 o 6 16 0 116.49 204.73 62.54 o 7 16 0 401.33 525.51 134.35 o 1 17 0 119.02 171.04 51.22 o 2 17 0 1084.77 1150.56 52.13 o 3 17 0 801.47 764.58 51.18 o 4 17 0 2.18 60.89 40.46 o 5 17 0 984.30 1093.10 100.66 o 6 17 0 2.66 8.52 49.57 o 7 17 0 962.06 1015.22 124.65 o 0 18 0 4063.22 4078.08 229.32 o 1 18 0 756.01 632.16 68.24 o 2 18 0 685.07 676.29 67.54 o 3 18 0 136.40 119.50 50.81 o 4 18 0 89.71 65.31 42.96 o 5 18 0 1183.86 1306.02 111.02 o 6 18 0 85.07 256.43 66.26 o 7 18 0 721.33 923.90 112.29 o 1 19 0 61.30 72.74 62.92 o 2 19 0 124.84 202.57 54.89 o 3 19 0 169.63 51.09 53.84 o 4 19 0 535.66 671.06 89.67 o 5 19 0 2870.51 3026.10 139.68 o 6 19 0 3037.43 3250.62 263.77 o 0 20 0 10243.70 10149.63 433.76 o 1 20 0 7788.59 7355.01 244.50 o 2 20 0 1102.06 1329.94 120.99 o 3 20 0 4226.51 4370.17 193.49 o 4 20 0 8.21 100.30 59.09 o 5 20 0 112.86 112.62 64.26 o 6 20 0 221.02 355.73 120.50 o 1 21 0 1784.83 1775.42 224.47 o 2 21 0 1644.39 1592.72 106.73 o 3 21 0 7918.52 8593.79 359.17 o 4 21 0 2094.74 2192.45 145.57 o 5 21 0 6777.84 6636.10 266.94 o 6 21 0 1696.91 2007.40 223.98 o 0 22 0 817.15 827.03 121.90 o 1 22 0 5695.86 5662.85 213.41 o 2 22 0 47.40 131.31 49.95 o 3 22 0 3719.08 3524.61 284.79 o 4 22 0 283.80 347.02 78.17 o 5 22 0 386.08 471.11 91.18 o 6 22 0 1.94 60.04 92.94 o 1 23 0 205.88 217.20 55.82 o 2 23 0 1203.93 1145.03 96.47 o 3 23 0 869.08 916.07 103.25 o 4 23 0 366.19 488.02 88.98 o 5 23 0 1966.07 2313.31 211.82 o 6 23 0 249.00 349.96 127.67 o 0 24 0 562.02 651.84 116.84 o 1 24 0 384.19 425.29 70.12 o 2 24 0 778.57 755.02 85.93 o 3 24 0 801.67 832.15 101.70 o 4 24 0 248.93 249.58 77.00 o 5 24 0 645.58 787.67 113.19 o 6 24 0 209.57 266.87 120.92 o 1 25 0 730.93 742.29 84.84 o 2 25 0 2746.30 2688.36 147.43 o 3 25 0 4458.05 4380.27 210.76 o 4 25 0 3086.71 3299.71 190.25 o 5 25 0 2917.79 3331.95 201.64 o 0 26 0 7317.05 7680.49 385.82 o 1 26 0 10581.69 10500.64 340.11 o 2 26 0 4095.83 4175.40 190.07 o 3 26 0 7104.06 7234.29 286.83 o 4 26 0 496.58 581.54 156.35 o 5 26 0 180.36 359.39 97.53 o 1 27 0 207.17 444.62 77.11 o 2 27 0 1394.95 1458.05 290.00 o 3 27 0 4358.68 4231.18 214.13 o 4 27 0 2510.61 2769.79 232.42 o 5 27 0 7543.55 8466.29 350.24 o 0 28 0 4188.47 4110.70 270.38 o 1 28 0 10980.06 10962.97 360.18 o 2 28 0 4115.96 4274.51 197.07 o 3 28 0 3854.08 4047.24 244.86 o 4 28 0 1118.40 1341.68 138.06 o 1 29 0 429.26 860.59 98.21 o 2 29 0 3143.88 3028.11 167.97 o 3 29 0 2303.97 2254.31 166.13 o 4 29 0 3309.80 3401.38 240.01 o 0 30 0 79.71 177.16 80.99 o 1 30 0 662.59 673.16 119.51 o 2 30 0 453.39 620.69 179.97 o 3 30 0 795.35 750.93 111.20 o 4 30 0 771.25 690.12 121.11 o 1 31 0 7.15 112.31 58.30 o 2 31 0 23.68 66.65 101.23 o 3 31 0 33.28 148.41 72.60 o 0 32 0 106.81 106.44 97.30 o 1 32 0 842.32 934.43 111.72 o 2 32 0 9.86 30.09 93.78 o 1 33 0 126.20 241.24 84.64 o 0 34 0 5320.95 5655.79 360.37 o 1 34 0 4039.29 4152.46 297.38 o -8 1 1 1287.08 1248.32 125.77 o -7 1 1 1761.49 1598.39 355.38 o -6 1 1 675.94 722.21 68.32 o -5 1 1 140.95 185.63 41.62 o -4 1 1 1613.41 1616.69 65.16 o -3 1 1 7226.67 7420.30 114.22 o -2 1 1 40310.65 41026.23 526.40 o -1 1 1 4005.08 4370.51 100.39 o 1 1 1 938.60 908.28 25.14 o 2 1 1 2674.62 2587.02 79.91 o 3 1 1 13.55 30.07 15.86 o 4 1 1 374.33 390.27 40.22 o 5 1 1 75.54 110.47 36.77 o 6 1 1 258.25 266.39 52.47 o 7 1 1 13.95 18.13 50.39 o -8 2 1 3511.32 3483.30 191.25 o -7 2 1 508.88 418.24 74.63 o -6 2 1 7333.46 6913.80 199.77 o -5 2 1 3385.60 3419.60 150.39 o -4 2 1 6070.05 6232.19 134.04 o -3 2 1 8010.59 8504.04 139.68 o -2 2 1 6365.29 6649.71 108.10 o -1 2 1 15738.89 17038.36 271.49 o 0 2 1 5657.18 5795.61 195.91 o 1 2 1 2085.87 2199.63 58.22 o 2 2 1 6493.73 6353.85 125.55 o 3 2 1 4636.22 4560.89 129.15 o 4 2 1 15097.22 15350.20 287.97 o 5 2 1 10928.60 10746.04 262.73 o 6 2 1 14154.14 13554.89 328.07 o 7 2 1 2868.15 2792.59 161.06 o -8 3 1 2525.92 2453.07 347.43 o -7 3 1 3931.83 3768.52 148.75 o -6 3 1 386.08 418.10 57.83 o -5 3 1 441.07 508.85 57.20 o -4 3 1 2692.17 2593.57 104.51 o -3 3 1 6541.71 7268.02 122.58 o -2 3 1 20733.47 21397.57 309.74 o -1 3 1 16233.04 16855.30 311.83 o 0 3 1 59153.05 37423.98 1166.03 o 1 3 1 42524.32 41494.03 751.70 o 2 3 1 4016.33 3995.86 87.37 o 3 3 1 20687.59 21499.47 363.65 o 4 3 1 4252.89 3949.37 125.77 o 5 3 1 144.77 127.95 41.13 o 6 3 1 121.24 105.85 44.19 o 7 3 1 844.93 915.07 94.66 o 8 3 1 2596.60 2458.04 248.73 o -8 4 1 4700.39 4441.01 215.88 o -7 4 1 3894.30 3959.33 184.24 o -6 4 1 24412.50 24448.58 515.91 o -5 4 1 27260.79 27612.81 556.32 o -4 4 1 26201.08 25438.93 430.91 o -3 4 1 25232.17 25488.56 421.14 o -2 4 1 10901.32 11317.60 225.96 o -1 4 1 20.28 18.37 13.39 o 0 4 1 3883.81 4386.09 180.61 o 1 4 1 1303.22 1365.88 38.73 o 2 4 1 26085.10 28616.40 412.62 o 3 4 1 16020.66 17424.27 303.06 o 4 4 1 5629.27 5570.47 156.38 o 5 4 1 3798.56 3578.61 128.88 o 6 4 1 8892.28 8980.22 244.49 o 7 4 1 2215.03 2107.18 116.58 o 8 4 1 4261.43 3852.27 292.17 o -8 5 1 2191.71 2184.68 156.84 o -7 5 1 1171.98 1154.07 86.94 o -6 5 1 488.76 480.11 58.55 o -5 5 1 1201.51 1205.37 75.91 o -4 5 1 457.45 501.60 38.74 o -3 5 1 3719.65 3833.93 89.96 o -2 5 1 3358.57 3324.21 89.99 o -1 5 1 11153.12 11792.89 225.55 o 0 5 1 28814.68 29106.41 2992.82 o 1 5 1 17649.91 18686.71 302.45 o 2 5 1 29040.02 30365.93 436.98 o 3 5 1 4764.77 4626.81 122.79 o 4 5 1 3234.28 3422.16 94.83 o 5 5 1 1718.34 1592.50 88.04 o 6 5 1 69.61 63.57 42.52 o 7 5 1 232.31 243.01 56.27 o 8 5 1 2355.12 2624.79 243.95 o -8 6 1 282.12 188.45 109.88 o -7 6 1 280.41 228.60 52.31 o -6 6 1 987.57 1008.14 76.62 o -5 6 1 1767.00 1893.51 95.74 o -4 6 1 384.54 407.02 41.73 o -3 6 1 3677.90 3506.28 86.35 o -2 6 1 293.72 339.77 33.20 o -1 6 1 31880.60 32601.27 726.31 o 0 6 1 3212.44 4018.51 117.05 o 1 6 1 808.66 780.07 30.30 o 2 6 1 191.21 157.57 22.87 o 3 6 1 1802.81 1793.50 76.12 o 4 6 1 85.72 112.56 29.52 o 5 6 1 7218.16 6928.24 227.48 o 6 6 1 226.36 240.27 51.29 o 7 6 1 1981.48 1983.42 137.62 o 8 6 1 569.06 638.90 139.48 o -8 7 1 2.85 -14.29 56.49 o -7 7 1 0.75 49.91 41.99 o -6 7 1 448.50 411.73 59.37 o -5 7 1 66.73 78.36 39.33 o -4 7 1 420.37 399.86 37.70 o -3 7 1 2277.71 2272.29 67.09 o -2 7 1 1908.68 1989.14 55.54 o -1 7 1 9564.66 10264.86 247.68 o 0 7 1 6498.95 7446.94 287.54 o 1 7 1 325.68 411.24 26.22 o 2 7 1 1500.66 1337.67 57.12 o 3 7 1 3731.12 4025.78 103.42 o 4 7 1 1199.92 1249.49 89.13 o 5 7 1 212.09 229.68 47.12 o 6 7 1 74.23 66.33 57.62 o 7 7 1 36.91 104.09 75.42 o -8 8 1 1038.65 1278.38 129.35 o -7 8 1 126.62 133.56 65.25 o -6 8 1 3240.79 3002.12 176.53 o -5 8 1 735.67 696.84 61.77 o -4 8 1 6169.72 6431.81 144.08 o -3 8 1 3987.90 4049.81 112.39 o -2 8 1 13654.19 15147.37 259.70 o -1 8 1 4215.69 4300.83 230.95 o 0 8 1 75.37 65.02 27.65 o 1 8 1 2090.53 2253.33 61.93 o 2 8 1 11.38 21.39 19.35 o 3 8 1 2027.18 2095.14 89.36 o 4 8 1 6165.00 6120.90 142.11 o 5 8 1 1032.44 1017.12 74.40 o 6 8 1 4882.55 4600.62 160.69 o 7 8 1 439.81 528.80 72.16 o -8 9 1 4373.05 4344.36 217.68 o -7 9 1 3456.86 3497.13 143.59 o -6 9 1 240.14 295.01 54.10 o -5 9 1 666.61 737.76 72.08 o -4 9 1 2353.59 2369.18 78.67 o -3 9 1 2671.81 2631.57 75.37 o -2 9 1 8323.03 8046.63 215.58 o -1 9 1 34823.68 36630.30 667.06 o 0 9 1 23117.41 22316.15 518.71 o 1 9 1 11106.66 11865.38 205.56 o 2 9 1 34901.75 37163.51 536.14 o 3 9 1 11791.03 12187.13 268.77 o 4 9 1 5058.34 5028.84 165.81 o 5 9 1 1690.42 1639.63 89.19 o 6 9 1 186.96 173.12 49.35 o 7 9 1 34.12 25.37 49.20 o -8 10 1 2354.90 2315.94 171.11 o -7 10 1 4073.98 3859.89 151.55 o -6 10 1 8754.12 8989.67 241.68 o -5 10 1 7525.45 7555.65 202.68 o -4 10 1 19482.47 19706.80 351.46 o -3 10 1 22598.05 23086.43 392.69 o -2 10 1 26879.35 28038.66 649.80 o -1 10 1 68.56 17.30 16.36 o 0 10 1 977.11 812.01 64.47 o 1 10 1 246.43 276.10 21.99 o 2 10 1 9867.33 10428.60 189.00 o 3 10 1 6226.43 6190.51 189.80 o 4 10 1 16407.15 16663.08 309.90 o 5 10 1 12857.07 12632.38 302.21 o 6 10 1 13746.12 13528.64 331.67 o 7 10 1 4251.35 4102.92 164.16 o -8 11 1 4457.26 4455.13 223.63 o -7 11 1 1220.94 1393.87 96.52 o -6 11 1 7.83 -10.64 35.58 o -5 11 1 14.72 47.22 37.53 o -4 11 1 2267.51 2352.46 95.47 o -3 11 1 9220.47 9427.27 163.68 o -2 11 1 8120.45 8377.33 183.34 o -1 11 1 32355.08 34161.52 729.75 o 0 11 1 40235.44 41158.54 765.71 o 1 11 1 25308.49 26095.92 507.60 o 2 11 1 25662.25 26744.91 397.88 o 3 11 1 20253.79 21092.24 425.00 o 4 11 1 6253.70 6378.58 177.45 o 5 11 1 699.52 745.39 67.46 o 6 11 1 244.64 311.92 96.06 o 7 11 1 49.63 162.64 76.91 o -7 12 1 2807.60 2882.96 130.43 o -6 12 1 5017.48 4832.92 163.38 o -5 12 1 11815.79 11717.67 241.27 o -4 12 1 5036.21 4837.84 142.74 o -3 12 1 11166.53 11335.64 231.50 o -2 12 1 4140.77 4185.35 95.88 o -1 12 1 388.42 425.21 26.60 o 0 12 1 9330.50 10105.08 219.30 o 1 12 1 4449.78 4619.39 114.22 o 2 12 1 1120.53 1037.85 58.47 o 3 12 1 5992.48 5941.31 136.60 o 4 12 1 550.56 471.73 58.33 o 5 12 1 5861.76 6008.22 181.23 o 6 12 1 911.63 908.67 80.40 o 7 12 1 2803.92 2855.06 171.08 o -7 13 1 7.85 20.88 49.44 o -6 13 1 104.33 50.29 38.35 o -5 13 1 1904.44 1927.28 81.37 o -4 13 1 765.03 799.19 52.22 o -3 13 1 4054.79 3978.81 104.68 o -2 13 1 1196.93 1161.27 47.32 o -1 13 1 4183.66 4258.08 122.23 o 0 13 1 1453.10 1657.56 48.92 o 1 13 1 4745.22 4727.48 101.50 o 2 13 1 1559.67 1589.16 51.61 o 3 13 1 2708.07 2651.77 130.74 o 4 13 1 4.88 -4.12 27.95 o 5 13 1 77.54 70.14 38.63 o 6 13 1 6.86 1.59 39.81 o 7 13 1 335.62 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