#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/76/2207621.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207621_Fobs loop_ _publ_author_name 'He, Xiang-Jiu' 'Lobkovsky, Emil' 'Liu, Rui Hai' _publ_section_title ; (R*)-Methyl 3-carboxy-2-hydroxypropanoate ; _journal_coeditor_code OM6268 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4104 _journal_page_last o4106 _journal_volume 61 _journal_year 2005 _space_group_IT_number 5 _symmetry_space_group_name_Hall 'C 2y' _symmetry_space_group_name_H-M 'C 1 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.415 _cell_angle_gamma 90.000 _cell_length_a 22.6989 _cell_length_b 4.1854 _cell_length_c 6.9782 _exptl_crystal_F_000 312.00 _reflns_d_resolution_high 0.6305 _[local]_cod_data_source_file om6268Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xh3 in C2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.06 -0.09 0.11 o 4 0 0 444.09 439.84 6.88 o 6 0 0 3518.70 3383.24 53.12 o 8 0 0 720.38 731.82 13.51 o 10 0 0 1508.13 1704.65 39.72 o 12 0 0 568.86 589.63 10.84 o 14 0 0 561.95 617.59 11.36 o 16 0 0 95.52 91.60 4.06 o 18 0 0 321.53 358.95 8.79 o 20 0 0 44.37 38.23 1.69 o 22 0 0 694.14 656.10 17.57 o 24 0 0 2.05 1.52 0.64 o 26 0 0 47.31 41.75 2.16 o 28 0 0 17.32 17.53 1.26 o 30 0 0 17.93 14.11 1.79 o 32 0 0 116.75 119.34 6.86 o 34 0 0 15.11 16.00 2.01 o 1 1 0 2760.13 2833.40 38.98 o 3 1 0 804.36 837.36 16.46 o 5 1 0 4117.51 4051.84 77.13 o 7 1 0 595.94 623.14 14.38 o 9 1 0 1080.49 1196.44 22.40 o 11 1 0 536.61 573.46 10.31 o 13 1 0 746.97 835.79 14.49 o 15 1 0 212.32 235.37 3.77 o 17 1 0 87.67 101.80 1.86 o 19 1 0 24.84 27.71 0.68 o 21 1 0 109.38 100.52 1.77 o 23 1 0 104.27 99.92 2.05 o 25 1 0 52.27 50.41 1.37 o 27 1 0 47.94 43.61 1.20 o 29 1 0 54.92 53.43 1.60 o 31 1 0 23.39 22.77 1.51 o 33 1 0 74.74 74.12 4.30 o 0 2 0 100.94 95.38 2.30 o 2 2 0 219.99 222.70 3.67 o 4 2 0 1276.30 1293.56 21.07 o 6 2 0 821.19 922.46 17.83 o 8 2 0 517.21 536.80 16.05 o 10 2 0 573.58 576.46 12.19 o 12 2 0 71.89 77.15 1.63 o 14 2 0 258.93 240.70 4.84 o 16 2 0 71.39 69.68 1.99 o 18 2 0 118.20 109.67 4.55 o 20 2 0 47.36 50.74 1.49 o 22 2 0 64.69 64.32 1.69 o 24 2 0 75.12 76.24 1.99 o 26 2 0 23.75 25.98 1.11 o 28 2 0 52.15 51.02 1.73 o 30 2 0 17.93 19.07 1.47 o 32 2 0 16.14 16.42 2.26 o 1 3 0 307.12 300.54 5.90 o 3 3 0 533.71 548.16 9.77 o 5 3 0 186.54 200.74 3.69 o 7 3 0 215.87 221.49 4.42 o 9 3 0 174.46 191.15 3.36 o 11 3 0 43.24 38.16 1.27 o 13 3 0 358.27 341.31 10.58 o 15 3 0 202.04 191.28 6.14 o 17 3 0 257.41 256.73 11.02 o 19 3 0 103.72 100.77 5.00 o 21 3 0 87.53 87.98 5.27 o 23 3 0 40.33 45.30 3.91 o 25 3 0 40.89 43.23 2.18 o 27 3 0 31.67 28.75 1.91 o 29 3 0 1.64 1.97 1.93 o 0 4 0 96.92 92.02 2.80 o 2 4 0 63.45 55.83 1.41 o 4 4 0 76.42 69.24 1.66 o 6 4 0 27.32 26.60 0.90 o 8 4 0 50.75 47.25 2.51 o 10 4 0 73.58 65.07 1.69 o 12 4 0 120.31 117.91 2.95 o 14 4 0 6.72 7.63 0.55 o 16 4 0 3.04 3.09 0.69 o 18 4 0 22.37 20.29 1.50 o 20 4 0 1.61 0.08 1.17 o 22 4 0 62.11 67.22 4.72 o 24 4 0 71.88 79.45 5.50 o 26 4 0 15.72 15.06 2.52 o 1 5 0 0.52 -0.72 0.72 o 3 5 0 0.20 -0.15 0.75 o 5 5 0 6.00 4.83 0.85 o 7 5 0 57.32 55.77 2.04 o 9 5 0 53.88 51.43 1.96 o 11 5 0 2.52 1.32 0.72 o 13 5 0 42.73 42.24 2.31 o 15 5 0 21.42 19.95 2.12 o 17 5 0 16.96 14.49 1.50 o 19 5 0 16.86 18.66 1.94 o 21 5 0 39.89 44.96 3.65 o 23 5 0 3.47 4.61 3.01 o 0 6 0 20.99 22.33 2.36 o 2 6 0 8.03 6.05 1.35 o 4 6 0 0.35 0.67 1.28 o 6 6 0 20.85 19.02 2.04 o 8 6 0 6.35 4.64 1.38 o 10 6 0 15.56 18.44 2.82 o -34 0 1 2.47 0.31 1.46 o -32 0 1 1.08 0.98 1.10 o -30 0 1 99.11 94.89 6.64 o -28 0 1 19.93 20.09 2.05 o -26 0 1 83.40 83.07 3.07 o -24 0 1 7.20 6.51 0.80 o -22 0 1 7.28 6.50 0.67 o -20 0 1 496.93 507.69 15.63 o -18 0 1 201.37 196.18 5.39 o -16 0 1 12.12 9.51 0.74 o -14 0 1 242.05 271.22 5.08 o -12 0 1 12.78 10.87 0.36 o -10 0 1 1550.16 1762.36 30.22 o -8 0 1 536.77 618.17 11.95 o -6 0 1 916.75 855.48 13.25 o -2 0 1 519.49 511.39 8.98 o 0 0 1 1333.90 1250.91 33.70 o 2 0 1 928.15 935.28 15.47 o 4 0 1 1607.57 1745.96 28.76 o 6 0 1 1633.20 1878.46 30.82 o 8 0 1 389.25 497.24 9.06 o 10 0 1 255.32 312.72 5.76 o 12 0 1 1261.35 1458.38 26.82 o 14 0 1 168.94 194.94 3.63 o 16 0 1 43.27 52.33 1.27 o 18 0 1 253.46 238.72 5.24 o 20 0 1 4.79 6.54 1.06 o 22 0 1 440.43 412.67 11.25 o 24 0 1 5.21 5.69 0.75 o 26 0 1 132.42 131.40 4.20 o 28 0 1 239.25 232.31 12.51 o 30 0 1 4.05 5.26 1.15 o 32 0 1 171.85 172.50 9.40 o 34 0 1 62.07 69.41 7.96 o -33 1 1 32.56 30.72 2.19 o -31 1 1 27.15 24.85 1.65 o -29 1 1 52.94 55.79 2.15 o -27 1 1 13.60 14.23 0.73 o -25 1 1 16.54 15.70 0.72 o -23 1 1 163.66 160.42 4.49 o -21 1 1 21.51 18.55 0.85 o -19 1 1 1.04 2.80 0.30 o -17 1 1 305.61 313.56 4.78 o -15 1 1 719.10 749.04 11.35 o -13 1 1 624.62 683.97 10.40 o -11 1 1 682.22 681.15 11.91 o -9 1 1 2419.39 2509.09 46.61 o -7 1 1 801.31 841.27 14.16 o -5 1 1 7021.80 6293.40 100.10 o -3 1 1 614.43 587.50 7.77 o -1 1 1 9649.23 7873.21 264.43 o 1 1 1 3069.74 3022.30 45.17 o 3 1 1 792.17 780.05 13.65 o 5 1 1 1512.32 1583.06 24.47 o 7 1 1 62.32 66.91 1.22 o 9 1 1 1827.73 1982.82 31.40 o 11 1 1 24.37 22.69 0.50 o 13 1 1 591.80 584.92 8.92 o 15 1 1 45.07 44.24 0.82 o 17 1 1 235.07 212.82 3.44 o 19 1 1 76.97 73.95 1.35 o 21 1 1 312.23 294.66 5.32 o 23 1 1 289.78 286.28 5.19 o 25 1 1 58.60 58.38 1.39 o 27 1 1 39.35 38.79 1.19 o 29 1 1 25.82 27.12 1.40 o 31 1 1 61.00 62.86 2.92 o 33 1 1 25.42 25.94 2.26 o -32 2 1 5.53 6.04 1.98 o -30 2 1 12.28 15.03 1.99 o -28 2 1 36.01 29.41 1.47 o -26 2 1 58.44 58.96 3.10 o -24 2 1 2.35 2.63 0.65 o -22 2 1 114.42 114.09 3.00 o -20 2 1 38.92 40.04 1.26 o -18 2 1 230.77 217.72 5.82 o -16 2 1 1189.51 1156.66 25.52 o -14 2 1 437.13 440.36 9.30 o -12 2 1 68.97 73.60 1.54 o -10 2 1 489.53 508.58 9.03 o -8 2 1 379.73 394.90 7.48 o -6 2 1 1798.87 1860.11 47.53 o -4 2 1 466.19 511.28 11.84 o -2 2 1 56.23 54.28 0.98 o 0 2 1 428.22 381.39 6.43 o 2 2 1 291.41 339.97 5.31 o 4 2 1 270.57 270.21 4.67 o 6 2 1 827.26 797.92 12.81 o 8 2 1 870.87 953.02 16.11 o 10 2 1 79.24 74.81 2.07 o 12 2 1 171.29 177.45 3.60 o 14 2 1 7.61 6.76 0.68 o 16 2 1 450.34 420.17 8.71 o 18 2 1 215.67 209.98 4.73 o 20 2 1 20.62 22.21 0.95 o 22 2 1 83.69 77.21 2.22 o 24 2 1 39.53 38.76 1.26 o 26 2 1 36.27 38.44 1.38 o 28 2 1 8.86 7.37 0.93 o 30 2 1 19.94 22.85 1.77 o -29 3 1 54.33 52.92 3.71 o -27 3 1 51.22 52.88 3.07 o -25 3 1 12.04 12.02 1.39 o -23 3 1 59.76 61.61 3.68 o -21 3 1 5.21 5.24 0.97 o -19 3 1 26.65 27.43 1.49 o -17 3 1 83.62 74.83 2.80 o -15 3 1 108.95 97.44 7.30 o -13 3 1 136.81 132.93 3.03 o -11 3 1 249.50 250.98 5.29 o -9 3 1 158.13 154.20 3.14 o -7 3 1 359.31 382.45 6.30 o -5 3 1 157.10 157.56 2.87 o -3 3 1 242.26 226.90 5.00 o -1 3 1 8.04 9.67 0.38 o 1 3 1 236.64 237.79 4.45 o 3 3 1 122.47 111.34 2.08 o 5 3 1 221.42 227.26 4.09 o 7 3 1 73.86 81.63 1.71 o 9 3 1 107.73 101.08 2.81 o 11 3 1 104.52 100.48 3.44 o 13 3 1 135.76 128.06 3.59 o 15 3 1 224.87 222.16 6.06 o 17 3 1 48.39 48.13 5.24 o 19 3 1 140.05 134.88 7.23 o 21 3 1 27.34 26.60 1.41 o 23 3 1 75.31 74.92 3.39 o 25 3 1 26.98 28.22 1.75 o 27 3 1 32.80 35.07 2.33 o 29 3 1 11.13 10.59 2.24 o -26 4 1 62.42 63.51 4.37 o -24 4 1 14.14 14.82 1.65 o -22 4 1 10.97 11.32 1.51 o -20 4 1 7.59 7.80 0.95 o -18 4 1 52.92 48.57 3.82 o -16 4 1 49.62 52.55 2.98 o -14 4 1 5.40 5.49 0.55 o -12 4 1 68.21 65.98 1.73 o -10 4 1 35.60 32.32 1.07 o -8 4 1 64.02 61.49 1.62 o -6 4 1 63.14 57.93 1.46 o -4 4 1 45.84 45.45 1.23 o -2 4 1 101.23 90.67 3.69 o 0 4 1 50.78 48.37 1.56 o 2 4 1 31.11 29.77 1.46 o 4 4 1 162.03 167.49 3.81 o 6 4 1 221.66 220.69 4.95 o 8 4 1 68.58 72.12 1.84 o 10 4 1 250.34 252.54 5.65 o 12 4 1 57.92 56.49 1.52 o 14 4 1 3.93 3.19 0.64 o 16 4 1 88.60 89.45 2.97 o 18 4 1 11.13 10.56 1.31 o 20 4 1 26.99 32.43 1.94 o 22 4 1 3.75 2.26 1.49 o 24 4 1 10.28 9.29 2.02 o -23 5 1 32.51 35.13 3.76 o -21 5 1 57.48 68.28 3.41 o -19 5 1 11.05 12.13 3.32 o -17 5 1 10.22 11.15 1.57 o -15 5 1 13.82 13.65 1.20 o -13 5 1 56.14 59.62 2.53 o -11 5 1 1.36 0.13 0.73 o -9 5 1 10.00 9.27 0.95 o -7 5 1 14.77 15.09 1.21 o -5 5 1 8.60 7.46 0.90 o -3 5 1 65.67 58.70 2.14 o -1 5 1 28.90 30.52 1.37 o 1 5 1 80.81 81.59 4.31 o 3 5 1 2.54 1.58 0.82 o 5 5 1 61.74 59.87 3.19 o 7 5 1 49.81 47.46 2.25 o 9 5 1 58.48 55.20 2.07 o 11 5 1 26.54 25.50 1.47 o 13 5 1 30.81 26.68 2.00 o 15 5 1 3.25 3.81 1.27 o 17 5 1 5.62 4.07 1.38 o 19 5 1 32.81 32.43 2.28 o 21 5 1 2.99 2.95 1.90 o -10 6 1 20.61 20.31 2.79 o -8 6 1 6.63 7.27 1.44 o -6 6 1 1.41 1.92 1.31 o -4 6 1 8.97 9.12 1.41 o -2 6 1 3.25 3.21 1.31 o 0 6 1 1.16 1.03 1.26 o 2 6 1 21.66 22.38 1.67 o 4 6 1 4.36 4.73 1.33 o 6 6 1 43.10 42.06 6.73 o 8 6 1 21.56 17.97 1.60 o 10 6 1 3.18 5.26 2.46 o -36 0 2 0.51 -0.94 1.89 o -34 0 2 18.39 15.28 1.94 o -32 0 2 18.17 18.65 1.63 o -30 0 2 53.53 65.41 2.60 o -28 0 2 11.09 12.19 2.28 o -26 0 2 1.10 1.28 0.71 o -24 0 2 44.47 41.52 1.56 o -22 0 2 132.45 135.29 3.82 o -20 0 2 25.77 23.31 1.00 o -18 0 2 100.15 115.22 2.74 o -16 0 2 191.35 214.29 4.59 o -14 0 2 767.42 801.84 16.95 o -12 0 2 2.99 3.18 0.25 o -10 0 2 111.87 131.20 3.98 o -8 0 2 2935.66 2988.38 50.70 o -6 0 2 43.43 47.96 0.90 o -4 0 2 129.03 132.66 2.76 o -2 0 2 670.44 579.36 12.60 o 0 0 2 1310.80 1359.66 29.37 o 2 0 2 188.56 184.04 3.46 o 4 0 2 6431.75 6282.85 128.77 o 6 0 2 1256.22 1470.79 27.36 o 8 0 2 721.62 838.49 14.70 o 10 0 2 252.26 297.09 6.15 o 12 0 2 786.89 847.96 17.89 o 14 0 2 21.06 16.69 0.62 o 16 0 2 9.01 10.57 1.29 o 18 0 2 211.10 190.33 4.97 o 20 0 2 50.19 46.37 2.12 o 22 0 2 531.51 536.74 16.33 o 24 0 2 5.32 5.04 0.84 o 26 0 2 5.98 4.90 0.98 o 28 0 2 9.93 10.94 1.22 o 30 0 2 2.13 1.78 1.21 o 32 0 2 1.02 0.70 1.55 o -33 1 2 11.74 9.38 1.74 o -31 1 2 30.18 31.43 2.00 o -29 1 2 46.94 47.27 1.54 o -27 1 2 41.64 40.33 1.18 o -25 1 2 125.70 121.57 2.52 o -23 1 2 146.04 145.29 2.81 o -21 1 2 393.55 408.18 7.18 o -19 1 2 484.77 476.19 7.68 o -17 1 2 404.96 399.43 6.04 o -15 1 2 294.16 304.47 4.75 o -13 1 2 168.91 158.55 2.39 o -11 1 2 206.20 214.63 3.52 o -9 1 2 749.27 818.33 15.49 o -7 1 2 1001.01 1047.15 14.88 o -5 1 2 452.17 525.12 10.45 o -3 1 2 2596.45 2688.00 43.23 o -1 1 2 1675.49 1825.21 33.00 o 1 1 2 176.08 175.21 2.78 o 3 1 2 1721.40 1938.82 25.61 o 5 1 2 1156.93 1186.69 17.78 o 7 1 2 400.99 424.40 6.93 o 9 1 2 282.25 298.55 4.22 o 11 1 2 449.36 486.46 7.31 o 13 1 2 38.03 38.45 0.76 o 15 1 2 257.16 265.78 4.65 o 17 1 2 1246.01 1216.76 19.06 o 19 1 2 67.27 64.90 1.28 o 21 1 2 85.39 80.12 1.65 o 23 1 2 46.34 45.67 1.17 o 25 1 2 7.44 7.03 0.62 o 27 1 2 114.78 111.06 3.78 o 29 1 2 43.26 46.92 1.90 o 31 1 2 53.70 52.56 2.91 o -32 2 2 43.67 40.03 3.03 o -30 2 2 1.58 1.59 1.31 o -28 2 2 2.76 3.39 0.93 o -26 2 2 32.96 32.68 1.88 o -24 2 2 56.62 55.42 1.80 o -22 2 2 89.11 86.31 1.88 o -20 2 2 271.93 269.07 5.24 o -18 2 2 12.33 13.99 0.52 o -16 2 2 120.08 115.95 2.54 o -14 2 2 67.89 64.79 1.26 o -12 2 2 307.46 280.06 4.67 o -10 2 2 1961.13 2046.85 35.90 o -8 2 2 55.18 72.66 1.63 o -6 2 2 867.87 918.82 15.79 o -4 2 2 2041.01 2088.40 33.06 o -2 2 2 572.66 598.10 9.12 o 0 2 2 823.11 881.24 14.56 o 2 2 2 182.50 192.59 3.57 o 4 2 2 622.87 661.69 9.93 o 6 2 2 165.34 171.16 2.61 o 8 2 2 32.24 36.74 0.71 o 10 2 2 91.23 98.32 1.67 o 12 2 2 704.48 677.92 11.06 o 14 2 2 532.11 519.79 9.34 o 16 2 2 292.84 288.57 5.40 o 18 2 2 422.88 398.95 7.13 o 20 2 2 95.71 99.88 2.00 o 22 2 2 95.24 100.06 2.36 o 24 2 2 43.95 42.26 1.36 o 26 2 2 40.24 43.08 1.66 o 28 2 2 24.24 24.09 1.48 o 30 2 2 16.19 18.07 2.12 o -29 3 2 14.54 12.63 2.02 o -27 3 2 33.33 30.53 1.92 o -25 3 2 2.16 1.88 0.81 o -23 3 2 4.87 5.08 0.70 o -21 3 2 65.28 65.43 1.94 o -19 3 2 21.66 18.88 0.91 o -17 3 2 200.34 194.58 4.37 o -15 3 2 110.04 121.09 2.80 o -13 3 2 5.95 6.29 0.70 o -11 3 2 15.46 14.91 0.59 o -9 3 2 4.17 4.70 0.41 o -7 3 2 480.44 473.45 8.43 o -5 3 2 151.84 138.40 2.68 o -3 3 2 0.09 0.27 0.28 o -1 3 2 52.56 49.66 1.06 o 1 3 2 67.55 72.22 1.38 o 3 3 2 254.03 264.44 4.63 o 5 3 2 399.46 399.69 7.22 o 7 3 2 2.77 2.41 0.39 o 9 3 2 469.71 458.48 9.58 o 11 3 2 41.02 44.38 1.16 o 13 3 2 10.49 11.28 0.50 o 15 3 2 15.86 15.24 0.80 o 17 3 2 5.85 6.20 0.84 o 19 3 2 35.55 35.11 1.43 o 21 3 2 44.39 46.97 2.85 o 23 3 2 13.08 14.59 1.96 o 25 3 2 42.48 48.49 2.35 o 27 3 2 0.73 0.54 1.76 o -26 4 2 20.69 22.88 2.76 o -24 4 2 54.42 57.64 3.79 o -22 4 2 76.06 77.55 4.03 o -20 4 2 51.44 54.54 4.31 o -18 4 2 7.90 8.49 0.86 o -16 4 2 72.05 65.81 2.02 o -14 4 2 6.86 4.95 0.60 o -12 4 2 21.83 25.75 0.96 o -10 4 2 53.66 45.16 1.33 o -8 4 2 30.52 29.52 1.05 o -6 4 2 47.93 46.81 1.29 o -4 4 2 341.07 341.41 7.14 o -2 4 2 6.75 5.77 0.55 o 0 4 2 300.55 316.47 7.89 o 2 4 2 69.64 69.94 1.72 o 4 4 2 67.69 72.54 1.77 o 6 4 2 43.79 43.90 1.30 o 8 4 2 60.38 53.90 1.49 o 10 4 2 35.71 36.48 1.17 o 12 4 2 32.71 33.02 1.41 o 14 4 2 54.58 55.35 3.04 o 16 4 2 1.92 2.15 0.70 o 18 4 2 65.37 67.32 3.10 o 20 4 2 8.83 6.71 0.97 o 22 4 2 5.75 5.71 1.58 o 24 4 2 6.98 9.38 2.36 o -23 5 2 24.94 26.38 3.43 o -21 5 2 3.34 0.93 1.78 o -19 5 2 4.66 4.40 1.66 o -17 5 2 3.16 2.38 1.49 o -15 5 2 17.00 18.05 1.42 o -13 5 2 27.09 26.63 1.20 o -11 5 2 11.38 12.51 1.07 o -9 5 2 9.41 9.58 1.01 o -7 5 2 27.50 27.17 2.31 o -5 5 2 63.04 66.00 2.31 o -3 5 2 97.30 94.29 3.06 o -1 5 2 38.80 37.93 1.88 o 1 5 2 27.14 32.01 2.08 o 3 5 2 39.15 41.44 1.78 o 5 5 2 176.20 170.77 7.57 o 7 5 2 29.82 34.92 1.98 o 9 5 2 74.33 71.61 2.52 o 11 5 2 13.97 12.92 1.28 o 13 5 2 18.96 16.18 2.67 o 15 5 2 18.46 17.07 4.79 o 17 5 2 11.09 10.46 1.73 o 19 5 2 9.40 8.67 1.88 o -10 6 2 11.20 8.61 1.52 o -8 6 2 20.66 25.58 2.31 o -6 6 2 16.96 16.22 2.23 o -4 6 2 11.25 10.63 1.47 o -2 6 2 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