#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2207622.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207622_Fobs loop_ _publ_author_name 'Dai, Yu-Mei' 'Huang, Jin-Feng' 'Shen, Hui-Ying' _publ_section_title ; Bis(1,10-phenanthroline-\k^2^N,N)bis(thiosalicylato-1\k^2^O,O':2\k^2^O',S)dizinc(II) ; _journal_coeditor_code OM6269 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2491 _journal_page_last m2492 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.924 _cell_angle_gamma 90.000 _cell_length_a 18.7855 _cell_length_b 9.5811 _cell_length_c 18.5225 _exptl_crystal_F_000 1616.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file om6269Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 567.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2139.17 2042.29 25.36 o 6 0 0 769.84 842.97 25.80 o 8 0 0 4605.01 4218.37 66.90 o 10 0 0 5244.94 5663.40 76.95 o 12 0 0 544.56 391.32 28.42 o 14 0 0 2387.72 2278.39 72.58 o 16 0 0 1373.57 1306.00 50.72 o 18 0 0 2784.57 2838.92 183.20 o 20 0 0 4502.40 4698.88 229.98 o 22 0 0 1660.99 1810.56 170.96 o 24 0 0 814.86 1206.31 160.90 o 3 1 0 22369.62 23049.30 100.56 o 5 1 0 452.11 411.43 8.74 o 7 1 0 780.02 681.20 13.99 o 9 1 0 306.37 420.61 14.43 o 11 1 0 1011.49 1034.92 34.54 o 13 1 0 381.71 330.98 22.74 o 15 1 0 25.06 34.98 9.18 o 17 1 0 27.75 48.97 17.49 o 19 1 0 672.10 713.12 49.41 o 21 1 0 61.18 93.13 49.84 o 23 1 0 135.20 121.55 53.78 o 0 2 0 6201.93 5547.97 59.46 o 2 2 0 46841.04 45225.89 114.99 o 4 2 0 30409.17 30517.13 100.12 o 6 2 0 947.64 825.48 16.18 o 8 2 0 304.86 297.31 25.36 o 10 2 0 18.42 12.68 9.62 o 12 2 0 262.05 356.78 27.55 o 14 2 0 448.59 445.97 36.73 o 16 2 0 1588.55 1541.23 64.27 o 18 2 0 4149.61 3986.64 135.54 o 20 2 0 1262.59 1290.26 78.70 o 22 2 0 1109.43 1266.65 111.06 o 24 2 0 579.29 662.40 96.19 o 1 3 0 9804.83 8944.35 56.40 o 3 3 0 20618.56 20635.80 82.64 o 5 3 0 173.62 170.52 11.81 o 7 3 0 2825.66 2605.44 41.10 o 9 3 0 7230.29 7483.58 106.68 o 11 3 0 1749.58 1772.08 56.40 o 13 3 0 1721.53 1526.80 59.90 o 15 3 0 41.23 61.21 23.17 o 17 3 0 1246.32 1145.97 52.90 o 19 3 0 2286.86 2154.65 73.89 o 21 3 0 1535.91 1516.30 80.01 o 23 3 0 283.57 363.34 64.27 o 0 4 0 15167.33 15751.10 119.80 o 2 4 0 31657.75 31641.68 132.04 o 4 4 0 8562.62 8060.72 68.64 o 6 4 0 5651.32 5713.68 65.58 o 8 4 0 3477.99 3323.36 53.34 o 10 4 0 1070.99 981.57 43.29 o 12 4 0 102.32 105.37 31.48 o 14 4 0 24.67 86.57 21.86 o 16 4 0 3012.78 3068.02 88.32 o 18 4 0 349.20 372.52 40.66 o 20 4 0 5.33 43.29 19.68 o 22 4 0 193.30 386.95 54.65 o 1 5 0 12191.90 12003.63 104.50 o 3 5 0 17529.81 16434.49 111.49 o 5 5 0 16598.87 15978.90 127.23 o 7 5 0 1958.89 1970.58 37.60 o 9 5 0 1840.16 1793.94 44.16 o 11 5 0 426.58 401.81 37.16 o 13 5 0 185.27 105.37 24.92 o 15 5 0 3656.61 3679.27 94.00 o 17 5 0 3530.57 3458.90 101.44 o 19 5 0 465.14 447.28 45.03 o 21 5 0 547.67 559.21 46.78 o 0 6 0 67.00 59.46 29.29 o 2 6 0 23.27 34.10 15.74 o 4 6 0 468.07 523.80 25.80 o 6 6 0 71.26 64.27 12.68 o 8 6 0 121.94 115.87 16.18 o 10 6 0 78.65 55.09 22.74 o 12 6 0 3647.11 3704.19 143.41 o 14 6 0 287.36 245.72 31.92 o 16 6 0 10.36 19.68 23.61 o 18 6 0 9.20 39.35 30.17 o 20 6 0 143.59 184.51 47.22 o 1 7 0 14639.33 14858.29 170.52 o 3 7 0 7430.45 7297.76 102.75 o 5 7 0 2155.12 2037.48 55.53 o 7 7 0 390.09 397.88 24.48 o 9 7 0 8798.24 8963.15 171.39 o 11 7 0 3918.64 3298.88 102.75 o 13 7 0 6.64 67.77 27.55 o 15 7 0 1213.38 1171.77 66.90 o 17 7 0 935.64 876.64 61.21 o 19 7 0 2552.63 2483.45 137.73 o 0 8 0 36.62 53.78 32.35 o 2 8 0 1816.89 1898.00 53.78 o 4 8 0 3991.48 3884.32 77.39 o 6 8 0 26.43 53.34 14.43 o 8 8 0 1066.39 975.45 46.78 o 10 8 0 68.92 100.12 28.42 o 12 8 0 0.11 14.87 26.23 o 14 8 0 221.09 237.85 37.60 o 16 8 0 288.24 342.35 41.54 o 18 8 0 246.46 194.57 42.41 o 1 9 0 3883.69 4093.32 77.39 o 3 9 0 403.55 438.10 34.54 o 5 9 0 316.40 266.27 29.29 o 7 9 0 2812.70 2817.05 84.82 o 9 9 0 172.47 139.48 31.04 o 11 9 0 29.48 51.16 21.86 o 13 9 0 499.10 494.50 46.78 o 15 9 0 92.44 132.92 34.54 o 0 10 0 9067.06 8973.65 192.82 o 2 10 0 4539.07 4510.87 96.63 o 4 10 0 15.14 11.37 12.68 o 6 10 0 913.86 895.44 48.09 o 8 10 0 108.78 108.87 34.54 o 10 10 0 51.38 81.76 27.98 o 12 10 0 61.74 91.82 37.60 o 14 10 0 2.48 71.27 25.36 o 1 11 0 15.22 58.15 20.55 o 3 11 0 836.79 881.01 47.22 o 5 11 0 293.88 306.06 38.04 o 7 11 0 17.92 27.55 22.30 o 9 11 0 34.70 31.92 21.86 o 11 11 0 30.63 59.90 25.36 o 0 12 0 870.90 677.26 73.02 o 2 12 0 1473.30 1413.12 83.07 o 4 12 0 1097.42 1083.01 65.58 o 6 12 0 169.14 165.71 36.29 o -23 1 1 1684.80 1747.16 118.93 o -21 1 1 1757.57 1909.37 123.74 o -19 1 1 82.75 177.08 56.40 o -17 1 1 132.43 125.48 20.55 o -15 1 1 134.30 148.66 17.93 o -13 1 1 921.40 827.67 22.74 o -11 1 1 7687.60 7573.21 69.52 o -9 1 1 12096.03 11768.40 66.02 o -7 1 1 5201.87 4622.36 40.22 o -5 1 1 5940.75 5537.48 68.21 o -3 1 1 27642.44 27023.69 66.46 o 3 1 1 11492.57 11316.75 63.40 o 5 1 1 285.01 243.54 10.49 o 7 1 1 0.01 19.24 7.43 o 9 1 1 4210.80 4365.71 60.34 o 11 1 1 23555.96 24377.16 186.70 o 13 1 1 7678.42 7813.68 87.88 o 15 1 1 2346.03 2294.57 60.77 o 17 1 1 6078.45 6272.02 109.31 o 19 1 1 5959.81 6256.72 221.67 o 21 1 1 1302.88 1199.31 103.62 o 23 1 1 7.79 88.32 44.16 o -24 2 1 2.59 17.93 40.66 o -22 2 1 647.51 649.28 81.76 o -20 2 1 629.98 640.97 56.84 o -18 2 1 20.15 39.35 19.68 o -16 2 1 35.85 29.73 20.99 o -14 2 1 9.90 46.35 21.42 o -12 2 1 183.83 240.91 25.36 o -10 2 1 8506.18 8241.29 105.81 o -8 2 1 8369.84 7968.90 89.19 o -6 2 1 196.64 159.59 17.49 o -4 2 1 14400.15 14731.93 44.60 o -2 2 1 117997.77 113498.02 317.43 o 0 2 1 19143.17 18875.97 69.08 o 2 2 1 25192.56 24907.95 94.44 o 4 2 1 6606.83 6687.39 49.84 o 6 2 1 1349.84 1322.17 21.86 o 8 2 1 1647.44 1741.91 32.35 o 10 2 1 9.47 39.79 12.24 o 12 2 1 73.79 36.73 9.62 o 14 2 1 1037.82 1081.70 51.16 o 16 2 1 416.11 422.36 34.98 o 18 2 1 2174.90 2387.70 101.44 o 20 2 1 1691.64 1659.28 89.19 o 22 2 1 351.38 260.15 61.21 o 24 2 1 84.49 65.15 47.66 o -23 3 1 382.49 360.28 77.83 o -21 3 1 22.95 23.61 31.04 o -19 3 1 402.10 417.11 41.10 o -17 3 1 476.69 440.29 38.91 o -15 3 1 954.53 886.26 48.53 o -13 3 1 1991.87 1876.14 65.58 o -11 3 1 378.76 334.48 30.61 o -9 3 1 106.23 114.99 24.92 o -7 3 1 6038.53 5400.19 94.44 o -5 3 1 51179.26 50611.66 122.42 o -3 3 1 1166.72 1008.25 21.86 o -1 3 1 43.23 42.85 11.81 o 1 3 1 3470.25 3481.64 41.97 o 3 3 1 12631.09 12290.01 68.21 o 5 3 1 451.07 440.29 18.80 o 7 3 1 2757.94 2513.62 43.72 o 9 3 1 12.43 22.30 6.12 o 11 3 1 2742.03 2874.77 73.02 o 13 3 1 644.46 636.60 40.22 o 15 3 1 4847.05 4813.87 110.18 o 17 3 1 1297.03 1235.17 63.40 o 19 3 1 1095.65 1054.59 55.97 o 21 3 1 712.94 832.04 61.21 o 23 3 1 1041.02 1044.97 112.37 o -22 4 1 881.76 758.15 81.32 o -20 4 1 2933.83 3029.98 106.25 o -18 4 1 1377.66 1358.90 65.58 o -16 4 1 384.49 395.69 38.04 o -14 4 1 701.04 592.44 42.41 o -12 4 1 407.35 399.19 35.85 o -10 4 1 7384.57 7108.87 109.31 o -8 4 1 5912.23 5913.93 63.40 o -6 4 1 32963.00 32755.30 161.34 o -4 4 1 29431.16 28999.52 147.78 o -2 4 1 13791.73 13540.48 79.58 o 0 4 1 31417.05 32253.80 132.92 o 2 4 1 42449.32 43231.27 139.04 o 4 4 1 6118.62 6220.87 59.46 o 6 4 1 2080.06 2157.28 44.16 o 8 4 1 7409.33 7306.94 92.25 o 10 4 1 3081.48 3182.58 49.84 o 12 4 1 2101.12 1992.88 71.71 o 14 4 1 3478.65 3544.60 88.32 o 16 4 1 2979.79 2956.97 90.51 o 18 4 1 1408.50 1448.10 66.46 o 20 4 1 715.77 694.75 48.53 o 22 4 1 371.33 234.35 41.10 o -21 5 1 382.94 339.29 44.60 o -19 5 1 33.33 56.40 27.55 o -17 5 1 489.66 639.23 56.84 o -15 5 1 2.39 44.60 29.73 o -13 5 1 202.60 202.44 33.23 o -11 5 1 273.74 238.29 32.35 o -9 5 1 918.58 879.26 23.17 o -7 5 1 1294.66 1291.57 36.73 o -5 5 1 59.95 76.08 12.68 o -3 5 1 2193.74 1933.42 39.79 o -1 5 1 4626.74 4945.04 67.77 o 1 5 1 20720.91 22692.08 135.98 o 3 5 1 11082.96 11872.46 93.57 o 5 5 1 78.88 70.39 16.18 o 7 5 1 373.42 332.73 24.05 o 9 5 1 100.64 77.39 13.55 o 11 5 1 73.92 94.44 26.23 o 13 5 1 1378.59 1318.68 62.09 o 15 5 1 974.02 1054.59 58.59 o 17 5 1 897.34 808.00 52.90 o 19 5 1 2.41 37.16 20.99 o 21 5 1 42.51 41.97 22.74 o -20 6 1 144.16 190.63 38.48 o -18 6 1 900.54 928.67 62.96 o -16 6 1 424.77 380.39 47.22 o -14 6 1 152.26 163.52 24.92 o -12 6 1 5442.13 5404.56 123.74 o -10 6 1 1098.42 972.83 62.96 o -8 6 1 4582.99 4720.74 71.27 o -6 6 1 11558.65 11289.20 105.37 o -4 6 1 20214.48 19791.96 185.82 o -2 6 1 11079.80 10949.91 105.37 o 0 6 1 16439.00 16507.07 138.60 o 2 6 1 14515.26 13933.99 123.74 o 4 6 1 4655.66 4207.87 71.27 o 6 6 1 687.24 710.49 27.98 o 8 6 1 6225.44 6259.78 100.12 o 10 6 1 3446.43 3298.44 87.01 o 12 6 1 2196.34 2065.90 73.02 o 14 6 1 2915.12 2869.52 85.70 o 16 6 1 2497.44 2627.73 88.32 o 18 6 1 1162.25 1256.15 72.58 o 20 6 1 1421.66 1554.78 89.19 o -19 7 1 2.87 74.77 21.86 o -17 7 1 197.33 167.02 36.73 o -15 7 1 267.05 183.20 31.92 o -13 7 1 68.75 118.05 30.61 o -11 7 1 103.37 53.78 19.24 o -9 7 1 995.77 926.05 41.97 o -7 7 1 2246.19 2263.96 55.97 o -5 7 1 2474.55 2314.68 58.59 o -3 7 1 122.11 156.96 19.24 o -1 7 1 8.15 -9.62 16.61 o 1 7 1 1071.59 1001.69 57.28 o 3 7 1 1962.12 1755.90 50.72 o 5 7 1 290.28 239.16 22.30 o 7 7 1 1456.47 1374.64 43.29 o 9 7 1 1119.37 1082.14 54.65 o 11 7 1 1015.38 1000.81 59.03 o 13 7 1 376.46 398.75 48.53 o 15 7 1 1425.38 1480.45 72.14 o 17 7 1 84.70 111.06 36.29 o 19 7 1 191.49 147.35 36.73 o -18 8 1 486.37 491.44 64.71 o -16 8 1 105.80 126.80 34.98 o -14 8 1 296.28 260.59 39.79 o -12 8 1 305.01 355.47 38.48 o -10 8 1 4338.45 4432.17 130.73 o -8 8 1 11664.67 12038.17 149.09 o -6 8 1 1695.57 1541.66 46.78 o -4 8 1 6374.74 6568.02 107.56 o -2 8 1 8615.29 8967.53 120.67 o 0 8 1 6153.14 6348.54 97.50 o 2 8 1 280.95 267.58 22.30 o 4 8 1 125.96 110.18 16.61 o 6 8 1 699.72 672.46 32.79 o 8 8 1 4.12 22.30 12.24 o 10 8 1 2578.10 2416.55 88.76 o 12 8 1 1367.55 1274.52 63.40 o 14 8 1 584.23 606.43 50.72 o 16 8 1 610.98 687.32 59.90 o 18 8 1 1737.69 1826.73 84.38 o -15 9 1 3.86 32.79 24.05 o -13 9 1 88.20 73.45 20.99 o -11 9 1 1071.71 945.28 59.90 o -9 9 1 1679.52 1833.73 71.27 o -7 9 1 567.18 574.08 41.10 o -5 9 1 419.91 372.52 34.54 o -3 9 1 4692.36 4579.95 79.58 o -1 9 1 4738.82 4487.70 79.14 o 1 9 1 3113.29 2672.77 62.52 o 3 9 1 2055.68 1888.82 54.22 o 5 9 1 145.05 125.48 25.80 o 7 9 1 58.63 52.03 18.80 o 9 9 1 55.50 29.29 20.55 o 11 9 1 261.51 292.07 40.22 o 13 9 1 178.09 173.14 36.29 o 15 9 1 87.34 45.03 21.86 o -14 10 1 5.60 62.52 21.42 o -12 10 1 4.37 48.53 24.48 o -10 10 1 217.23 223.42 40.22 o -8 10 1 685.54 601.19 50.28 o -6 10 1 1862.96 1935.17 72.14 o -4 10 1 1212.38 1314.74 48.09 o -2 10 1 2768.88 2722.18 72.14 o 0 10 1 4084.87 3999.75 88.76 o 2 10 1 560.36 612.56 38.48 o 4 10 1 277.49 296.88 28.42 o 6 10 1 351.07 331.86 32.79 o 8 10 1 454.01 448.16 44.60 o 10 10 1 1223.53 1248.28 68.64 o 12 10 1 721.01 780.01 57.28 o 14 10 1 894.45 839.48 66.90 o -11 11 1 112.21 129.86 39.35 o -9 11 1 885.94 854.78 79.58 o -7 11 1 931.21 1126.73 65.15 o -5 11 1 915.74 906.81 58.59 o -3 11 1 1085.57 1075.14 48.09 o -1 11 1 3934.61 4253.78 88.76 o 1 11 1 1663.59 1707.37 59.46 o 3 11 1 38.96 32.79 20.55 o 5 11 1 404.68 367.27 39.79 o 7 11 1 57.74 35.42 23.61 o 9 11 1 158.60 101.87 26.67 o 11 11 1 236.94 144.28 33.67 o -6 12 1 267.08 274.58 57.71 o -4 12 1 169.43 148.22 38.48 o -2 12 1 6.36 38.48 20.11 o 0 12 1 179.54 118.93 20.99 o 2 12 1 388.54 381.26 35.85 o 4 12 1 0.42 -5.25 25.80 o 6 12 1 83.07 74.33 29.73 o -24 0 2 943.38 1154.28 153.47 o -22 0 2 2972.82 2729.17 195.00 o -20 0 2 2360.23 2183.51 168.77 o -18 0 2 545.09 513.30 93.57 o -16 0 2 352.30 292.94 26.67 o -14 0 2 4797.76 4722.93 96.63 o -12 0 2 29914.49 30802.21 277.20 o -10 0 2 33335.04 32740.44 288.13 o -8 0 2 9383.25 8851.66 77.39 o -6 0 2 677.89 906.81 28.86 o -4 0 2 50896.50 49141.70 113.68 o -2 0 2 13694.07 13977.27 71.71 o 2 0 2 6481.36 6926.55 48.97 o 6 0 2 750.46 617.80 30.61 o 8 0 2 39636.70 39823.95 223.86 o 10 0 2 50205.11 51296.35 408.81 o 12 0 2 4103.17 3641.66 109.31 o 14 0 2 7200.82 7623.49 176.64 o 16 0 2 5339.38 5635.42 160.03 o 18 0 2 7600.74 7845.60 280.70 o 20 0 2 911.53 818.49 113.24 o 22 0 2 2019.60 1901.50 186.70 o 24 0 2 889.92 539.10 127.67 o -23 1 2 107.64 240.91 51.16 o -21 1 2 322.92 234.35 75.20 o -19 1 2 5104.84 5497.26 208.12 o -17 1 2 383.42 466.08 32.79 o -15 1 2 11.77 36.29 14.87 o -13 1 2 489.54 438.98 24.48 o -11 1 2 3774.68 3639.04 56.84 o -9 1 2 2617.93 2632.54 36.73 o -7 1 2 76.89 68.64 7.00 o -5 1 2 599.84 700.88 16.61 o -3 1 2 10698.17 10991.89 61.65 o -1 1 2 66417.69 66590.55 133.35 o 1 1 2 2502.44 2698.13 31.92 o 3 1 2 5983.85 6244.48 51.59 o 5 1 2 3961.47 3959.97 47.66 o 7 1 2 5951.07 6353.78 55.09 o 9 1 2 19694.01 20603.01 135.10 o 11 1 2 5669.98 5560.22 77.39 o 13 1 2 179.11 174.02 19.24 o 15 1 2 134.00 122.86 18.80 o 17 1 2 320.74 291.63 39.35 o 19 1 2 1425.98 1305.12 104.93 o 21 1 2 55.43 45.91 57.71 o 23 1 2 316.86 293.82 81.32 o -24 2 2 161.08 208.12 66.90 o -22 2 2 440.60 546.10 81.32 o -20 2 2 234.38 172.70 43.29 o -18 2 2 83.11 94.00 27.55 o -16 2 2 3724.40 3568.65 90.94 o -14 2 2 932.24 871.83 48.53 o -12 2 2 9915.89 9596.70 121.55 o -10 2 2 26247.03 26940.18 234.79 o -8 2 2 42405.66 42451.25 250.97 o -6 2 2 15615.53 14219.06 58.15 o -4 2 2 46601.24 46480.29 115.43 o -2 2 2 2105.44 2151.59 28.86 o 0 2 2 3767.54 3619.37 41.10 o 2 2 2 3199.50 3082.89 45.47 o 4 2 2 57.96 58.15 15.74 o 6 2 2 16317.54 16703.82 155.65 o 8 2 2 8664.13 8328.74 73.02 o 10 2 2 6416.72 6202.07 90.94 o 12 2 2 15787.87 16199.70 143.41 o 14 2 2 7137.03 7325.74 108.87 o 16 2 2 2760.76 2730.48 78.70 o 18 2 2 512.52 565.33 45.91 o 20 2 2 1030.10 1009.56 69.08 o 22 2 2 1404.84 1467.77 128.98 o -23 3 2 284.70 353.28 75.20 o -21 3 2 631.54 628.73 75.20 o -19 3 2 47.86 30.17 22.30 o -17 3 2 613.01 594.63 45.03 o -15 3 2 873.05 826.80 44.60 o -13 3 2 346.83 322.67 34.10 o -11 3 2 8763.65 8323.05 114.99 o -9 3 2 8401.39 7631.80 105.37 o -7 3 2 7043.54 6755.16 83.51 o -5 3 2 15812.86 15681.15 68.21 o -3 3 2 44385.88 45812.65 122.86 o -1 3 2 3129.73 2789.51 36.73 o 1 3 2 11.65 10.49 9.62 o 3 3 2 238.06 215.12 15.74 o 5 3 2 6745.32 6505.94 73.45 o 7 3 2 10105.95 10405.57 107.56 o 9 3 2 12723.08 12399.32 116.74 o 11 3 2 6342.26 6338.92 80.01 o 13 3 2 475.95 466.52 44.60 o 15 3 2 78.88 56.84 25.80 o 17 3 2 1785.11 1685.51 77.83 o 19 3 2 720.77 806.25 59.03 o 21 3 2 274.00 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