#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:17:38 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180996 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/76/2207665.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207665_Fobs loop_ _publ_author_name 'Xing, Jun-De' 'Zeng, Tao' _publ_section_title ; 4-Methyl-N-(4-nitrophenyl)benzenesulfonamide ; _journal_coeditor_code SU6243 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4318 _journal_page_last o4319 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.358 _cell_angle_gamma 90.000 _cell_length_a 13.8005 _cell_length_b 8.2320 _cell_length_c 11.9588 _exptl_crystal_F_000 608.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file su6243Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' B in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 269.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 513.79 563.50 9.53 o 3 0 0 5515.42 5698.26 199.11 o 4 0 0 610.21 430.70 185.91 o 5 0 0 2512.01 2641.92 62.26 o 6 0 0 2863.93 2783.76 67.48 o 7 0 0 85.30 97.58 1.71 o 8 0 0 1108.33 1108.57 21.83 o 9 0 0 263.34 300.51 6.12 o 10 0 0 1333.93 1414.73 31.79 o 11 0 0 3436.15 3557.57 104.32 o 12 0 0 20.19 26.01 1.28 o 13 0 0 16.05 21.76 1.17 o 14 0 0 339.22 346.66 9.19 o 15 0 0 18.98 17.57 1.24 o 16 0 0 6.06 3.11 1.45 o 17 0 0 39.48 41.09 2.46 o 2 1 0 5192.88 4787.33 165.43 o 3 1 0 6466.18 6487.25 150.82 o 4 1 0 90.00 64.65 0.69 o 5 1 0 2702.46 2860.86 49.27 o 6 1 0 39.80 24.18 0.56 o 7 1 0 1808.17 1826.68 30.86 o 8 1 0 190.39 225.28 2.81 o 9 1 0 957.25 1008.03 15.45 o 10 1 0 80.89 79.94 1.37 o 11 1 0 276.39 304.47 4.23 o 12 1 0 170.98 167.38 2.42 o 13 1 0 0.86 2.20 0.60 o 14 1 0 26.46 24.84 1.30 o 15 1 0 56.88 51.63 1.72 o 16 1 0 30.71 31.72 1.28 o 17 1 0 26.04 25.37 1.38 o 0 2 0 960.60 938.09 25.84 o 1 2 0 5086.13 4665.67 107.36 o 2 2 0 2869.62 2728.84 47.90 o 3 2 0 5.76 2.38 0.19 o 4 2 0 9.20 22.66 0.64 o 5 2 0 556.28 630.22 7.69 o 6 2 0 21.65 15.76 0.47 o 7 2 0 245.03 281.10 3.69 o 8 2 0 617.26 666.64 11.01 o 9 2 0 8.31 10.15 0.76 o 10 2 0 166.35 171.09 2.84 o 11 2 0 232.80 250.32 4.22 o 12 2 0 1.20 0.38 0.63 o 13 2 0 0.64 0.49 0.53 o 14 2 0 39.26 35.82 1.19 o 15 2 0 2.12 2.67 0.72 o 16 2 0 81.05 79.38 2.31 o 17 2 0 0.92 0.57 0.72 o 1 3 0 389.08 380.67 4.30 o 2 3 0 479.27 517.48 6.43 o 3 3 0 194.40 202.62 2.47 o 4 3 0 29.18 25.96 0.58 o 5 3 0 1.87 3.82 0.28 o 6 3 0 97.92 100.87 1.09 o 7 3 0 40.75 36.91 0.64 o 8 3 0 46.56 39.24 0.85 o 9 3 0 261.71 276.56 3.67 o 10 3 0 3.14 3.93 0.55 o 11 3 0 8.32 10.40 0.98 o 12 3 0 26.56 26.01 1.07 o 13 3 0 3.26 3.69 0.91 o 14 3 0 0.11 1.21 0.75 o 15 3 0 0.05 0.66 0.72 o 16 3 0 1.04 1.44 0.75 o 0 4 0 254.37 334.38 7.62 o 1 4 0 21.44 25.71 1.17 o 2 4 0 1550.22 1605.32 27.94 o 3 4 0 910.46 882.19 11.79 o 4 4 0 43.74 43.56 0.81 o 5 4 0 7.49 9.46 0.41 o 6 4 0 7.06 6.25 0.34 o 7 4 0 48.48 50.56 0.89 o 8 4 0 67.63 68.14 1.22 o 9 4 0 3.43 5.43 0.47 o 10 4 0 18.20 13.47 0.66 o 11 4 0 47.58 45.66 1.01 o 12 4 0 40.34 40.76 1.18 o 13 4 0 15.30 12.47 1.02 o 14 4 0 56.57 57.14 1.59 o 15 4 0 0.06 -0.13 0.86 o 16 4 0 1.28 0.58 0.66 o 1 5 0 542.29 498.78 6.46 o 2 5 0 282.90 326.25 4.16 o 3 5 0 359.67 388.08 4.43 o 4 5 0 122.83 134.95 2.31 o 5 5 0 120.68 118.44 2.29 o 6 5 0 40.52 43.60 0.86 o 7 5 0 338.14 328.21 5.65 o 8 5 0 49.90 47.60 1.22 o 9 5 0 150.30 142.04 1.94 o 10 5 0 1.00 0.40 0.36 o 11 5 0 78.34 80.37 1.54 o 12 5 0 3.04 3.43 0.54 o 13 5 0 107.28 103.84 2.32 o 14 5 0 12.18 12.10 1.27 o 15 5 0 0.53 -0.16 0.56 o 0 6 0 2581.59 2385.35 101.70 o 1 6 0 572.82 532.62 7.88 o 2 6 0 746.12 762.01 11.79 o 3 6 0 11.84 18.00 0.56 o 4 6 0 72.39 65.94 0.93 o 5 6 0 4.00 2.39 0.41 o 6 6 0 273.28 273.69 3.65 o 7 6 0 3.13 3.05 0.46 o 8 6 0 258.56 244.57 3.49 o 9 6 0 129.01 130.85 2.03 o 10 6 0 73.10 73.97 1.41 o 11 6 0 46.54 45.73 0.98 o 12 6 0 123.18 122.17 2.94 o 13 6 0 25.63 30.19 2.22 o 14 6 0 13.46 18.25 3.85 o 1 7 0 28.98 30.88 0.79 o 2 7 0 1508.39 1488.33 28.49 o 3 7 0 2273.12 2331.17 45.37 o 4 7 0 78.67 79.96 1.43 o 5 7 0 670.59 650.30 10.55 o 6 7 0 13.53 11.87 0.56 o 7 7 0 285.13 265.40 3.51 o 8 7 0 99.02 96.24 1.74 o 9 7 0 140.37 137.35 2.56 o 10 7 0 0.01 0.20 0.90 o 11 7 0 37.45 41.32 2.25 o 12 7 0 4.98 5.72 1.47 o 13 7 0 12.53 12.11 2.34 o 0 8 0 608.60 632.64 14.45 o 1 8 0 50.14 49.56 1.00 o 2 8 0 217.98 204.33 2.66 o 3 8 0 7.23 7.79 0.52 o 4 8 0 103.56 98.29 1.37 o 5 8 0 42.42 41.93 1.24 o 6 8 0 99.69 97.28 1.53 o 7 8 0 33.59 37.51 1.74 o 8 8 0 93.63 88.20 2.69 o 9 8 0 11.26 12.00 1.39 o 10 8 0 32.32 39.14 3.35 o 11 8 0 80.27 91.45 3.63 o 1 9 0 12.54 12.33 0.63 o 2 9 0 3.32 3.84 0.43 o 3 9 0 1.58 0.19 0.37 o 4 9 0 33.24 32.22 2.10 o 5 9 0 22.56 23.24 1.58 o 6 9 0 6.68 6.93 1.35 o 7 9 0 36.39 34.00 2.01 o 8 9 0 17.30 15.85 1.56 o 9 9 0 9.65 11.80 2.30 o 0 10 0 0.00 0.13 0.99 o 1 10 0 8.35 11.42 1.17 o 2 10 0 35.29 37.53 1.69 o 3 10 0 0.79 0.23 0.71 o 4 10 0 2.07 3.12 1.08 o 5 10 0 1.20 1.87 1.23 o 6 10 0 0.65 0.47 0.92 o -17 1 1 0.98 0.37 0.68 o -16 1 1 15.57 15.60 1.11 o -15 1 1 6.70 5.45 0.71 o -14 1 1 22.39 25.05 1.00 o -13 1 1 17.30 18.98 0.90 o -12 1 1 248.83 239.69 4.33 o -11 1 1 58.99 67.12 1.51 o -10 1 1 635.37 632.26 16.21 o -9 1 1 6.02 3.38 0.51 o -8 1 1 1287.27 1367.20 21.90 o -7 1 1 77.77 107.75 1.57 o -6 1 1 693.77 806.55 9.69 o -5 1 1 2176.11 2265.93 35.84 o -4 1 1 104.11 96.30 0.94 o -3 1 1 1431.19 1445.31 19.28 o -2 1 1 42.00 33.58 0.36 o -1 1 1 1135.38 1100.98 12.42 o 0 1 1 99.45 78.00 2.40 o 1 1 1 10751.67 10119.06 282.89 o 2 1 1 986.15 935.37 11.83 o 3 1 1 750.62 860.64 10.74 o 4 1 1 1349.29 1398.10 20.72 o 5 1 1 0.40 4.24 0.30 o 6 1 1 952.96 969.27 15.06 o 7 1 1 2.37 1.78 0.51 o 8 1 1 829.50 881.90 14.68 o 9 1 1 88.54 102.86 1.92 o 10 1 1 19.21 22.06 0.81 o 11 1 1 117.15 113.08 1.97 o 12 1 1 248.75 242.92 3.61 o 13 1 1 13.32 16.03 1.02 o 14 1 1 1.88 1.88 0.57 o 15 1 1 1.73 2.19 0.63 o 16 1 1 29.38 28.98 1.44 o 17 1 1 3.76 3.86 0.81 o -17 2 1 37.85 37.37 1.56 o -16 2 1 3.87 3.20 0.78 o -15 2 1 75.55 73.98 1.74 o -14 2 1 8.81 8.21 0.79 o -13 2 1 44.28 37.54 1.24 o -12 2 1 8.59 7.90 1.02 o -11 2 1 1397.93 1422.59 28.60 o -10 2 1 583.43 583.66 8.26 o -9 2 1 383.46 414.19 4.99 o -8 2 1 137.95 150.31 1.87 o -7 2 1 352.54 331.76 3.79 o -6 2 1 718.82 738.49 8.75 o -5 2 1 123.83 108.67 1.29 o -4 2 1 496.64 473.93 5.55 o -3 2 1 660.53 696.59 8.26 o -2 2 1 447.79 362.16 5.83 o -1 2 1 423.33 434.46 4.89 o 0 2 1 9638.86 8121.13 221.61 o 1 2 1 3485.40 3504.90 74.99 o 2 2 1 80.56 87.17 1.13 o 3 2 1 1268.22 1376.90 22.55 o 4 2 1 1.12 1.57 0.27 o 5 2 1 2061.24 2305.74 40.76 o 6 2 1 0.90 2.84 0.35 o 7 2 1 703.49 734.19 10.37 o 8 2 1 891.03 907.50 17.48 o 9 2 1 251.28 240.35 3.58 o 10 2 1 147.68 138.34 2.50 o 11 2 1 396.74 375.83 6.71 o 12 2 1 1.66 2.09 0.70 o 13 2 1 11.04 9.40 0.83 o 14 2 1 33.40 32.63 1.93 o 15 2 1 43.45 43.96 1.42 o 16 2 1 15.36 19.48 1.07 o -16 3 1 15.50 20.17 1.60 o -15 3 1 21.62 18.17 1.13 o -14 3 1 139.51 133.25 2.92 o -13 3 1 122.67 129.10 2.57 o -12 3 1 409.66 397.81 6.61 o -11 3 1 101.22 94.43 1.79 o -10 3 1 388.88 380.88 6.83 o -9 3 1 64.82 90.00 1.50 o -8 3 1 0.18 -0.06 0.33 o -7 3 1 1989.03 2100.22 38.53 o -6 3 1 242.71 218.86 2.65 o -5 3 1 12.44 14.35 0.32 o -4 3 1 201.73 217.84 2.46 o -3 3 1 82.62 57.04 1.20 o -2 3 1 100.25 113.01 1.18 o -1 3 1 6.15 1.09 0.30 o 0 3 1 406.88 416.32 4.98 o 1 3 1 780.04 869.56 12.35 o 2 3 1 377.81 401.44 4.89 o 3 3 1 4060.38 4204.53 90.26 o 4 3 1 1141.89 1192.01 19.49 o 5 3 1 837.39 1087.20 17.47 o 6 3 1 6.90 3.60 0.38 o 7 3 1 0.34 2.34 0.40 o 8 3 1 543.37 570.19 7.08 o 9 3 1 398.70 427.16 5.43 o 10 3 1 139.19 140.18 2.27 o 11 3 1 278.50 266.60 4.38 o 12 3 1 192.92 195.04 3.70 o 13 3 1 4.19 1.60 0.79 o 14 3 1 242.32 244.50 4.91 o 15 3 1 127.19 117.79 2.62 o 16 3 1 0.03 -0.22 0.68 o -16 4 1 34.55 33.25 1.23 o -15 4 1 19.38 19.48 0.95 o -14 4 1 26.91 27.82 1.25 o -13 4 1 54.21 56.47 1.39 o -12 4 1 52.82 57.05 1.44 o -11 4 1 26.45 26.82 0.75 o -10 4 1 407.57 428.04 5.50 o -9 4 1 555.07 587.70 7.50 o -8 4 1 52.01 45.40 0.71 o -7 4 1 352.35 332.43 3.72 o -6 4 1 120.14 147.05 2.02 o -5 4 1 86.70 141.65 1.79 o -4 4 1 74.10 100.28 1.51 o -3 4 1 1094.01 1196.70 17.09 o -2 4 1 1124.51 1086.09 15.01 o -1 4 1 5.26 1.35 0.20 o 0 4 1 97.72 73.40 0.90 o 1 4 1 996.73 1125.55 17.76 o 2 4 1 434.83 565.53 7.45 o 3 4 1 219.71 212.54 2.33 o 4 4 1 11.88 10.60 0.47 o 5 4 1 432.67 505.03 7.19 o 6 4 1 859.68 928.35 13.26 o 7 4 1 269.92 257.44 3.42 o 8 4 1 730.99 720.15 10.27 o 9 4 1 73.76 67.69 1.28 o 10 4 1 6.86 5.96 0.55 o 11 4 1 62.27 61.58 1.34 o 12 4 1 131.45 138.13 2.67 o 13 4 1 1.14 1.05 0.60 o 14 4 1 7.83 6.63 0.88 o 15 4 1 23.04 23.39 1.26 o -15 5 1 0.68 1.69 0.61 o -14 5 1 61.03 57.00 1.60 o -13 5 1 2.62 3.11 0.55 o -12 5 1 33.33 34.00 0.99 o -11 5 1 0.65 0.72 0.40 o -10 5 1 2.06 2.43 0.39 o -9 5 1 140.03 134.29 1.89 o -8 5 1 252.17 258.39 3.56 o -7 5 1 119.94 103.69 2.14 o -6 5 1 11.14 11.97 0.38 o -5 5 1 73.99 66.20 0.75 o -4 5 1 61.31 70.17 0.97 o -3 5 1 154.96 151.01 1.61 o -2 5 1 49.94 54.06 0.87 o -1 5 1 216.81 194.61 2.49 o 0 5 1 39.62 36.24 0.65 o 1 5 1 120.99 119.73 1.48 o 2 5 1 29.02 19.55 0.51 o 3 5 1 169.58 162.04 1.98 o 4 5 1 331.94 354.18 4.19 o 5 5 1 479.70 410.73 6.13 o 6 5 1 121.61 121.64 1.95 o 7 5 1 8.04 7.94 0.52 o 8 5 1 0.65 0.40 0.43 o 9 5 1 62.26 73.16 1.41 o 10 5 1 75.98 73.23 1.48 o 11 5 1 19.41 23.43 1.00 o 12 5 1 39.17 34.50 1.38 o 13 5 1 25.02 23.46 1.05 o 14 5 1 50.50 52.53 1.80 o 15 5 1 8.76 7.25 1.11 o -14 6 1 11.33 13.21 1.89 o -13 6 1 11.03 13.86 1.64 o -12 6 1 0.11 0.19 0.35 o -11 6 1 2.03 2.64 0.68 o -10 6 1 70.07 69.74 1.93 o -9 6 1 25.54 23.16 0.48 o -8 6 1 172.34 161.58 3.77 o -7 6 1 78.33 68.00 1.16 o -6 6 1 333.07 320.98 4.29 o -5 6 1 313.78 281.74 5.68 o -4 6 1 1.81 0.58 0.36 o -3 6 1 59.65 58.84 0.90 o -2 6 1 182.34 168.23 2.34 o -1 6 1 0.88 0.28 0.49 o 0 6 1 11.00 6.36 0.40 o 1 6 1 529.86 495.00 6.94 o 2 6 1 89.42 80.91 1.21 o 3 6 1 34.30 30.05 0.71 o 4 6 1 613.88 620.32 8.83 o 5 6 1 7.84 9.32 0.62 o 6 6 1 159.86 144.12 3.85 o 7 6 1 17.50 14.60 0.75 o 8 6 1 18.31 21.60 0.88 o 9 6 1 6.46 5.78 0.54 o 10 6 1 33.24 26.94 0.97 o 11 6 1 4.46 4.01 0.81 o 12 6 1 0.02 -0.21 0.55 o 13 6 1 16.06 16.42 1.32 o 14 6 1 9.87 12.36 1.66 o -13 7 1 1.35 0.80 1.19 o -12 7 1 2.86 3.47 1.48 o -11 7 1 13.29 13.87 1.78 o -10 7 1 88.21 85.39 3.66 o -9 7 1 4.02 2.67 0.27 o -8 7 1 1.26 0.48 1.08 o -7 7 1 49.41 47.58 2.10 o -6 7 1 71.64 66.21 1.14 o -5 7 1 11.41 12.00 1.41 o -4 7 1 53.76 46.94 3.74 o -3 7 1 131.19 124.93 2.39 o -2 7 1 4.97 5.33 0.38 o -1 7 1 70.89 64.73 1.10 o 0 7 1 14.26 11.39 0.88 o 1 7 1 91.47 103.33 1.90 o 2 7 1 131.86 128.87 2.49 o 3 7 1 79.59 69.56 1.80 o 4 7 1 10.22 11.35 0.61 o 5 7 1 94.17 83.85 1.60 o 6 7 1 0.45 0.63 0.56 o 7 7 1 0.02 0.20 0.38 o 8 7 1 0.44 0.46 0.41 o 9 7 1 10.03 6.63 0.70 o 10 7 1 4.89 3.57 0.45 o 11 7 1 2.42 2.20 1.06 o 12 7 1 4.05 3.57 1.28 o -11 8 1 7.58 11.89 2.41 o -10 8 1 2.51 1.77 1.35 o -9 8 1 35.02 35.54 2.33 o -8 8 1 143.54 148.68 3.92 o -7 8 1 52.08 50.57 2.09 o -6 8 1 26.92 31.73 1.61 o -5 8 1 49.98 52.73 2.24 o -4 8 1 22.57 20.47 1.04 o -3 8 1 1.16 1.71 0.33 o -2 8 1 69.94 77.81 1.48 o -1 8 1 92.54 100.65 2.44 o 0 8 1 1.31 0.47 0.47 o 1 8 1 11.87 13.66 0.70 o 2 8 1 92.18 102.57 1.86 o 3 8 1 235.49 243.08 3.52 o 4 8 1 26.46 28.81 0.85 o 5 8 1 0.52 0.59 0.44 o 6 8 1 7.22 7.21 0.57 o 7 8 1 2.25 1.12 0.52 o 8 8 1 6.09 6.08 1.11 o 9 8 1 28.18 24.23 1.62 o 10 8 1 5.20 5.21 1.69 o 11 8 1 36.93 34.96 2.46 o -9 9 1 57.38 62.52 4.27 o -8 9 1 41.36 39.67 2.28 o -7 9 1 170.90 172.85 4.43 o -6 9 1 74.48 75.98 2.85 o -5 9 1 5.00 4.87 1.10 o -4 9 1 0.08 0.62 0.85 o -3 9 1 57.55 60.14 1.33 o -2 9 1 21.33 22.63 1.09 o -1 9 1 72.32 73.89 1.73 o 0 9 1 84.30 89.72 2.43 o 1 9 1 88.98 106.32 1.88 o 2 9 1 222.23 218.21 4.74 o 3 9 1 131.41 137.91 2.99 o 4 9 1 28.15 26.50 0.73 o 5 9 1 60.83 65.03 2.28 o 6 9 1 3.86 3.28 1.10 o 7 9 1 2.84 3.37 1.01 o 8 9 1 18.39 18.34 1.55 o 9 9 1 5.07 5.29 1.69 o -6 10 1 9.78 12.25 2.10 o -5 10 1 0.38 1.00 1.05 o -4 10 1 48.60 51.14 2.34 o -3 10 1 3.23 4.29 0.92 o -2 10 1 14.21 15.24 1.33 o -1 10 1 68.25 68.37 2.02 o 0 10 1 219.83 226.70 4.04 o 1 10 1 0.07 -0.37 0.68 o 2 10 1 0.10 -0.44 0.62 o 3 10 1 48.47 50.51 2.00 o 4 10 1 38.60 43.64 2.47 o 5 10 1 80.17 86.30 2.72 o -17 0 2 46.70 50.70 2.24 o -16 0 2 122.53 123.55 3.53 o -15 0 2 346.03 332.60 7.56 o -14 0 2 104.31 123.29 3.04 o -13 0 2 123.61 124.40 3.11 o -12 0 2 158.73 169.70 4.68 o -11 0 2 469.05 487.44 9.29 o -10 0 2 727.49 704.54 13.05 o -9 0 2 1747.91 1843.48 41.70 o -8 0 2 731.77 866.93 16.02 o -7 0 2 16.02 20.36 0.78 o -6 0 2 4236.98 4652.68 135.65 o -5 0 2 18838.50 19242.33 926.62 o -4 0 2 72873.83 71525.32 4984.10 o -3 0 2 11429.58 10919.41 451.26 o -2 0 2 6220.78 5783.14 200.41 o -1 0 2 6605.88 5835.56 295.29 o 0 0 2 83.10 77.24 1.41 o 1 0 2 565.50 612.19 10.07 o 3 0 2 121.06 82.22 2.12 o 4 0 2 3201.62 3074.09 90.95 o 5 0 2 2709.89 2966.83 89.56 o 6 0 2 7.45 1.39 0.39 o 7 0 2 1953.44 2050.05 47.21 o 8 0 2 2336.32 2596.98 64.71 o 9 0 2 142.37 129.45 2.74 o 10 0 2 1507.76 1556.06 49.97 o 11 0 2 238.62 266.78 5.83 o 12 0 2 41.40 35.77 2.37 o 13 0 2 195.43 210.26 4.91 o 14 0 2 4.28 3.38 1.47 o 15 0 2 57.87 63.01 2.25 o 16 0 2 0.25 0.44 1.20 o -17 1 2 1.52 2.99 0.85 o -16 1 2 22.80 24.53 1.14 o -15 1 2 37.54 41.64 1.47 o -14 1 2 64.10 62.84 1.50 o -13 1 2 224.30 244.13 3.93 o -12 1 2 3.02 5.10 0.78 o -11 1 2 8.77 10.43 0.74 o -10 1 2 514.00 496.11 6.28 o -9 1 2 1168.95 1182.35 18.64 o -8 1 2 595.62 546.66 7.01 o -7 1 2 4714.27 5171.12 122.19 o -6 1 2 331.00 258.31 2.73 o -5 1 2 170.81 167.78 2.30 o -4 1 2 15.78 11.31 0.37 o 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