#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/76/2207672.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207672_Fobs loop_ _publ_author_name 'Zhao, Shu-Min' 'Wu, Tian-Xing' _publ_section_title ; trans-Diaqua(malonato)(1,10-phenanthroline)nickel(II) trihydrate ; _journal_coeditor_code TK6278 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2544 _journal_page_last m2545 _journal_volume 61 _journal_year 2005 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yac' _symmetry_space_group_name_H-M 'P 1 2/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 116.189 _cell_angle_gamma 90.000 _cell_length_a 8.9389 _cell_length_b 12.1466 _cell_length_c 9.4334 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.7721 _[local]_cod_data_source_file tk6278Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ZSM' _shelx_refln_list_code 4 _shelx_f_calc_maximum 217.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 360.55 299.39 4.42 o 4 0 0 1664.51 1649.85 17.94 o 6 0 0 2082.30 2114.06 20.64 o 8 0 0 83.22 102.30 4.88 o 10 0 0 71.20 72.13 6.46 o 0 1 0 120.17 0.14 0.14 o 1 1 0 3352.06 3083.66 63.17 o 2 1 0 103.19 121.73 1.67 o 3 1 0 1924.58 1894.94 20.46 o 4 1 0 3467.96 3834.08 54.72 o 5 1 0 1519.29 1521.98 9.02 o 6 1 0 262.83 267.61 3.44 o 7 1 0 678.00 676.48 8.69 o 8 1 0 172.35 156.91 4.73 o 9 1 0 115.62 124.27 5.38 o 10 1 0 9.92 12.58 5.15 o 0 2 0 67.68 71.07 2.04 o 1 2 0 2182.92 2183.32 31.74 o 2 2 0 2415.20 2434.74 16.89 o 3 2 0 18.41 10.89 1.04 o 4 2 0 2667.96 2730.59 29.84 o 5 2 0 410.69 400.17 2.79 o 6 2 0 310.14 311.10 6.54 o 7 2 0 0.73 1.73 2.32 o 8 2 0 352.62 342.99 6.05 o 9 2 0 5.40 6.52 2.54 o 10 2 0 73.93 81.89 2.83 o 0 3 0 1532.50 1595.77 27.98 o 1 3 0 4623.63 4545.38 146.19 o 2 3 0 1371.05 1329.48 30.64 o 3 3 0 7562.60 7328.60 107.13 o 4 3 0 2103.81 2155.99 22.29 o 5 3 0 315.91 314.44 3.94 o 6 3 0 40.36 38.66 2.00 o 7 3 0 509.85 504.75 7.90 o 8 3 0 274.43 284.42 6.50 o 9 3 0 61.00 60.55 4.10 o 10 3 0 94.74 96.06 6.12 o 0 4 0 161.01 145.83 0.77 o 1 4 0 5063.46 5027.17 103.66 o 2 4 0 682.09 676.51 12.28 o 3 4 0 6120.79 6357.32 70.65 o 4 4 0 335.68 298.56 5.19 o 5 4 0 167.96 177.50 2.53 o 6 4 0 249.45 257.07 5.53 o 7 4 0 941.14 949.66 7.48 o 8 4 0 160.48 159.05 4.85 o 9 4 0 173.56 181.27 5.53 o 10 4 0 5.77 5.42 4.28 o 0 5 0 2187.70 2037.90 75.59 o 1 5 0 186.75 195.55 9.74 o 2 5 0 4141.25 4452.67 72.11 o 3 5 0 0.24 0.58 1.26 o 4 5 0 1360.13 1310.45 19.59 o 5 5 0 8.88 11.79 1.95 o 6 5 0 40.84 42.37 2.60 o 7 5 0 7.95 10.64 3.18 o 8 5 0 280.80 274.71 4.68 o 9 5 0 37.89 41.90 3.63 o 0 6 0 52.09 64.42 0.95 o 1 6 0 1339.91 1264.54 12.49 o 2 6 0 277.03 297.82 3.86 o 3 6 0 1870.42 1780.51 19.45 o 4 6 0 359.36 333.23 10.23 o 5 6 0 1071.57 1041.55 28.37 o 6 6 0 180.86 180.21 2.70 o 7 6 0 329.08 329.07 5.65 o 8 6 0 1.13 4.00 2.45 o 9 6 0 119.92 107.44 5.83 o 0 7 0 6160.37 6610.69 8.60 o 1 7 0 70.11 86.18 2.71 o 2 7 0 486.06 407.74 20.93 o 3 7 0 361.94 358.00 8.92 o 4 7 0 2389.65 2241.55 106.61 o 5 7 0 15.07 12.50 2.12 o 6 7 0 777.02 775.32 5.64 o 7 7 0 41.74 43.86 2.48 o 8 7 0 280.69 279.22 6.82 o 9 7 0 32.21 26.14 2.64 o 0 8 0 2865.34 2911.80 92.04 o 1 8 0 1662.00 1678.35 40.83 o 2 8 0 143.82 137.48 2.51 o 3 8 0 256.41 239.65 10.68 o 4 8 0 677.89 698.25 6.78 o 5 8 0 544.22 539.04 4.49 o 6 8 0 24.29 28.04 3.64 o 7 8 0 331.51 327.11 5.53 o 8 8 0 44.77 38.55 3.12 o 0 9 0 2732.30 2895.46 5.98 o 1 9 0 814.87 871.51 23.68 o 2 9 0 224.38 218.96 3.51 o 3 9 0 96.02 107.71 3.96 o 4 9 0 5.20 10.43 1.87 o 5 9 0 246.26 237.80 5.37 o 6 9 0 498.14 479.88 4.32 o 7 9 0 47.18 42.24 3.14 o 8 9 0 1.40 -0.73 3.39 o 0 10 0 256.97 270.58 5.92 o 1 10 0 366.79 340.24 8.50 o 2 10 0 280.42 285.01 3.40 o 3 10 0 420.66 423.20 7.00 o 4 10 0 644.97 581.61 5.02 o 5 10 0 56.70 55.41 2.69 o 6 10 0 245.10 235.55 3.77 o 7 10 0 48.41 44.34 3.27 o 8 10 0 143.63 138.08 3.96 o 0 11 0 216.58 200.39 2.17 o 1 11 0 699.79 685.10 5.32 o 2 11 0 200.41 199.95 2.05 o 3 11 0 926.38 917.20 6.16 o 4 11 0 118.17 116.11 2.99 o 5 11 0 244.18 225.50 3.60 o 6 11 0 0.75 2.84 4.20 o 7 11 0 229.71 223.53 5.68 o 0 12 0 185.60 200.94 1.84 o 1 12 0 0.67 -0.21 1.85 o 2 12 0 680.35 679.13 5.73 o 3 12 0 1.97 1.33 2.48 o 4 12 0 329.93 340.29 8.21 o 5 12 0 9.07 10.49 3.93 o 6 12 0 56.35 54.67 2.86 o 0 13 0 2.82 1.63 2.17 o 1 13 0 196.64 204.30 2.34 o 2 13 0 82.19 87.90 3.23 o 3 13 0 303.00 297.51 5.71 o 4 13 0 5.92 11.25 3.16 o 5 13 0 160.29 144.68 3.07 o 0 14 0 458.89 435.21 2.62 o 1 14 0 58.75 56.66 2.54 o 2 14 0 350.46 375.40 3.61 o 3 14 0 30.21 27.89 2.44 o 4 14 0 184.68 181.11 3.04 o 0 15 0 260.88 257.18 10.46 o 1 15 0 92.40 86.63 3.01 o 2 15 0 1.89 1.87 1.97 o 3 15 0 52.42 54.68 2.56 o -9 0 1 15.14 26.19 6.82 o -7 0 1 2030.14 2032.19 7.57 o -5 0 1 489.27 453.82 7.08 o -3 0 1 2351.18 2399.44 19.52 o -1 0 1 17826.76 14415.29 125.65 o 1 0 1 2594.19 2714.34 28.67 o 3 0 1 858.40 971.55 16.32 o 5 0 1 1443.48 1500.81 9.67 o 7 0 1 60.72 65.98 4.02 o 9 0 1 16.94 17.61 5.24 o -10 1 1 276.13 271.55 8.44 o -9 1 1 14.05 17.49 3.15 o -8 1 1 159.63 167.43 3.54 o -7 1 1 363.52 363.38 6.16 o -6 1 1 3316.86 3285.48 24.65 o -5 1 1 251.52 258.22 3.94 o -4 1 1 375.26 359.52 4.31 o -3 1 1 176.68 172.88 2.43 o -2 1 1 3288.53 3032.19 16.97 o -1 1 1 245.16 143.87 107.35 o 0 1 1 6607.17 6634.07 104.78 o 1 1 1 1186.33 1182.87 14.08 o 2 1 1 988.84 984.19 3.93 o 3 1 1 19.87 22.71 1.72 o 4 1 1 662.33 610.00 3.14 o 5 1 1 62.63 59.35 3.08 o 6 1 1 724.66 755.72 7.62 o 7 1 1 117.04 113.77 3.45 o 8 1 1 47.71 56.69 3.10 o 9 1 1 39.80 39.41 3.97 o -10 2 1 65.83 67.99 3.58 o -9 2 1 447.73 452.20 10.42 o -8 2 1 35.89 33.66 3.37 o -7 2 1 508.36 500.79 9.13 o -6 2 1 1175.42 1146.68 13.62 o -5 2 1 711.92 713.58 8.49 o -4 2 1 55.53 61.09 1.70 o -3 2 1 5386.25 5033.20 30.59 o -2 2 1 4325.32 3964.04 21.27 o -1 2 1 3.90 4.91 0.50 o 0 2 1 80.84 74.20 1.18 o 1 2 1 5836.52 5723.65 43.73 o 2 2 1 351.70 368.23 4.77 o 3 2 1 1273.01 1252.47 9.81 o 4 2 1 298.59 311.96 2.46 o 5 2 1 492.94 486.42 7.09 o 6 2 1 117.96 121.00 3.26 o 7 2 1 49.14 52.89 3.24 o 8 2 1 49.57 50.08 3.00 o 9 2 1 144.33 156.86 4.64 o -10 3 1 31.23 31.97 4.24 o -9 3 1 223.75 226.32 7.54 o -8 3 1 386.88 394.64 5.61 o -7 3 1 106.99 107.06 3.65 o -6 3 1 507.82 492.05 6.62 o -5 3 1 959.21 971.43 7.26 o -4 3 1 2640.38 2742.90 8.35 o -3 3 1 3961.67 4003.29 62.97 o -2 3 1 54.21 47.89 0.86 o -1 3 1 205.85 203.60 1.61 o 0 3 1 927.40 958.40 20.47 o 1 3 1 1719.87 1724.04 40.01 o 2 3 1 51.43 42.15 0.98 o 3 3 1 284.68 262.80 2.34 o 4 3 1 360.45 358.73 3.97 o 5 3 1 633.84 640.57 13.26 o 6 3 1 45.76 48.78 2.27 o 7 3 1 17.43 21.82 2.57 o 8 3 1 223.77 228.95 5.28 o 9 3 1 107.92 108.23 4.92 o -10 4 1 299.48 322.68 6.25 o -9 4 1 109.22 100.95 5.20 o -8 4 1 570.59 569.35 15.16 o -7 4 1 238.19 224.60 4.17 o -6 4 1 63.85 67.51 2.46 o -5 4 1 438.28 403.66 6.19 o -4 4 1 1992.96 2067.51 10.60 o -3 4 1 1148.46 1129.71 39.71 o -2 4 1 4353.04 4348.54 58.78 o -1 4 1 59.89 53.86 1.09 o 0 4 1 899.97 939.97 15.40 o 1 4 1 385.53 347.05 7.16 o 2 4 1 2112.37 2369.43 55.66 o 3 4 1 276.02 254.17 6.84 o 4 4 1 1337.36 1367.59 7.13 o 5 4 1 270.12 265.77 2.91 o 6 4 1 197.56 200.86 5.05 o 7 4 1 85.06 81.17 2.57 o 8 4 1 176.92 176.26 4.66 o 9 4 1 3.14 3.16 3.46 o -10 5 1 97.90 107.35 4.65 o -9 5 1 317.75 313.26 6.06 o -8 5 1 43.23 40.66 2.02 o -7 5 1 665.49 667.37 8.39 o -6 5 1 255.70 238.25 3.63 o -5 5 1 793.38 774.63 4.12 o -4 5 1 3.46 2.82 1.26 o -3 5 1 4368.11 4464.63 47.44 o -2 5 1 3142.47 3450.93 103.44 o -1 5 1 355.02 311.98 3.06 o 0 5 1 131.79 156.39 4.33 o 1 5 1 5087.21 5196.40 114.45 o 2 5 1 2246.42 2393.97 55.52 o 3 5 1 293.62 291.41 5.23 o 4 5 1 65.80 80.30 13.29 o 5 5 1 204.39 188.47 3.65 o 6 5 1 268.00 250.96 3.11 o 7 5 1 246.28 249.51 5.66 o 8 5 1 1.73 1.28 2.83 o 9 5 1 153.21 149.50 5.05 o -9 6 1 3.31 4.19 3.69 o -8 6 1 228.44 227.24 6.07 o -7 6 1 10.82 10.61 2.58 o -6 6 1 2041.24 2017.00 18.13 o -5 6 1 67.63 69.51 1.70 o -4 6 1 872.02 878.26 25.97 o -3 6 1 24.53 24.17 1.31 o -2 6 1 1079.13 1050.20 6.80 o -1 6 1 19.35 25.62 0.87 o 0 6 1 479.96 420.57 4.37 o 1 6 1 249.20 245.23 2.23 o 2 6 1 634.70 514.59 22.25 o 3 6 1 0.33 1.71 1.44 o 4 6 1 465.05 453.37 17.81 o 5 6 1 170.58 159.76 2.59 o 6 6 1 527.24 518.88 4.10 o 7 6 1 7.38 7.96 1.94 o 8 6 1 182.69 177.40 3.56 o 9 6 1 0.89 3.14 2.95 o -9 7 1 113.51 114.62 8.27 o -8 7 1 17.57 16.36 2.61 o -7 7 1 508.18 492.24 4.20 o -6 7 1 30.08 21.99 2.35 o -5 7 1 281.56 284.39 2.92 o -4 7 1 43.06 46.48 1.94 o -3 7 1 1243.61 1215.21 32.66 o -2 7 1 297.46 333.08 2.20 o -1 7 1 1279.91 1271.12 32.21 o 0 7 1 8.19 14.72 1.63 o 1 7 1 1121.45 1085.26 26.49 o 2 7 1 251.01 266.38 3.45 o 3 7 1 756.22 761.97 25.93 o 4 7 1 21.41 28.21 2.12 o 5 7 1 337.71 335.88 6.04 o 6 7 1 6.50 4.03 2.39 o 7 7 1 33.35 36.19 2.89 o 8 7 1 30.11 28.93 2.69 o -9 8 1 21.43 22.95 2.87 o -8 8 1 120.40 116.55 3.39 o -7 8 1 210.82 204.61 3.35 o -6 8 1 1205.08 1145.80 14.32 o -5 8 1 35.62 35.22 2.06 o -4 8 1 360.18 330.36 6.82 o -3 8 1 785.36 707.61 32.59 o -2 8 1 822.53 844.22 13.13 o -1 8 1 87.68 91.31 2.60 o 0 8 1 1218.78 1282.72 10.44 o 1 8 1 131.34 134.39 2.51 o 2 8 1 160.39 146.88 3.85 o 3 8 1 138.79 128.28 5.30 o 4 8 1 259.86 253.52 2.95 o 5 8 1 26.48 23.66 2.40 o 6 8 1 456.02 451.35 4.17 o 7 8 1 49.03 42.59 3.73 o 8 8 1 8.56 4.05 2.89 o -8 9 1 6.88 2.67 2.57 o -7 9 1 246.17 237.29 3.49 o -6 9 1 564.96 548.87 6.51 o -5 9 1 237.04 244.29 4.08 o -4 9 1 3.74 6.10 1.88 o -3 9 1 25.56 27.14 1.80 o -2 9 1 759.43 814.58 21.01 o -1 9 1 1387.53 1417.98 26.59 o 0 9 1 1756.94 1849.85 56.83 o 1 9 1 356.93 363.68 8.02 o 2 9 1 440.05 439.74 15.90 o 3 9 1 22.13 19.05 1.43 o 4 9 1 60.79 67.21 2.40 o 5 9 1 315.33 294.38 4.35 o 6 9 1 133.83 130.39 3.05 o 7 9 1 3.84 3.48 3.10 o 8 9 1 8.34 7.32 3.29 o -8 10 1 15.58 12.23 2.94 o -7 10 1 202.55 195.68 3.26 o -6 10 1 26.25 22.84 2.57 o -5 10 1 543.63 524.26 4.26 o -4 10 1 80.85 91.08 2.57 o -3 10 1 128.61 128.08 2.14 o -2 10 1 3.45 3.11 1.45 o -1 10 1 112.85 112.42 2.60 o 0 10 1 1290.99 1246.22 31.29 o 1 10 1 548.28 557.22 9.52 o 2 10 1 58.77 55.95 2.17 o 3 10 1 36.75 32.11 1.71 o 4 10 1 2.56 6.21 2.74 o 5 10 1 416.18 405.50 4.26 o 6 10 1 1.94 4.81 2.39 o 7 10 1 72.17 76.95 3.54 o -7 11 1 26.70 33.84 3.73 o -6 11 1 99.72 95.70 4.84 o -5 11 1 57.91 44.21 2.37 o -4 11 1 1073.59 975.25 9.72 o -3 11 1 293.00 274.57 5.87 o -2 11 1 507.68 524.12 5.61 o -1 11 1 43.33 42.14 1.56 o 0 11 1 38.91 34.94 1.98 o 1 11 1 3.11 6.23 2.04 o 2 11 1 194.25 197.49 2.45 o 3 11 1 237.04 234.52 2.79 o 4 11 1 664.79 606.99 4.66 o 5 11 1 4.33 6.32 2.59 o 6 11 1 16.64 17.30 3.20 o -7 12 1 59.54 50.58 3.03 o -6 12 1 4.45 3.58 2.79 o -5 12 1 185.27 189.26 7.13 o -4 12 1 5.45 2.35 2.36 o -3 12 1 758.04 775.73 4.63 o -2 12 1 37.07 35.42 1.33 o -1 12 1 236.98 238.01 3.64 o 0 12 1 227.31 206.93 3.07 o 1 12 1 540.53 554.35 5.19 o 2 12 1 3.92 7.88 1.86 o 3 12 1 379.85 386.58 11.89 o 4 12 1 9.42 18.27 2.56 o 5 12 1 72.57 75.92 3.22 o 6 12 1 0.27 -0.69 3.04 o -6 13 1 57.34 52.00 3.31 o -5 13 1 5.74 1.75 2.84 o -4 13 1 122.27 121.85 3.16 o -3 13 1 104.36 107.03 2.20 o -2 13 1 319.97 326.06 10.11 o -1 13 1 6.07 8.65 1.94 o 0 13 1 52.03 52.40 1.76 o 1 13 1 59.13 65.96 3.03 o 2 13 1 363.14 379.03 8.87 o 3 13 1 17.47 21.44 2.45 o 4 13 1 75.94 76.91 3.03 o 5 13 1 3.09 5.21 4.13 o -5 14 1 69.01 69.35 3.13 o -4 14 1 14.37 14.61 3.06 o -3 14 1 187.11 198.63 4.71 o -2 14 1 17.83 16.92 2.05 o -1 14 1 228.99 215.52 4.07 o 0 14 1 56.79 61.94 2.98 o 1 14 1 250.07 248.89 9.94 o 2 14 1 15.41 14.88 2.04 o 3 14 1 59.74 56.22 2.82 o 4 14 1 8.74 10.21 6.19 o -3 15 1 74.42 62.26 2.83 o -2 15 1 71.05 65.21 3.08 o -1 15 1 63.53 62.29 3.82 o 0 15 1 84.58 77.52 3.09 o 1 15 1 20.02 20.78 2.48 o 2 15 1 29.53 32.87 4.31 o -10 0 2 136.58 139.13 5.70 o -8 0 2 268.10 286.16 11.56 o -6 0 2 2670.18 2739.12 40.13 o -4 0 2 110.88 137.51 2.54 o -2 0 2 446.39 435.89 4.02 o 0 0 2 23164.18 22830.70 79.56 o 2 0 2 233.52 229.26 5.46 o 4 0 2 163.69 138.21 3.53 o 6 0 2 852.85 851.98 15.98 o 8 0 2 2.48 5.92 4.06 o -11 1 2 27.51 27.62 4.46 o -10 1 2 4.40 2.94 3.19 o -9 1 2 125.59 133.89 3.54 o -8 1 2 289.59 272.54 7.04 o -7 1 2 470.88 467.87 7.53 o -6 1 2 307.60 288.19 5.33 o -5 1 2 863.67 725.50 6.52 o -4 1 2 1053.86 1138.22 10.79 o -3 1 2 103.88 114.09 1.67 o -2 1 2 1140.32 1149.46 11.16 o -1 1 2 1935.06 2101.08 53.04 o 0 1 2 98.45 103.02 2.50 o 1 1 2 73.81 80.37 3.15 o 2 1 2 430.24 448.34 3.86 o 3 1 2 5.14 12.51 1.43 o 4 1 2 665.96 696.69 6.83 o 5 1 2 961.10 986.81 8.43 o 6 1 2 146.48 146.46 3.36 o 7 1 2 15.49 20.50 3.75 o 8 1 2 1.42 1.47 3.75 o 9 1 2 108.84 111.70 5.59 o -10 2 2 144.85 163.10 6.57 o -9 2 2 65.88 65.40 2.26 o -8 2 2 100.85 99.84 3.98 o -7 2 2 4.43 3.57 2.43 o -6 2 2 247.00 240.18 3.78 o -5 2 2 321.70 291.22 2.76 o -4 2 2 314.72 278.61 2.45 o -3 2 2 663.48 705.21 4.79 o -2 2 2 2414.47 2435.83 151.51 o -1 2 2 27.69 27.37 0.97 o 0 2 2 4159.61 4580.26 34.94 o 1 2 2 162.24 164.16 3.20 o 2 2 2 1565.58 1639.70 7.90 o 3 2 2 14.06 19.97 1.98 o 4 2 2 4.98 2.92 1.44 o 5 2 2 317.60 313.45 3.93 o 6 2 2 189.18 184.25 4.47 o 7 2 2 2.31 2.27 2.66 o 8 2 2 112.83 118.05 3.84 o 9 2 2 18.38 21.40 4.00 o -10 3 2 122.31 123.93 4.17 o -9 3 2 380.08 390.16 11.39 o -8 3 2 81.68 93.96 4.39 o -7 3 2 412.00 424.29 8.87 o -6 3 2 424.50 413.09 7.95 o -5 3 2 472.99 468.47 11.07 o -4 3 2 109.77 86.50 3.64 o -3 3 2 912.75 945.88 8.76 o -2 3 2 842.99 794.50 25.01 o -1 3 2 469.54 497.13 16.92 o 0 3 2 1673.06 1792.63 19.32 o 1 3 2 154.68 138.29 1.27 o 2 3 2 1493.69 1562.13 7.84 o 3 3 2 1556.63 1614.77 11.74 o 4 3 2 257.91 239.44 3.37 o 5 3 2 178.43 182.97 2.88 o 6 3 2 26.96 24.47 2.24 o 7 3 2 227.26 232.34 4.85 o 8 3 2 72.98 78.16 4.88 o 9 3 2 3.12 3.60 2.79 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10 82.99 83.51 3.68 o -7 3 10 56.07 56.69 3.90 o -6 3 10 121.41 121.02 3.15 o -5 3 10 90.14 88.51 1.89 o -4 3 10 25.50 22.51 2.02 o -3 3 10 0.92 2.00 2.42 o -2 3 10 22.59 22.94 2.50 o -1 3 10 49.15 49.68 2.79 o 0 3 10 25.68 22.41 2.95 o 1 3 10 6.03 8.22 4.73 o -9 4 10 0.57 2.65 3.11 o -8 4 10 94.48 93.67 3.82 o -7 4 10 60.97 65.39 3.80 o -6 4 10 29.85 30.29 2.41 o -5 4 10 572.43 536.93 5.17 o -4 4 10 0.49 0.05 2.26 o -3 4 10 1.89 4.65 2.13 o -2 4 10 14.05 12.54 3.27 o -1 4 10 381.68 372.64 4.08 o 0 4 10 11.43 11.47 2.77 o 1 4 10 23.91 25.70 3.29 o -9 5 10 145.97 136.78 3.23 o -8 5 10 75.35 76.35 2.94 o -7 5 10 20.68 19.74 4.11 o -6 5 10 99.48 89.61 5.24 o -5 5 10 88.43 74.76 3.50 o -4 5 10 60.14 54.95 2.71 o -3 5 10 1.04 1.21 1.58 o -2 5 10 118.96 110.72 2.66 o -1 5 10 54.52 46.80 2.67 o 0 5 10 33.93 33.80 2.80 o -8 6 10 0.11 2.17 4.88 o -7 6 10 99.89 95.72 3.30 o -6 6 10 0.51 0.95 4.24 o -5 6 10 40.04 37.32 4.11 o -4 6 10 1.90 2.39 1.76 o -3 6 10 67.22 61.08 2.90 o -2 6 10 4.94 2.72 2.30 o -1 6 10 7.62 10.46 2.58 o 0 6 10 1.56 0.04 2.93 o -7 7 10 3.27 5.31 3.27 o -6 7 10 103.42 104.39 4.88 o -5 7 10 36.24 32.52 4.74 o -4 7 10 129.98 126.82 2.00 o -3 7 10 3.30 2.40 2.34 o -2 7 10 73.58 72.94 2.38 o -1 7 10 21.48 21.45 2.65 o -6 8 10 26.38 29.99 5.33 o -5 8 10 27.02 27.96 5.42 o -4 8 10 22.57 22.45 6.77 o -3 8 10 35.39 34.57 2.63 o -2 8 10 17.43 19.68 2.22 o -4 9 10 52.55 50.11 3.57 o -9 0 11 124.98 130.01 5.43 o -7 0 11 44.16 36.28 3.89 o -5 0 11 6.87 9.98 2.98 o -3 0 11 477.83 417.98 5.45 o -1 0 11 43.63 46.49 4.20 o -9 1 11 13.81 17.26 3.73 o -8 1 11 55.21 56.73 3.59 o -7 1 11 24.45 24.34 2.98 o -6 1 11 14.47 14.45 1.88 o -5 1 11 22.22 24.27 2.25 o -4 1 11 117.79 107.54 3.71 o -3 1 11 150.64 127.21 3.69 o -2 1 11 0.90 2.57 3.05 o -1 1 11 0.53 2.94 3.70 o -8 2 11 30.53 28.64 3.31 o -7 2 11 132.20 116.24 4.00 o -6 2 11 1.08 -0.43 1.63 o -5 2 11 45.63 36.26 2.10 o -4 2 11 26.53 25.11 2.71 o -3 2 11 1.70 2.04 2.33 o -2 2 11 12.39 11.52 2.67 o -1 2 11 9.75 9.34 2.84 o 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