#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/76/2207675.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207675_Fobs loop_ _publ_author_name 'Cui, Jian-Zhong' 'Zhang, Dan' 'Lu, Fan-Li' 'Gao, Hong-Ling' 'Wang, Hai-Tao' _publ_section_title ; N,N'-Bis(3-dimethylaminopropyl)dithiooxamide ; _journal_coeditor_code TK6282 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4011 _journal_page_last o4012 _journal_volume 61 _journal_year 2005 _space_group_IT_number 135 _symmetry_space_group_name_Hall '-P 4c 2ab' _symmetry_space_group_name_H-M 'P 42/m b c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.4361 _cell_length_b 14.4361 _cell_length_c 8.2304 _exptl_crystal_F_000 632.00 _reflns_d_resolution_high 0.7982 _[local]_cod_data_source_file tk6282Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 51019E in P4(2)/mbc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 283.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x, z+1/2' '-x, -y, z' 'y, -x, z+1/2' 'x+1/2, -y+1/2, -z' 'y+1/2, x+1/2, -z+1/2' '-x+1/2, y+1/2, -z' '-y+1/2, -x+1/2, -z+1/2' '-x, -y, -z' 'y, -x, -z-1/2' 'x, y, -z' '-y, x, -z-1/2' '-x-1/2, y-1/2, z' '-y-1/2, -x-1/2, z-1/2' 'x-1/2, -y-1/2, z' 'y-1/2, x-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 9312.00 8594.50 1012.22 o 0 2 0 1489.48 1681.75 28.21 o 1 2 0 1613.67 1541.90 57.18 o 2 2 0 692.38 724.00 10.97 o 1 3 0 275.88 228.25 2.96 o 2 3 0 1318.61 1419.74 25.78 o 3 3 0 11607.46 10744.63 453.50 o 0 4 0 2117.76 2110.82 29.88 o 1 4 0 6.69 9.62 1.01 o 2 4 0 1052.47 1040.67 17.28 o 3 4 0 500.28 519.66 10.48 o 4 4 0 2065.38 1990.06 75.14 o 1 5 0 10372.89 10257.33 159.53 o 2 5 0 3452.58 3282.62 32.65 o 3 5 0 134.74 117.08 2.77 o 4 5 0 202.78 189.53 3.57 o 5 5 0 989.31 1128.76 26.59 o 0 6 0 89.01 65.02 3.00 o 1 6 0 1130.18 1103.11 12.73 o 2 6 0 161.41 174.31 3.10 o 3 6 0 2897.20 3124.28 54.51 o 4 6 0 1680.90 1601.02 24.97 o 5 6 0 664.60 602.98 8.21 o 6 6 0 65.96 92.24 3.20 o 1 7 0 2.63 8.97 1.32 o 2 7 0 1456.90 1709.42 18.38 o 3 7 0 2088.90 1880.63 20.23 o 4 7 0 25.04 28.22 1.97 o 5 7 0 16.97 11.79 1.72 o 6 7 0 244.23 231.60 5.11 o 7 7 0 223.57 193.35 6.79 o 0 8 0 16.56 29.80 2.83 o 1 8 0 12.04 2.95 1.25 o 2 8 0 94.09 112.59 2.83 o 3 8 0 884.76 888.10 10.40 o 4 8 0 52.17 63.51 2.56 o 5 8 0 67.77 67.69 2.90 o 6 8 0 238.18 214.82 4.71 o 7 8 0 0.90 -1.24 2.24 o 8 8 0 2132.65 1969.47 36.22 o 1 9 0 0.05 -1.42 1.42 o 2 9 0 1807.56 1700.33 23.52 o 3 9 0 101.89 165.14 3.73 o 4 9 0 25.42 19.45 2.02 o 5 9 0 235.95 220.71 4.47 o 6 9 0 18.33 18.65 2.43 o 7 9 0 367.45 359.20 7.20 o 8 9 0 175.75 163.19 4.95 o 9 9 0 302.71 319.00 17.72 o 0 10 0 248.40 215.76 6.14 o 1 10 0 1354.37 1274.82 14.51 o 2 10 0 7.73 10.54 2.05 o 3 10 0 1428.52 1402.05 15.83 o 4 10 0 28.03 37.18 4.90 o 5 10 0 180.20 176.04 4.13 o 6 10 0 35.66 44.59 3.18 o 7 10 0 244.74 204.52 4.80 o 8 10 0 2.58 0.90 2.18 o 9 10 0 5.93 2.97 1.99 o 10 10 0 8.70 14.18 3.40 o 1 11 0 0.38 0.41 1.92 o 2 11 0 1424.70 1446.01 16.41 o 3 11 0 40.06 43.52 3.21 o 4 11 0 98.50 116.26 3.65 o 5 11 0 49.27 53.46 3.38 o 6 11 0 15.55 15.95 2.17 o 7 11 0 16.49 20.66 2.39 o 8 11 0 41.69 44.44 3.66 o 9 11 0 89.36 84.71 4.17 o 10 11 0 56.61 60.43 3.58 o 11 11 0 166.79 183.85 11.62 o 0 12 0 0.37 2.42 2.78 o 1 12 0 3.67 0.28 1.92 o 2 12 0 48.34 56.03 2.94 o 3 12 0 133.56 133.95 3.87 o 4 12 0 139.23 110.28 3.57 o 5 12 0 0.91 2.11 2.41 o 6 12 0 0.58 -1.71 1.71 o 7 12 0 1.39 -1.84 2.06 o 8 12 0 190.48 174.28 5.29 o 9 12 0 24.69 23.36 3.81 o 10 12 0 33.64 37.22 3.21 o 11 12 0 0.03 1.30 2.29 o 12 12 0 114.60 123.57 6.73 o 1 13 0 96.01 79.42 3.24 o 2 13 0 185.79 190.13 4.48 o 3 13 0 184.87 178.83 4.36 o 4 13 0 0.97 -0.76 1.96 o 5 13 0 30.29 32.14 3.06 o 6 13 0 0.58 -2.17 2.17 o 7 13 0 83.27 82.32 4.18 o 8 13 0 0.81 0.70 2.46 o 9 13 0 10.42 13.09 2.70 o 10 13 0 0.86 -2.68 3.85 o 11 13 0 47.03 42.53 5.24 o 12 13 0 0.49 2.53 2.56 o 0 14 0 169.75 180.61 6.35 o 1 14 0 39.18 34.41 2.83 o 2 14 0 42.19 40.02 3.24 o 3 14 0 70.33 71.94 3.98 o 4 14 0 70.87 75.29 3.59 o 5 14 0 0.19 -2.16 2.16 o 6 14 0 1.82 -0.19 2.38 o 7 14 0 83.20 85.95 4.13 o 8 14 0 2.66 -0.08 2.35 o 9 14 0 4.26 5.25 2.96 o 10 14 0 5.42 3.89 2.35 o 11 14 0 0.85 2.22 3.55 o 1 15 0 57.99 69.90 3.46 o 2 15 0 81.15 85.60 3.50 o 3 15 0 0.02 -2.19 2.19 o 4 15 0 1.15 -2.27 2.27 o 5 15 0 23.18 18.96 2.90 o 6 15 0 121.55 116.87 4.41 o 7 15 0 8.70 2.82 3.28 o 8 15 0 13.81 12.67 2.87 o 9 15 0 6.42 4.09 2.82 o 10 15 0 0.85 0.02 2.27 o 0 16 0 42.98 57.09 5.29 o 1 16 0 12.36 13.59 2.44 o 2 16 0 3.38 -0.25 2.36 o 3 16 0 15.45 16.32 2.76 o 4 16 0 4.37 1.64 2.86 o 5 16 0 37.40 38.95 3.33 o 6 16 0 13.80 14.06 2.82 o 7 16 0 23.34 27.73 3.39 o 8 16 0 6.54 11.73 3.19 o 1 17 0 11.67 18.35 2.83 o 2 17 0 0.90 -0.13 2.35 o 3 17 0 1.37 0.66 2.56 o 4 17 0 8.17 2.32 2.65 o 5 17 0 5.22 6.77 3.13 o 6 17 0 21.50 18.20 2.95 o 0 18 0 9.28 3.88 4.04 o 1 18 0 2.42 -1.97 5.80 o 0 2 1 5299.81 5577.82 83.88 o 1 2 1 1166.37 1076.12 8.61 o 1 3 1 9411.54 9662.84 115.88 o 2 3 1 2989.16 3046.55 33.71 o 0 4 1 459.44 514.24 8.02 o 1 4 1 1056.21 1196.90 9.96 o 2 4 1 1036.29 1003.72 7.17 o 3 4 1 248.86 219.48 2.43 o 1 5 1 849.25 767.67 5.64 o 2 5 1 223.12 236.58 2.37 o 3 5 1 250.12 226.79 2.48 o 4 5 1 1871.62 1968.25 18.36 o 0 6 1 2729.04 2814.56 24.27 o 1 6 1 0.25 -0.65 0.65 o 2 6 1 1382.95 1473.98 10.13 o 3 6 1 233.24 202.87 2.41 o 4 6 1 850.88 814.16 6.59 o 5 6 1 962.05 946.03 7.50 o 1 7 1 2.43 -0.54 0.72 o 2 7 1 842.84 777.09 8.47 o 3 7 1 326.83 348.93 3.27 o 4 7 1 38.86 43.28 1.50 o 5 7 1 1435.60 1302.26 11.44 o 6 7 1 201.56 161.23 2.64 o 0 8 1 716.07 651.21 10.82 o 1 8 1 221.17 264.01 2.85 o 2 8 1 5.81 1.86 0.88 o 3 8 1 1.29 1.95 0.87 o 4 8 1 422.55 384.03 3.83 o 5 8 1 54.54 65.46 1.84 o 6 8 1 140.86 161.34 2.83 o 7 8 1 40.33 34.24 1.96 o 1 9 1 101.52 103.94 1.96 o 2 9 1 48.88 51.15 1.63 o 3 9 1 69.44 62.04 1.72 o 4 9 1 484.71 489.65 4.49 o 5 9 1 310.84 337.98 3.85 o 6 9 1 492.78 482.09 5.38 o 7 9 1 16.79 16.88 1.83 o 8 9 1 603.52 612.58 6.93 o 0 10 1 758.14 723.63 10.15 o 1 10 1 51.43 47.57 1.83 o 2 10 1 451.84 444.71 4.44 o 3 10 1 361.69 370.94 3.84 o 4 10 1 1.47 -1.15 1.15 o 5 10 1 645.14 597.13 5.51 o 6 10 1 32.59 35.27 1.99 o 7 10 1 37.19 33.57 2.13 o 8 10 1 11.96 22.45 1.89 o 9 10 1 136.47 146.20 4.61 o 1 11 1 527.91 513.23 5.26 o 2 11 1 18.00 31.31 1.92 o 3 11 1 185.04 167.32 2.77 o 4 11 1 4.98 0.91 1.22 o 5 11 1 245.18 243.86 3.43 o 6 11 1 71.22 79.45 2.37 o 7 11 1 33.68 35.81 2.08 o 8 11 1 239.62 238.15 4.06 o 9 11 1 1.56 -1.47 1.47 o 10 11 1 61.04 77.09 2.68 o 0 12 1 369.65 351.66 6.06 o 1 12 1 40.10 37.79 1.92 o 2 12 1 108.39 113.68 2.55 o 3 12 1 14.53 12.59 1.47 o 4 12 1 86.46 74.58 2.36 o 5 12 1 62.29 52.31 2.12 o 6 12 1 110.11 115.96 2.83 o 7 12 1 0.26 -0.58 1.38 o 8 12 1 11.76 13.11 1.65 o 9 12 1 0.45 0.09 1.41 o 10 12 1 0.32 0.28 1.43 o 11 12 1 3.92 3.32 1.47 o 1 13 1 179.40 188.87 3.16 o 2 13 1 79.95 73.75 2.16 o 3 13 1 29.41 41.08 2.08 o 4 13 1 108.18 95.99 2.45 o 5 13 1 60.96 64.75 2.54 o 6 13 1 1.85 -0.87 1.51 o 7 13 1 21.89 24.53 1.95 o 8 13 1 45.81 49.61 2.50 o 9 13 1 6.23 7.46 1.94 o 10 13 1 70.35 71.78 2.65 o 11 13 1 11.89 15.14 1.88 o 12 13 1 62.15 76.24 3.02 o 0 14 1 149.26 158.29 4.27 o 1 14 1 25.11 29.29 2.02 o 2 14 1 18.69 15.14 1.68 o 3 14 1 104.60 112.90 2.66 o 4 14 1 5.78 10.06 1.62 o 5 14 1 93.62 97.54 2.75 o 6 14 1 69.85 72.77 2.78 o 7 14 1 5.50 1.92 1.69 o 8 14 1 64.25 67.02 4.82 o 9 14 1 50.13 52.61 3.65 o 10 14 1 7.16 8.72 1.98 o 11 14 1 38.18 43.41 3.93 o 1 15 1 38.80 38.14 2.07 o 2 15 1 0.00 -1.43 1.43 o 3 15 1 21.21 24.81 2.39 o 4 15 1 38.90 41.75 2.26 o 5 15 1 29.61 33.47 2.19 o 6 15 1 36.06 36.72 2.59 o 7 15 1 83.18 89.45 3.35 o 8 15 1 0.73 -1.90 1.90 o 9 15 1 0.78 -1.79 1.79 o 0 16 1 88.52 93.14 4.89 o 1 16 1 44.74 54.59 2.38 o 2 16 1 30.13 35.52 2.13 o 3 16 1 24.57 26.91 2.13 o 4 16 1 0.06 -1.70 1.70 o 5 16 1 16.64 17.36 2.31 o 6 16 1 37.33 39.24 2.70 o 7 16 1 3.81 3.56 2.28 o 8 16 1 10.13 11.15 3.18 o 1 17 1 12.85 8.05 1.80 o 2 17 1 53.16 60.77 2.59 o 3 17 1 2.91 -0.78 1.94 o 4 17 1 5.15 1.54 1.86 o 5 17 1 13.59 13.20 2.11 o 0 18 1 4.11 -4.06 4.06 o 0 0 2 80196.39 78880.74 1578.60 o 1 1 2 14950.54 14773.26 214.89 o 0 2 2 785.90 873.41 7.79 o 1 2 2 1302.65 1217.40 7.58 o 2 2 2 653.61 675.69 5.97 o 1 3 2 38.42 34.68 0.83 o 2 3 2 246.07 276.94 2.11 o 3 3 2 309.77 306.07 3.28 o 0 4 2 3140.56 3076.52 25.62 o 1 4 2 280.18 269.73 2.11 o 2 4 2 11.83 15.86 0.67 o 3 4 2 42.47 37.00 0.93 o 4 4 2 2123.03 2280.34 18.71 o 1 5 2 2616.09 2603.11 14.58 o 2 5 2 1747.43 1728.85 10.18 o 3 5 2 101.24 83.65 1.24 o 4 5 2 429.76 473.03 3.43 o 5 5 2 1505.31 1475.56 13.46 o 0 6 2 817.89 840.25 7.61 o 1 6 2 1283.38 1326.50 7.85 o 2 6 2 119.79 132.96 1.51 o 3 6 2 1817.83 1808.07 11.91 o 4 6 2 604.33 616.76 4.69 o 5 6 2 237.93 275.12 2.59 o 6 6 2 2.50 2.00 1.26 o 1 7 2 17.01 17.17 0.84 o 2 7 2 317.00 348.89 2.86 o 3 7 2 564.85 598.68 4.42 o 4 7 2 72.28 69.24 1.38 o 5 7 2 2.19 3.90 0.82 o 6 7 2 51.08 47.13 1.58 o 7 7 2 178.31 152.35 3.73 o 0 8 2 11.52 9.25 1.13 o 1 8 2 1.44 -0.69 0.69 o 2 8 2 14.91 15.14 0.90 o 3 8 2 425.35 448.68 4.03 o 4 8 2 145.22 126.22 2.11 o 5 8 2 32.37 36.72 1.56 o 6 8 2 185.31 179.38 2.68 o 7 8 2 17.58 18.86 1.47 o 8 8 2 1089.98 1023.20 12.39 o 1 9 2 6.10 6.12 1.00 o 2 9 2 1359.49 1339.06 9.71 o 3 9 2 2.57 5.92 1.11 o 4 9 2 0.58 -1.10 1.10 o 5 9 2 149.87 157.58 2.64 o 6 9 2 13.95 15.95 1.49 o 7 9 2 367.05 342.38 4.26 o 8 9 2 103.45 97.52 2.43 o 9 9 2 210.52 204.66 5.53 o 0 10 2 62.73 66.90 2.71 o 1 10 2 538.22 536.13 4.90 o 2 10 2 7.92 14.54 1.35 o 3 10 2 1139.93 1079.70 9.01 o 4 10 2 27.20 26.39 1.58 o 5 10 2 47.26 51.42 1.96 o 6 10 2 55.57 59.58 2.18 o 7 10 2 194.07 176.12 3.11 o 8 10 2 1.27 -1.00 1.26 o 9 10 2 0.18 -1.26 1.26 o 10 10 2 0.58 0.51 1.92 o 1 11 2 12.88 10.39 1.43 o 2 11 2 1109.93 1105.19 8.98 o 3 11 2 27.83 34.80 1.82 o 4 11 2 32.81 42.50 1.80 o 5 11 2 8.10 4.17 1.28 o 6 11 2 11.54 15.89 1.54 o 7 11 2 17.19 21.44 1.78 o 8 11 2 22.21 21.32 2.04 o 9 11 2 48.60 54.19 2.57 o 10 11 2 24.67 34.37 2.93 o 11 11 2 88.80 98.49 5.77 o 0 12 2 5.84 8.11 1.95 o 1 12 2 8.82 6.93 1.43 o 2 12 2 25.85 37.73 1.84 o 3 12 2 94.30 92.85 2.48 o 4 12 2 134.37 116.36 2.54 o 5 12 2 0.05 -0.86 1.34 o 6 12 2 1.59 -0.08 1.41 o 7 12 2 4.12 2.31 1.41 o 8 12 2 119.29 117.88 2.87 o 9 12 2 16.88 22.11 2.69 o 10 12 2 26.72 31.77 2.38 o 11 12 2 0.00 0.69 1.72 o 12 12 2 75.59 81.34 4.34 o 1 13 2 57.49 67.17 2.17 o 2 13 2 71.63 78.83 2.22 o 3 13 2 138.12 130.86 2.90 o 4 13 2 6.29 3.68 1.54 o 5 13 2 22.50 18.03 1.90 o 6 13 2 5.06 6.40 1.67 o 7 13 2 39.32 50.13 2.47 o 8 13 2 1.41 0.22 1.55 o 9 13 2 6.93 8.01 2.31 o 10 13 2 0.53 -1.62 1.62 o 11 13 2 35.30 42.56 2.58 o 12 13 2 0.17 4.37 2.27 o 0 14 2 134.81 141.35 4.13 o 1 14 2 43.87 47.40 2.43 o 2 14 2 40.20 42.94 2.14 o 3 14 2 44.91 45.05 2.25 o 4 14 2 37.54 37.89 2.19 o 5 14 2 2.55 0.53 1.64 o 6 14 2 1.18 -1.06 1.54 o 7 14 2 39.86 42.24 3.82 o 8 14 2 4.45 4.52 1.76 o 9 14 2 4.28 4.16 1.73 o 10 14 2 4.32 2.66 2.07 o 1 15 2 39.91 39.92 2.39 o 2 15 2 45.89 51.99 2.58 o 3 15 2 0.23 -1.49 1.49 o 4 15 2 1.65 0.04 1.64 o 5 15 2 12.30 12.91 2.02 o 6 15 2 85.23 98.33 2.98 o 7 15 2 8.09 6.99 1.92 o 8 15 2 11.79 10.35 2.04 o 9 15 2 3.74 4.48 2.14 o 0 16 2 28.51 42.68 4.01 o 1 16 2 14.48 16.66 2.10 o 2 16 2 2.02 -1.68 1.68 o 3 16 2 7.03 3.84 2.44 o 4 16 2 4.34 -1.82 1.82 o 5 16 2 26.98 29.78 2.25 o 6 16 2 8.61 8.30 2.01 o 7 16 2 16.81 21.20 3.51 o 1 17 2 8.95 8.95 2.07 o 2 17 2 0.12 -1.76 1.76 o 3 17 2 2.52 -1.01 1.75 o 4 17 2 2.99 0.12 2.00 o 5 17 2 4.03 0.78 2.71 o 0 2 3 341.51 391.54 4.09 o 1 2 3 55.51 54.90 0.99 o 1 3 3 71.71 80.87 1.17 o 2 3 3 1166.88 1189.24 7.59 o 0 4 3 1452.26 1347.22 10.87 o 1 4 3 50.62 54.04 0.98 o 2 4 3 486.95 469.89 3.75 o 3 4 3 153.47 154.44 1.63 o 1 5 3 95.05 76.99 1.23 o 2 5 3 17.20 10.40 0.72 o 3 5 3 831.06 779.72 5.98 o 4 5 3 926.80 996.49 6.37 o 0 6 3 562.94 585.89 5.77 o 1 6 3 52.15 73.55 1.28 o 2 6 3 0.08 3.74 0.72 o 3 6 3 64.40 46.57 1.26 o 4 6 3 97.79 83.44 1.40 o 5 6 3 219.89 190.00 2.10 o 1 7 3 5.29 3.85 0.77 o 2 7 3 168.15 155.28 1.81 o 3 7 3 365.58 392.39 3.18 o 4 7 3 193.69 195.60 2.16 o 5 7 3 544.75 527.04 4.15 o 6 7 3 45.56 49.13 1.48 o 0 8 3 45.14 33.53 1.64 o 1 8 3 246.65 236.47 2.40 o 2 8 3 19.89 21.34 1.11 o 3 8 3 0.01 0.54 0.91 o 4 8 3 267.61 264.18 3.08 o 5 8 3 151.33 141.23 2.54 o 6 8 3 179.95 174.51 2.66 o 7 8 3 0.59 -1.26 1.26 o 1 9 3 0.27 -1.03 1.03 o 2 9 3 88.64 95.37 1.98 o 3 9 3 2.19 1.75 1.22 o 4 9 3 120.10 130.42 2.49 o 5 9 3 23.44 27.58 1.71 o 6 9 3 242.28 240.91 3.66 o 7 9 3 10.56 10.92 1.72 o 8 9 3 199.52 231.73 3.87 o 0 10 3 470.20 518.79 7.34 o 1 10 3 92.07 83.48 2.40 o 2 10 3 186.51 190.18 2.85 o 3 10 3 172.61 157.87 2.77 o 4 10 3 0.89 -1.30 1.30 o 5 10 3 242.37 239.25 3.39 o 6 10 3 7.56 7.23 1.57 o 7 10 3 35.07 45.80 2.35 o 8 10 3 0.55 -1.50 1.50 o 9 10 3 81.22 87.93 3.76 o 1 11 3 388.08 392.67 5.07 o 2 11 3 0.56 -1.46 1.46 o 3 11 3 119.32 117.42 2.70 o 4 11 3 1.26 0.00 1.33 o 5 11 3 62.45 74.86 2.16 o 6 11 3 44.06 49.50 2.20 o 7 11 3 6.94 3.00 1.64 o 8 11 3 81.26 87.06 2.80 o 9 11 3 0.07 -1.21 1.56 o 10 11 3 35.54 40.77 3.17 o 0 12 3 201.33 205.44 5.88 o 1 12 3 59.25 67.39 2.55 o 2 12 3 16.89 12.58 1.86 o 3 12 3 5.46 4.33 1.42 o 4 12 3 34.39 48.63 2.30 o 5 12 3 8.63 9.26 1.66 o 6 12 3 58.88 62.91 3.02 o 7 12 3 3.64 0.57 1.56 o 8 12 3 9.97 8.05 1.76 o 9 12 3 0.26 -0.51 1.56 o 10 12 3 0.24 -1.61 1.61 o 11 12 3 5.82 8.32 1.95 o 1 13 3 71.61 81.25 2.64 o 2 13 3 20.10 19.69 1.99 o 3 13 3 6.00 5.35 1.71 o 4 13 3 94.19 100.45 2.81 o 5 13 3 38.67 36.90 2.56 o 6 13 3 0.26 -1.61 1.61 o 7 13 3 10.93 13.53 1.86 o 8 13 3 17.00 23.74 2.11 o 9 13 3 2.24 -0.01 1.62 o 10 13 3 35.82 35.03 3.74 o 11 13 3 9.28 8.64 2.08 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