#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:17:54 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180997 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/77/2207713.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207713_Fobs loop_ _publ_author_name 'Sch\"odel, Frauke' 'Lerner, Hans-Wolfram' 'Bru Roig, Miriam' 'Bolte, Michael' _publ_section_title ; Tetra-n-butylammonium tetrakis(pentafluorophenyl)borate ; _journal_coeditor_code AT6058 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o372 _journal_page_last o373 _journal_volume 62 _journal_year 2006 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 130.629 _cell_angle_gamma 90.000 _cell_length_a 24.1040 _cell_length_b 12.8925 _cell_length_c 17.5363 _exptl_crystal_F_000 1872.00 _reflns_d_resolution_high 0.8222 _cod_data_source_file at6058Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa499 in Cc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 283.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 4848.69 4884.47 117.96 o 6 0 0 17827.53 17051.61 909.17 o 8 0 0 11061.59 10529.72 145.07 o 10 0 0 968.10 978.99 31.13 o 12 0 0 2043.28 1980.76 79.38 o 14 0 0 2985.65 3014.15 46.90 o 16 0 0 3941.19 4249.77 51.28 o 18 0 0 578.38 565.83 41.96 o 20 0 0 42.25 -5.70 31.67 o 22 0 0 250.37 160.34 36.23 o 3 1 0 2974.73 2796.35 71.17 o 5 1 0 42549.66 43540.47 566.35 o 7 1 0 14177.72 13348.78 322.83 o 9 1 0 8250.23 8158.15 158.43 o 11 1 0 1317.45 1404.77 46.12 o 13 1 0 2765.77 2900.74 72.82 o 15 1 0 970.55 1076.56 42.17 o 17 1 0 436.72 418.45 22.07 o 19 1 0 332.99 344.59 25.93 o 21 1 0 41.08 52.95 25.17 o 2 2 0 2937.67 2532.10 60.27 o 4 2 0 59516.39 64365.77 496.55 o 6 2 0 8518.38 8702.55 68.08 o 8 2 0 3315.10 3106.57 33.75 o 10 2 0 1145.84 1367.39 54.45 o 12 2 0 2277.00 2292.16 45.70 o 14 2 0 147.02 176.18 20.70 o 16 2 0 174.72 170.10 21.10 o 18 2 0 419.01 430.04 27.86 o 20 2 0 314.94 304.14 24.65 o 1 3 0 4389.64 4246.53 72.84 o 3 3 0 4169.20 3647.29 61.42 o 5 3 0 20064.83 20826.92 159.50 o 7 3 0 38404.11 41401.12 338.47 o 9 3 0 10151.43 10192.07 87.72 o 11 3 0 2368.84 2647.76 101.32 o 13 3 0 1285.47 1205.88 24.29 o 15 3 0 1261.41 1313.84 33.33 o 17 3 0 402.21 423.48 21.73 o 19 3 0 328.77 336.54 22.77 o 21 3 0 73.02 139.20 25.74 o 0 4 0 152.90 123.76 26.49 o 2 4 0 2527.32 2236.26 47.95 o 4 4 0 7701.63 7852.37 236.85 o 6 4 0 4560.28 5324.45 143.87 o 8 4 0 2056.16 2254.35 60.37 o 10 4 0 2058.12 2007.43 36.84 o 12 4 0 2758.08 2754.03 64.48 o 14 4 0 1184.11 1137.63 65.13 o 16 4 0 397.85 408.28 22.25 o 18 4 0 86.28 81.28 26.44 o 20 4 0 679.36 577.44 44.35 o 1 5 0 2260.79 2151.28 36.50 o 3 5 0 11596.42 11139.20 102.11 o 5 5 0 11278.04 11451.31 388.56 o 7 5 0 1020.56 1057.99 30.48 o 9 5 0 134.16 165.41 24.86 o 11 5 0 3017.94 3099.35 38.19 o 13 5 0 1269.19 1259.23 27.62 o 15 5 0 1440.80 1455.42 29.34 o 17 5 0 242.52 245.61 31.69 o 19 5 0 820.79 725.51 56.33 o 21 5 0 420.53 429.18 45.55 o 0 6 0 36.91 60.30 21.02 o 2 6 0 1894.23 1752.40 42.91 o 4 6 0 9603.82 10017.16 372.43 o 6 6 0 7450.78 7934.48 211.18 o 8 6 0 2164.64 2315.03 37.25 o 10 6 0 460.21 483.45 27.91 o 12 6 0 569.23 584.68 37.55 o 14 6 0 246.35 308.69 25.44 o 16 6 0 54.34 54.48 26.29 o 18 6 0 1051.50 1080.04 33.48 o 20 6 0 203.51 212.41 27.94 o 1 7 0 9321.44 8963.14 309.01 o 3 7 0 75.05 31.52 24.50 o 5 7 0 2084.13 2220.71 44.46 o 7 7 0 622.91 668.74 25.67 o 9 7 0 320.07 344.95 21.67 o 11 7 0 310.03 341.71 24.21 o 13 7 0 1562.13 1474.14 32.78 o 15 7 0 708.84 650.29 29.29 o 17 7 0 81.62 70.79 28.24 o 19 7 0 444.49 358.54 31.81 o 0 8 0 62.39 35.17 30.09 o 2 8 0 1466.30 1528.76 32.80 o 4 8 0 3753.18 3777.48 78.87 o 6 8 0 36.39 5.15 82.64 o 8 8 0 1051.18 1020.10 28.24 o 10 8 0 3114.99 3220.06 82.40 o 12 8 0 1490.82 1520.51 32.29 o 14 8 0 439.02 423.17 25.71 o 16 8 0 191.16 265.06 32.71 o 18 8 0 217.11 203.65 30.97 o 1 9 0 7987.89 7729.40 108.83 o 3 9 0 2577.14 2824.82 62.06 o 5 9 0 470.12 496.55 35.72 o 7 9 0 764.00 758.64 36.20 o 9 9 0 1789.35 1796.51 35.64 o 11 9 0 2129.32 2137.04 58.82 o 13 9 0 442.08 427.45 32.05 o 15 9 0 126.06 136.27 27.64 o 17 9 0 120.64 149.73 30.97 o 0 10 0 649.27 607.13 51.11 o 2 10 0 2866.44 2721.37 63.96 o 4 10 0 629.54 635.55 32.43 o 6 10 0 1028.73 1080.46 42.27 o 8 10 0 3026.11 3047.60 60.31 o 10 10 0 949.93 880.07 28.86 o 12 10 0 544.95 558.78 23.00 o 14 10 0 357.59 382.91 28.89 o 16 10 0 102.13 150.11 30.49 o 1 11 0 403.57 455.60 36.70 o 3 11 0 250.39 226.03 36.83 o 5 11 0 1314.17 1317.46 33.67 o 7 11 0 646.29 675.33 34.14 o 9 11 0 31.98 80.86 25.62 o 11 11 0 629.71 555.42 29.00 o 13 11 0 428.62 410.60 35.22 o 15 11 0 286.33 332.21 31.57 o 0 12 0 34.62 -20.99 50.09 o 2 12 0 39.18 36.88 43.49 o 4 12 0 116.38 110.07 29.18 o 6 12 0 641.18 737.67 40.74 o 8 12 0 632.75 685.03 37.66 o 10 12 0 280.28 339.61 30.51 o 12 12 0 8.86 38.98 29.88 o 14 12 0 1.36 18.78 58.16 o 1 13 0 409.34 405.50 38.85 o 3 13 0 465.23 503.34 39.48 o 5 13 0 239.47 211.15 56.41 o 7 13 0 116.62 115.79 36.69 o 9 13 0 164.11 134.77 31.30 o 11 13 0 328.97 328.47 32.64 o 0 14 0 232.13 318.07 60.10 o 2 14 0 185.98 189.62 46.53 o 4 14 0 627.95 692.06 43.27 o 6 14 0 374.18 337.31 33.48 o 8 14 0 147.40 65.96 35.68 o 1 15 0 35.80 36.86 41.16 o 3 15 0 188.48 171.36 30.34 o 5 15 0 202.42 248.78 55.92 o -23 1 1 17.69 19.67 30.50 o -21 1 1 201.65 185.06 25.69 o -19 1 1 1394.86 1417.89 26.43 o -17 1 1 2144.77 2231.27 29.69 o -15 1 1 4355.86 4291.26 103.76 o -13 1 1 1297.66 1282.79 53.26 o -11 1 1 238.78 201.72 19.01 o -9 1 1 11075.25 11114.74 247.15 o -7 1 1 7665.14 7877.29 182.64 o -5 1 1 32048.12 33178.90 511.93 o 3 1 1 4854.21 4208.53 110.59 o 5 1 1 7570.96 7776.03 105.40 o 7 1 1 4170.19 4555.70 80.72 o 9 1 1 2391.08 2410.09 44.06 o 11 1 1 617.24 536.98 35.25 o 13 1 1 169.02 177.72 20.91 o 15 1 1 1668.88 1738.36 35.61 o 17 1 1 939.80 936.93 27.89 o 19 1 1 584.10 573.28 27.78 o 21 1 1 188.60 185.19 24.94 o -22 2 1 105.94 123.44 31.42 o -20 2 1 379.17 405.94 26.52 o -18 2 1 395.50 449.34 32.83 o -16 2 1 85.87 101.52 19.04 o -14 2 1 1131.36 1199.52 26.52 o -12 2 1 215.35 227.44 23.33 o -10 2 1 1051.82 1164.68 30.55 o -8 2 1 24670.03 24790.09 346.40 o -6 2 1 46964.33 49621.18 659.36 o -4 2 1 1911.48 1746.30 39.51 o -2 2 1 6714.90 5158.45 123.98 o 2 2 1 32380.05 33963.58 509.99 o 4 2 1 4178.09 4146.53 85.33 o 6 2 1 510.97 522.48 30.43 o 8 2 1 7644.40 7688.35 116.17 o 10 2 1 7989.55 8366.01 284.14 o 12 2 1 623.35 579.96 23.34 o 14 2 1 1863.73 1898.63 34.97 o 16 2 1 1022.74 907.49 23.39 o 18 2 1 244.11 241.40 25.12 o 20 2 1 146.69 166.14 31.14 o -21 3 1 242.73 238.08 23.55 o -19 3 1 256.16 268.84 21.39 o -17 3 1 253.51 264.65 19.63 o -15 3 1 855.14 874.92 30.82 o -13 3 1 832.29 880.07 23.81 o -11 3 1 3921.68 4232.69 102.88 o -9 3 1 406.14 418.05 22.50 o -7 3 1 18502.17 20184.48 213.98 o -5 3 1 46790.51 47403.52 516.95 o -3 3 1 37639.52 36118.13 481.94 o -1 3 1 3338.97 2796.90 61.47 o 1 3 1 3571.89 3422.46 66.20 o 3 3 1 6763.80 6187.64 77.03 o 5 3 1 2961.36 2886.90 39.36 o 7 3 1 549.46 616.80 28.50 o 9 3 1 3302.17 3148.81 67.88 o 11 3 1 189.92 242.18 30.81 o 13 3 1 577.78 546.90 20.38 o 15 3 1 308.63 303.04 19.67 o 17 3 1 49.61 41.49 19.92 o 19 3 1 135.29 124.17 24.22 o -22 4 1 359.58 326.90 26.64 o -20 4 1 27.40 31.83 37.88 o -18 4 1 727.79 691.55 40.37 o -16 4 1 2993.28 2918.31 49.06 o -14 4 1 1118.11 1114.25 26.81 o -12 4 1 2417.10 2486.02 51.33 o -10 4 1 2832.64 2834.20 39.85 o -8 4 1 22015.31 23250.24 354.97 o -6 4 1 6876.75 6416.24 103.73 o -4 4 1 2910.28 2866.74 48.17 o -2 4 1 1087.26 1040.23 33.98 o 0 4 1 5900.09 5865.89 78.40 o 2 4 1 6209.00 5832.98 101.87 o 4 4 1 3028.08 2775.73 39.12 o 6 4 1 9531.55 9689.81 244.06 o 8 4 1 4962.41 5067.21 62.35 o 10 4 1 1888.54 1985.53 67.71 o 12 4 1 52.29 51.68 17.80 o 14 4 1 267.74 294.62 21.06 o 16 4 1 561.07 598.71 23.70 o 18 4 1 28.60 57.88 22.84 o 20 4 1 261.42 229.51 31.44 o -21 5 1 257.99 230.81 36.26 o -19 5 1 5.83 5.64 28.19 o -17 5 1 209.53 203.19 20.03 o -15 5 1 583.05 581.55 25.35 o -13 5 1 316.91 305.27 29.17 o -11 5 1 1427.61 1601.30 31.89 o -9 5 1 7295.41 7351.94 156.06 o -7 5 1 7683.74 7706.50 70.39 o -5 5 1 4754.71 4496.96 55.02 o -3 5 1 1963.59 2033.66 41.81 o -1 5 1 761.54 603.28 31.07 o 1 5 1 13863.22 13310.06 103.88 o 3 5 1 3518.12 3311.10 91.39 o 5 5 1 914.56 831.17 36.99 o 7 5 1 1188.62 1231.66 35.88 o 9 5 1 11.01 0.26 22.24 o 11 5 1 236.67 254.32 22.84 o 13 5 1 1241.26 1277.46 30.35 o 15 5 1 940.45 862.83 26.71 o 17 5 1 2300.17 2364.93 65.78 o 19 5 1 150.43 134.13 25.05 o -20 6 1 230.95 213.40 27.40 o -18 6 1 1159.96 1153.89 36.37 o -16 6 1 442.31 439.47 22.57 o -14 6 1 135.70 141.78 28.67 o -12 6 1 5280.96 5446.49 198.04 o -10 6 1 2004.22 1960.34 65.17 o -8 6 1 1673.25 1634.77 31.19 o -6 6 1 12165.97 12886.73 642.06 o -4 6 1 21387.40 20987.53 514.81 o -2 6 1 5534.14 5373.94 65.02 o 0 6 1 94.34 94.53 26.84 o 2 6 1 8185.23 8532.32 87.52 o 4 6 1 9150.25 9414.38 80.01 o 6 6 1 939.17 927.88 36.01 o 8 6 1 2437.89 2660.33 59.37 o 10 6 1 309.96 322.03 21.77 o 12 6 1 3821.53 3690.97 83.50 o 14 6 1 1760.47 1688.79 56.80 o 16 6 1 130.94 128.56 30.11 o 18 6 1 1034.35 990.67 38.48 o -19 7 1 233.52 261.10 26.29 o -17 7 1 93.28 104.99 24.06 o -15 7 1 603.77 546.63 34.16 o -13 7 1 3649.68 3535.27 44.77 o -11 7 1 553.67 559.21 28.93 o -9 7 1 318.86 233.51 20.50 o -7 7 1 1094.15 1106.05 48.66 o -5 7 1 286.83 298.82 35.68 o -3 7 1 574.52 588.28 25.36 o -1 7 1 6780.86 6414.07 68.75 o 1 7 1 11044.06 11498.75 318.79 o 3 7 1 306.27 386.56 50.44 o 5 7 1 613.86 668.97 44.84 o 7 7 1 919.89 889.79 27.34 o 9 7 1 4980.73 5063.75 195.27 o 11 7 1 203.90 226.26 35.26 o 13 7 1 990.96 942.76 33.86 o 15 7 1 55.10 96.16 27.63 o 17 7 1 45.64 81.68 30.24 o -18 8 1 202.08 190.34 33.80 o -16 8 1 4.10 -7.75 22.83 o -14 8 1 1613.59 1559.39 61.31 o -12 8 1 39.52 45.01 21.13 o -10 8 1 827.11 846.03 38.07 o -8 8 1 43.60 21.08 17.11 o -6 8 1 1943.15 1979.64 73.77 o -4 8 1 1353.03 1364.86 35.31 o -2 8 1 200.08 276.66 64.82 o 0 8 1 4142.89 4239.83 85.37 o 2 8 1 390.45 397.78 32.82 o 4 8 1 527.71 580.23 33.75 o 6 8 1 1524.36 1606.03 125.27 o 8 8 1 3179.36 3302.46 38.74 o 10 8 1 544.47 473.45 26.04 o 12 8 1 1836.28 1735.70 44.70 o 14 8 1 683.34 653.94 50.32 o 16 8 1 133.25 135.13 38.30 o 18 8 1 98.79 108.02 31.27 o -17 9 1 127.21 119.46 28.76 o -15 9 1 46.49 87.30 30.60 o -13 9 1 1052.70 968.21 28.41 o -11 9 1 136.29 129.01 28.37 o -9 9 1 4212.67 4068.83 142.67 o -7 9 1 645.85 639.86 30.05 o -5 9 1 104.57 114.33 29.70 o -3 9 1 1526.87 1593.45 60.75 o -1 9 1 3154.62 3052.44 45.63 o 1 9 1 255.57 231.33 36.66 o 3 9 1 376.38 372.64 32.04 o 5 9 1 2938.22 2843.88 98.24 o 7 9 1 6745.26 6790.88 196.74 o 9 9 1 269.87 319.15 29.08 o 11 9 1 455.80 511.36 26.28 o 13 9 1 253.93 280.48 31.12 o 15 9 1 3.57 29.50 28.59 o 17 9 1 79.07 104.88 37.27 o -16 10 1 164.00 214.43 30.06 o -14 10 1 62.75 53.14 29.79 o -12 10 1 147.50 122.05 31.48 o -10 10 1 1342.35 1252.81 72.38 o -8 10 1 2.65 4.52 28.00 o -6 10 1 1411.63 1436.75 39.63 o -4 10 1 1387.95 1406.12 40.90 o -2 10 1 1439.73 1302.80 36.09 o 0 10 1 888.99 881.86 39.11 o 2 10 1 1870.62 1791.12 52.54 o 4 10 1 2504.67 2526.01 49.50 o 6 10 1 2356.23 2398.42 43.92 o 8 10 1 593.76 653.04 34.98 o 10 10 1 177.64 187.21 26.17 o 12 10 1 111.51 120.35 24.91 o 14 10 1 31.91 44.91 34.28 o 16 10 1 169.77 174.58 28.19 o -15 11 1 442.74 483.00 35.91 o -13 11 1 12.45 47.35 23.24 o -11 11 1 266.87 300.14 31.01 o -9 11 1 47.43 53.63 29.53 o -7 11 1 933.02 885.07 91.46 o -5 11 1 328.38 388.67 27.08 o -3 11 1 1663.65 1617.54 43.91 o -1 11 1 1159.15 1196.20 35.93 o 1 11 1 125.85 162.83 34.17 o 3 11 1 112.30 114.70 29.67 o 5 11 1 159.94 215.00 24.93 o 7 11 1 83.39 61.18 21.88 o 9 11 1 277.39 273.74 27.58 o 11 11 1 334.21 304.40 26.28 o 13 11 1 515.02 428.16 27.96 o -14 12 1 267.76 305.35 35.72 o -12 12 1 5.67 55.43 26.26 o -10 12 1 285.10 331.18 26.29 o -8 12 1 339.29 312.34 25.53 o -6 12 1 1262.05 1254.32 38.17 o -4 12 1 656.77 661.94 56.60 o -2 12 1 577.16 528.09 32.26 o 0 12 1 540.85 494.20 37.70 o 2 12 1 357.74 390.16 46.87 o 4 12 1 426.19 385.88 32.28 o 6 12 1 295.22 343.49 31.11 o 8 12 1 55.14 70.55 23.96 o 10 12 1 182.19 150.45 25.16 o 12 12 1 44.81 49.92 24.45 o -13 13 1 101.37 193.29 43.99 o -11 13 1 478.44 581.02 53.48 o -9 13 1 762.30 857.13 27.75 o -7 13 1 627.21 633.68 36.71 o -5 13 1 0.57 90.97 37.07 o -3 13 1 323.74 296.83 34.61 o -1 13 1 539.02 579.42 40.57 o 1 13 1 56.57 48.63 37.13 o 3 13 1 243.25 288.08 43.79 o 5 13 1 347.82 369.29 39.57 o 7 13 1 434.02 418.62 28.51 o 9 13 1 281.90 331.78 43.70 o 11 13 1 175.54 242.00 45.66 o -10 14 1 76.06 75.79 35.54 o -8 14 1 120.25 114.02 43.02 o -6 14 1 38.35 108.43 42.14 o -4 14 1 5.71 41.64 55.71 o -2 14 1 187.53 227.37 37.86 o 0 14 1 232.21 303.47 48.46 o 2 14 1 480.69 465.50 35.01 o 4 14 1 28.70 78.87 33.85 o 6 14 1 84.90 43.24 48.66 o 8 14 1 531.86 494.39 27.67 o -5 15 1 215.34 227.46 35.40 o -3 15 1 81.13 85.65 33.82 o -1 15 1 96.47 80.78 93.26 o 1 15 1 61.16 68.65 76.37 o 3 15 1 59.72 40.46 34.55 o 5 15 1 159.57 206.43 36.27 o -22 0 2 804.48 735.54 62.88 o -20 0 2 129.69 171.27 30.76 o -18 0 2 1347.19 1380.65 37.14 o -16 0 2 8606.93 8783.28 85.36 o -14 0 2 709.42 682.36 29.67 o -12 0 2 487.05 508.47 27.78 o -10 0 2 3297.89 3236.28 74.31 o -8 0 2 187.51 170.26 25.19 o -6 0 2 15151.95 14589.52 1235.10 o 2 0 2 8611.89 8508.10 101.95 o 4 0 2 16026.73 14869.52 209.86 o 6 0 2 32493.13 33377.16 3107.78 o 8 0 2 19995.78 19683.89 186.36 o 10 0 2 2425.89 2512.26 68.94 o 12 0 2 3254.39 3440.12 60.99 o 14 0 2 68.64 76.24 24.96 o 16 0 2 1149.70 1193.22 36.65 o 18 0 2 426.30 344.63 40.61 o 20 0 2 66.93 83.89 35.05 o -23 1 2 278.90 268.02 24.24 o -21 1 2 135.01 163.13 31.69 o -19 1 2 1119.09 1116.45 26.34 o -17 1 2 361.53 403.34 24.47 o -15 1 2 1261.54 1319.20 26.22 o -13 1 2 259.27 282.29 19.81 o -11 1 2 1711.09 1696.76 27.54 o -9 1 2 11596.54 11973.97 200.21 o -7 1 2 2553.67 2582.95 58.54 o -5 1 2 19255.77 19715.44 610.37 o 1 1 2 5944.92 5397.31 62.31 o 3 1 2 4782.78 4236.51 74.88 o 5 1 2 734.51 720.30 22.19 o 7 1 2 2632.48 2597.13 53.67 o 9 1 2 439.53 445.56 21.57 o 11 1 2 3925.03 4140.27 59.54 o 13 1 2 3506.91 3390.94 92.90 o 15 1 2 1656.09 1658.15 28.64 o 17 1 2 594.51 547.45 24.48 o 19 1 2 220.04 243.16 43.21 o -22 2 2 381.02 330.36 52.39 o -20 2 2 747.68 740.54 31.06 o -18 2 2 689.27 732.13 25.68 o -16 2 2 1181.25 1110.83 32.60 o -14 2 2 266.14 234.30 25.49 o -12 2 2 4637.57 4913.51 105.64 o -10 2 2 1009.26 946.12 38.31 o -8 2 2 3880.74 3770.00 41.17 o -6 2 2 19972.92 19296.49 171.02 o -4 2 2 24638.40 23767.09 151.93 o -2 2 2 8022.10 6966.67 115.68 o 0 2 2 34464.86 35989.76 1123.06 o 2 2 2 25097.84 24724.35 420.56 o 4 2 2 2801.17 2905.05 35.05 o 6 2 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