#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/78/2207822.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207822_Fobs loop_ _publ_author_name 'Xiang, Jing' 'Yin, Ye-Gao' 'Huang, Xiao-Chun' _publ_section_title ; Diammine(pyridine-2,6-dicarboxylato)copper(II) ; _journal_coeditor_code LH6539 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m4 _journal_page_last m6 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 76.927 _cell_angle_beta 86.987 _cell_angle_gamma 86.618 _cell_length_a 4.8654 _cell_length_b 9.1161 _cell_length_c 10.0916 _exptl_crystal_F_000 255.00 _reflns_d_resolution_high 0.7630 _[local]_cod_data_source_file lh6539Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 0615am in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 162.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7.70 5.08 0.57 o 2 0 0 3.60 4.99 1.31 o 3 0 0 522.48 586.45 12.23 o 4 0 0 169.02 163.97 7.40 o 5 0 0 158.81 169.59 8.07 o 6 0 0 126.14 119.76 7.63 o -6 1 0 25.78 31.08 4.53 o -5 1 0 155.53 155.20 7.88 o -4 1 0 836.25 946.85 28.55 o -3 1 0 1.04 1.29 0.84 o -2 1 0 68.56 118.15 3.12 o -1 1 0 382.72 385.74 10.85 o 0 1 0 1972.86 2228.48 42.27 o 1 1 0 2679.02 2681.77 71.65 o 2 1 0 30.80 20.43 1.14 o 3 1 0 2507.79 2722.45 52.08 o 4 1 0 18.98 24.62 3.02 o 5 1 0 249.53 254.76 10.53 o 6 1 0 144.17 151.17 8.62 o -6 2 0 20.02 16.99 3.99 o -5 2 0 45.41 54.48 4.80 o -4 2 0 1327.46 1404.65 40.76 o -3 2 0 18.55 14.10 1.39 o -2 2 0 1266.48 1191.30 23.29 o -1 2 0 2834.90 3074.87 58.05 o 0 2 0 8.47 10.08 0.61 o 1 2 0 345.06 278.19 5.83 o 2 2 0 121.65 146.29 4.51 o 3 2 0 515.50 567.15 11.70 o 4 2 0 155.94 149.31 6.84 o 5 2 0 6.55 6.71 2.55 o 6 2 0 52.55 55.33 5.42 o -5 3 0 10.18 10.23 2.97 o -4 3 0 348.54 341.51 8.23 o -3 3 0 94.27 91.68 6.88 o -2 3 0 1568.81 1609.14 31.19 o -1 3 0 2412.58 2665.24 50.54 o 0 3 0 156.33 131.39 3.20 o 1 3 0 3505.21 3543.91 67.14 o 2 3 0 436.86 480.59 8.13 o 3 3 0 435.02 457.32 9.70 o 4 3 0 645.07 699.81 21.50 o 5 3 0 1.75 3.24 2.35 o 6 3 0 6.89 6.69 3.27 o -5 4 0 70.24 59.21 5.08 o -4 4 0 58.32 54.74 2.64 o -3 4 0 2323.44 2274.19 44.14 o -2 4 0 128.39 130.02 3.65 o -1 4 0 926.02 963.74 18.91 o 0 4 0 328.99 301.69 6.56 o 1 4 0 538.28 533.33 10.93 o 2 4 0 49.01 46.25 1.48 o 3 4 0 16.27 18.30 2.15 o 4 4 0 780.02 837.21 24.91 o -5 5 0 172.79 190.17 9.24 o -4 5 0 0.86 1.17 1.08 o -3 5 0 344.67 345.59 8.18 o -2 5 0 345.90 295.12 18.70 o -1 5 0 387.50 356.42 7.71 o 0 5 0 5865.11 6339.97 119.90 o 1 5 0 19.73 13.64 2.07 o 2 5 0 286.97 265.29 6.32 o 3 5 0 168.75 178.96 6.10 o 4 5 0 73.90 78.06 4.83 o 5 5 0 22.67 20.08 3.19 o -5 6 0 149.21 155.25 8.32 o -4 6 0 194.18 173.91 5.37 o -3 6 0 76.83 71.93 2.96 o -2 6 0 10.66 7.40 1.20 o -1 6 0 265.57 265.11 8.94 o 0 6 0 1636.99 1526.04 64.50 o 1 6 0 454.22 458.19 9.97 o 2 6 0 375.81 365.08 11.50 o 3 6 0 258.92 257.03 7.62 o 4 6 0 0.13 0.32 2.06 o 5 6 0 106.71 101.98 6.22 o -4 7 0 524.69 519.03 16.77 o -3 7 0 18.06 19.34 2.40 o -2 7 0 420.04 436.34 14.09 o -1 7 0 29.22 35.74 2.80 o 0 7 0 302.60 296.69 16.57 o 1 7 0 185.12 157.24 4.49 o 2 7 0 27.75 27.31 1.91 o 3 7 0 156.74 164.98 10.03 o 4 7 0 2.96 1.49 2.30 o 5 7 0 69.02 68.08 5.50 o -4 8 0 290.96 272.39 10.40 o -3 8 0 2.29 0.79 1.41 o -2 8 0 550.92 528.29 16.91 o -1 8 0 519.23 555.21 17.41 o 0 8 0 10.29 9.56 1.30 o 1 8 0 490.31 463.07 10.57 o 2 8 0 138.54 125.83 4.22 o 3 8 0 436.39 440.75 10.54 o 4 8 0 20.91 25.48 3.67 o -3 9 0 123.04 126.90 6.41 o -2 9 0 96.38 93.61 5.25 o -1 9 0 412.03 426.60 14.44 o 0 9 0 38.68 40.74 3.34 o 1 9 0 157.53 158.96 4.97 o 2 9 0 23.50 25.19 2.11 o 3 9 0 0.66 1.05 1.18 o 4 9 0 225.70 249.36 10.92 o -2 10 0 71.33 67.44 4.85 o -1 10 0 312.90 292.43 11.02 o 0 10 0 49.27 50.47 3.99 o 1 10 0 1.01 2.62 1.19 o 2 10 0 122.45 121.84 4.54 o 3 10 0 0.06 0.17 2.35 o 0 11 0 219.76 201.66 8.87 o 1 11 0 0.14 0.98 1.30 o 2 11 0 138.38 155.99 9.68 o -1 -11 1 59.28 59.97 3.38 o 0 -11 1 10.65 10.33 2.43 o -3 -10 1 9.33 11.59 3.39 o -2 -10 1 4.38 4.97 1.46 o -1 -10 1 15.72 16.29 1.86 o 0 -10 1 17.36 18.82 2.75 o 1 -10 1 286.03 266.82 10.60 o 2 -10 1 204.06 198.86 8.84 o -4 -9 1 3.57 -0.15 2.67 o -3 -9 1 180.26 181.40 8.67 o -2 -9 1 133.63 133.36 5.01 o -1 -9 1 310.77 306.22 7.92 o 0 -9 1 48.49 53.68 4.05 o 1 -9 1 0.63 -0.22 1.26 o 2 -9 1 297.76 272.00 10.57 o 3 -9 1 1.07 0.67 1.54 o -4 -8 1 9.62 13.74 3.29 o -3 -8 1 73.27 71.50 5.10 o -2 -8 1 161.91 172.73 5.21 o -1 -8 1 182.61 181.76 5.23 o 0 -8 1 417.35 397.96 9.45 o 1 -8 1 507.42 489.56 15.87 o 2 -8 1 425.03 391.19 13.37 o 3 -8 1 82.60 100.35 5.50 o 4 -8 1 30.67 35.84 3.59 o -5 -7 1 50.57 38.86 4.53 o -4 -7 1 40.25 46.06 4.38 o -3 -7 1 9.13 7.03 2.53 o -2 -7 1 265.29 273.24 6.93 o -1 -7 1 22.18 25.28 1.74 o 0 -7 1 303.24 264.74 6.61 o 1 -7 1 327.84 325.07 11.00 o 2 -7 1 18.91 20.56 2.48 o 3 -7 1 344.29 324.92 11.49 o 4 -7 1 83.35 75.09 4.66 o -5 -6 1 66.74 53.37 4.85 o -4 -6 1 99.33 92.23 5.75 o -3 -6 1 145.00 145.98 4.45 o -2 -6 1 633.61 616.12 24.93 o -1 -6 1 353.29 336.64 28.08 o 0 -6 1 208.72 190.78 4.98 o 1 -6 1 806.01 836.54 24.32 o 2 -6 1 155.30 156.74 6.44 o 3 -6 1 67.70 66.47 4.38 o 4 -6 1 360.59 324.06 8.37 o 5 -6 1 1.23 3.07 2.67 o -5 -5 1 5.12 7.40 2.70 o -4 -5 1 610.74 567.30 18.67 o -3 -5 1 41.03 38.48 1.95 o -2 -5 1 17.09 11.73 1.21 o -1 -5 1 1391.02 1479.92 28.94 o 0 -5 1 81.38 90.67 2.85 o 1 -5 1 824.63 803.41 17.78 o 2 -5 1 936.57 931.41 18.87 o 3 -5 1 838.20 838.09 17.56 o 4 -5 1 233.69 220.37 6.24 o 5 -5 1 1.51 2.20 2.45 o -4 -4 1 219.11 219.02 8.92 o -3 -4 1 605.93 619.75 10.62 o -2 -4 1 330.99 383.49 6.74 o -1 -4 1 551.22 594.27 12.15 o 0 -4 1 464.85 427.12 9.02 o 1 -4 1 495.66 425.84 12.83 o 2 -4 1 1983.33 2114.03 57.68 o 3 -4 1 21.35 22.58 2.11 o 4 -4 1 151.97 141.46 4.60 o 5 -4 1 148.20 146.71 7.88 o -5 -3 1 166.13 174.94 8.10 o -4 -3 1 52.82 51.56 3.76 o -3 -3 1 450.96 414.24 8.80 o -2 -3 1 940.27 1051.06 16.90 o -1 -3 1 1679.25 1864.79 29.04 o 0 -3 1 395.20 338.23 7.12 o 1 -3 1 351.14 425.84 12.58 o 2 -3 1 1983.53 2025.22 54.98 o 3 -3 1 297.32 275.24 9.31 o 4 -3 1 117.79 127.93 4.25 o 5 -3 1 215.25 223.48 10.10 o -6 -2 1 0.27 5.50 3.05 o -5 -2 1 305.25 290.17 11.39 o -4 -2 1 151.83 139.85 6.46 o -3 -2 1 96.94 86.50 2.54 o -2 -2 1 862.73 931.88 18.12 o -1 -2 1 3013.29 3480.97 57.70 o 0 -2 1 679.88 678.76 13.36 o 1 -2 1 861.07 976.19 26.85 o 2 -2 1 265.81 255.85 8.17 o 3 -2 1 1057.71 1025.97 28.90 o 4 -2 1 19.31 16.56 1.74 o 5 -2 1 218.10 225.93 10.23 o -6 -1 1 2.69 3.29 2.90 o -5 -1 1 213.57 203.12 8.96 o -4 -1 1 955.55 1019.26 30.14 o -3 -1 1 6.29 6.60 1.20 o -2 -1 1 890.96 949.12 18.43 o -1 -1 1 952.56 1062.26 20.29 o 0 -1 1 5212.07 4855.94 75.29 o 1 -1 1 2068.99 2202.17 58.84 o 2 -1 1 1074.83 1264.43 34.60 o 3 -1 1 683.67 582.08 17.09 o 4 -1 1 353.46 365.71 10.34 o 5 -1 1 106.88 111.67 6.56 o 6 -1 1 57.55 58.77 5.62 o -6 0 1 51.47 59.51 5.67 o -5 0 1 54.25 59.98 4.85 o -4 0 1 306.59 298.79 11.09 o -3 0 1 400.89 405.30 8.72 o -2 0 1 901.83 931.99 18.14 o -1 0 1 4830.19 4971.96 94.34 o 0 0 1 225.89 215.73 3.02 o 1 0 1 1105.75 1154.33 31.23 o 2 0 1 91.90 71.50 3.10 o 3 0 1 2184.17 2294.44 62.06 o 4 0 1 546.29 557.45 12.28 o 5 0 1 3.26 3.84 2.45 o 6 0 1 202.84 240.27 11.29 o -6 1 1 58.07 72.07 6.22 o -5 1 1 93.71 98.74 6.07 o -4 1 1 683.69 718.73 22.39 o -3 1 1 135.63 109.91 3.15 o -2 1 1 86.99 86.00 2.36 o -1 1 1 999.51 1089.17 20.84 o 0 1 1 2606.35 2597.87 49.06 o 1 1 1 970.13 1042.39 28.08 o 2 1 1 1102.16 982.42 18.80 o 3 1 1 115.60 93.61 5.93 o 4 1 1 520.50 555.40 12.24 o 5 1 1 8.37 3.64 2.43 o 6 1 1 33.78 48.51 5.27 o -5 2 1 156.97 146.88 7.75 o -4 2 1 227.62 236.66 9.44 o -3 2 1 1145.82 1060.42 24.89 o -2 2 1 25.67 26.49 1.28 o -1 2 1 805.09 870.04 16.86 o 0 2 1 717.39 814.82 13.11 o 1 2 1 1615.10 1742.12 33.24 o 2 2 1 2396.86 2386.91 63.89 o 4 2 1 304.57 307.53 6.11 o 5 2 1 11.43 10.13 2.87 o 6 2 1 0.44 0.67 2.80 o -5 3 1 176.84 159.14 8.12 o -4 3 1 54.55 47.25 4.04 o -3 3 1 961.24 951.90 19.23 o -2 3 1 1266.19 1327.30 25.85 o -1 3 1 1030.92 1150.42 22.25 o 0 3 1 326.63 306.98 5.14 o 1 3 1 98.08 94.27 2.80 o 2 3 1 1755.43 1870.68 50.50 o 3 3 1 714.86 721.98 20.51 o 4 3 1 64.44 62.29 2.22 o 5 3 1 152.90 178.41 8.47 o 6 3 1 87.83 98.42 7.16 o -5 4 1 234.49 223.31 10.18 o -4 4 1 602.82 583.59 19.09 o -3 4 1 181.67 176.11 4.81 o -2 4 1 983.51 1065.28 21.12 o -1 4 1 137.61 125.59 4.67 o 0 4 1 2567.41 2512.51 39.01 o 1 4 1 435.10 505.96 10.38 o 2 4 1 128.71 123.96 3.39 o 3 4 1 1586.05 1635.42 44.85 o 4 4 1 21.77 25.12 2.28 o 5 4 1 88.29 113.99 6.64 o -5 5 1 242.28 226.68 10.30 o -4 5 1 71.72 66.52 4.83 o -3 5 1 260.06 266.91 6.64 o -2 5 1 756.12 827.45 16.84 o -1 5 1 355.99 311.54 10.77 o 0 5 1 204.26 156.25 3.04 o 1 5 1 1847.37 2015.32 38.87 o 2 5 1 489.13 558.20 11.79 o 3 5 1 195.55 166.14 8.89 o 4 5 1 327.55 311.84 11.34 o 5 5 1 35.94 30.78 3.47 o -5 6 1 9.15 11.74 3.42 o -4 6 1 343.97 333.59 12.48 o -3 6 1 43.84 41.82 2.27 o -2 6 1 417.84 442.73 13.72 o -1 6 1 695.61 657.94 13.47 o 0 6 1 163.48 205.74 5.11 o 1 6 1 670.89 713.44 14.72 o 2 6 1 3.48 2.65 0.95 o 3 6 1 57.21 58.94 2.62 o 4 6 1 171.95 159.12 7.40 o 5 6 1 43.23 42.84 4.06 o -4 7 1 66.37 61.64 4.71 o -3 7 1 518.06 502.19 15.80 o -2 7 1 319.35 329.82 11.14 o -1 7 1 643.79 626.88 18.90 o 0 7 1 410.13 441.55 16.58 o 1 7 1 527.72 536.71 11.65 o 2 7 1 527.63 556.73 12.21 o 3 7 1 0.18 -0.08 0.93 o 4 7 1 223.56 210.13 8.92 o -3 8 1 339.63 335.05 11.79 o -2 8 1 95.04 86.43 4.56 o -1 8 1 39.89 44.48 3.22 o 0 8 1 417.86 409.52 13.37 o 1 8 1 204.98 198.07 5.47 o 2 8 1 559.18 594.03 13.16 o 3 8 1 62.24 64.11 3.95 o -3 9 1 143.49 138.83 6.51 o -2 9 1 697.46 694.51 21.74 o -1 9 1 38.31 29.02 2.92 o 0 9 1 25.97 28.73 2.90 o 1 9 1 11.13 13.77 1.62 o 2 9 1 62.52 65.92 4.66 o 3 9 1 351.74 371.54 9.42 o -3 10 1 8.34 7.45 2.15 o -2 10 1 309.07 263.25 10.23 o -1 10 1 17.42 15.68 2.70 o 0 10 1 116.40 118.30 6.07 o 1 10 1 130.30 133.84 7.48 o 2 10 1 212.83 203.48 8.79 o 3 10 1 28.25 33.75 3.47 o -1 11 1 53.61 57.33 4.63 o 0 11 1 1.52 4.73 1.91 o 1 11 1 255.97 261.99 10.75 o 2 11 1 12.66 20.18 3.07 o -2 -10 2 65.55 69.03 3.43 o -1 -10 2 6.08 8.05 1.52 o 0 -10 2 239.57 225.24 9.19 o 1 -10 2 85.68 94.65 5.55 o -3 -9 2 23.79 22.49 3.67 o -2 -9 2 143.48 140.67 4.97 o -1 -9 2 1.71 3.23 1.15 o 0 -9 2 143.43 141.55 5.98 o 1 -9 2 263.23 264.94 10.30 o 2 -9 2 1.45 2.90 1.81 o 3 -9 2 454.37 431.16 15.38 o -4 -8 2 21.34 28.31 4.01 o -3 -8 2 28.73 27.59 3.74 o -2 -8 2 72.51 79.42 5.35 o -1 -8 2 250.58 244.99 6.52 o 0 -8 2 24.53 30.94 4.33 o 1 -8 2 126.18 126.65 5.94 o 2 -8 2 12.19 13.89 2.43 o 3 -8 2 359.93 344.26 12.61 o 4 -8 2 270.21 259.91 10.53 o -4 -7 2 20.87 29.07 3.89 o -3 -7 2 179.25 177.57 8.15 o -2 -7 2 226.22 239.47 6.30 o -1 -7 2 634.91 609.09 13.19 o 0 -7 2 247.41 240.00 6.25 o 1 -7 2 18.23 23.77 2.58 o 2 -7 2 78.56 72.71 4.33 o 3 -7 2 23.93 26.25 3.05 o 4 -7 2 192.79 194.55 8.47 o -5 -6 2 24.73 27.84 4.14 o -4 -6 2 11.70 11.42 2.75 o -3 -6 2 180.59 171.10 7.73 o -2 -6 2 4.14 4.61 1.08 o -1 -6 2 1157.56 1124.69 22.61 o 0 -6 2 288.26 277.50 8.75 o 1 -6 2 505.37 520.76 16.12 o 2 -6 2 357.16 355.63 12.04 o 3 -6 2 35.79 33.59 2.23 o 4 -6 2 319.82 316.28 8.35 o 5 -6 2 93.72 92.45 6.46 o -5 -5 2 171.86 172.76 8.72 o -4 -5 2 2.92 0.37 1.96 o -3 -5 2 149.24 159.02 7.28 o -2 -5 2 276.21 264.00 8.06 o -1 -5 2 22.40 33.50 1.68 o 0 -5 2 1032.20 1153.50 23.01 o 1 -5 2 185.42 171.70 6.54 o 2 -5 2 1465.70 1525.78 42.74 o 3 -5 2 1.71 1.26 1.09 o 4 -5 2 78.81 73.50 3.39 o 5 -5 2 115.29 122.96 7.28 o -5 -4 2 78.14 71.52 5.32 o -4 -4 2 206.26 187.74 8.40 o -3 -4 2 151.35 143.91 6.71 o 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1.45 o -1 -1 2 26252.70 18183.99 342.78 o 0 -1 2 103.55 91.96 1.83 o 1 -1 2 265.82 242.13 7.50 o 2 -1 2 1571.81 1883.17 51.16 o 3 -1 2 87.85 91.33 4.36 o 4 -1 2 398.98 399.44 13.00 o 5 -1 2 440.50 422.84 15.68 o 6 -1 2 143.89 146.86 8.87 o -6 0 2 66.10 60.13 5.75 o -5 0 2 282.23 300.45 11.86 o -4 0 2 10.40 12.78 2.58 o -3 0 2 196.79 200.99 7.63 o -2 0 2 1.33 0.30 0.37 o -1 0 2 246.78 308.60 9.19 o 0 0 2 2993.22 2806.89 43.38 o 1 0 2 86.05 87.22 3.37 o 2 0 2 3199.94 3524.77 94.23 o 3 0 2 8.42 3.71 1.39 o 4 0 2 544.20 546.59 16.87 o 5 0 2 225.03 228.16 10.15 o 6 0 2 9.09 9.41 3.67 o -6 1 2 9.01 6.44 3.34 o -5 1 2 307.81 324.50 12.68 o -4 1 2 20.01 22.31 3.10 o -3 1 2 1435.92 1497.18 42.22 o -2 1 2 1954.57 2006.42 38.25 o -1 1 2 261.90 276.36 5.69 o 0 1 2 1425.50 1423.68 52.19 o 1 1 2 114.60 119.90 2.80 o 2 1 2 308.12 278.45 6.11 o 3 1 2 976.06 993.09 19.47 o 4 1 2 0.38 -0.59 1.51 o 5 1 2 38.42 48.61 4.51 o 6 1 2 10.01 12.90 3.89 o -5 2 2 51.16 59.63 5.10 o -4 2 2 220.72 211.89 8.87 o -3 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