#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:18:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180999 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/79/2207916.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207916_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Lensink, Cornelis' 'Falshaw, Andrew' 'Mee, Simon P.H.' _publ_section_title ; Non-classical hydrogen bonding involving bound diazides in an inositol derivative ; _journal_coeditor_code TK6297 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o303 _journal_page_last o305 _journal_volume 62 _journal_year 2006 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.0059 _cell_length_b 15.3237 _cell_length_c 25.4241 _exptl_crystal_F_000 1377.60 _reflns_d_resolution_high 0.7986 _cod_data_source_file tk6297Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mtss in P2(1)2(1)2(1) Final Labels 29/4/05 ~ 0.6 DCM' _shelx_refln_list_code 4 _shelx_f_calc_maximum 373.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 139180.34 140163.95 867.88 o 4 0 0 3390.68 3264.96 139.44 o 6 0 0 313.84 427.18 169.10 o 8 0 0 124.10 -94.70 205.00 o 10 0 0 134.31 -291.90 291.90 o 1 1 0 1207.10 1151.45 55.67 o 2 1 0 0.12 -28.02 37.51 o 3 1 0 1928.52 2051.86 84.80 o 4 1 0 11.75 105.65 78.31 o 5 1 0 1886.40 1936.34 114.41 o 6 1 0 77.28 109.91 187.57 o 7 1 0 88.45 112.76 133.69 o 8 1 0 209.19 -38.57 145.35 o 9 1 0 11.02 -116.92 172.58 o 10 1 0 153.93 -159.34 201.23 o 11 1 0 6.63 -321.55 321.55 o 0 2 0 1516.58 1592.68 65.04 o 1 2 0 412.41 520.82 32.14 o 2 2 0 20071.69 19116.11 259.79 o 3 2 0 3390.93 3360.69 92.47 o 4 2 0 1259.47 1216.45 91.56 o 5 2 0 0.62 -25.50 65.65 o 6 2 0 110.65 81.19 117.91 o 7 2 0 104.06 250.75 132.96 o 8 2 0 41.58 -92.63 143.89 o 9 2 0 47.21 -143.97 178.26 o 10 2 0 3.53 -279.93 279.93 o 11 2 0 3.23 -352.25 352.25 o 1 3 0 27672.00 25992.02 298.70 o 2 3 0 27733.00 27745.21 425.05 o 3 3 0 1005.76 1081.85 51.46 o 4 3 0 122.34 139.26 46.66 o 5 3 0 5.04 101.44 91.30 o 6 3 0 443.17 420.92 123.42 o 7 3 0 92.18 100.65 138.01 o 8 3 0 89.88 -155.33 155.87 o 9 3 0 18.02 -270.56 270.56 o 10 3 0 72.27 -292.42 292.42 o 11 3 0 1.20 -362.14 362.14 o 0 4 0 979.25 890.26 98.86 o 1 4 0 12128.40 11597.47 223.41 o 2 4 0 608.54 638.76 40.45 o 3 4 0 131.94 127.98 39.11 o 4 4 0 1600.43 1559.40 65.53 o 5 4 0 46.92 44.16 69.31 o 6 4 0 56.65 69.60 83.12 o 7 4 0 0.99 104.80 110.70 o 8 4 0 0.36 -250.27 250.27 o 9 4 0 4.77 -195.64 285.65 o 10 4 0 11.65 -284.61 284.61 o 1 5 0 808.23 831.47 51.99 o 2 5 0 84.69 87.94 41.16 o 3 5 0 75.38 97.34 52.27 o 4 5 0 129.67 98.23 47.12 o 5 5 0 0.12 -33.01 63.27 o 6 5 0 41.40 -31.03 107.55 o 7 5 0 0.91 -45.20 123.11 o 8 5 0 94.57 -79.97 161.30 o 9 5 0 15.21 -134.38 258.86 o 10 5 0 16.40 -316.87 316.87 o 0 6 0 690.12 723.13 79.12 o 1 6 0 3.33 13.42 46.81 o 2 6 0 1848.02 1807.70 66.17 o 3 6 0 2711.16 2744.70 72.16 o 4 6 0 600.17 486.63 68.21 o 5 6 0 682.13 609.49 92.07 o 6 6 0 22.34 -45.15 129.07 o 7 6 0 1.45 -38.53 204.48 o 8 6 0 3.89 4.78 150.14 o 9 6 0 0.94 -158.89 266.66 o 10 6 0 30.71 -138.25 174.35 o 1 7 0 45.07 50.37 51.47 o 2 7 0 429.32 528.74 57.17 o 3 7 0 2007.46 2137.06 74.81 o 4 7 0 22.39 -24.67 57.13 o 5 7 0 433.72 558.40 99.71 o 6 7 0 1.46 65.56 138.95 o 7 7 0 5.21 -87.39 144.66 o 8 7 0 102.75 -96.25 215.67 o 9 7 0 2.05 -34.92 174.84 o 10 7 0 25.22 -44.23 235.70 o 0 8 0 13.35 -54.67 87.28 o 1 8 0 230.73 257.41 57.50 o 2 8 0 49.75 124.29 67.12 o 3 8 0 419.78 542.03 68.55 o 4 8 0 22.07 128.55 70.62 o 5 8 0 4.16 -2.69 82.94 o 6 8 0 1.94 210.80 144.86 o 7 8 0 163.55 129.88 154.80 o 8 8 0 73.24 160.37 165.75 o 9 8 0 36.16 -208.65 208.65 o 10 8 0 40.75 -95.74 271.60 o 1 9 0 64.73 -64.78 64.78 o 2 9 0 58.28 -9.71 71.50 o 3 9 0 3.20 12.80 68.20 o 4 9 0 252.11 266.34 80.17 o 5 9 0 391.52 469.18 95.80 o 6 9 0 192.41 16.68 119.70 o 7 9 0 176.06 -83.58 166.97 o 8 9 0 1.73 -177.63 177.63 o 9 9 0 14.95 126.44 270.04 o 0 10 0 562.70 326.62 106.86 o 1 10 0 16.88 53.13 77.12 o 2 10 0 100.16 171.80 85.27 o 3 10 0 7.97 -45.37 87.86 o 4 10 0 20.36 130.46 91.96 o 5 10 0 9.00 -41.75 100.38 o 6 10 0 133.54 73.74 131.28 o 7 10 0 0.28 -86.48 147.14 o 8 10 0 61.70 -111.35 245.07 o 9 10 0 19.26 -40.58 236.22 o 1 11 0 627.83 609.25 111.47 o 2 11 0 8.83 10.56 106.75 o 3 11 0 1245.96 1243.95 107.68 o 4 11 0 26.25 221.77 121.92 o 5 11 0 221.02 285.96 125.95 o 6 11 0 7.98 1.51 140.84 o 7 11 0 53.45 98.71 204.74 o 8 11 0 40.71 -20.14 166.35 o 9 11 0 1.55 -55.67 270.56 o 0 12 0 281.88 289.88 141.27 o 1 12 0 3.07 120.09 111.66 o 2 12 0 10.90 -49.19 117.50 o 3 12 0 37.80 71.58 121.39 o 4 12 0 123.31 253.11 134.77 o 5 12 0 109.83 162.54 136.75 o 6 12 0 29.87 69.38 215.15 o 7 12 0 52.23 142.83 188.70 o 8 12 0 36.04 132.25 190.76 o 1 13 0 47.06 54.11 120.88 o 2 13 0 20.58 107.57 129.14 o 3 13 0 164.28 126.80 143.20 o 4 13 0 24.95 -125.90 168.32 o 5 13 0 157.05 157.31 159.47 o 6 13 0 0.30 49.29 179.69 o 7 13 0 0.00 62.32 191.11 o 8 13 0 8.15 84.74 205.00 o 0 14 0 232.90 218.53 259.12 o 1 14 0 1.78 -142.18 142.18 o 2 14 0 255.72 74.08 139.74 o 3 14 0 32.48 22.74 154.28 o 4 14 0 16.63 5.71 201.20 o 5 14 0 19.72 9.67 193.13 o 6 14 0 5.03 125.92 259.64 o 7 14 0 0.00 28.35 212.64 o 1 15 0 3.07 6.31 198.49 o 2 15 0 47.60 25.96 147.13 o 3 15 0 19.59 -25.83 165.19 o 4 15 0 19.34 -53.06 203.47 o 5 15 0 0.03 -58.80 287.21 o 6 15 0 14.02 166.50 318.43 o 7 15 0 0.14 45.79 344.45 o 0 16 0 85.02 399.08 314.79 o 1 16 0 94.65 46.70 216.31 o 2 16 0 5.54 101.43 182.14 o 3 16 0 79.80 36.82 174.40 o 4 16 0 0.02 92.82 216.30 o 5 16 0 9.27 54.11 313.23 o 6 16 0 1.52 -319.99 319.99 o 1 17 0 5.86 158.06 254.41 o 2 17 0 6.40 228.28 247.29 o 3 17 0 0.80 -148.84 233.41 o 4 17 0 3.49 -42.15 305.94 o 5 17 0 3.95 0.52 331.96 o 0 18 0 87.65 236.22 341.33 o 1 18 0 0.13 10.10 250.78 o 2 18 0 48.14 178.47 370.98 o 1 0 1 10.82 1.82 26.05 o 2 0 1 1618.81 1997.62 111.35 o 3 0 1 144.11 120.79 67.64 o 4 0 1 1131.01 1239.07 104.59 o 5 0 1 268.06 427.79 94.50 o 6 0 1 187.94 118.57 102.15 o 7 0 1 18.99 -131.66 131.66 o 8 0 1 306.03 300.15 158.38 o 9 0 1 25.15 31.58 169.63 o 10 0 1 108.60 -181.50 199.20 o 11 0 1 3.29 -330.40 330.40 o 1 1 1 3764.11 3368.69 34.68 o 2 1 1 38685.53 38938.61 357.93 o 3 1 1 7214.40 7475.06 99.88 o 4 1 1 3284.17 3333.87 79.15 o 5 1 1 1503.65 1644.12 80.65 o 6 1 1 407.92 483.82 76.47 o 7 1 1 28.80 -94.94 94.94 o 8 1 1 81.60 -52.79 107.78 o 9 1 1 11.31 -115.80 115.80 o 10 1 1 49.42 -96.86 167.98 o 11 1 1 12.67 -178.99 329.36 o 0 2 1 33.86 64.10 31.58 o 1 2 1 2658.68 2636.88 32.53 o 2 2 1 859.55 919.11 34.96 o 3 2 1 105.85 73.64 38.29 o 4 2 1 672.63 699.35 43.24 o 5 2 1 1712.41 1736.83 66.81 o 6 2 1 66.53 105.04 74.36 o 7 2 1 279.73 383.49 98.52 o 8 2 1 2.14 -25.51 107.39 o 9 2 1 29.25 -126.62 126.62 o 10 2 1 2.65 -202.65 202.65 o 11 2 1 17.11 -327.28 327.28 o 0 3 1 1280.65 1140.75 68.02 o 1 3 1 7063.79 6208.64 107.00 o 2 3 1 4507.61 4445.16 86.11 o 3 3 1 3040.44 3068.04 44.94 o 4 3 1 701.14 695.28 39.62 o 5 3 1 229.38 194.41 49.94 o 6 3 1 20.80 19.07 89.14 o 7 3 1 1.34 -44.43 97.38 o 8 3 1 81.06 -129.12 129.12 o 9 3 1 34.51 -189.21 189.21 o 10 3 1 0.89 -222.95 222.95 o 11 3 1 24.91 -338.72 338.72 o 0 4 1 6077.15 5816.19 174.73 o 1 4 1 1930.21 2040.26 44.22 o 2 4 1 379.06 349.86 27.35 o 3 4 1 2385.80 2418.82 53.21 o 4 4 1 578.39 555.99 40.81 o 5 4 1 160.94 180.24 43.45 o 6 4 1 655.90 663.19 61.27 o 7 4 1 14.57 54.03 157.19 o 8 4 1 276.06 -82.10 172.68 o 9 4 1 31.08 -25.80 196.30 o 10 4 1 56.26 -226.53 226.53 o 11 4 1 0.95 -368.38 368.38 o 0 5 1 1417.66 1435.38 51.58 o 1 5 1 146.14 190.59 35.83 o 2 5 1 2030.23 1994.73 41.20 o 3 5 1 1693.13 1653.70 44.03 o 4 5 1 43.35 82.07 36.03 o 5 5 1 125.13 116.64 48.57 o 6 5 1 8.61 -13.34 80.31 o 7 5 1 18.03 -87.24 87.24 o 8 5 1 38.83 -97.56 97.56 o 9 5 1 10.59 36.32 98.33 o 10 5 1 7.81 -125.77 125.77 o 0 6 1 814.61 811.45 69.39 o 1 6 1 152.05 159.87 34.93 o 2 6 1 48.70 18.85 33.17 o 3 6 1 46.67 57.78 36.62 o 4 6 1 34.86 15.31 43.57 o 5 6 1 371.42 427.61 68.38 o 6 6 1 129.63 98.47 85.99 o 7 6 1 131.08 136.55 92.49 o 8 6 1 45.34 -48.01 147.20 o 9 6 1 7.49 -115.89 115.89 o 10 6 1 19.22 -60.05 136.05 o 0 7 1 337.75 357.01 60.48 o 1 7 1 621.76 653.05 38.06 o 2 7 1 407.03 491.65 43.27 o 3 7 1 8.94 -39.51 39.51 o 4 7 1 577.44 618.87 47.81 o 5 7 1 666.75 706.28 77.49 o 6 7 1 188.49 218.05 85.35 o 7 7 1 3.43 -66.42 104.37 o 8 7 1 67.75 -79.91 112.79 o 9 7 1 37.98 -65.48 135.14 o 10 7 1 24.33 -141.58 141.58 o 0 8 1 23.32 -63.12 63.12 o 1 8 1 261.38 306.89 43.82 o 2 8 1 753.83 747.35 48.86 o 3 8 1 117.98 98.82 45.97 o 4 8 1 91.41 113.99 51.46 o 5 8 1 253.34 179.90 58.68 o 6 8 1 70.53 132.88 93.39 o 7 8 1 54.27 -2.83 109.25 o 8 8 1 33.92 15.78 124.27 o 9 8 1 13.14 90.82 147.79 o 10 8 1 11.11 -153.57 153.57 o 0 9 1 31.51 51.84 69.59 o 1 9 1 10.24 -25.04 46.60 o 2 9 1 74.29 92.07 48.64 o 3 9 1 0.43 42.62 51.97 o 4 9 1 331.52 307.78 56.97 o 5 9 1 29.28 62.05 69.36 o 6 9 1 24.47 14.26 76.94 o 7 9 1 41.36 -135.71 135.71 o 8 9 1 24.87 -136.19 136.19 o 9 9 1 14.34 -127.41 147.54 o 0 10 1 13.45 55.00 74.92 o 1 10 1 466.68 432.09 57.08 o 2 10 1 310.72 341.90 61.54 o 3 10 1 217.31 133.66 59.40 o 4 10 1 309.28 382.52 64.85 o 5 10 1 214.01 145.54 74.78 o 6 10 1 97.74 114.29 84.61 o 7 10 1 149.21 42.61 94.90 o 8 10 1 12.28 -18.67 210.80 o 9 10 1 17.25 87.62 184.75 o 0 11 1 197.70 267.00 86.33 o 1 11 1 369.66 373.09 74.29 o 2 11 1 148.47 116.58 74.82 o 3 11 1 41.68 56.62 70.44 o 4 11 1 32.81 75.16 77.10 o 5 11 1 188.90 273.04 83.34 o 6 11 1 1.20 -50.32 96.58 o 7 11 1 19.06 -54.18 110.00 o 8 11 1 10.06 -52.85 126.03 o 9 11 1 3.38 85.63 187.43 o 0 12 1 9.54 -65.00 93.67 o 1 12 1 301.96 283.99 81.41 o 2 12 1 19.38 0.92 85.72 o 3 12 1 201.07 178.94 91.45 o 4 12 1 4.14 129.30 93.72 o 5 12 1 132.22 239.20 104.40 o 6 12 1 5.93 -67.01 105.17 o 7 12 1 34.11 -10.76 122.75 o 8 12 1 2.42 -31.29 128.17 o 0 13 1 596.69 299.00 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51.33 164.71 o 4 17 1 0.38 34.52 194.33 o 5 17 1 0.70 -14.40 197.50 o 0 18 1 8.10 394.92 382.43 o 1 18 1 3.32 131.99 278.19 o 2 18 1 0.58 58.08 274.23 o 3 18 1 4.23 75.45 378.79 o 0 19 1 0.85 92.10 376.19 o 1 19 1 9.55 293.98 425.62 o 2 0 2 82.59 139.77 46.53 o 3 0 2 1.93 94.63 66.02 o 4 0 2 300.17 456.39 79.29 o 5 0 2 1216.75 1359.39 114.59 o 6 0 2 188.02 234.76 110.65 o 7 0 2 369.44 312.06 131.78 o 8 0 2 5.64 -144.05 212.03 o 9 0 2 5.90 -144.26 172.03 o 10 0 2 0.81 -292.94 292.94 o 11 0 2 0.05 -347.05 347.05 o 0 1 2 57.92 65.56 33.30 o 1 1 2 508.52 492.22 29.33 o 2 1 2 16335.41 15223.42 116.77 o 3 1 2 3838.07 3941.72 102.54 o 4 1 2 532.57 546.46 58.55 o 5 1 2 645.08 761.32 71.87 o 6 1 2 144.81 133.83 76.75 o 7 1 2 35.41 -10.38 92.07 o 8 1 2 68.82 91.06 108.59 o 9 1 2 33.65 -122.58 122.58 o 10 1 2 18.74 -203.78 203.78 o 11 1 2 11.78 -242.99 353.81 o 0 2 2 1195.52 1153.19 48.83 o 1 2 2 245.99 248.38 26.61 o 2 2 2 5778.57 5292.13 51.92 o 3 2 2 488.17 581.85 37.14 o 4 2 2 2090.10 2270.18 54.82 o 5 2 2 1513.84 1459.80 70.23 o 6 2 2 21.34 -3.18 75.12 o 7 2 2 128.42 181.78 92.33 o 8 2 2 0.97 -107.88 107.88 o 9 2 2 19.17 -146.07 146.07 o 10 2 2 1.88 -308.55 308.55 o 11 2 2 21.80 -359.54 359.54 o 0 3 2 2774.07 2423.92 390.75 o 1 3 2 17567.45 18237.74 253.93 o 2 3 2 4852.84 4781.55 49.38 o 3 3 2 1715.17 1723.56 46.95 o 4 3 2 1248.76 1345.12 45.69 o 5 3 2 130.20 96.13 42.71 o 6 3 2 233.90 138.32 77.97 o 7 3 2 9.45 105.97 91.39 o 8 3 2 64.43 -86.70 133.60 o 9 3 2 25.84 -126.45 187.23 o 10 3 2 11.84 -308.55 324.15 o 11 3 2 79.28 -188.35 365.78 o 0 4 2 19.84 64.67 43.57 o 1 4 2 1194.95 1099.66 41.27 o 2 4 2 3117.41 2968.95 41.85 o 3 4 2 1041.21 1130.85 40.93 o 4 4 2 19.14 15.35 37.00 o 5 4 2 174.92 129.73 42.57 o 6 4 2 78.85 34.56 58.08 o 7 4 2 44.46 -3.91 88.99 o 8 4 2 65.08 -27.67 172.78 o 9 4 2 4.83 78.05 270.56 o 10 4 2 26.44 -157.65 326.76 o 0 5 2 3.71 -36.33 36.33 o 1 5 2 2014.02 2166.18 47.68 o 2 5 2 952.23 950.67 35.55 o 3 5 2 1653.80 1622.02 40.66 o 4 5 2 248.11 263.38 40.84 o 5 5 2 886.18 954.27 48.06 o 6 5 2 64.50 174.56 76.96 o 7 5 2 241.58 189.94 85.06 o 8 5 2 116.30 77.13 96.76 o 9 5 2 15.96 -88.10 122.31 o 10 5 2 19.66 -39.60 178.33 o 0 6 2 1112.91 1132.89 50.09 o 1 6 2 966.75 966.30 38.31 o 2 6 2 472.86 496.47 37.46 o 3 6 2 269.44 202.51 39.98 o 4 6 2 116.00 132.85 45.21 o 5 6 2 93.82 62.62 62.11 o 6 6 2 144.76 107.20 86.69 o 7 6 2 35.62 75.21 98.30 o 8 6 2 97.25 144.01 154.01 o 9 6 2 15.38 -121.14 121.14 o 10 6 2 49.33 -99.96 133.34 o 0 7 2 3708.83 3802.54 69.77 o 1 7 2 914.13 997.13 38.77 o 2 7 2 2651.87 2650.35 54.81 o 3 7 2 749.07 729.38 49.77 o 4 7 2 1015.87 1166.93 54.62 o 5 7 2 91.86 149.11 73.82 o 6 7 2 107.68 172.33 85.17 o 7 7 2 67.27 -102.31 108.53 o 8 7 2 65.69 -108.03 126.98 o 9 7 2 1.06 -10.32 133.98 o 10 7 2 29.47 -11.22 136.49 o 0 8 2 170.28 99.77 63.42 o 1 8 2 103.67 135.33 40.98 o 2 8 2 210.41 304.51 48.61 o 3 8 2 93.10 65.02 49.57 o 4 8 2 232.82 324.13 55.40 o 5 8 2 134.68 164.03 66.48 o 6 8 2 229.61 263.03 98.46 o 7 8 2 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4 9 25 11.96 10.01 143.61 o 0 10 25 11.84 61.24 212.73 o 1 10 25 6.74 106.30 152.74 o 2 10 25 6.15 45.76 156.49 o 3 10 25 2.99 15.09 170.25 o 0 11 25 0.65 26.96 232.88 o 1 11 25 43.50 6.87 167.49 o 2 11 25 10.35 -2.96 166.73 o 0 0 26 253.96 327.80 279.93 o 1 0 26 9.24 -42.12 204.37 o 2 0 26 3.93 -122.30 209.28 o 3 0 26 43.63 168.54 209.40 o 4 0 26 0.46 89.16 177.93 o 5 0 26 9.35 -34.70 214.51 o 6 0 26 17.64 -32.83 304.90 o 0 1 26 2.34 -27.70 205.60 o 1 1 26 28.73 71.66 146.15 o 2 1 26 72.25 133.58 145.36 o 3 1 26 55.56 151.41 151.02 o 4 1 26 24.85 70.75 122.98 o 5 1 26 51.07 59.83 153.88 o 6 1 26 16.00 97.34 157.29 o 0 2 26 83.00 214.92 198.34 o 1 2 26 82.34 101.60 140.49 o 2 2 26 27.80 105.30 149.43 o 3 2 26 48.55 22.88 148.91 o 4 2 26 48.48 192.79 140.22 o 5 2 26 5.47 103.12 137.88 o 6 2 26 7.34 82.44 158.42 o 0 3 26 72.87 -66.87 203.82 o 1 3 26 13.55 4.63 144.11 o 2 3 26 64.97 90.37 144.70 o 3 3 26 0.21 -6.45 149.67 o 4 3 26 34.97 -80.92 135.07 o 5 3 26 11.67 120.97 143.41 o 6 3 26 19.54 22.45 187.38 o 0 4 26 8.19 -107.08 198.61 o 1 4 26 8.01 28.34 146.23 o 2 4 26 13.77 139.84 150.79 o 3 4 26 36.07 72.95 151.29 o 4 4 26 8.11 72.35 154.91 o 5 4 26 52.73 -122.71 157.14 o 6 4 26 7.37 -28.29 205.21 o 0 5 26 8.90 19.71 206.82 o 1 5 26 21.13 -86.01 145.74 o 2 5 26 18.15 -38.85 146.81 o 3 5 26 29.89 -22.91 152.96 o 4 5 26 3.53 -151.69 151.69 o 5 5 26 4.04 63.44 178.18 o 0 6 26 2.37 -95.13 206.19 o 1 6 26 12.83 14.14 145.96 o 2 6 26 0.89 69.41 151.66 o 3 6 26 7.97 -86.10 157.76 o 4 6 26 5.76 -5.22 154.19 o 5 6 26 16.01 245.33 281.23 o 0 7 26 7.27 79.70 220.04 o 1 7 26 10.97 -5.77 152.48 o 2 7 26 4.92 42.06 150.98 o 3 7 26 5.26 28.06 159.64 o 4 7 26 10.41 39.00 160.47 o 5 7 26 13.92 -121.58 223.16 o 0 8 26 13.25 -28.37 218.08 o 1 8 26 2.84 -124.41 149.88 o 2 8 26 2.70 -104.74 159.35 o 3 8 26 7.18 -87.12 157.86 o 4 8 26 5.78 -84.28 157.92 o 0 9 26 12.68 84.76 216.65 o 1 9 26 19.97 -32.15 158.19 o 2 9 26 0.04 27.51 160.45 o 3 9 26 4.86 65.07 167.63 o 0 10 26 0.03 137.24 270.82 o 1 10 26 7.37 17.92 154.71 o 2 10 26 3.02 -85.89 167.85 o 1 0 27 4.41 47.86 213.62 o 2 0 27 1.08 200.60 218.98 o 3 0 27 11.13 68.35 269.52 o 4 0 27 2.73 -149.05 232.08 o 5 0 27 24.58 173.48 236.22 o 0 1 27 25.10 113.53 218.36 o 1 1 27 51.23 126.07 153.17 o 2 1 27 46.06 14.25 154.59 o 3 1 27 7.77 -90.22 159.58 o 4 1 27 6.31 6.78 144.63 o 5 1 27 10.47 -6.08 166.19 o 0 2 27 9.21 -202.40 202.40 o 1 2 27 75.13 207.32 152.03 o 2 2 27 6.54 -91.70 156.37 o 3 2 27 6.96 68.74 155.62 o 4 2 27 4.63 136.65 146.46 o 5 2 27 22.34 -160.40 160.40 o 0 3 27 1.71 -190.75 214.69 o 1 3 27 4.24 28.27 154.13 o 2 3 27 7.81 11.17 156.14 o 3 3 27 14.73 106.83 161.78 o 4 3 27 25.19 116.62 146.22 o 5 3 27 12.05 48.62 188.99 o 0 4 27 22.64 -15.65 209.83 o 1 4 27 67.54 156.76 153.10 o 2 4 27 1.17 147.99 154.65 o 3 4 27 31.67 -78.88 157.14 o 4 4 27 2.41 -103.86 164.00 o 5 4 27 6.99 -3.24 239.92 o 0 5 27 0.00 27.02 248.71 o 1 5 27 3.23 67.33 152.16 o 2 5 27 3.50 83.54 157.29 o 3 5 27 30.28 -141.90 160.14 o 4 5 27 3.24 -163.11 163.11 o 5 5 27 11.97 -114.92 232.88 o 0 6 27 1.94 -97.02 209.90 o 1 6 27 5.04 56.23 152.31 o 2 6 27 6.35 -66.75 155.45 o 3 6 27 16.19 82.56 168.11 o 4 6 27 5.41 -158.72 158.72 o 0 7 27 22.39 11.63 232.08 o 1 7 27 5.95 -73.37 161.04 o 2 7 27 3.50 126.50 161.71 o 3 7 27 17.40 -86.20 167.93 o 4 7 27 2.16 -42.22 206.19 o 0 8 27 39.93 57.03 226.28 o 1 8 27 3.78 -68.45 160.57 o 2 8 27 32.80 97.60 168.36 o 3 8 27 5.81 41.98 173.38 o 0 9 27 10.24 -81.76 235.47 o 1 9 27 0.42 -47.04 166.01 o 2 9 27 15.09 37.79 169.52 o 0 10 27 12.59 207.08 314.27 o 0 0 28 0.63 -163.38 317.39 o 1 0 28 18.58 56.86 228.54 o 2 0 28 17.01 95.30 234.35 o 3 0 28 7.88 -172.73 233.09 o 4 0 28 5.51 13.64 253.01 o 5 0 28 14.19 196.48 244.48 o 0 1 28 19.62 22.31 225.11 o 1 1 28 21.88 25.12 163.38 o 2 1 28 17.96 -105.22 165.26 o 3 1 28 0.86 -29.90 172.04 o 4 1 28 9.23 21.53 179.86 o 5 1 28 4.35 144.34 174.88 o 0 2 28 0.01 29.87 215.96 o 1 2 28 7.74 22.82 159.58 o 2 2 28 14.20 97.58 162.87 o 3 2 28 11.87 -2.81 165.84 o 4 2 28 2.32 3.95 178.95 o 5 2 28 37.66 35.07 196.98 o 0 3 28 0.35 -143.51 225.92 o 1 3 28 8.94 -79.95 159.64 o 2 3 28 45.00 17.53 162.74 o 3 3 28 5.40 182.92 171.16 o 4 3 28 26.04 -196.46 196.46 o 5 3 28 5.88 -150.08 202.64 o 0 4 28 10.80 -138.27 220.29 o 1 4 28 38.51 82.70 160.89 o 2 4 28 24.33 -55.31 162.15 o 3 4 28 25.69 37.90 165.84 o 4 4 28 0.06 63.81 203.07 o 0 5 28 5.09 49.95 227.35 o 1 5 28 1.59 -65.56 162.74 o 2 5 28 4.37 -116.12 165.88 o 3 5 28 2.16 -28.52 174.42 o 4 5 28 17.83 -45.21 211.17 o 0 6 28 73.49 144.03 231.10 o 1 6 28 11.97 82.56 160.70 o 2 6 28 12.54 -68.48 163.93 o 3 6 28 8.94 -61.36 173.28 o 4 6 28 1.01 -197.64 197.64 o 0 7 28 12.64 164.97 238.25 o 1 7 28 6.14 -62.36 167.08 o 2 7 28 6.95 -25.95 172.79 o 3 7 28 8.87 -19.27 177.07 o 0 8 28 17.04 76.82 260.16 o 1 8 28 0.29 -89.09 171.67 o 2 8 28 20.85 133.04 174.65 o 1 0 29 0.10 -235.76 240.02 o 2 0 29 9.55 122.91 250.77 o 3 0 29 0.44 -53.95 250.15 o 4 0 29 0.01 15.41 267.37 o 0 1 29 0.21 142.61 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30 7.88 -1.50 191.31 o 0 2 30 8.62 73.28 258.07 o 1 2 30 10.14 -3.22 179.10 o 2 2 30 2.38 -18.95 185.93 o 3 2 30 1.47 -131.68 185.52 o 0 3 30 20.43 -51.71 249.03 o 1 3 30 8.14 57.83 181.30 o 2 3 30 0.31 118.52 184.19 o 3 3 30 0.59 -100.70 191.67 o 0 4 30 0.00 -35.18 251.56 o 1 4 30 3.95 -38.66 179.42 o 2 4 30 9.12 -45.90 179.63 o 0 5 30 33.83 -101.79 255.03 o 1 5 30 3.09 -76.77 180.25 o 2 5 30 8.06 -79.65 230.62 o 0 6 30 0.96 18.21 339.76 o 1 6 30 12.79 -214.37 341.33 o 1 0 31 3.39 104.67 269.31 o 2 0 31 10.53 61.86 285.68 o 0 1 31 10.86 96.75 262.50 o 1 1 31 14.92 -45.85 188.27 o 2 1 31 1.14 13.15 199.44 o 0 2 31 20.74 115.98 270.77 o 1 2 31 2.06 144.62 194.41 o 2 2 31 4.74 24.23 299.99 o 0 3 31 1.21 -26.28 264.12 o 1 3 31 6.03 -125.79 217.43 o