#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/79/2207964.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207964_Fobs loop_ _publ_author_name 'Wang, Dan-Hua' 'Pan, Yuan-Jiang' _publ_section_title ; Risperidone chloride 2.5-hydrate: a new crystalline form ; _journal_coeditor_code AT6075 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o768 _journal_page_last o770 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _[local]_cod_data_source_file at6075Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_calc _refln_observed_status 2 0 0 2946.32 0.28 3944.38 o 4 0 0 11075.46 0.98 10622.90 o 6 0 0 7354.78 0.90 7834.52 o 8 0 0 365.57 2.56 336.50 o 10 0 0 1173.75 0.74 1207.18 o 12 0 0 26.83 14.75 11.17 o 2 1 0 1889.64 0.23 1681.13 o 3 1 0 2161.32 0.31 2169.56 o 4 1 0 80.82 1.59 6.28 o 5 1 0 152.52 1.44 90.29 o 6 1 0 13277.95 1.39 12203.85 o 7 1 0 10.89 12.53 27.94 o 8 1 0 7.13 22.28 0.55 o 9 1 0 53.73 5.06 65.98 o 10 1 0 7.84 44.62 27.94 o 11 1 0 223.50 2.22 210.14 o 12 1 0 22.18 17.56 33.76 o 1 2 0 1180.61 0.10 1279.80 o 2 2 0 30909.16 2.89 34100.23 o 3 2 0 17171.48 1.54 16829.40 o 4 2 0 8.29 10.11 9.19 o 5 2 0 4990.01 0.58 5307.22 o 6 2 0 40.20 3.20 53.10 o 7 2 0 1223.60 0.62 1307.76 o 8 2 0 103.02 2.25 106.87 o 9 2 0 543.82 1.06 515.14 o 10 2 0 60.84 4.93 41.37 o 11 2 0 215.50 2.69 196.84 o 12 2 0 115.35 5.62 139.13 o 1 3 0 2730.06 0.26 2576.22 o 2 3 0 2261.95 0.27 2246.26 o 3 3 0 14332.88 1.25 14092.11 o 4 3 0 1066.68 0.27 1204.48 o 5 3 0 2651.22 0.48 2449.59 o 6 3 0 5973.74 0.66 6239.60 o 7 3 0 135.72 1.42 93.27 o 8 3 0 622.00 0.71 577.80 o 9 3 0 179.56 1.85 227.97 o 10 3 0 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