#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:18:50 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181000 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/80/2208067.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208067_Fobs loop_ _publ_author_name 'Chen, Xin' 'Fan, Zhi' 'Yu, Ming' 'Jing, Zuo-Liang' 'Diao, Chun-Hua' 'Deng, Qi-Liang' _publ_section_title ; 1-(Carbamoylmethyl)-5-oxopyrrolidin-3-yl acetate ; _journal_coeditor_code GH6031 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o478 _journal_page_last o479 _journal_volume 62 _journal_year 2006 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.8380 _cell_length_b 26.1844 _cell_length_c 8.4195 _exptl_crystal_F_000 1696.00 _reflns_d_resolution_high 0.7643 _cod_data_source_file gh6031Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50808H in Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 356.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 61944.99 53404.25 1670.95 o 8 0 0 18634.47 17801.88 358.40 o 12 0 0 203.21 196.16 20.98 o 16 0 0 1396.49 1281.45 68.88 o 20 0 0 6.83 -45.00 45.00 o 2 2 0 2631.96 2461.83 41.20 o 4 2 0 61614.82 49365.66 1178.18 o 6 2 0 4985.91 4807.96 62.58 o 8 2 0 3040.08 3438.23 67.15 o 10 2 0 6291.38 5855.11 87.64 o 12 2 0 674.92 684.98 59.58 o 14 2 0 196.90 171.76 18.87 o 16 2 0 60.41 82.48 21.50 o 18 2 0 270.37 335.89 41.34 o 20 2 0 19.28 17.20 35.39 o 2 4 0 23489.30 23478.09 285.16 o 4 4 0 30.65 19.48 5.44 o 6 4 0 14541.79 15035.00 210.82 o 8 4 0 1681.69 1617.64 29.56 o 10 4 0 88.21 83.98 10.67 o 12 4 0 2541.18 2571.73 47.46 o 14 4 0 882.15 945.70 38.07 o 16 4 0 697.22 634.48 30.31 o 18 4 0 2.01 3.25 24.06 o 20 4 0 208.59 171.75 38.26 o 2 6 0 94193.73 88653.87 1597.86 o 4 6 0 3197.73 3100.18 40.89 o 6 6 0 3282.65 3606.63 58.63 o 8 6 0 1179.85 1035.35 22.38 o 10 6 0 9634.62 10384.68 149.92 o 12 6 0 292.96 323.72 21.27 o 14 6 0 240.80 187.00 17.97 o 16 6 0 1077.32 1040.84 55.55 o 18 6 0 19.92 50.16 28.60 o 20 6 0 230.70 190.46 34.91 o 0 8 0 673.47 563.56 26.52 o 2 8 0 17482.54 19310.55 347.42 o 4 8 0 17648.54 18741.29 230.12 o 6 8 0 113.63 96.24 7.43 o 8 8 0 1262.33 1213.55 22.06 o 10 8 0 569.04 703.37 22.59 o 12 8 0 21.98 10.13 13.37 o 14 8 0 2751.79 2913.03 53.50 o 16 8 0 1120.99 1247.81 40.20 o 18 8 0 46.94 46.08 27.03 o 20 8 0 15.53 11.36 32.29 o 2 10 0 10406.72 10730.39 168.96 o 4 10 0 7047.63 6539.38 100.17 o 6 10 0 6716.58 6677.34 85.89 o 8 10 0 10378.75 10540.40 132.97 o 10 10 0 29.56 16.49 9.83 o 12 10 0 33.83 33.59 12.80 o 14 10 0 1937.71 2039.37 38.19 o 16 10 0 403.87 432.41 24.42 o 18 10 0 68.58 70.84 29.39 o 20 10 0 1.53 3.26 32.09 o 0 12 0 3140.18 2874.56 85.21 o 2 12 0 1997.13 2018.08 47.24 o 4 12 0 648.20 659.70 16.38 o 6 12 0 2289.87 2417.60 35.91 o 8 12 0 6.15 16.01 9.54 o 10 12 0 1724.68 1924.52 33.71 o 12 12 0 98.30 69.33 14.07 o 14 12 0 2671.26 2524.01 49.62 o 16 12 0 236.57 246.08 22.74 o 18 12 0 566.54 481.44 64.00 o 20 12 0 186.61 271.79 38.34 o 2 14 0 7999.54 8465.20 135.84 o 4 14 0 813.07 834.33 17.29 o 6 14 0 915.27 1098.13 21.68 o 8 14 0 2307.10 2478.68 54.04 o 10 14 0 1094.37 1258.62 26.68 o 12 14 0 8.06 2.51 14.47 o 14 14 0 382.81 431.03 25.68 o 16 14 0 1.39 10.55 26.42 o 18 14 0 3.21 30.74 41.06 o 20 14 0 61.22 91.93 54.12 o 0 16 0 23094.87 24178.10 624.64 o 2 16 0 11786.09 11453.01 199.93 o 4 16 0 689.91 635.88 18.37 o 6 16 0 888.46 935.66 28.84 o 8 16 0 5533.27 5621.25 87.53 o 10 16 0 1448.93 1462.70 33.85 o 12 16 0 97.48 96.51 18.45 o 14 16 0 4793.12 4900.93 94.62 o 16 16 0 152.88 141.95 30.49 o 18 16 0 24.65 46.80 51.00 o 2 18 0 3561.05 3217.79 91.99 o 4 18 0 1.05 11.79 16.43 o 6 18 0 212.21 173.18 28.62 o 8 18 0 648.87 648.61 23.22 o 10 18 0 5103.79 5588.34 102.02 o 12 18 0 1.22 -1.82 19.57 o 14 18 0 9.84 -4.00 26.61 o 16 18 0 356.11 377.32 97.03 o 18 18 0 30.77 11.52 55.32 o 0 20 0 1905.37 1808.65 68.40 o 2 20 0 401.12 445.14 24.95 o 4 20 0 813.66 733.88 31.68 o 6 20 0 637.26 701.81 28.81 o 8 20 0 194.38 161.13 23.64 o 10 20 0 336.96 334.29 28.46 o 12 20 0 690.81 721.48 44.49 o 14 20 0 341.60 356.31 55.92 o 16 20 0 0.03 38.28 57.36 o 2 22 0 100.56 122.37 24.12 o 4 22 0 789.66 801.19 45.36 o 6 22 0 1429.47 1428.21 47.09 o 8 22 0 186.23 147.50 26.12 o 10 22 0 578.72 587.37 34.29 o 12 22 0 13.79 11.96 33.53 o 14 22 0 17.66 -19.44 52.56 o 16 22 0 9.67 -5.28 59.88 o 0 24 0 15775.82 15396.24 413.43 o 2 24 0 399.46 379.66 32.28 o 4 24 0 882.81 881.17 34.20 o 6 24 0 0.18 -11.42 23.14 o 8 24 0 54.47 41.25 28.05 o 10 24 0 286.23 278.71 38.73 o 12 24 0 9.54 13.92 41.09 o 14 24 0 14.72 22.44 59.16 o 2 26 0 5.38 -9.35 26.26 o 4 26 0 86.48 54.13 27.12 o 6 26 0 2054.57 2040.17 55.70 o 8 26 0 440.00 492.20 39.94 o 10 26 0 5.44 16.31 40.94 o 12 26 0 63.97 6.60 58.92 o 14 26 0 23.54 9.00 59.88 o 0 28 0 355.18 319.70 47.52 o 2 28 0 160.40 112.00 40.26 o 4 28 0 31.44 12.09 29.08 o 6 28 0 3.26 11.61 34.88 o 8 28 0 4.18 18.14 41.37 o 10 28 0 2.31 21.65 43.10 o 12 28 0 54.96 52.80 62.64 o 2 30 0 221.70 141.48 34.78 o 4 30 0 407.55 544.12 66.90 o 6 30 0 116.30 154.19 71.04 o 8 30 0 0.25 -18.43 43.74 o 10 30 0 14.91 24.99 52.28 o 0 32 0 24.51 20.52 52.44 o 2 32 0 106.29 103.97 38.97 o 4 32 0 10.27 26.78 40.13 o 6 32 0 1.85 22.13 47.63 o 2 34 0 0.94 13.76 43.02 o 1 1 1 9348.68 8815.68 86.79 o 3 1 1 31611.42 31367.11 287.87 o 5 1 1 54135.60 52507.69 452.47 o 7 1 1 82.45 71.30 5.61 o 9 1 1 6794.77 7362.43 76.72 o 11 1 1 2383.56 2480.91 31.38 o 13 1 1 1081.81 1115.57 23.85 o 15 1 1 727.65 726.89 21.13 o 17 1 1 752.53 759.61 35.03 o 19 1 1 621.28 582.11 31.61 o 21 1 1 87.34 95.21 29.54 o 1 3 1 15823.82 15371.65 161.20 o 3 3 1 97447.43 93191.09 799.12 o 5 3 1 27705.47 27830.18 240.66 o 7 3 1 3900.21 3936.82 41.99 o 9 3 1 6843.33 7284.35 71.02 o 11 3 1 1637.00 1631.98 21.73 o 13 3 1 769.18 760.00 19.97 o 15 3 1 478.97 438.94 20.69 o 17 3 1 430.37 414.94 22.12 o 19 3 1 523.58 505.66 27.93 o 21 3 1 45.95 39.84 28.11 o 1 5 1 10855.30 10356.05 100.55 o 3 5 1 32186.13 31710.20 289.10 o 5 5 1 37994.01 38501.73 373.52 o 7 5 1 2538.14 2366.61 25.28 o 9 5 1 503.01 545.61 21.56 o 11 5 1 2723.86 2883.18 34.80 o 13 5 1 285.02 333.49 13.85 o 15 5 1 498.30 514.69 19.91 o 17 5 1 388.32 391.91 20.63 o 19 5 1 570.16 526.77 28.19 o 21 5 1 61.57 53.18 28.27 o 1 7 1 6647.99 7029.15 73.38 o 3 7 1 6252.29 6398.65 56.72 o 5 7 1 13404.76 12672.84 117.67 o 7 7 1 16118.65 15546.28 144.31 o 9 7 1 203.91 220.99 8.08 o 11 7 1 5408.22 5574.90 56.04 o 13 7 1 102.69 127.39 11.12 o 15 7 1 30.06 17.99 13.62 o 17 7 1 308.64 319.75 20.59 o 19 7 1 17.69 27.65 20.17 o 21 7 1 5.68 13.20 28.39 o 1 9 1 7660.24 7090.71 81.11 o 3 9 1 3.27 0.26 3.52 o 5 9 1 1801.20 1909.70 21.30 o 7 9 1 7885.79 7908.22 75.70 o 9 9 1 359.90 387.89 16.36 o 11 9 1 2162.66 1995.45 25.53 o 13 9 1 118.85 118.58 11.62 o 15 9 1 45.64 34.46 14.30 o 17 9 1 37.05 33.24 18.45 o 19 9 1 58.54 67.77 22.23 o 21 9 1 129.40 143.10 28.77 o 1 11 1 634.18 680.34 12.91 o 3 11 1 18998.19 19427.86 189.44 o 5 11 1 1946.37 2324.80 23.89 o 7 11 1 139.50 145.15 9.41 o 9 11 1 309.77 307.60 9.34 o 11 11 1 881.89 920.42 15.42 o 13 11 1 2700.26 2710.52 33.58 o 15 11 1 867.87 785.35 21.76 o 17 11 1 140.48 123.95 18.20 o 19 11 1 21.54 43.34 24.97 o 1 13 1 2846.21 3020.27 48.46 o 3 13 1 9915.54 10444.64 110.09 o 5 13 1 6558.13 6899.75 63.04 o 7 13 1 1026.80 1058.27 19.89 o 9 13 1 269.93 248.32 10.21 o 11 13 1 3110.07 3088.27 33.86 o 13 13 1 1411.89 1469.07 25.96 o 15 13 1 1121.12 1118.99 24.86 o 17 13 1 252.39 254.65 22.73 o 19 13 1 127.28 130.71 30.32 o 1 15 1 1038.40 1099.46 19.21 o 3 15 1 967.19 878.16 27.54 o 5 15 1 248.52 257.38 9.18 o 7 15 1 3285.59 3122.11 34.40 o 9 15 1 39.15 26.24 9.26 o 11 15 1 468.29 478.53 14.16 o 13 15 1 399.55 430.68 23.43 o 15 15 1 269.54 230.34 22.20 o 17 15 1 238.98 227.60 28.49 o 19 15 1 389.62 474.60 47.93 o 1 17 1 389.58 411.59 20.15 o 3 17 1 2183.28 2100.84 32.97 o 5 17 1 6876.34 7131.35 77.63 o 7 17 1 78.30 84.83 10.66 o 9 17 1 93.47 92.44 11.81 o 11 17 1 106.21 118.56 13.67 o 13 17 1 257.24 260.81 18.94 o 15 17 1 218.57 221.25 29.76 o 17 17 1 90.70 57.31 26.99 o 1 19 1 1497.25 1390.18 41.62 o 3 19 1 3136.13 3082.93 69.43 o 5 19 1 4560.60 4600.73 57.96 o 7 19 1 611.12 597.20 20.37 o 9 19 1 1281.98 1339.40 53.43 o 11 19 1 755.79 844.13 33.15 o 13 19 1 218.49 210.79 22.24 o 15 19 1 34.76 57.47 32.23 o 17 19 1 73.97 63.49 36.63 o 1 21 1 2045.78 2085.40 39.58 o 3 21 1 1928.80 1942.58 39.42 o 5 21 1 738.87 715.37 28.78 o 7 21 1 1123.07 1167.41 25.64 o 9 21 1 1058.19 1112.75 29.49 o 11 21 1 393.23 378.09 26.60 o 13 21 1 11.21 -5.10 25.10 o 15 21 1 206.93 249.64 48.21 o 17 21 1 199.86 162.07 52.58 o 1 23 1 1196.95 1137.90 35.94 o 3 23 1 4766.87 4634.67 72.31 o 5 23 1 947.49 885.48 23.77 o 7 23 1 1403.40 1427.18 58.34 o 9 23 1 417.64 412.66 24.44 o 11 23 1 407.16 428.09 32.08 o 13 23 1 141.04 157.29 30.28 o 15 23 1 125.90 144.82 50.95 o 1 25 1 683.54 732.83 26.17 o 3 25 1 795.25 792.72 28.55 o 5 25 1 70.08 76.69 19.78 o 7 25 1 197.02 208.68 22.73 o 9 25 1 134.75 171.64 24.03 o 11 25 1 144.78 156.01 29.29 o 13 25 1 15.26 24.70 32.11 o 1 27 1 232.09 202.42 23.14 o 3 27 1 340.53 365.33 30.59 o 5 27 1 43.65 74.33 22.72 o 7 27 1 17.43 17.89 23.73 o 9 27 1 20.18 16.74 25.57 o 11 27 1 210.02 201.82 33.93 o 13 27 1 64.96 38.80 41.65 o 1 29 1 369.19 342.93 25.96 o 3 29 1 157.23 107.57 24.71 o 5 29 1 135.00 112.14 28.09 o 7 29 1 120.03 156.84 28.84 o 9 29 1 5.73 -3.74 30.67 o 11 29 1 80.26 62.60 39.80 o 1 31 1 22.85 26.30 26.87 o 3 31 1 1.76 -0.96 27.05 o 5 31 1 186.00 184.69 27.96 o 7 31 1 183.91 178.80 32.77 o 9 31 1 80.12 68.50 42.98 o 1 33 1 52.98 43.07 30.79 o 3 33 1 163.65 173.57 29.87 o 5 33 1 17.20 53.92 34.00 o 2 0 2 127203.15 117263.34 1415.61 o 6 0 2 16025.21 15670.46 193.15 o 10 0 2 1256.69 1323.46 29.12 o 14 0 2 1858.49 1934.71 99.01 o 18 0 2 1092.89 1005.17 119.70 o 0 2 2 12474.39 12974.07 180.60 o 2 2 2 9900.20 9699.61 104.33 o 4 2 2 20933.40 20792.66 190.74 o 6 2 2 7790.12 7740.40 78.80 o 8 2 2 11041.85 10890.30 110.04 o 10 2 2 1992.54 1779.62 23.73 o 12 2 2 382.83 447.91 14.33 o 14 2 2 6329.33 6118.35 73.82 o 16 2 2 42.18 21.91 14.83 o 18 2 2 12.04 4.48 18.71 o 20 2 2 130.73 131.10 26.45 o 2 4 2 3479.41 3730.28 36.20 o 4 4 2 13060.21 13496.96 117.76 o 6 4 2 4615.00 4878.57 44.91 o 8 4 2 3421.26 3433.24 33.37 o 10 4 2 10417.31 10358.40 99.52 o 12 4 2 698.66 789.01 17.63 o 14 4 2 79.42 89.00 13.29 o 16 4 2 1162.27 1162.32 34.23 o 18 4 2 384.15 367.11 24.25 o 20 4 2 34.68 23.04 24.55 o 0 6 2 6658.64 6271.39 88.57 o 2 6 2 54347.88 54169.86 554.37 o 4 6 2 7273.88 7417.21 69.65 o 6 6 2 11279.89 11163.63 104.40 o 8 6 2 3823.70 3721.60 40.20 o 10 6 2 2754.27 3007.27 35.43 o 12 6 2 221.07 202.98 11.68 o 14 6 2 456.36 485.72 16.87 o 16 6 2 337.64 386.17 19.58 o 18 6 2 267.97 266.86 24.47 o 20 6 2 167.61 126.63 26.50 o 2 8 2 2572.62 2696.75 29.02 o 4 8 2 5237.36 5435.88 65.64 o 6 8 2 875.24 858.07 13.58 o 8 8 2 7713.52 7838.40 75.37 o 10 8 2 46.52 46.84 8.46 o 12 8 2 4170.40 4102.02 51.74 o 14 8 2 444.44 506.92 17.53 o 16 8 2 2086.67 2164.34 44.24 o 18 8 2 775.40 760.60 35.48 o 20 8 2 181.47 174.71 28.31 o 0 10 2 47455.33 45785.59 624.63 o 2 10 2 14774.56 15299.90 149.28 o 4 10 2 1407.78 1616.66 18.94 o 6 10 2 4233.94 4306.19 43.34 o 8 10 2 2215.99 2425.85 36.54 o 10 10 2 2208.37 2255.43 29.19 o 12 10 2 1426.98 1396.03 25.32 o 14 10 2 512.20 509.73 19.48 o 16 10 2 311.00 327.33 20.08 o 18 10 2 77.04 67.17 21.61 o 20 10 2 28.14 49.12 28.33 o 2 12 2 819.17 857.39 17.09 o 4 12 2 21022.05 22698.87 196.32 o 6 12 2 838.69 961.66 14.19 o 8 12 2 2553.91 2596.50 30.67 o 10 12 2 998.95 957.35 19.74 o 12 12 2 1795.99 1809.47 31.06 o 14 12 2 78.68 81.61 15.61 o 16 12 2 322.06 349.90 21.46 o 18 12 2 92.20 60.59 23.68 o 20 12 2 149.56 122.18 33.81 o 0 14 2 32722.13 32737.18 505.62 o 2 14 2 1623.60 1761.61 23.69 o 4 14 2 1158.59 1337.43 18.00 o 6 14 2 1024.06 1107.32 17.06 o 8 14 2 678.62 671.38 20.49 o 10 14 2 555.83 521.24 15.76 o 12 14 2 366.95 380.39 16.36 o 14 14 2 66.71 43.69 16.16 o 16 14 2 237.57 259.60 21.98 o 18 14 2 260.33 217.39 26.94 o 2 16 2 163.03 140.40 12.38 o 4 16 2 4322.97 4302.73 53.86 o 6 16 2 152.62 171.26 11.67 o 8 16 2 2619.90 2524.46 32.40 o 10 16 2 44.29 39.81 13.96 o 12 16 2 1850.05 1828.84 33.95 o 14 16 2 454.32 446.86 29.98 o 16 16 2 177.91 200.20 26.11 o 18 16 2 141.00 147.21 32.06 o 0 18 2 420.02 409.43 23.48 o 2 18 2 587.69 628.38 17.39 o 4 18 2 1762.85 1577.76 30.59 o 6 18 2 1543.60 1456.32 27.05 o 8 18 2 1102.86 1069.01 33.03 o 10 18 2 1750.14 1678.30 35.88 o 12 18 2 283.42 256.85 21.57 o 14 18 2 280.08 327.09 29.84 o 16 18 2 28.76 28.46 30.42 o 18 18 2 101.68 101.31 40.55 o 2 20 2 3732.75 3539.52 56.49 o 4 20 2 2210.08 2154.44 41.97 o 6 20 2 896.31 855.32 23.53 o 8 20 2 1733.67 1766.33 36.11 o 10 20 2 1103.25 1155.69 76.58 o 12 20 2 609.08 694.88 31.62 o 14 20 2 186.08 134.57 34.90 o 16 20 2 81.71 94.20 40.84 o 0 22 2 2307.87 2274.82 70.50 o 2 22 2 500.76 472.22 39.79 o 4 22 2 1027.49 922.33 28.38 o 6 22 2 423.96 415.52 20.67 o 8 22 2 195.13 140.40 19.26 o 10 22 2 60.18 45.88 24.32 o 12 22 2 587.39 599.93 33.52 o 14 22 2 340.35 276.50 87.69 o 16 22 2 56.79 69.42 53.78 o 2 24 2 4148.69 4232.60 68.18 o 4 24 2 382.83 386.04 22.19 o 6 24 2 1144.84 1174.59 52.57 o 8 24 2 559.51 559.21 38.53 o 10 24 2 14.33 18.91 24.76 o 12 24 2 297.69 332.63 33.29 o 14 24 2 346.44 382.76 43.74 o 0 26 2 883.33 874.61 41.71 o 2 26 2 466.04 466.87 30.11 o 4 26 2 486.51 435.59 39.20 o 6 26 2 386.40 389.41 26.13 o 8 26 2 295.27 379.86 30.59 o 10 26 2 155.12 191.97 32.19 o 12 26 2 176.58 161.67 35.69 o 2 28 2 133.62 144.23 25.19 o 4 28 2 300.15 274.28 25.60 o 6 28 2 48.14 23.54 24.44 o 8 28 2 83.06 99.05 29.22 o 10 28 2 161.68 176.50 35.41 o 12 28 2 82.60 52.88 40.84 o 0 30 2 261.10 341.18 121.03 o 2 30 2 206.37 195.36 29.23 o 4 30 2 29.35 42.20 26.01 o 6 30 2 83.06 108.06 29.42 o 8 30 2 108.88 146.66 34.57 o 2 32 2 141.52 111.51 31.38 o 4 32 2 108.87 85.05 29.47 o 6 32 2 2.00 18.54 31.17 o 1 1 3 12301.44 12499.25 103.72 o 3 1 3 455.47 435.65 8.22 o 5 1 3 13486.43 13547.71 157.71 o 7 1 3 4313.78 5029.23 56.05 o 9 1 3 1993.29 1941.42 25.94 o 11 1 3 31.62 16.57 9.44 o 13 1 3 187.15 187.91 12.99 o 15 1 3 310.95 244.25 17.00 o 17 1 3 8.80 6.49 17.91 o 19 1 3 256.28 289.34 25.16 o 21 1 3 10.61 10.39 29.63 o 1 3 3 12085.41 11741.06 117.03 o 3 3 3 6177.03 5997.93 66.93 o 5 3 3 17366.55 18053.04 189.44 o 7 3 3 7396.60 7942.23 81.85 o 9 3 3 1675.19 1795.82 26.52 o 11 3 3 351.48 298.17 12.82 o 13 3 3 33.23 21.76 11.82 o 15 3 3 1479.20 1566.90 34.34 o 17 3 3 66.55 66.88 18.86 o 19 3 3 62.43 47.74 24.39 o 21 3 3 78.42 48.35 29.54 o 1 5 3 16278.09 16853.86 179.29 o 3 5 3 11745.63 11885.82 111.00 o 5 5 3 1316.79 1399.19 19.00 o 7 5 3 6333.49 6524.38 68.18 o 9 5 3 2699.34 2556.88 34.58 o 11 5 3 4030.24 4157.71 52.04 o 13 5 3 38.69 25.41 11.95 o 15 5 3 342.38 349.48 27.09 o 17 5 3 382.00 422.48 37.64 o 19 5 3 673.87 774.43 59.48 o 1 7 3 13272.18 13760.67 145.76 o 3 7 3 2371.35 2399.96 29.26 o 5 7 3 1265.00 1142.55 21.69 o 7 7 3 1139.02 1214.05 16.32 o 9 7 3 5775.49 5647.94 70.73 o 11 7 3 102.84 99.15 11.97 o 13 7 3 2505.73 2408.45 39.00 o 15 7 3 1117.21 1062.68 52.99 o 17 7 3 86.20 60.25 19.76 o 19 7 3 94.28 82.61 24.69 o 1 9 3 4817.47 5100.53 52.80 o 3 9 3 2096.61 1991.65 24.35 o 5 9 3 701.83 606.21 14.09 o 7 9 3 4040.19 4321.76 44.08 o 9 9 3 103.37 123.33 10.08 o 11 9 3 261.79 241.06 14.33 o 13 9 3 1937.28 1960.32 35.44 o 15 9 3 339.35 312.28 19.25 o 17 9 3 206.23 240.42 21.82 o 19 9 3 18.93 6.13 24.07 o 1 11 3 5944.33 6313.63 70.88 o 3 11 3 8994.10 9380.59 84.02 o 5 11 3 861.72 843.15 20.02 o 7 11 3 3382.20 3354.70 38.46 o 9 11 3 2068.59 2010.96 29.48 o 11 11 3 851.36 796.07 21.59 o 13 11 3 1382.13 1442.63 30.38 o 15 11 3 1100.63 1055.65 35.43 o 17 11 3 632.84 618.58 28.29 o 19 11 3 80.34 28.45 28.09 o 1 13 3 3561.32 3571.68 39.14 o 3 13 3 1052.57 1102.75 17.22 o 5 13 3 135.00 151.23 8.56 o 7 13 3 3007.54 2858.60 34.56 o 9 13 3 157.05 131.88 12.57 o 11 13 3 67.55 45.20 15.40 o 13 13 3 841.37 840.74 26.29 o 15 13 3 1264.30 1207.65 78.52 o 17 13 3 90.92 60.47 25.11 o 19 13 3 51.79 42.23 26.67 o 1 15 3 1304.80 1367.72 23.40 o 3 15 3 572.15 617.95 15.48 o 5 15 3 281.94 278.31 13.70 o 7 15 3 3826.88 3597.72 47.73 o 9 15 3 1168.55 1171.68 22.66 o 11 15 3 544.33 525.73 19.67 o 13 15 3 407.20 458.14 28.86 o 15 15 3 6.76 0.79 19.28 o 17 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1646.82 1543.23 22.13 o 3 5 5 100.96 70.49 8.82 o 5 5 5 7276.20 7100.42 92.46 o 7 5 5 2779.50 2774.22 38.35 o 9 5 5 2648.60 2630.75 55.78 o 11 5 5 272.55 235.60 15.46 o 13 5 5 29.69 19.30 14.82 o 15 5 5 330.68 314.18 20.70 o 17 5 5 264.66 261.32 25.41 o 19 5 5 195.48 184.11 31.87 o 1 7 5 703.73 639.12 21.23 o 3 7 5 218.12 277.11 13.02 o 5 7 5 4270.96 4387.56 64.56 o 7 7 5 386.74 351.78 14.26 o 9 7 5 199.73 209.56 14.03 o 11 7 5 755.75 820.74 28.09 o 13 7 5 594.52 543.90 24.38 o 15 7 5 131.68 109.74 21.02 o 17 7 5 92.55 68.59 23.41 o 19 7 5 32.04 7.19 30.77 o 1 9 5 3573.08 3532.25 43.88 o 3 9 5 960.21 903.64 16.75 o 5 9 5 1073.94 1104.00 21.29 o 7 9 5 145.98 147.48 14.31 o 9 9 5 2315.17 2350.23 39.33 o 11 9 5 296.83 295.91 18.49 o 13 9 5 275.50 281.96 19.92 o 15 9 5 49.01 25.62 20.35 o 17 9 5 109.56 70.37 24.06 o 1 11 5 4644.31 4794.20 52.63 o 3 11 5 1052.86 988.40 18.51 o 5 11 5 1992.76 1852.83 47.77 o 7 11 5 1608.59 1544.45 35.91 o 9 11 5 2815.64 2866.98 57.01 o 11 11 5 313.09 279.13 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575.45 24.33 o 14 8 6 37.63 50.82 21.36 o 16 8 6 189.42 245.53 28.34 o 0 10 6 1983.73 1963.36 48.10 o 2 10 6 543.81 525.36 17.20 o 4 10 6 996.72 1009.93 27.51 o 6 10 6 1316.07 1299.61 43.42 o 8 10 6 1885.82 1870.34 36.61 o 10 10 6 612.89 522.06 22.33 o 12 10 6 277.91 329.28 25.34 o 14 10 6 17.95 13.79 22.43 o 16 10 6 5.34 7.74 29.18 o 2 12 6 46.42 56.17 13.21 o 4 12 6 3490.84 3439.45 56.64 o 6 12 6 78.56 90.09 17.58 o 8 12 6 689.60 690.16 41.88 o 10 12 6 602.93 612.25 31.81 o 12 12 6 517.04 474.58 31.83 o 14 12 6 13.00 15.70 25.28 o 16 12 6 120.15 80.76 30.15 o 0 14 6 35.70 50.24 20.18 o 2 14 6 1072.64 1124.08 30.61 o 4 14 6 550.51 567.43 26.52 o 6 14 6 2044.26 2174.83 44.19 o 8 14 6 413.52 414.11 23.97 o 10 14 6 242.75 275.59 23.96 o 12 14 6 34.02 10.46 23.94 o 14 14 6 41.05 58.94 27.32 o 16 14 6 23.13 0.30 35.52 o 2 16 6 6503.51 6392.36 81.44 o 4 16 6 899.17 996.99 31.73 o 6 16 6 85.54 121.87 20.07 o 8 16 6 585.51 554.60 31.16 o 10 16 6 593.16 568.37 33.22 o 12 16 6 80.21 53.36 31.01 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163.54 17.77 o 9 1 7 487.54 490.98 22.74 o 11 1 7 63.76 47.85 18.78 o 13 1 7 13.02 4.99 20.85 o 15 1 7 90.94 70.00 25.41 o 1 3 7 161.68 130.55 15.67 o 3 3 7 1589.26 1537.76 47.22 o 5 3 7 3572.18 3645.68 87.35 o 7 3 7 1079.42 1151.92 26.27 o 9 3 7 475.92 486.41 20.94 o 11 3 7 603.86 753.32 25.63 o 13 3 7 123.48 98.22 22.24 o 15 3 7 21.24 12.59 26.36 o 1 5 7 929.30 961.48 23.65 o 3 5 7 1090.92 1008.37 25.62 o 5 5 7 1931.64 2085.70 58.59 o 7 5 7 67.61 44.42 15.32 o 9 5 7 321.13 329.09 21.37 o 11 5 7 635.67 681.46 24.43 o 13 5 7 63.95 65.95 21.75 o 15 5 7 218.43 171.16 26.02 o 1 7 7 4716.24 4433.61 57.63 o 3 7 7 1393.22 1329.48 38.58 o 5 7 7 1900.85 1859.23 36.49 o 7 7 7 449.27 413.71 21.92 o 9 7 7 296.40 265.33 21.68 o 11 7 7 60.10 42.28 21.48 o 13 7 7 25.92 6.91 21.40 o 15 7 7 163.87 171.72 27.97 o 1 9 7 3226.63 3175.51 42.11 o 3 9 7 683.47 655.25 31.87 o 5 9 7 619.91 522.19 22.26 o 7 9 7 527.23 547.49 27.52 o 9 9 7 2747.70 2875.84 50.70 o 11 9 7 346.44 347.62 24.14 o 13 9 7 150.34 166.27 25.18 o 15 9 7 16.93 -13.51 28.17 o 1 11 7 39.11 23.27 15.01 o 3 11 7 171.03 138.13 18.68 o 5 11 7 1449.61 1442.48 45.78 o 7 11 7 323.90 345.57 21.54 o 9 11 7 168.08 151.51 24.00 o 11 11 7 338.13 356.15 27.01 o 13 11 7 188.45 203.67 28.76 o 15 11 7 88.38 56.76 31.45 o 1 13 7 546.72 547.71 36.64 o 3 13 7 809.05 760.17 34.71 o 5 13 7 1039.63 1050.61 33.82 o 7 13 7 116.50 110.46 22.76 o 9 13 7 103.76 99.65 23.20 o 11 13 7 137.16 143.54 27.13 o 13 13 7 255.01 290.02 33.82 o 1 15 7 576.99 489.23 21.82 o 3 15 7 247.78 216.76 22.17 o 5 15 7 378.74 410.29 41.82 o 7 15 7 665.21 704.74 47.01 o 9 15 7 1252.77 1440.48 48.72 o 11 15 7 497.03 553.19 59.21 o 13 15 7 263.44 288.71 37.16 o 1 17 7 97.21 79.44 23.28 o 3 17 7 5.33 -2.32 21.37 o 5 17 7 81.65 97.50 24.37 o 7 17 7 206.00 179.97 26.32 o 9 17 7 0.48 12.03 26.12 o 11 17 7 44.55 32.90 28.26 o 13 17 7 11.99 31.05 50.43 o 1 19 7 63.12 63.40 24.80 o 3 19 7 30.45 20.73 23.48 o 5 19 7 825.63 814.46 34.30 o 7 19 7 76.00 43.67 27.22 o 9 19 7 108.93 140.23 33.19 o 11 19 7 28.10 20.23 35.41 o 1 21 7 14.85 18.21 29.07 o 3 21 7 34.29 45.80 28.62 o 5 21 7 197.36 172.51 32.01 o 7 21 7 101.59 88.49 34.79 o 9 21 7 97.46 89.44 35.65 o 1 23 7 81.69 43.75 40.50 o 3 23 7 48.96 23.92 37.30 o 5 23 7 5.17 -9.39 38.31 o 7 23 7 53.09 86.57 42.12 o 1 25 7 26.76 25.38 43.97 o 3 25 7 100.24 117.54 41.43 o 5 25 7 23.29 20.51 41.22 o 0 0 8 2614.99 2754.55 124.33 o 4 0 8 742.03 856.18 37.74 o 8 0 8 418.99 376.21 98.53 o 12 0 8 400.60 421.72 40.60 o 2 2 8 430.40 424.61 24.28 o 4 2 8 1127.63 1127.28 33.24 o 6 2 8 758.44 864.75 49.69 o 8 2 8 3.96 8.42 20.38 o 10 2 8 169.00 165.14 23.90 o 12 2 8 2.27 6.16 25.62 o 14 2 8 27.19 14.34 27.11 o 0 4 8 1985.00 2041.44 73.51 o 2 4 8 1621.10 1582.50 37.63 o 4 4 8 947.45 980.05 41.61 o 6 4 8 2369.09 2354.27 45.42 o 8 4 8 189.47 152.94 22.22 o 10 4 8 213.52 178.81 28.97 o 12 4 8 149.79 141.91 25.97 o 14 4 8 17.91 13.43 28.25 o 2 6 8 1442.12 1345.27 51.76 o 4 6 8 351.45 399.67 29.79 o 6 6 8 747.75 787.54 27.70 o 8 6 8 1019.01 1051.63 31.07 o 10 6 8 166.58 157.49 24.29 o 12 6 8 199.08 212.97 26.38 o 14 6 8 87.09 56.14 28.11 o 0 8 8 2037.65 2293.55 78.55 o 2 8 8 530.73 507.67 23.29 o 4 8 8 586.75 671.61 32.04 o 6 8 8 545.49 549.56 25.46 o 8 8 8 52.22 36.95 21.26 o 10 8 8 160.39 119.23 25.41 o 12 8 8 141.94 147.06 26.90 o 14 8 8 575.95 630.72 34.03 o 2 10 8 214.41 204.59 22.28 o 4 10 8 1950.49 1866.24 51.16 o 6 10 8 321.58 320.23 24.44 o 8 10 8 378.01 355.47 28.01 o 10 10 8 534.93 639.69 32.36 o 12 10 8 181.44 157.50 29.95 o 0 12 8 14.03 12.74 35.32 o 2 12 8 576.63 543.85 28.53 o 4 12 8 143.66 126.49 23.73 o 6 12 8 906.38 933.13 54.00 o 8 12 8 47.78 31.25 25.01 o 10 12 8 593.68 624.58 34.20 o 12 12 8 9.25 -6.23 30.15 o 2 14 8 79.54 75.05 27.53 o 4 14 8 465.33 532.42 44.04 o 6 14 8 133.80 95.71 30.88 o 8 14 8 644.52 681.35 39.03 o 10 14 8 220.57 235.28 45.47 o 12 14 8 61.24 43.55 54.82 o 0 16 8 306.63 294.17 37.38 o 2 16 8 76.79 48.77 30.56 o 4 16 8 630.75 662.86 32.61 o 6 16 8 36.10 44.57 27.34 o 8 16 8 157.09 201.30 30.17 o 10 16 8 152.18 104.06 35.89 o 2 18 8 49.55 69.95 32.01 o 4 18 8 10.32 12.62 27.12 o 6 18 8 108.24 104.52 28.53 o 8 18 8 285.63 374.16 33.68 o 0 20 8 45.33 11.00 38.92 o 2 20 8 10.54 11.23 34.34 o 4 20 8 87.17 54.80 35.37 o 6 20 8 64.30 65.09 35.55 o 8 20 8 35.98 72.25 80.65 o 2 22 8 69.61 57.94 57.35 o 4 22 8 211.31 199.82 89.65 o 1 1 9 128.78 108.12 29.23 o 3 1 9 148.69 95.98 29.30 o 5 1 9 347.47 330.61 31.66 o 7 1 9 87.51 81.69 29.29 o 9 1 9 426.04 439.36 38.06 o 11 1 9 94.98 58.64 33.23 o 1 3 9 178.95 184.20 30.33 o 3 3 9 315.89 380.71 36.67 o 5 3 9 69.17 37.76 26.92 o 7 3 9 99.11 106.67 25.43 o 9 3 9 37.18 43.61 28.65 o 11 3 9 272.96 282.64 35.72 o 1 5 9 1122.19 1195.82 59.59 o 3 5 9 588.72 571.93 35.24 o 5 5 9 172.24 139.24 27.50 o 7 5 9 74.65 59.08 24.01 o 9 5 9 259.36 296.35 32.56 o 11 5 9 209.33 249.78 33.82 o 1 7 9 983.50 1105.25 91.95 o 3 7 9 441.06 506.51 42.59 o 5 7 9 55.91 61.12 26.58 o 7 7 9 171.68 202.00 30.08 o 9 7 9 37.20 29.95 29.91 o 11 7 9 101.31 135.71 29.67 o 1 9 9 129.10 128.89 30.63 o 3 9 9 195.28 221.15 27.28 o 5 9 9 118.94 89.52 27.67 o 7 9 9 237.48 242.61 30.38 o 9 9 9 190.40 131.75 29.64 o 11 9 9 115.52 115.79 33.24 o 1 11 9 149.38 142.26 45.91 o 3 11 9 60.54 29.30 32.62 o 5 11 9 206.62 210.57 30.25 o 7 11 9 292.39 293.06 28.91 o 9 11 9 68.40 62.64 31.80 o 1 13 9 83.16 57.44 43.17 o 3 13 9 304.43 364.38 38.82 o 5 13 9 66.35 119.52 34.78 o 7 13 9 133.45 158.21 35.11 o 9 13 9 60.35 38.81 36.33 o 1 15 9 16.38 19.41 40.14 o 3 15 9 114.12 85.56 35.57 o 5 15 9 73.10 49.42 36.07 o 7 15 9 572.39 563.51 41.94 o 1 17 9 5.43 5.98 37.03 o 3 17 9 88.10 91.15 37.34 o 5 17 9 262.84 301.78 41.30 o 1 19 9 338.83 370.87 49.15 o 3 19 9 188.74 215.86 45.51 o 2 0 10 297.50 338.87 51.80 o 6 0 10 3.80 -19.84 46.23 o 0 2 10 13.14 18.81 45.57 o 2 2 10 6.75 8.55 34.86 o 4 2 10 151.57 184.81 37.47 o 6 2 10 188.56 179.28 34.40 o 8 2 10 525.77 534.50 43.33 o 2 4 10 204.56 239.19 36.26 o 4 4 10 233.18 199.38 36.75 o 6 4 10 172.73 118.18 36.36 o 8 4 10 5.41 2.18 33.36 o 0 6 10 271.61 279.57 50.45 o 2 6 10 70.26 76.57 36.63 o 4 6 10 90.68 137.10 36.05 o 6 6 10 98.08 87.34 32.36 o 8 6 10 144.75 177.43 37.04 o 2 8 10 51.09 37.29 35.17 o 4 8 10 129.18 106.98 37.19 o 6 8 10 38.04 70.40 33.55 o 0 10 10 17.51 -3.84 62.88 o 2 10 10 190.62 192.33 53.02 o 4 10 10 58.15 51.87 43.16 o 6 10 10 54.39 36.02 38.26 o 2 12 10 1.41 -6.72 51.55 o 4 12 10 459.85 517.23 107.95 o 0 14 10 524.25 643.37 93.49 o