#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:19:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181001 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/81/2208111.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208111_Fobs loop_ _publ_author_name 'Kolev, Tsonko' 'Yancheva, Denitsa' 'Spiteller, Michael' 'Sheldrick, William S.' 'Mayer-Figge, Heike' _publ_section_title ; L-Prolinamidium hydrogensquarate ; _journal_coeditor_code KP6078 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o463 _journal_page_last o465 _journal_volume 62 _journal_year 2006 _space_group_IT_number 5 _symmetry_space_group_name_Hall 'C 2y' _symmetry_space_group_name_H-M 'C 1 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.724 _cell_angle_gamma 90.000 _cell_length_a 25.9044 _cell_length_b 5.9781 _cell_length_c 6.5805 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file kp6078Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Kolev 27-69 in C2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 61.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 3.75 2.79 0.12 o 8 0 0 264.85 275.40 3.00 o 10 0 0 2516.19 2290.35 9.68 o 12 0 0 672.17 648.08 5.61 o 14 0 0 353.14 312.85 7.18 o 16 0 0 1312.34 1299.22 9.16 o 18 0 0 1510.01 1527.86 27.45 o 20 0 0 55.40 59.73 2.34 o 22 0 0 131.80 131.85 2.97 o 24 0 0 118.56 116.16 2.47 o 26 0 0 363.32 369.16 6.88 o 28 0 0 125.68 140.04 3.05 o 30 0 0 15.71 24.13 0.92 o 1 1 0 249.24 240.74 4.12 o 5 1 0 1973.64 1975.29 5.83 o 11 1 0 800.61 782.45 14.92 o 13 1 0 107.39 104.55 2.66 o 15 1 0 43.78 50.29 1.24 o 17 1 0 353.85 342.58 6.80 o 19 1 0 35.89 31.04 0.81 o 21 1 0 482.96 468.06 11.35 o 23 1 0 4.77 4.41 0.37 o 25 1 0 35.90 38.52 0.74 o 27 1 0 37.05 39.05 1.22 o 29 1 0 5.59 6.15 0.47 o 0 2 0 711.97 562.13 6.03 o 2 2 0 388.96 358.93 10.25 o 4 2 0 3318.09 3501.75 64.52 o 6 2 0 1552.79 1681.84 47.25 o 8 2 0 663.99 676.91 17.59 o 10 2 0 514.91 470.03 18.78 o 12 2 0 444.53 481.21 10.94 o 14 2 0 76.14 98.09 1.77 o 16 2 0 6.09 8.16 0.49 o 18 2 0 647.06 612.25 13.96 o 20 2 0 969.17 906.92 9.26 o 22 2 0 961.42 912.34 9.75 o 24 2 0 962.24 972.71 16.60 o 26 2 0 5.39 8.43 0.65 o 28 2 0 61.40 72.47 1.98 o 1 3 0 298.31 274.74 3.84 o 3 3 0 714.74 639.56 11.90 o 5 3 0 98.81 101.93 2.54 o 7 3 0 535.27 599.59 11.11 o 9 3 0 467.15 533.70 5.77 o 11 3 0 1597.10 1619.90 20.78 o 13 3 0 2140.36 2252.62 37.57 o 15 3 0 818.46 824.21 8.21 o 17 3 0 33.64 50.14 2.01 o 19 3 0 159.96 155.76 5.41 o 21 3 0 436.50 429.18 6.99 o 23 3 0 16.63 11.54 0.67 o 25 3 0 15.25 14.32 1.35 o 27 3 0 68.38 76.22 1.70 o 0 4 0 2840.75 2710.50 19.51 o 2 4 0 1244.71 1266.34 9.37 o 4 4 0 214.81 245.74 5.22 o 6 4 0 281.11 257.14 7.26 o 8 4 0 133.86 104.82 2.20 o 10 4 0 124.46 116.59 3.54 o 12 4 0 96.72 112.61 3.03 o 14 4 0 21.47 23.53 1.21 o 16 4 0 318.72 314.45 16.53 o 18 4 0 17.89 27.37 1.58 o 20 4 0 102.53 96.03 2.18 o 22 4 0 49.89 58.43 1.15 o 24 4 0 56.74 51.77 1.19 o 1 5 0 100.41 123.15 5.43 o 3 5 0 259.74 251.42 5.06 o 5 5 0 0.10 0.49 0.88 o 7 5 0 1713.68 1689.92 24.33 o 9 5 0 1213.68 1124.39 29.74 o 11 5 0 249.67 236.86 8.99 o 13 5 0 79.98 84.51 1.82 o 15 5 0 12.18 9.76 0.66 o 17 5 0 98.30 101.79 2.14 o 19 5 0 16.00 14.77 0.77 o 21 5 0 7.77 8.07 0.81 o 0 6 0 1134.34 1080.90 15.84 o 2 6 0 40.68 37.89 1.05 o 4 6 0 1.92 2.52 0.84 o 6 6 0 9.31 15.00 0.74 o 8 6 0 0.81 0.81 0.55 o 10 6 0 72.66 68.01 3.85 o 12 6 0 164.76 181.03 5.44 o 14 6 0 21.89 32.28 1.12 o 16 6 0 5.26 3.50 0.90 o 1 7 0 36.17 38.80 1.06 o 3 7 0 7.46 6.49 0.66 o 5 7 0 2.15 2.12 0.71 o -30 0 1 8.43 12.14 0.77 o -28 0 1 263.23 253.73 6.13 o -26 0 1 122.16 117.93 2.45 o -24 0 1 171.48 183.12 10.75 o -22 0 1 496.98 495.21 9.87 o -20 0 1 2.32 3.70 0.48 o -18 0 1 1255.91 1260.26 18.06 o -16 0 1 7.68 7.90 0.44 o -14 0 1 47.12 52.00 1.10 o -12 0 1 267.17 279.47 3.80 o -8 0 1 2773.64 2621.03 9.48 o -4 0 1 1373.31 1499.33 5.49 o 0 0 1 1203.17 964.73 651.88 o 2 0 1 374.93 323.51 2.48 o 6 0 1 2158.45 2393.04 8.82 o 8 0 1 34.84 42.88 0.75 o 10 0 1 206.40 204.13 3.13 o 12 0 1 639.56 636.55 5.81 o 14 0 1 2373.48 2279.87 18.67 o 16 0 1 253.33 282.20 4.57 o 18 0 1 762.63 818.86 12.16 o 20 0 1 57.55 63.49 1.24 o 22 0 1 519.16 482.97 15.30 o 24 0 1 5.72 3.69 0.56 o 26 0 1 0.85 2.29 0.56 o 28 0 1 155.74 155.77 5.80 o -29 1 1 3.53 4.31 0.48 o -27 1 1 5.91 4.22 0.40 o -25 1 1 136.65 130.72 1.88 o -23 1 1 12.75 12.09 0.43 o -21 1 1 320.06 331.00 7.81 o -19 1 1 507.79 477.16 5.08 o -17 1 1 263.97 236.76 3.01 o -15 1 1 1216.89 1158.19 22.84 o -13 1 1 192.71 198.79 2.98 o -11 1 1 578.22 587.14 10.43 o -9 1 1 291.21 254.07 4.40 o -7 1 1 1993.36 2113.94 8.34 o -5 1 1 217.17 232.06 3.96 o -1 1 1 633.19 542.53 4.88 o 3 1 1 996.30 1093.28 12.26 o 5 1 1 648.45 666.36 10.07 o 9 1 1 233.02 283.68 3.04 o 11 1 1 1983.55 1936.32 21.17 o 13 1 1 511.79 456.54 5.87 o 15 1 1 306.51 310.89 3.94 o 17 1 1 169.64 182.19 2.87 o 19 1 1 153.13 146.49 4.48 o 21 1 1 0.21 2.02 0.67 o 23 1 1 59.21 59.11 1.01 o 25 1 1 66.76 56.85 0.82 o 27 1 1 169.65 173.62 3.43 o -28 2 1 82.06 75.69 3.18 o -26 2 1 172.41 164.17 7.71 o -24 2 1 35.39 33.78 0.87 o -22 2 1 10.09 10.96 0.61 o -20 2 1 484.60 494.38 7.10 o -18 2 1 19.80 27.24 0.70 o -16 2 1 293.97 291.88 4.80 o -14 2 1 88.26 71.19 1.45 o -12 2 1 56.60 76.75 1.50 o -10 2 1 484.42 523.89 5.18 o -8 2 1 1186.47 1248.82 49.22 o -6 2 1 2432.83 2441.62 76.56 o -2 2 1 427.59 372.04 3.67 o 0 2 1 2036.12 1974.72 15.65 o 2 2 1 3323.24 3354.99 41.62 o 4 2 1 78.38 91.53 4.31 o 6 2 1 20.49 19.01 1.00 o 8 2 1 507.40 546.90 7.42 o 10 2 1 1108.85 1158.48 20.61 o 12 2 1 19.54 29.39 0.63 o 14 2 1 214.34 217.23 4.30 o 16 2 1 383.03 399.65 5.71 o 18 2 1 210.88 181.11 4.27 o 20 2 1 292.38 284.64 5.53 o 22 2 1 384.16 370.61 6.49 o 24 2 1 24.54 25.32 0.83 o 26 2 1 42.99 52.59 1.20 o 28 2 1 0.68 4.34 0.64 o -27 3 1 62.38 67.19 1.49 o -25 3 1 1.08 0.49 0.82 o -23 3 1 131.14 135.43 2.73 o -21 3 1 176.79 179.48 8.03 o -19 3 1 317.45 328.46 5.82 o -17 3 1 99.92 100.33 2.09 o -15 3 1 117.18 123.09 2.88 o -13 3 1 957.73 951.97 15.54 o -11 3 1 2.71 2.64 0.55 o -9 3 1 254.01 219.17 11.43 o -7 3 1 473.14 482.91 5.35 o -5 3 1 804.54 826.13 10.38 o -3 3 1 452.06 457.46 11.29 o -1 3 1 485.07 435.34 9.09 o 1 3 1 12.42 13.21 0.42 o 3 3 1 1659.59 1522.69 30.65 o 5 3 1 189.53 164.06 5.31 o 7 3 1 646.45 713.76 6.59 o 9 3 1 1551.19 1536.83 36.12 o 11 3 1 118.70 126.05 3.38 o 13 3 1 51.57 58.92 1.07 o 15 3 1 3.53 5.21 0.52 o 17 3 1 108.54 103.64 2.07 o 19 3 1 3.31 4.00 0.54 o 21 3 1 8.11 6.43 0.60 o 23 3 1 100.10 106.41 2.45 o 25 3 1 3.20 3.06 0.85 o -24 4 1 19.55 23.51 0.89 o -22 4 1 70.50 67.17 1.56 o -20 4 1 167.68 155.07 3.14 o -18 4 1 88.51 94.25 4.32 o -16 4 1 32.95 32.65 0.82 o -14 4 1 85.55 81.40 1.79 o -12 4 1 372.87 340.27 9.46 o -10 4 1 2.73 3.70 0.65 o -8 4 1 74.51 67.64 1.82 o -6 4 1 120.59 113.55 2.60 o -4 4 1 430.57 450.46 5.83 o -2 4 1 206.79 183.92 3.86 o 0 4 1 181.67 199.85 3.98 o 2 4 1 199.74 226.68 6.81 o 4 4 1 52.27 49.51 1.00 o 6 4 1 77.88 72.99 1.59 o 8 4 1 428.29 386.82 5.72 o 10 4 1 190.65 215.92 4.57 o 12 4 1 0.63 1.52 0.51 o 14 4 1 31.57 25.94 0.99 o 16 4 1 51.59 41.36 0.92 o 18 4 1 138.63 124.01 2.64 o 20 4 1 151.89 156.49 6.46 o 22 4 1 180.78 174.95 5.95 o -21 5 1 3.07 4.78 1.43 o -19 5 1 77.89 79.61 1.91 o -17 5 1 99.13 102.09 2.56 o -15 5 1 311.97 290.98 6.15 o -13 5 1 113.84 112.66 5.35 o -11 5 1 340.44 319.89 6.05 o -9 5 1 59.72 57.20 2.31 o -7 5 1 124.56 116.48 6.20 o -5 5 1 30.38 31.46 0.79 o -3 5 1 124.72 108.18 2.73 o -1 5 1 193.97 183.95 10.82 o 1 5 1 110.41 108.93 2.31 o 3 5 1 61.12 57.87 1.29 o 5 5 1 51.01 51.79 1.05 o 7 5 1 436.88 411.18 6.60 o 9 5 1 137.07 126.27 2.50 o 11 5 1 414.96 395.34 6.73 o 13 5 1 38.34 37.99 0.94 o 15 5 1 148.91 159.29 4.87 o 17 5 1 26.37 24.48 1.38 o 19 5 1 42.55 50.07 1.16 o -16 6 1 0.95 -0.22 0.58 o -14 6 1 23.57 26.02 0.91 o -12 6 1 22.22 22.46 0.85 o -10 6 1 58.23 53.98 1.19 o -8 6 1 57.49 60.67 1.54 o -6 6 1 28.22 28.57 0.88 o -4 6 1 113.20 114.18 2.50 o -2 6 1 25.83 26.35 1.67 o 0 6 1 131.25 136.66 2.84 o 2 6 1 58.62 57.59 1.14 o 4 6 1 100.18 98.84 2.15 o 6 6 1 0.40 -0.02 0.56 o 8 6 1 72.71 73.75 1.76 o 10 6 1 16.57 20.17 0.85 o 12 6 1 48.76 51.15 1.14 o 14 6 1 8.16 5.33 0.98 o -3 7 1 0.73 0.36 0.70 o -1 7 1 3.24 3.79 0.84 o 1 7 1 1.85 0.63 0.57 o -30 0 2 0.76 1.24 0.57 o -28 0 2 130.05 144.25 3.15 o -26 0 2 76.77 74.74 3.67 o -24 0 2 51.37 52.06 1.08 o -22 0 2 326.26 337.73 12.20 o -20 0 2 626.38 633.36 19.14 o -18 0 2 469.96 447.47 5.96 o -16 0 2 87.34 76.81 3.51 o -14 0 2 605.06 594.63 9.44 o -12 0 2 321.90 371.03 5.21 o -10 0 2 5.99 1.22 0.32 o -6 0 2 551.96 568.51 11.92 o 2 0 2 1786.18 1636.71 12.08 o 4 0 2 3365.23 3358.59 11.60 o 6 0 2 2290.39 2260.30 11.95 o 8 0 2 26.36 33.81 0.66 o 10 0 2 35.38 43.57 0.78 o 12 0 2 1816.46 1807.44 10.71 o 14 0 2 1033.02 1002.94 8.36 o 16 0 2 98.86 104.27 6.04 o 18 0 2 0.08 -0.45 0.45 o 20 0 2 165.26 148.96 5.10 o 22 0 2 47.62 44.19 1.10 o 24 0 2 98.95 101.09 2.22 o 26 0 2 147.55 133.08 6.30 o -29 1 2 42.48 41.64 0.93 o -27 1 2 170.13 172.95 3.16 o -25 1 2 104.63 107.28 2.04 o -23 1 2 172.10 178.37 3.18 o -21 1 2 7.13 6.67 0.36 o -19 1 2 54.15 50.95 1.30 o -17 1 2 335.26 319.38 4.30 o -15 1 2 124.40 114.23 2.71 o -13 1 2 1094.39 983.68 22.69 o -11 1 2 3779.42 3829.69 68.89 o -9 1 2 1645.07 1556.84 38.10 o -7 1 2 1872.70 1922.13 18.40 o -5 1 2 1832.48 1849.74 7.11 o -3 1 2 1188.68 1251.92 15.22 o -1 1 2 526.07 564.56 12.57 o 1 1 2 1982.83 2088.08 33.43 o 7 1 2 369.15 407.26 3.17 o 9 1 2 1096.33 1064.86 8.77 o 11 1 2 43.27 47.10 0.96 o 13 1 2 91.19 95.96 2.93 o 15 1 2 0.35 2.15 0.32 o 17 1 2 305.30 291.91 5.61 o 19 1 2 129.65 122.90 1.73 o 21 1 2 198.91 192.46 3.49 o 23 1 2 101.86 105.71 1.67 o 25 1 2 99.72 90.58 1.67 o 27 1 2 79.83 77.85 1.54 o -28 2 2 467.20 469.48 10.32 o -26 2 2 363.66 352.07 12.90 o -24 2 2 656.31 605.40 11.00 o -22 2 2 492.13 492.71 7.26 o -20 2 2 168.23 144.53 3.10 o -18 2 2 864.35 912.63 10.69 o -16 2 2 160.91 165.30 3.79 o -14 2 2 341.17 392.07 5.24 o -12 2 2 411.32 393.78 10.86 o -10 2 2 849.15 950.08 12.17 o -8 2 2 2117.88 2056.31 12.70 o -6 2 2 633.83 534.16 17.18 o -4 2 2 400.77 390.11 17.14 o -2 2 2 867.92 887.61 27.00 o 0 2 2 1354.02 1354.15 7.84 o 2 2 2 3244.99 3385.89 44.32 o 4 2 2 281.72 334.41 7.97 o 6 2 2 6.07 5.85 0.36 o 8 2 2 358.66 396.62 4.85 o 10 2 2 645.14 687.75 6.72 o 12 2 2 318.77 309.36 7.74 o 14 2 2 166.06 161.88 4.97 o 16 2 2 1285.90 1216.97 10.31 o 18 2 2 1453.73 1374.56 24.07 o 20 2 2 625.78 626.69 8.40 o 22 2 2 92.84 73.84 2.69 o 24 2 2 119.18 136.30 2.86 o 26 2 2 2.10 4.21 0.63 o -27 3 2 8.79 6.84 1.11 o -25 3 2 229.42 237.48 6.00 o -23 3 2 228.61 228.33 5.47 o -21 3 2 237.44 260.66 5.57 o -19 3 2 432.87 425.89 6.64 o -17 3 2 50.58 62.23 1.38 o -15 3 2 2007.31 2095.61 13.35 o -13 3 2 26.22 19.18 0.61 o -11 3 2 74.95 77.34 2.06 o -9 3 2 16.29 15.84 0.52 o -7 3 2 61.21 75.00 1.55 o -5 3 2 51.30 46.82 1.07 o -3 3 2 193.63 193.32 5.76 o -1 3 2 259.60 258.04 4.01 o 1 3 2 139.11 164.88 3.29 o 3 3 2 162.58 160.04 3.33 o 5 3 2 244.33 252.26 6.53 o 7 3 2 502.95 461.55 5.75 o 9 3 2 802.87 818.55 18.13 o 11 3 2 1079.91 1160.68 9.64 o 13 3 2 513.76 561.74 8.28 o 15 3 2 90.98 84.83 1.57 o 17 3 2 273.58 286.86 5.70 o 19 3 2 14.26 14.20 0.69 o 21 3 2 84.46 83.19 1.72 o 23 3 2 15.62 20.91 0.85 o -24 4 2 85.03 98.31 2.12 o -22 4 2 38.80 44.16 1.05 o -20 4 2 216.22 213.88 5.46 o -18 4 2 94.18 98.53 2.20 o -16 4 2 33.79 34.00 0.87 o -14 4 2 472.13 436.89 11.32 o -12 4 2 0.59 0.96 0.57 o -10 4 2 121.53 109.19 2.16 o -8 4 2 12.10 9.82 0.54 o -6 4 2 1065.03 1059.94 9.23 o -4 4 2 2373.06 2357.64 13.61 o -2 4 2 1020.22 1074.20 10.61 o 0 4 2 48.51 47.52 1.02 o 2 4 2 35.75 38.11 1.29 o 4 4 2 95.84 87.56 1.98 o 6 4 2 348.04 349.08 5.61 o 8 4 2 182.70 190.60 4.65 o 10 4 2 33.69 36.55 0.85 o 12 4 2 695.02 695.95 8.60 o 14 4 2 98.83 95.59 1.99 o 16 4 2 99.05 96.44 3.04 o 18 4 2 62.66 71.40 2.60 o 20 4 2 15.91 16.67 0.80 o 22 4 2 200.11 217.49 6.03 o -21 5 2 37.96 44.89 1.94 o -19 5 2 39.22 39.13 1.01 o -17 5 2 22.57 21.64 0.82 o -15 5 2 134.19 146.31 9.02 o -13 5 2 641.18 621.33 8.60 o -11 5 2 1449.59 1405.08 12.35 o -9 5 2 88.34 91.98 1.93 o -7 5 2 44.82 40.66 0.88 o -5 5 2 41.76 32.95 0.82 o -3 5 2 4.41 4.43 0.51 o -1 5 2 98.86 89.98 1.86 o 1 5 2 32.37 33.98 0.86 o 3 5 2 1761.88 1699.55 35.93 o 5 5 2 1372.67 1309.67 11.65 o 7 5 2 176.54 168.16 4.58 o 9 5 2 136.50 136.82 2.70 o 11 5 2 13.58 15.85 0.74 o 13 5 2 78.56 87.48 1.95 o 15 5 2 21.73 23.66 1.26 o 17 5 2 6.35 7.62 0.95 o -14 6 2 4.14 3.97 0.63 o -12 6 2 6.60 4.94 0.85 o -10 6 2 11.53 7.53 0.87 o -8 6 2 60.26 60.00 2.04 o -6 6 2 20.58 22.12 1.20 o -4 6 2 279.97 263.46 5.97 o -2 6 2 166.16 160.99 3.21 o 0 6 2 57.25 60.04 1.24 o 2 6 2 0.91 -0.28 0.69 o 4 6 2 37.93 41.68 2.90 o 6 6 2 39.02 35.32 1.86 o 8 6 2 86.17 101.05 2.27 o 10 6 2 57.78 64.68 2.53 o 12 6 2 16.31 13.19 0.81 o -30 0 3 70.98 77.08 1.86 o -28 0 3 42.28 37.52 1.01 o -26 0 3 590.07 545.61 16.33 o -24 0 3 145.18 125.00 2.59 o -22 0 3 32.30 47.51 2.78 o -20 0 3 79.17 78.28 2.80 o -18 0 3 49.39 58.64 1.26 o -16 0 3 46.13 45.96 1.25 o -14 0 3 846.97 793.02 7.34 o -12 0 3 82.47 98.04 2.75 o -10 0 3 209.65 213.07 3.73 o -8 0 3 1677.16 1755.30 19.99 o -6 0 3 798.52 830.18 6.55 o -4 0 3 1538.92 1649.75 16.42 o -2 0 3 1190.93 1144.94 7.35 o 0 0 3 863.83 823.57 6.41 o 2 0 3 2587.07 2623.71 11.64 o 4 0 3 112.99 134.14 3.02 o 6 0 3 87.29 76.71 1.43 o 8 0 3 771.59 783.60 12.61 o 10 0 3 900.85 907.72 16.76 o 12 0 3 171.22 175.79 3.88 o 14 0 3 401.56 416.64 8.08 o 16 0 3 547.26 535.09 17.29 o 18 0 3 421.88 406.51 9.45 o 20 0 3 366.48 332.22 10.60 o 22 0 3 8.10 6.87 0.63 o 24 0 3 0.21 0.01 0.54 o -29 1 3 0.93 0.84 0.42 o -27 1 3 16.36 15.19 0.51 o -25 1 3 22.07 27.37 0.58 o -23 1 3 43.57 44.44 1.48 o -21 1 3 22.41 20.19 0.52 o -19 1 3 71.61 68.65 1.88 o -17 1 3 541.51 528.29 8.60 o -15 1 3 150.36 145.44 3.62 o -13 1 3 13.47 12.74 0.36 o -11 1 3 57.42 57.10 0.76 o -9 1 3 271.95 278.64 6.99 o -7 1 3 221.38 217.38 4.70 o -5 1 3 144.96 158.00 2.05 o -3 1 3 242.96 255.01 2.65 o -1 1 3 1528.65 1431.11 7.65 o 1 1 3 95.83 113.03 1.81 o 3 1 3 681.85 699.49 6.54 o 5 1 3 417.18 451.20 5.18 o 7 1 3 1212.44 1235.96 6.76 o 9 1 3 536.66 504.87 4.21 o 11 1 3 777.27 779.18 7.63 o 13 1 3 315.00 324.51 3.95 o 15 1 3 60.49 53.01 0.89 o 17 1 3 100.73 104.52 2.16 o 19 1 3 12.53 15.64 0.88 o 21 1 3 0.74 0.65 0.37 o 23 1 3 96.52 95.76 1.51 o 25 1 3 5.10 4.24 0.47 o -28 2 3 36.83 38.25 1.03 o -26 2 3 5.85 4.51 0.98 o -24 2 3 140.47 147.86 4.25 o -22 2 3 22.54 20.13 0.72 o -20 2 3 54.93 56.15 1.27 o -18 2 3 264.44 248.07 4.99 o -16 2 3 402.38 402.21 5.93 o -14 2 3 269.44 310.14 6.46 o -12 2 3 1.00 1.22 0.37 o -10 2 3 234.14 199.68 6.57 o -8 2 3 2551.70 2693.24 107.95 o -6 2 3 154.97 165.07 4.15 o -4 2 3 854.43 842.11 13.61 o -2 2 3 1084.80 1132.48 21.54 o 0 2 3 124.19 122.75 2.83 o 2 2 3 508.87 531.52 15.80 o 4 2 3 525.44 567.37 5.96 o 6 2 3 34.17 38.38 0.90 o 8 2 3 367.37 358.70 5.15 o 10 2 3 78.28 77.96 1.36 o 12 2 3 421.50 405.10 9.51 o 14 2 3 288.51 266.34 5.18 o 16 2 3 107.55 111.69 2.34 o 18 2 3 193.15 186.05 4.94 o 20 2 3 56.85 55.39 2.10 o 22 2 3 8.72 9.36 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