#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/81/2208122.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208122_Fobs loop_ _publ_author_name 'Scholz, Stefan' 'Lerner, Hans-Wolfram' 'Bolte, Michael' _publ_section_title ; Carbonatobis(triphenylphosphine)platinum(II) benzene solvate: a redetermination ; _journal_coeditor_code LH6579 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m312 _journal_page_last m313 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 85.150 _cell_angle_beta 71.340 _cell_angle_gamma 70.910 _cell_length_a 10.5940 _cell_length_b 12.5120 _cell_length_c 15.1950 _exptl_crystal_F_000 852.00 _reflns_d_resolution_high 0.8362 _[local]_cod_data_source_file lh6579Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa107 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 266.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9259.08 38506.18 3559.46 o 2 0 0 20849.19 20511.36 1036.03 o 3 0 0 19501.51 19070.53 923.77 o 4 0 0 125.81 -430.98 674.69 o 5 0 0 1502.46 972.33 617.99 o 6 0 0 7310.94 7021.85 589.90 o 7 0 0 19.39 226.86 506.08 o 8 0 0 1771.76 1806.68 499.28 o 9 0 0 2290.87 2407.18 456.54 o 10 0 0 736.67 1088.84 451.15 o 11 0 0 1730.54 1411.33 443.13 o -11 1 0 1836.78 1614.79 500.11 o -10 1 0 79.29 157.82 446.46 o -9 1 0 5112.39 5234.44 478.08 o -8 1 0 1201.73 1282.98 506.87 o -7 1 0 3441.18 3622.40 559.07 o -6 1 0 4953.93 5099.13 554.49 o -5 1 0 126.84 371.44 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o 9 8 0 3193.07 3339.71 419.73 o 10 8 0 253.87 253.84 420.12 o 11 8 0 2422.05 2209.51 381.38 o -6 9 0 2928.50 2784.75 473.03 o -5 9 0 484.22 525.72 465.13 o -4 9 0 1092.98 1108.37 499.66 o -3 9 0 3303.68 3142.55 527.99 o -2 9 0 4.49 -89.18 610.97 o -1 9 0 1265.58 1378.01 675.81 o 0 9 0 1162.81 1415.87 677.23 o 1 9 0 1585.64 1867.55 670.26 o 2 9 0 9901.96 9746.66 644.92 o 3 9 0 6176.41 6393.41 821.57 o 4 9 0 1193.23 1056.79 553.87 o 5 9 0 8511.53 8712.91 541.13 o 6 9 0 2250.60 2851.92 463.63 o 7 9 0 887.33 1120.13 492.23 o 8 9 0 4220.02 4421.47 572.62 o 9 9 0 2737.04 2954.90 408.79 o 10 9 0 1985.41 1943.63 419.00 o 11 9 0 4733.71 4942.91 421.57 o -5 10 0 468.89 527.29 485.94 o -4 10 0 4882.78 4902.34 479.53 o -3 10 0 1043.80 1340.07 518.43 o -2 10 0 2923.58 3496.83 543.83 o -1 10 0 4146.37 3808.37 613.39 o 0 10 0 993.59 1601.18 628.33 o 1 10 0 2998.64 3301.01 514.25 o 2 10 0 5115.49 5057.78 552.87 o 3 10 0 38.27 74.96 535.24 o 4 10 0 6736.69 6707.95 537.70 o 5 10 0 1916.17 1921.01 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