#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/81/2208124.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208124_Fobs loop_ _publ_author_name 'Sui, Ruohong' 'Charpentier, P. A.' 'Rizkalla, A. S.' 'Jennings, M. C.' _publ_section_title ; Hexakis(\m-acetato-\k^2^O,O')hexaisopropoxyhexa-\m~3~-oxo-hexatitanium ; _journal_coeditor_code LH6581 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m373 _journal_page_last m375 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.861 _cell_angle_beta 83.883 _cell_angle_gamma 75.461 _cell_length_a 10.2466 _cell_length_b 12.2908 _cell_length_c 20.2250 _exptl_crystal_F_000 1128.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file lh6581Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 05101 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 199.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l 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0 15.43 -209.77 209.77 o -10 2 0 225.48 197.01 151.05 o -9 2 0 302.47 257.85 133.61 o -8 2 0 57.71 216.82 234.24 o -7 2 0 242.47 233.80 45.26 o -6 2 0 2590.39 2569.86 97.27 o -5 2 0 2396.40 2553.75 166.06 o -4 2 0 89.92 89.24 39.92 o -3 2 0 676.85 712.69 39.13 o -2 2 0 768.43 893.99 38.30 o -1 2 0 750.63 825.97 30.52 o 0 2 0 90.53 106.04 12.31 o 1 2 0 4520.71 4712.12 114.02 o 2 2 0 288.48 389.05 20.52 o 3 2 0 1180.26 1186.16 104.03 o 4 2 0 5245.61 5485.68 215.06 o 5 2 0 241.89 336.90 81.06 o 6 2 0 4176.53 4677.82 218.39 o 7 2 0 334.32 254.42 81.53 o 8 2 0 347.80 377.84 118.29 o 9 2 0 344.11 522.51 155.31 o 11 2 0 125.56 354.87 191.47 o 12 2 0 4.14 -185.94 213.60 o -10 3 0 40.21 -114.03 146.37 o -9 3 0 165.98 137.86 123.82 o -8 3 0 1.80 -56.49 56.49 o -7 3 0 97.07 189.17 84.69 o -6 3 0 25.97 31.15 37.26 o -5 3 0 986.18 894.49 50.22 o -4 3 0 554.20 684.90 132.65 o -3 3 0 19.36 80.72 29.79 o -2 3 0 930.01 855.79 35.10 o -1 3 0 96.62 40.36 15.91 o 0 3 0 5689.95 6111.06 176.63 o 1 3 0 327.39 412.54 45.49 o 2 3 0 12112.74 12191.69 238.50 o 3 3 0 441.44 383.21 23.58 o 4 3 0 850.94 1214.58 195.94 o 5 3 0 6389.27 7375.62 304.02 o 6 3 0 1360.76 1492.81 101.34 o 7 3 0 24.73 -72.15 72.15 o 8 3 0 0.22 -47.66 114.46 o 9 3 0 716.38 806.32 180.41 o 10 3 0 60.37 103.82 165.52 o 12 3 0 1.05 131.05 238.70 o -10 4 0 54.69 241.68 182.11 o -9 4 0 0.04 -128.07 128.07 o -8 4 0 289.41 196.34 68.11 o -7 4 0 164.75 185.64 55.42 o -6 4 0 871.61 910.63 147.01 o -5 4 0 424.37 454.70 60.48 o -4 4 0 36.81 46.18 32.51 o -3 4 0 855.33 894.52 46.90 o -2 4 0 1453.92 1307.87 43.19 o -1 4 0 2958.98 2354.50 61.63 o 0 4 0 1456.01 1368.46 41.09 o 1 4 0 20.55 10.01 18.56 o 2 4 0 401.17 364.68 33.41 o 3 4 0 5586.19 5501.54 126.33 o 4 4 0 81.53 63.34 18.96 o 5 4 0 9059.07 9900.98 457.01 o 6 4 0 610.42 638.45 81.10 o 7 4 0 24.94 113.64 76.09 o 9 4 0 97.86 14.47 134.03 o 10 4 0 243.53 371.46 171.48 o 12 4 0 163.13 -70.63 226.36 o -9 5 0 12.26 -27.23 123.39 o -8 5 0 0.65 -45.95 101.27 o -7 5 0 548.63 407.88 72.99 o -6 5 0 717.65 803.71 83.53 o -5 5 0 66.77 137.16 40.87 o -4 5 0 132.81 154.06 35.02 o -3 5 0 6.67 26.10 30.59 o -2 5 0 407.33 378.58 33.90 o -1 5 0 25.92 38.35 19.05 o 0 5 0 193.81 160.94 51.50 o 1 5 0 146.55 264.16 43.36 o 2 5 0 115.32 67.87 23.18 o 3 5 0 121.25 83.20 35.01 o 4 5 0 323.87 371.16 48.21 o 5 5 0 999.46 839.89 47.04 o 6 5 0 2898.28 2758.93 243.81 o 7 5 0 279.43 165.09 111.48 o 8 5 0 669.60 899.50 159.56 o 9 5 0 362.08 462.52 154.03 o 10 5 0 19.25 158.29 119.99 o 12 5 0 55.57 314.02 157.96 o -9 6 0 21.27 -68.51 178.28 o -8 6 0 1.39 -81.68 81.68 o -7 6 0 10.38 62.13 113.61 o -6 6 0 254.34 338.09 66.05 o -5 6 0 193.27 241.37 94.46 o -4 6 0 160.85 121.62 79.82 o -3 6 0 864.49 834.95 60.86 o -2 6 0 333.00 365.96 30.63 o -1 6 0 1496.48 1667.46 62.95 o 0 6 0 7.97 38.25 27.76 o 1 6 0 42.81 39.25 22.77 o 2 6 0 5.32 45.31 24.08 o 3 6 0 192.50 211.10 29.39 o 4 6 0 2191.84 2221.35 88.36 o 5 6 0 2.30 -32.89 32.89 o 6 6 0 6.45 -27.57 44.51 o 7 6 0 172.55 214.88 117.01 o 8 6 0 0.28 151.05 136.16 o 9 6 0 918.33 1183.31 194.03 o 10 6 0 12.99 -101.27 164.24 o -7 7 0 141.76 169.46 77.79 o -6 7 0 27.60 61.22 61.67 o -5 7 0 49.59 54.23 58.31 o -4 7 0 123.76 81.39 62.61 o -3 7 0 1003.37 1037.42 68.30 o -2 7 0 41.72 -3.21 31.32 o -1 7 0 226.05 224.44 26.90 o 0 7 0 536.63 528.56 31.91 o 1 7 0 524.35 507.56 31.81 o 2 7 0 4.96 -28.35 30.38 o 3 7 0 406.71 366.23 36.64 o 4 7 0 13.77 0.73 50.02 o 5 7 0 382.08 394.66 53.56 o 6 7 0 306.08 287.90 35.92 o 7 7 0 486.63 508.44 75.31 o 8 7 0 38.61 39.15 137.01 o 11 7 0 36.31 72.76 208.07 o -8 8 0 21.00 -93.18 134.88 o -7 8 0 22.36 -144.24 144.24 o -6 8 0 236.38 284.28 76.08 o -5 8 0 26.14 45.36 91.27 o -4 8 0 53.07 186.17 64.31 o -3 8 0 219.14 161.69 65.90 o -2 8 0 248.45 264.04 68.75 o -1 8 0 1057.71 1108.60 65.84 o 0 8 0 1199.72 1354.51 53.76 o 1 8 0 872.79 848.54 60.37 o 2 8 0 6.42 28.96 32.43 o 3 8 0 3129.98 3343.38 101.78 o 4 8 0 1240.30 1144.93 67.21 o 5 8 0 11.67 -44.39 44.39 o 6 8 0 0.94 22.95 46.06 o 7 8 0 241.52 288.06 141.69 o 8 8 0 57.47 166.37 146.80 o -7 9 0 53.83 -74.46 172.33 o -6 9 0 5.04 -79.14 167.65 o -5 9 0 43.78 144.67 154.03 o -4 9 0 29.14 -3.35 56.50 o -3 9 0 13.84 46.93 47.06 o -2 9 0 15.77 18.33 48.45 o -1 9 0 179.41 150.22 38.40 o 0 9 0 1557.99 1608.04 68.97 o 1 9 0 208.80 297.53 41.26 o 2 9 0 4415.08 4361.42 169.08 o 3 9 0 702.53 784.38 89.48 o 4 9 0 1183.47 1048.76 155.26 o 5 9 0 61.93 -42.16 59.06 o 6 9 0 1100.13 1224.61 212.75 o 7 9 0 324.13 252.32 131.05 o 8 9 0 9.15 -107.23 146.37 o 9 9 0 1.22 131.90 180.41 o 10 9 0 4.83 19.57 185.09 o 11 9 0 34.96 -58.29 228.49 o -6 10 0 161.44 9.36 181.69 o -5 10 0 32.10 0.00 168.07 o -3 10 0 326.08 497.41 168.92 o -2 10 0 186.19 196.15 55.83 o -1 10 0 149.20 57.95 37.28 o 0 10 0 62.16 116.27 64.96 o 1 10 0 670.93 596.73 53.44 o 2 10 0 770.66 754.06 95.66 o 3 10 0 1173.96 1149.70 69.25 o 4 10 0 0.34 13.35 77.08 o 5 10 0 176.79 203.60 68.05 o 6 10 0 168.26 162.14 58.54 o 7 10 0 185.57 207.06 87.48 o 8 10 0 143.54 191.05 94.91 o -4 11 0 224.66 149.78 191.90 o -3 11 0 322.09 389.33 154.88 o -2 11 0 3.21 136.58 169.35 o -1 11 0 182.89 182.62 108.93 o 0 11 0 164.52 242.54 66.61 o 1 11 0 138.86 90.92 70.85 o 2 11 0 1136.82 1326.09 83.48 o 3 11 0 93.07 46.75 65.48 o 4 11 0 121.49 88.95 71.96 o 5 11 0 11.26 92.40 74.88 o 6 11 0 442.32 489.65 157.65 o 7 11 0 2.50 37.87 151.05 o 8 11 0 26.65 61.22 102.02 o 9 11 0 28.92 -72.33 192.33 o 10 11 0 3.09 -67.65 221.68 o -3 12 0 108.49 168.92 215.73 o -2 12 0 131.77 291.89 202.11 o -1 12 0 195.43 94.46 193.60 o 0 12 0 181.90 231.90 189.35 o 1 12 0 0.04 19.15 171.05 o 2 12 0 4.84 -8.72 78.47 o 3 12 0 99.96 104.81 89.50 o 4 12 0 220.73 271.26 115.10 o 5 12 0 303.95 277.08 107.47 o 6 12 0 1.95 161.35 184.88 o 7 12 0 322.62 259.77 117.78 o 8 12 0 3.28 -32.76 173.60 o 9 12 0 0.73 218.28 256.15 o -2 13 0 0.02 -145.95 221.26 o -1 13 0 55.22 108.50 146.37 o 0 13 0 23.23 -85.10 208.49 o 1 13 0 30.03 -199.56 209.34 o 2 13 0 241.27 491.45 205.09 o 3 13 0 195.11 268.06 191.47 o 4 13 0 29.89 -76.51 98.30 o 5 13 0 12.58 -65.13 121.48 o 6 13 0 217.86 60.12 187.86 o 7 13 0 0.57 141.67 141.90 o 8 13 0 2.23 -179.56 179.56 o 0 14 0 24.18 -189.77 194.45 o 2 14 0 23.22 234.45 172.33 o 3 14 0 19.92 -91.06 216.15 o 4 14 0 55.46 578.68 226.79 o 5 14 0 46.09 43.40 208.07 o -5 -14 1 16.02 135.73 228.07 o -3 -14 1 167.00 317.85 221.68 o -2 -14 1 76.81 38.29 230.19 o -1 -14 1 8.57 -143.39 248.49 o -7 -13 1 57.83 -65.62 131.90 o -6 -13 1 11.42 -13.95 121.57 o -5 -13 1 78.79 199.98 108.42 o -4 -13 1 28.06 81.70 192.33 o -3 -13 1 115.61 -57.44 196.58 o -2 -13 1 100.45 344.65 210.62 o -1 -13 1 23.14 171.90 214.45 o 0 -13 1 94.74 -14.47 209.34 o 1 -13 1 154.36 251.04 227.22 o 2 -13 1 1.82 -174.88 231.47 o -9 -12 1 73.50 86.38 196.58 o -8 -12 1 4.96 94.89 223.39 o -7 -12 1 35.03 113.45 137.22 o -6 -12 1 612.08 481.24 183.82 o -5 -12 1 5.04 22.55 134.46 o -4 -12 1 112.33 61.19 153.18 o -3 -12 1 40.97 41.83 84.37 o -2 -12 1 1102.00 1381.09 116.91 o -1 -12 1 44.07 90.21 185.52 o 0 -12 1 199.80 161.26 189.77 o 1 -12 1 66.83 -71.06 194.03 o 3 -12 1 45.63 -145.95 145.95 o -9 -11 1 10.78 53.19 252.32 o -8 -11 1 143.12 337.85 212.32 o -7 -11 1 204.68 240.26 192.96 o -6 -11 1 86.09 44.89 100.00 o -5 -11 1 269.31 214.77 67.00 o -4 -11 1 226.80 261.00 68.72 o -3 -11 1 260.07 376.55 67.48 o -2 -11 1 116.39 147.26 51.44 o -1 -11 1 343.75 293.85 70.23 o 0 -11 1 12.51 37.50 95.95 o 1 -11 1 256.58 274.02 170.20 o 2 -11 1 137.24 259.13 122.54 o 3 -11 1 152.09 -168.92 183.39 o 4 -11 1 9.57 -65.53 145.09 o -10 -10 1 20.56 278.28 234.45 o -8 -10 1 235.42 448.90 190.20 o -7 -10 1 0.98 -83.73 83.73 o -6 -10 1 82.49 52.70 59.99 o -5 -10 1 475.14 429.58 64.72 o -4 -10 1 70.42 137.17 78.13 o -3 -10 1 1331.62 1395.93 83.67 o -2 -10 1 102.65 86.05 107.86 o -1 -10 1 0.22 -67.88 67.88 o 0 -10 1 203.73 252.13 75.87 o 1 -10 1 471.30 452.22 65.67 o 2 -10 1 255.83 150.33 40.91 o 4 -10 1 103.47 182.54 131.05 o 5 -10 1 12.42 -130.63 177.43 o -11 -9 1 1.97 -29.36 229.34 o -10 -9 1 5.52 161.69 200.83 o -9 -9 1 0.76 250.19 191.47 o -8 -9 1 0.07 -108.08 162.11 o -7 -9 1 431.88 459.63 79.72 o -6 -9 1 121.77 207.89 58.20 o -5 -9 1 202.98 199.17 78.17 o -4 -9 1 449.63 381.68 100.59 o -3 -9 1 1543.96 1536.01 117.61 o -2 -9 1 178.68 223.77 37.77 o -1 -9 1 221.95 235.98 35.14 o 0 -9 1 1094.78 1150.23 52.81 o 1 -9 1 83.17 129.81 30.52 o 2 -9 1 203.38 184.21 36.67 o 3 -9 1 42.81 -0.88 33.93 o 4 -9 1 6.97 -27.98 59.72 o 5 -9 1 15.97 -107.23 158.71 o 6 -9 1 5.63 -60.42 172.33 o 7 -9 1 130.34 9.36 162.97 o -11 -8 1 50.94 574.42 277.42 o -10 -8 1 0.15 351.89 205.09 o -7 -8 1 571.43 511.45 152.33 o -6 -8 1 150.81 153.01 61.03 o -5 -8 1 1046.36 1002.02 63.43 o -4 -8 1 10.38 25.32 49.02 o -3 -8 1 1625.44 1651.56 84.94 o -2 -8 1 3244.30 3657.11 158.13 o -1 -8 1 1052.47 1069.10 132.73 o 0 -8 1 334.36 332.62 29.33 o 1 -8 1 2017.15 2292.47 73.66 o 2 -8 1 456.55 466.92 38.26 o 3 -8 1 324.22 373.58 40.01 o 4 -8 1 8.02 9.00 40.00 o 5 -8 1 99.77 77.60 62.45 o 6 -8 1 1.10 34.22 71.92 o 7 -8 1 14.81 79.14 153.60 o 8 -8 1 45.97 162.97 139.56 o -11 -7 1 11.23 106.80 213.17 o -10 -7 1 3.43 233.60 185.09 o -9 -7 1 329.45 371.03 165.94 o -8 -7 1 236.73 441.24 147.22 o -7 -7 1 30.66 -9.79 117.86 o -6 -7 1 94.92 147.65 108.08 o -5 -7 1 56.74 -26.16 32.59 o -4 -7 1 1193.49 1153.35 51.46 o -3 -7 1 1098.97 966.16 71.73 o -2 -7 1 20.87 -31.20 31.20 o -1 -7 1 314.77 250.78 28.54 o 0 -7 1 2813.31 3123.79 79.73 o 1 -7 1 32.62 61.28 32.80 o 2 -7 1 767.92 846.15 40.83 o 3 -7 1 2.00 21.82 48.17 o 4 -7 1 307.97 232.29 57.07 o 5 -7 1 79.33 60.58 54.29 o 6 -7 1 751.41 694.60 168.92 o 7 -7 1 28.56 -82.82 82.82 o 8 -7 1 3.38 -23.40 139.56 o -11 -6 1 21.04 -197.43 197.43 o -10 -6 1 106.98 106.37 174.03 o -9 -6 1 1.48 48.51 145.52 o -8 -6 1 215.75 355.72 146.37 o -7 -6 1 696.19 708.88 146.80 o -6 -6 1 2019.53 2161.79 215.30 o -5 -6 1 120.14 145.86 61.26 o -4 -6 1 0.57 29.84 42.54 o -3 -6 1 2.94 2.16 32.72 o -2 -6 1 10.73 62.95 26.40 o -1 -6 1 165.35 184.69 23.07 o 0 -6 1 1947.62 1855.13 93.68 o 1 -6 1 123.46 112.04 21.74 o 2 -6 1 443.51 528.39 37.56 o 3 -6 1 1434.75 1524.74 73.44 o 4 -6 1 92.64 122.18 39.92 o 5 -6 1 118.40 44.63 55.25 o 6 -6 1 4.99 -7.10 60.75 o 7 -6 1 682.66 784.63 104.03 o 8 -6 1 23.70 -22.84 79.92 o 9 -6 1 232.11 286.79 168.50 o -12 -5 1 82.61 437.84 257.00 o -9 -5 1 534.64 882.06 202.54 o -8 -5 1 209.09 227.22 101.69 o -7 -5 1 93.05 -106.80 106.80 o -6 -5 1 507.97 540.81 117.01 o -5 -5 1 1364.16 1337.32 94.57 o -4 -5 1 1062.54 1058.51 48.03 o -3 -5 1 42.86 15.57 24.30 o -2 -5 1 114.76 108.77 24.58 o -1 -5 1 0.32 -19.84 19.84 o 0 -5 1 292.34 258.95 18.51 o 1 -5 1 1057.16 1175.59 45.20 o 2 -5 1 1876.07 2085.78 74.33 o 3 -5 1 0.29 -28.37 28.37 o 4 -5 1 58.83 86.45 31.90 o 5 -5 1 703.18 729.98 49.38 o 6 -5 1 3.03 -27.30 53.06 o 7 -5 1 45.09 49.00 58.79 o 8 -5 1 119.71 27.66 96.16 o 9 -5 1 17.03 300.83 136.58 o 10 -5 1 38.42 40.85 167.65 o -12 -4 1 8.02 51.91 231.47 o -11 -4 1 70.28 -19.15 151.90 o -10 -4 1 51.99 66.80 166.80 o -9 -4 1 162.21 124.25 143.39 o -8 -4 1 998.16 983.75 144.24 o 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