#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2208246.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208246_Fobs loop_ _publ_author_name 'Wang, Chun-Xiang' 'Li, Yong' 'Zhang, Qing-Hua' 'Cai, Ding-Jian' 'Xie, Xiao-Bing' _publ_section_title ; Poly[diaquadi-\m~5~-succinato-\m~6~-succinato-didysprosium(III)] ; _journal_coeditor_code BH2001 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m545 _journal_page_last m547 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 96.915 _cell_angle_beta 97.004 _cell_angle_gamma 103.057 _cell_length_a 7.6463 _cell_length_b 8.0413 _cell_length_c 14.0861 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7632 _[local]_cod_data_source_file bh2001Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shx97 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 281.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 796.06 867.81 29.30 o 2 0 0 1238.08 1242.78 40.01 o 3 0 0 671.35 669.39 30.35 o 4 0 0 42149.20 47644.73 807.64 o 5 0 0 2331.10 2684.52 69.05 o 6 0 0 1934.95 2216.15 102.91 o 7 0 0 12053.27 12443.09 378.07 o 8 0 0 2979.64 3102.14 152.02 o -9 1 0 569.69 564.67 86.17 o -8 1 0 4847.20 5099.76 202.05 o -7 1 0 3057.47 3305.61 91.70 o -6 1 0 7215.79 7903.12 161.61 o -5 1 0 101.53 116.83 20.73 o -4 1 0 27345.31 28480.71 766.47 o -3 1 0 147.62 171.49 23.01 o -2 1 0 11360.43 11884.23 324.29 o -1 1 0 476.78 490.45 20.78 o 0 1 0 79054.93 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