#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:19:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181003 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/83/2208316.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208316_Fobs loop_ _publ_author_name 'Bolte, Michael' 'Wissler, J\"org' _publ_section_title ; Methyl 4-bromobenzoate ; _journal_coeditor_code FL2004 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1192 _journal_page_last o1193 _journal_volume 62 _journal_year 2006 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.8485 _cell_length_b 5.8921 _cell_length_c 19.6130 _exptl_crystal_F_000 848.00 _reflns_d_resolution_high 0.8400 _cod_data_source_file fl2004Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ta3 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 265.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 2852.97 2841.01 387.80 o 2 1 0 70642.52 79622.97 2312.82 o 4 1 0 29989.91 35746.07 1568.15 o 6 1 0 32172.58 34375.21 529.82 o 8 1 0 23454.15 25846.90 286.52 o 10 1 0 8904.77 9799.65 193.47 o 12 1 0 8713.64 8098.61 223.14 o 0 2 0 44919.34 50285.20 364.04 o 2 2 0 1354.30 1555.66 78.39 o 4 2 0 27263.28 28687.08 2405.05 o 6 2 0 5967.83 6913.55 157.88 o 8 2 0 8590.88 8552.90 184.61 o 10 2 0 4687.11 4517.96 155.97 o 12 2 0 1728.63 1744.97 120.83 o 14 2 0 1491.52 1370.49 124.30 o 2 3 0 4635.01 4830.71 284.18 o 4 3 0 581.47 577.83 68.34 o 6 3 0 2897.87 2934.97 138.75 o 8 3 0 1459.43 1393.64 72.35 o 10 3 0 706.42 715.74 69.00 o 12 3 0 1444.87 1366.86 83.11 o 14 3 0 42.85 44.36 86.95 o 0 4 0 5967.24 6256.70 612.77 o 2 4 0 42.83 43.06 57.92 o 4 4 0 4154.55 4336.55 72.77 o 6 4 0 75.29 76.59 50.75 o 8 4 0 1652.41 1774.42 107.07 o 10 4 0 7.73 58.37 76.98 o 12 4 0 365.54 367.82 81.44 o 2 5 0 80.69 27.57 56.80 o 4 5 0 76.63 30.49 65.33 o 6 5 0 35.06 46.79 53.56 o 8 5 0 153.15 162.89 77.85 o 10 5 0 223.52 142.82 86.92 o 0 6 0 105.60 61.29 70.17 o 2 6 0 9.17 27.61 59.53 o 4 6 0 89.23 96.00 50.62 o 6 6 0 22.93 31.19 57.07 o 8 6 0 53.87 102.23 60.57 o 1 1 1 8680.12 10645.58 181.40 o 2 1 1 4164.98 5249.83 87.91 o 3 1 1 4431.82 5058.15 85.36 o 4 1 1 6372.84 7707.76 216.61 o 5 1 1 6181.36 6908.67 169.11 o 6 1 1 505.43 646.20 79.52 o 7 1 1 858.86 969.64 129.00 o 8 1 1 2913.48 3289.99 103.63 o 9 1 1 2443.90 2714.48 104.29 o 10 1 1 9.17 5.15 92.89 o 11 1 1 86.63 95.62 102.01 o 12 1 1 452.56 416.94 105.84 o 13 1 1 759.46 649.74 137.76 o 0 2 1 11962.23 13890.50 261.15 o 1 2 1 6907.54 7948.85 261.13 o 2 2 1 60.69 72.06 64.57 o 3 2 1 9807.53 11501.64 243.89 o 4 2 1 4009.31 4396.44 67.33 o 5 2 1 1869.53 2055.62 57.28 o 6 2 1 250.79 271.49 55.40 o 7 2 1 6446.54 6960.94 123.20 o 8 2 1 128.50 131.30 66.37 o 9 2 1 197.15 192.37 67.51 o 10 2 1 224.11 258.73 72.59 o 11 2 1 2544.78 2718.72 101.93 o 12 2 1 86.24 95.09 83.31 o 13 2 1 3.29 11.58 92.58 o 14 2 1 98.87 91.51 82.05 o 15 2 1 675.21 667.61 103.52 o 1 3 1 4003.56 4114.55 69.29 o 2 3 1 11665.05 13167.76 208.69 o 3 3 1 2114.84 2291.40 51.80 o 4 3 1 527.06 566.44 46.32 o 5 3 1 3758.82 3961.18 52.41 o 6 3 1 4088.45 4338.43 145.80 o 7 3 1 282.21 266.60 50.64 o 8 3 1 666.68 683.92 48.41 o 9 3 1 2227.34 2205.04 58.25 o 10 3 1 441.72 432.69 48.48 o 11 3 1 17.48 17.62 51.70 o 12 3 1 290.50 314.42 61.73 o 13 3 1 865.06 873.26 58.81 o 14 3 1 7.12 -11.26 63.07 o 0 4 1 6416.76 6826.09 192.43 o 1 4 1 1994.00 1888.78 55.23 o 2 4 1 379.93 411.46 47.86 o 3 4 1 3010.36 2982.68 80.32 o 4 4 1 4629.80 4903.14 71.39 o 5 4 1 834.31 797.66 42.32 o 6 4 1 1668.73 1770.16 44.03 o 7 4 1 2613.02 2621.11 75.48 o 8 4 1 1884.40 1899.30 48.01 o 9 4 1 162.27 153.54 56.66 o 10 4 1 1145.74 1084.34 49.68 o 11 4 1 1383.96 1458.34 60.56 o 12 4 1 505.83 457.71 62.92 o 13 4 1 0.03 24.08 67.24 o 1 5 1 1484.57 1417.73 44.91 o 2 5 1 2416.04 2343.65 45.13 o 3 5 1 1027.77 979.44 40.36 o 4 5 1 518.97 473.93 41.42 o 5 5 1 1546.06 1593.01 43.64 o 6 5 1 1200.35 1217.45 43.56 o 7 5 1 417.55 428.94 48.58 o 8 5 1 872.36 756.86 46.84 o 9 5 1 1266.43 1281.61 49.89 o 10 5 1 301.94 282.75 50.64 o 11 5 1 86.85 87.74 52.57 o 0 6 1 1786.70 1609.68 52.88 o 1 6 1 412.11 368.75 44.74 o 2 6 1 7.95 -1.88 44.52 o 3 6 1 623.16 594.58 38.27 o 4 6 1 1199.17 1116.47 46.97 o 5 6 1 242.03 204.94 42.56 o 6 6 1 64.75 66.05 40.46 o 7 6 1 679.39 643.68 46.26 o 8 6 1 321.09 301.74 46.39 o 1 0 2 2115.27 1248.96 528.44 o 2 0 2 16.59 3.26 192.79 o 3 0 2 7831.75 6960.43 286.86 o 4 0 2 667.60 527.07 156.80 o 5 0 2 958.36 780.86 124.69 o 6 0 2 15.44 20.98 127.44 o 7 0 2 14496.39 13444.45 2752.46 o 8 0 2 2255.69 2187.27 494.04 o 9 0 2 145.52 136.02 193.44 o 1 1 2 28018.81 30016.09 489.45 o 2 1 2 4586.14 5605.99 101.43 o 3 1 2 25673.44 28568.71 434.33 o 4 1 2 72.89 72.46 73.98 o 5 1 2 17787.50 18462.77 486.90 o 6 1 2 143.03 192.94 71.49 o 7 1 2 8347.28 9401.23 303.99 o 8 1 2 61.87 74.76 93.42 o 9 1 2 10258.18 10950.78 481.23 o 10 1 2 69.89 61.28 87.90 o 11 1 2 759.92 775.06 101.24 o 12 1 2 280.27 272.76 107.61 o 13 1 2 4670.78 4313.69 345.50 o 0 2 2 4645.25 4816.46 368.96 o 1 2 2 11462.95 12403.31 274.24 o 2 2 2 937.39 1129.42 66.38 o 3 2 2 18407.85 19813.43 510.26 o 4 2 2 1650.04 1709.91 64.98 o 5 2 2 4345.47 4752.53 99.89 o 6 2 2 2549.62 3000.62 65.21 o 7 2 2 16635.86 17890.10 414.44 o 8 2 2 107.75 94.72 57.15 o 9 2 2 1057.62 1133.47 66.96 o 10 2 2 930.98 969.42 73.19 o 11 2 2 9341.81 9764.57 116.73 o 12 2 2 10.77 3.66 82.65 o 13 2 2 101.31 78.78 82.77 o 14 2 2 33.19 36.48 91.04 o 15 2 2 3568.25 3507.71 159.49 o 1 3 2 11080.03 12560.19 429.65 o 2 3 2 2609.50 3032.87 67.83 o 3 3 2 7231.32 7701.53 257.18 o 4 3 2 231.81 213.37 50.68 o 5 3 2 8857.63 9201.43 168.38 o 6 3 2 230.15 278.73 53.48 o 7 3 2 2203.38 2309.94 59.40 o 8 3 2 203.84 202.81 52.27 o 9 3 2 5116.32 4648.07 251.72 o 10 3 2 75.73 61.40 44.03 o 11 3 2 329.99 258.06 52.73 o 12 3 2 51.53 111.27 62.91 o 13 3 2 2224.82 2147.00 101.48 o 14 3 2 187.34 177.85 62.38 o 0 4 2 7.70 30.68 59.19 o 1 4 2 572.18 531.44 51.76 o 2 4 2 4.22 42.96 41.28 o 3 4 2 1307.98 1279.93 55.35 o 4 4 2 5.95 1.78 40.71 o 5 4 2 67.44 62.78 45.31 o 6 4 2 8.19 19.98 45.04 o 7 4 2 1207.21 1227.43 50.92 o 8 4 2 8.53 71.51 53.29 o 9 4 2 8.31 39.45 49.10 o 10 4 2 10.09 31.71 51.18 o 11 4 2 659.86 628.52 55.28 o 12 4 2 17.76 -31.53 56.29 o 13 4 2 89.42 98.85 73.67 o 1 5 2 145.31 173.77 37.90 o 2 5 2 0.47 31.72 36.80 o 3 5 2 108.58 121.44 39.38 o 4 5 2 3.11 -29.12 37.06 o 5 5 2 61.80 98.74 41.53 o 6 5 2 28.78 18.23 42.07 o 7 5 2 10.73 51.76 45.63 o 8 5 2 9.37 31.26 51.61 o 9 5 2 14.69 15.01 48.77 o 10 5 2 105.15 121.34 49.92 o 11 5 2 13.44 23.20 49.56 o 0 6 2 0.12 58.81 54.96 o 1 6 2 204.95 204.33 40.17 o 2 6 2 13.08 9.89 42.16 o 3 6 2 89.82 34.19 40.94 o 4 6 2 6.47 11.01 37.77 o 5 6 2 160.69 176.68 38.68 o 6 6 2 39.22 50.65 43.20 o 7 6 2 5.80 9.22 45.50 o 8 6 2 30.87 28.40 43.36 o 1 1 3 602.52 644.62 69.75 o 2 1 3 428.63 402.90 72.61 o 3 1 3 1580.86 1644.93 109.82 o 4 1 3 2122.03 2345.71 71.32 o 5 1 3 190.27 195.48 60.86 o 6 1 3 203.83 126.42 69.78 o 7 1 3 1118.13 1129.81 71.50 o 8 1 3 575.19 667.04 78.58 o 9 1 3 167.43 197.77 79.46 o 10 1 3 23.23 35.11 94.46 o 11 1 3 321.71 290.15 97.48 o 12 1 3 3.34 9.39 109.76 o 13 1 3 137.24 120.60 123.49 o 14 1 3 16.83 16.45 205.99 o 0 2 3 993.55 863.88 89.73 o 1 2 3 31.59 109.29 62.67 o 2 2 3 5.64 -0.11 54.49 o 3 2 3 16.28 22.99 58.14 o 4 2 3 2168.65 1969.16 64.69 o 5 2 3 118.85 137.45 60.16 o 6 2 3 6.69 47.61 48.48 o 7 2 3 513.87 504.03 54.80 o 8 2 3 3022.47 3184.68 73.07 o 9 2 3 199.50 236.61 57.99 o 10 2 3 148.50 162.11 59.68 o 11 2 3 817.66 812.97 75.10 o 12 2 3 1751.28 1728.84 87.32 o 13 2 3 103.62 119.32 104.63 o 14 2 3 282.17 316.76 86.11 o 15 2 3 406.00 374.63 100.83 o 1 3 3 533.30 400.50 59.60 o 2 3 3 4428.14 4299.56 165.68 o 3 3 3 1039.28 998.85 54.34 o 4 3 3 435.77 516.28 51.33 o 5 3 3 350.79 361.10 57.87 o 6 3 3 5404.88 5770.37 84.16 o 7 3 3 743.13 747.75 49.78 o 8 3 3 939.16 979.57 50.91 o 9 3 3 329.22 367.92 58.45 o 10 3 3 4724.31 4548.11 275.51 o 11 3 3 133.19 145.89 57.56 o 12 3 3 899.02 863.10 61.19 o 13 3 3 219.34 207.61 66.90 o 14 3 3 2215.83 2021.93 89.44 o 0 4 3 13093.34 13228.73 236.02 o 1 4 3 235.98 213.34 44.39 o 2 4 3 6.45 39.94 43.38 o 3 4 3 302.85 269.19 50.55 o 4 4 3 9743.31 9676.92 245.72 o 5 4 3 126.16 145.13 43.44 o 6 4 3 10.82 37.93 48.43 o 7 4 3 351.84 386.13 45.04 o 8 4 3 4194.62 4312.92 115.85 o 9 4 3 5.27 42.97 44.12 o 10 4 3 191.22 191.94 49.80 o 11 4 3 297.05 317.40 50.62 o 12 4 3 1089.82 1090.54 54.52 o 13 4 3 47.77 57.11 60.77 o 1 5 3 640.95 597.31 50.28 o 2 5 3 3983.98 4027.91 78.02 o 3 5 3 286.68 302.88 43.10 o 4 5 3 440.94 433.29 43.47 o 5 5 3 883.10 905.29 43.86 o 6 5 3 2735.94 2598.79 66.56 o 7 5 3 98.72 129.56 46.29 o 8 5 3 949.29 950.82 44.56 o 9 5 3 778.97 760.63 46.79 o 10 5 3 1142.95 1071.54 49.40 o 11 5 3 34.74 27.81 48.12 o 0 6 3 4544.98 4150.17 216.34 o 1 6 3 259.98 240.44 38.91 o 2 6 3 70.13 102.47 46.09 o 3 6 3 442.99 406.40 42.29 o 4 6 3 3366.76 3165.13 62.80 o 5 6 3 113.84 85.82 41.36 o 6 6 3 392.72 368.02 44.20 o 7 6 3 483.94 448.65 46.26 o 8 6 3 1389.15 1321.92 47.88 o 0 0 4 15002.95 9426.19 298.04 o 1 0 4 527.71 438.94 132.29 o 2 0 4 983.97 714.57 130.34 o 3 0 4 137.07 10.07 146.47 o 4 0 4 21206.04 17215.73 1795.99 o 5 0 4 1694.50 1809.37 194.71 o 6 0 4 3904.29 3434.30 488.93 o 7 0 4 534.39 424.01 126.63 o 8 0 4 17462.30 15269.82 2364.90 o 9 0 4 739.07 832.75 112.27 o 10 0 4 4195.36 4480.51 414.42 o 11 0 4 306.00 324.71 166.69 o 1 1 4 4427.52 4412.69 210.49 o 2 1 4 38241.54 37855.71 946.73 o 3 1 4 2231.13 2290.65 78.94 o 4 1 4 327.75 297.71 63.53 o 5 1 4 2123.87 1973.34 70.56 o 6 1 4 18266.38 17398.67 1124.94 o 7 1 4 444.94 423.92 67.40 o 8 1 4 1674.71 1665.21 71.01 o 9 1 4 332.96 300.46 69.35 o 10 1 4 6873.54 6913.60 292.52 o 11 1 4 12.39 -4.32 92.12 o 12 1 4 2020.40 2087.76 226.53 o 13 1 4 17.24 24.19 118.01 o 14 1 4 1584.39 1621.93 259.54 o 0 2 4 20540.33 21241.65 693.58 o 1 2 4 277.22 272.24 60.09 o 2 2 4 103.44 92.98 59.52 o 3 2 4 1574.27 1620.94 56.58 o 4 2 4 13775.01 14602.00 196.56 o 5 2 4 257.52 325.88 55.05 o 6 2 4 635.63 599.32 48.87 o 7 2 4 1429.94 1440.66 51.65 o 8 2 4 4378.16 4441.57 132.43 o 9 2 4 433.19 443.25 52.71 o 10 2 4 1277.96 1299.30 58.51 o 11 2 4 551.12 519.47 62.88 o 12 2 4 594.45 617.14 67.55 o 13 2 4 151.44 179.27 71.33 o 14 2 4 1298.23 1328.70 76.54 o 15 2 4 71.72 89.33 79.16 o 1 3 4 2726.15 2964.54 56.71 o 2 3 4 7271.54 7235.95 284.45 o 3 3 4 1571.42 1516.71 63.53 o 4 3 4 1775.21 1901.73 51.47 o 5 3 4 1230.76 1228.39 49.16 o 6 3 4 3762.92 3660.29 97.53 o 7 3 4 146.63 142.69 46.84 o 8 3 4 2730.75 2833.28 110.35 o 9 3 4 64.23 64.50 47.81 o 10 3 4 1222.28 1204.35 51.17 o 11 3 4 87.83 97.57 54.60 o 12 3 4 1357.64 1206.79 136.06 o 13 3 4 33.47 30.66 63.92 o 14 3 4 213.74 212.63 66.82 o 0 4 4 4408.92 4753.30 173.62 o 1 4 4 18.50 8.63 43.67 o 2 4 4 237.07 262.01 45.95 o 3 4 4 276.02 235.89 41.63 o 4 4 4 3230.31 3444.97 84.27 o 5 4 4 484.74 480.93 45.78 o 6 4 4 1121.25 1169.57 50.49 o 7 4 4 591.92 561.92 43.19 o 8 4 4 1056.69 1004.98 52.14 o 9 4 4 500.03 544.86 47.59 o 10 4 4 856.00 863.95 48.30 o 11 4 4 284.84 264.98 52.70 o 12 4 4 143.60 124.39 55.51 o 13 4 4 134.37 131.52 57.90 o 1 5 4 418.15 416.31 45.15 o 2 5 4 1127.02 1141.22 40.42 o 3 5 4 163.16 155.80 41.97 o 4 5 4 152.00 181.60 43.66 o 5 5 4 450.04 390.96 43.45 o 6 5 4 247.95 255.65 40.28 o 7 5 4 29.00 47.87 41.88 o 8 5 4 217.19 195.61 44.05 o 9 5 4 190.91 164.22 49.15 o 10 5 4 1.08 21.47 44.38 o 11 5 4 3.92 39.71 47.88 o 0 6 4 43.42 72.22 62.92 o 1 6 4 280.66 194.17 43.39 o 2 6 4 8.04 33.17 41.67 o 3 6 4 120.65 141.42 39.54 o 4 6 4 6.17 21.90 37.56 o 5 6 4 204.00 198.84 39.01 o 6 6 4 19.41 36.24 43.50 o 7 6 4 7.64 14.62 43.10 o 8 6 4 26.79 -1.96 50.25 o 1 1 5 5265.01 5352.97 193.62 o 2 1 5 3045.10 2991.53 112.82 o 3 1 5 3781.04 4098.86 141.76 o 4 1 5 76.94 81.13 62.78 o 5 1 5 2876.90 3024.53 149.06 o 6 1 5 974.99 993.06 60.99 o 7 1 5 1003.75 1074.54 57.02 o 8 1 5 1.01 4.65 62.56 o 9 1 5 1185.02 1243.80 67.98 o 10 1 5 57.13 60.04 71.16 o 11 1 5 161.56 175.03 82.66 o 12 1 5 53.41 37.78 100.42 o 13 1 5 391.59 348.20 107.60 o 14 1 5 12.88 26.10 125.37 o 15 1 5 22.93 52.06 212.89 o 0 2 5 1618.76 1685.43 90.90 o 1 2 5 3098.45 3186.88 68.69 o 2 2 5 128.80 195.18 59.41 o 3 2 5 4539.42 5000.94 80.23 o 4 2 5 1333.22 1294.28 51.57 o 5 2 5 796.17 896.94 56.32 o 6 2 5 599.11 625.34 57.33 o 7 2 5 3293.64 3167.21 120.05 o 8 2 5 808.01 765.04 57.16 o 9 2 5 31.89 40.56 50.22 o 10 2 5 560.61 513.21 55.14 o 11 2 5 1490.53 1597.71 63.49 o 12 2 5 315.07 312.78 65.62 o 13 2 5 35.08 33.18 58.12 o 14 2 5 299.19 285.28 67.53 o 15 2 5 516.16 557.20 65.19 o 1 3 5 7844.27 8184.03 182.27 o 2 3 5 2623.11 2731.80 51.03 o 3 3 5 3819.16 3749.60 141.33 o 4 3 5 263.97 270.47 42.02 o 5 3 5 7329.97 7813.05 216.27 o 6 3 5 1741.14 1768.56 54.48 o 7 3 5 824.16 873.02 50.42 o 8 3 5 389.72 439.32 54.76 o 9 3 5 3777.84 3961.63 125.24 o 10 3 5 906.75 909.25 55.45 o 11 3 5 46.74 57.28 59.36 o 12 3 5 321.42 348.82 61.18 o 13 3 5 1251.22 1369.56 66.04 o 14 3 5 290.41 236.36 60.54 o 0 4 5 3026.48 3097.35 145.50 o 1 4 5 2830.77 2713.26 100.63 o 2 4 5 7.65 -4.55 45.52 o 3 4 5 6731.67 6824.02 171.55 o 4 4 5 2474.66 2326.52 70.83 o 5 4 5 389.63 410.93 41.25 o 6 4 5 65.61 99.93 42.87 o 7 4 5 7271.35 7210.24 158.70 o 8 4 5 1349.94 1411.61 53.08 o 9 4 5 7.84 57.34 48.06 o 10 4 5 130.67 156.99 47.50 o 11 4 5 4093.66 3704.79 160.83 o 12 4 5 466.58 464.13 54.93 o 13 4 5 0.39 32.05 65.21 o 1 5 5 8822.45 9050.09 161.65 o 2 5 5 1939.21 1941.08 40.80 o 3 5 5 6565.59 6557.90 153.41 o 4 5 5 3.06 6.30 33.91 o 5 5 5 5938.69 5885.01 182.78 o 6 5 5 1119.71 1043.90 45.77 o 7 5 5 2141.32 2061.19 55.96 o 8 5 5 28.90 66.92 42.05 o 9 5 5 2260.36 2219.31 49.97 o 10 5 5 345.84 300.47 51.12 o 0 6 5 157.73 175.89 56.90 o 1 6 5 1074.40 1064.81 39.27 o 2 6 5 46.78 93.82 41.66 o 3 6 5 2216.05 2090.75 97.36 o 4 6 5 116.83 126.38 37.39 o 5 6 5 150.06 129.08 44.28 o 6 6 5 233.46 243.65 42.89 o 7 6 5 2217.94 2128.32 46.88 o 0 0 6 13090.01 9389.16 579.58 o 1 0 6 24609.46 18184.94 753.59 o 2 0 6 38.57 10.55 101.98 o 3 0 6 32480.34 24664.08 2405.75 o 4 0 6 8677.45 8003.91 980.43 o 5 0 6 5622.48 4662.70 239.39 o 6 0 6 65.50 55.57 101.71 o 7 0 6 18540.12 15776.41 1303.05 o 8 0 6 2437.35 2236.68 240.77 o 9 0 6 85.08 77.49 103.10 o 10 0 6 146.87 129.83 115.88 o 11 0 6 6323.32 6159.31 404.78 o 12 0 6 309.43 299.62 114.78 o 13 0 6 273.05 314.18 178.52 o 1 1 6 17854.42 18158.41 560.75 o 2 1 6 3094.69 2775.04 67.15 o 3 1 6 4449.50 4300.12 113.54 o 4 1 6 698.60 703.83 73.46 o 5 1 6 21455.25 19763.70 935.42 o 6 1 6 1635.30 1380.30 64.04 o 7 1 6 172.99 165.66 59.48 o 8 1 6 1249.65 1233.40 55.86 o 9 1 6 11648.86 11375.40 253.86 o 10 1 6 875.31 834.17 68.24 o 11 1 6 89.85 98.75 68.90 o 12 1 6 672.07 668.35 85.07 o 13 1 6 3562.25 3599.33 535.78 o 14 1 6 292.55 280.12 123.88 o 15 1 6 151.00 193.22 175.35 o 0 2 6 2124.77 2170.74 69.08 o 1 2 6 10214.60 10928.23 184.15 o 2 2 6 0.69 51.72 52.51 o 3 2 6 11907.04 12289.81 314.87 o 4 2 6 2404.65 2355.66 64.46 o 5 2 6 3309.67 3507.46 160.65 o 6 2 6 44.12 62.76 48.54 o 7 2 6 7088.22 7311.56 206.54 o 8 2 6 1460.02 1362.23 58.65 o 9 2 6 282.94 289.62 51.68 o 10 2 6 194.79 181.30 49.09 o 11 2 6 2771.86 2896.01 89.12 o 12 2 6 451.68 433.83 56.82 o 13 2 6 13.62 25.83 70.89 o 14 2 6 187.09 215.68 60.54 o 15 2 6 688.02 747.68 89.51 o 1 3 6 2737.39 3003.86 57.61 o 2 3 6 1118.63 1122.18 45.34 o 3 3 6 1667.04 1715.29 49.62 o 4 3 6 30.84 137.80 47.61 o 5 3 6 2231.93 2326.82 47.21 o 6 3 6 1224.05 1222.84 50.51 o 7 3 6 397.71 375.60 46.68 o 8 3 6 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43.59 44.32 o 3 5 12 24.93 69.65 39.07 o 4 5 12 16.38 23.71 34.23 o 5 5 12 34.62 44.55 34.97 o 6 5 12 31.92 45.44 41.43 o 7 5 12 25.26 67.59 41.73 o 0 6 12 7.27 84.12 90.15 o 1 6 12 40.43 34.67 86.82 o 1 1 13 941.45 748.22 55.65 o 2 1 13 513.17 430.30 53.89 o 3 1 13 364.44 253.89 51.68 o 4 1 13 21.32 49.41 48.30 o 5 1 13 721.66 576.24 54.46 o 6 1 13 2.96 73.07 58.57 o 7 1 13 6.24 79.56 52.98 o 8 1 13 27.55 67.66 50.14 o 9 1 13 191.98 208.28 46.16 o 10 1 13 212.74 190.46 51.33 o 11 1 13 74.66 93.13 51.00 o 12 1 13 2.59 29.63 47.67 o 13 1 13 18.29 30.70 51.08 o 0 2 13 117.39 159.96 69.01 o 1 2 13 2307.28 2328.89 62.03 o 2 2 13 157.33 137.48 49.06 o 3 2 13 3560.88 3360.35 79.23 o 4 2 13 67.11 106.61 47.90 o 5 2 13 425.21 453.11 49.39 o 6 2 13 623.07 578.76 45.11 o 7 2 13 2405.21 2407.28 101.30 o 8 2 13 9.49 -8.88 44.33 o 9 2 13 2.01 27.25 50.94 o 10 2 13 320.78 310.66 53.53 o 11 2 13 920.62 942.34 48.50 o 12 2 13 0.32 8.72 48.00 o 1 3 13 4075.26 4262.10 162.12 o 2 3 13 1231.17 1219.27 46.59 o 3 3 13 1448.53 1417.49 48.64 o 4 3 13 242.62 229.74 41.85 o 5 3 13 5181.46 5337.87 200.70 o 6 3 13 607.16 659.43 42.28 o 7 3 13 241.89 256.09 44.93 o 8 3 13 312.03 267.05 44.65 o 9 3 13 3452.18 3525.61 150.37 o 10 3 13 163.43 151.17 46.62 o 11 3 13 25.88 35.83 45.71 o 0 4 13 1258.47 1244.22 51.98 o 1 4 13 2743.92 2626.09 49.92 o 2 4 13 13.36 12.37 40.37 o 3 4 13 3254.47 3012.73 52.86 o 4 4 13 724.86 745.16 37.29 o 5 4 13 1262.05 1255.06 39.23 o 6 4 13 58.28 90.38 40.11 o 7 4 13 2331.08 2458.30 89.10 o 8 4 13 97.69 88.36 40.40 o 9 4 13 250.74 260.69 48.30 o 1 5 13 1054.57 1022.20 39.97 o 2 5 13 367.85 416.58 38.34 o 3 5 13 699.38 740.12 39.88 o 4 5 13 43.77 48.78 39.38 o 5 5 13 1084.70 1138.91 36.67 o 6 5 13 151.11 174.62 40.18 o 7 5 13 246.74 215.61 111.97 o 0 0 14 8404.50 8662.29 549.21 o 1 0 14 5010.03 5039.14 338.40 o 2 0 14 1588.80 1782.09 69.50 o 3 0 14 6092.60 6516.37 151.10 o 4 0 14 6353.18 6319.73 181.80 o 5 0 14 2528.73 2398.15 184.71 o 6 0 14 6975.99 6534.24 372.55 o 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15 89.76 87.83 39.98 o 2 5 15 3864.66 3821.63 98.88 o 3 5 15 79.32 91.64 38.35 o 4 5 15 186.94 138.47 39.04 o 0 0 16 222.43 288.52 99.67 o 1 0 16 5421.49 6026.83 83.15 o 2 0 16 183.25 213.49 62.71 o 3 0 16 3711.92 3812.45 121.06 o 4 0 16 137.15 168.07 79.70 o 5 0 16 4149.13 4013.40 213.27 o 6 0 16 800.34 841.95 68.86 o 7 0 16 1950.08 1823.57 76.53 o 8 0 16 49.04 93.41 80.81 o 9 0 16 1283.01 1346.01 71.12 o 10 0 16 511.16 475.83 80.77 o 11 0 16 1088.39 1160.03 83.59 o 1 1 16 1000.30 954.10 49.03 o 2 1 16 944.86 889.50 47.70 o 3 1 16 284.70 256.92 46.42 o 4 1 16 154.67 133.01 43.41 o 5 1 16 2284.94 2049.27 54.98 o 6 1 16 356.09 375.05 49.54 o 7 1 16 82.27 110.15 46.53 o 8 1 16 236.61 214.93 50.86 o 9 1 16 2679.80 2664.92 76.77 o 10 1 16 28.82 26.46 55.91 o 11 1 16 9.09 29.93 57.05 o 0 2 16 3323.39 2820.61 95.96 o 1 2 16 2060.14 1712.38 50.70 o 2 2 16 0.21 4.48 50.21 o 3 2 16 2235.20 1985.96 79.36 o 4 2 16 2194.34 2029.14 106.55 o 5 2 16 1197.24 1091.08 63.53 o 6 2 16 2.81 11.42 50.05 o 7 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4151.76 4486.37 208.55 o 2 1 20 65.92 34.10 39.54 o 3 1 20 1941.04 2243.85 48.14 o 4 1 20 5.98 34.01 38.70 o 5 1 20 4193.67 4459.58 141.46 o 6 1 20 22.61 51.53 54.78 o 7 1 20 304.09 384.88 45.14 o 8 1 20 12.40 65.10 61.77 o 0 2 20 3.57 6.91 79.89 o 1 2 20 1581.17 1491.71 59.05 o 2 2 20 1.29 13.84 45.21 o 3 2 20 2223.41 2227.59 85.63 o 4 2 20 1.21 16.28 40.00 o 5 2 20 493.27 453.80 46.23 o 6 2 20 3.97 80.38 53.94 o 7 2 20 1711.87 1886.03 90.19 o 1 3 20 647.05 624.76 47.23 o 2 3 20 0.04 -35.92 46.79 o 3 3 20 288.17 249.37 47.23 o 4 3 20 35.57 55.80 43.04 o 1 1 21 145.11 204.93 35.06 o 2 1 21 488.65 593.36 41.27 o 3 1 21 92.95 114.19 41.84 o 4 1 21 7.17 8.97 45.62 o 5 1 21 104.34 93.72 45.69 o 6 1 21 190.34 234.29 41.55 o 0 2 21 300.34 327.10 66.64 o 1 2 21 138.99 190.47 49.62 o 2 2 21 31.66 40.61 43.19 o 3 2 21 362.83 369.75 39.04 o 4 2 21 190.21 225.48 44.11 o 5 2 21 18.06 26.77 42.21 o 1 3 21 608.24 588.69 126.49 o 0 0 22 3812.06 4557.82 109.12 o 1 0 22 93.60 127.22 45.69 o 2 0 22 48.19 94.86 57.75 o 3 0 22 72.82 121.78 54.91 o 4 0 22 3043.80 3574.33 151.34 o 5 0 22 55.16 137.10 72.48 o 1 1 22 3.18 31.47 35.57 o 2 1 22 3380.78 4152.75 80.25 o 3 1 22 1.98 18.80 43.28 o 4 1 22 170.60 168.81 39.21 o 5 1 22 33.71 45.64 102.80 o 0 2 22 2534.96 2817.49 74.87 o 1 2 22 15.32 64.72 40.83 o 2 2 22 19.16 -3.49 41.11 o 1 1 23 2.88 22.42 48.59 o