#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:19:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181003 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/83/2208344.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208344_Fobs loop_ _publ_author_name 'Song, Yan-Wei' 'Yu, Zhan' 'Zhang, Qian-Feng' _publ_section_title ; Tetraethylammonium dichlorotris(2,6-dimethylphenylsulfanyl-\kS)ruthenium dichloromethane solvate ; _journal_coeditor_code HG6298 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m454 _journal_page_last m456 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.162 _cell_angle_gamma 90.000 _cell_length_a 13.9279 _cell_length_b 12.4525 _cell_length_c 21.2361 _exptl_crystal_F_000 1656.00 _reflns_d_resolution_high 0.7487 _cod_data_source_file hg6298Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zhang2 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 334.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9133.45 9023.68 174.83 o 2 0 0 67233.32 60715.07 4400.77 o 3 0 0 152.18 184.83 151.89 o 4 0 0 29947.63 28280.14 2603.64 o 5 0 0 34287.85 32664.58 2109.98 o 6 0 0 3808.56 3907.28 311.39 o 7 0 0 4622.46 3910.17 467.62 o 8 0 0 28654.92 28045.20 1004.09 o 9 0 0 53.70 -234.77 314.66 o 10 0 0 2372.86 2968.58 748.43 o 11 0 0 5794.06 6458.06 919.67 o 12 0 0 522.16 335.90 819.08 o 13 0 0 84.88 -172.44 783.16 o 14 0 0 119.44 41.31 850.22 o 15 0 0 380.78 228.72 917.28 o 16 0 0 1279.34 205.97 933.44 o 17 0 0 7.95 -690.95 1019.06 o 1 1 0 39384.83 44941.81 842.79 o 2 1 0 3718.00 3734.06 122.65 o 3 1 0 1518.60 1849.23 141.56 o 4 1 0 11813.50 10632.03 283.60 o 5 1 0 14151.07 13519.23 449.08 o 6 1 0 22275.86 19578.02 885.65 o 7 1 0 9360.93 8798.07 307.77 o 8 1 0 1437.69 1429.96 219.66 o 9 1 0 4436.00 4486.78 282.86 o 10 1 0 209.53 581.98 683.77 o 11 1 0 2378.62 3036.81 594.20 o 12 1 0 215.62 412.13 574.27 o 13 1 0 1331.22 870.93 572.53 o 14 1 0 152.36 -132.19 589.01 o 15 1 0 345.65 -332.10 633.70 o 16 1 0 221.05 -628.74 628.74 o 17 1 0 661.61 -427.35 706.07 o 0 2 0 14694.47 15315.59 182.49 o 1 2 0 1607.70 1740.35 95.00 o 2 2 0 48522.21 51085.90 835.79 o 3 2 0 553.34 613.58 149.17 o 4 2 0 4868.72 4380.54 193.95 o 5 2 0 9610.73 9640.06 303.94 o 6 2 0 1.69 -87.72 138.41 o 7 2 0 8202.17 8177.56 280.33 o 8 2 0 4365.39 4051.50 255.77 o 9 2 0 80.02 -102.63 228.10 o 10 2 0 2880.66 2819.97 380.59 o 11 2 0 1200.73 1076.44 563.10 o 12 2 0 7107.95 7904.98 710.20 o 13 2 0 3918.44 4129.04 649.14 o 14 2 0 1672.33 1465.71 644.77 o 15 2 0 1163.78 573.00 648.81 o 16 2 0 2336.80 1673.37 699.21 o 17 2 0 83.68 -684.28 684.28 o 1 3 0 8174.03 7956.33 413.02 o 2 3 0 2447.21 2741.20 192.59 o 3 3 0 52923.58 54848.88 1025.06 o 4 3 0 6604.27 6428.31 232.93 o 5 3 0 137.11 111.38 128.62 o 6 3 0 3851.59 3967.95 219.54 o 7 3 0 16463.46 16266.01 415.17 o 8 3 0 800.95 738.70 209.94 o 9 3 0 3512.44 3714.39 292.62 o 10 3 0 22.99 147.16 336.79 o 11 3 0 11223.79 11951.54 1201.68 o 12 3 0 1315.08 1009.91 577.74 o 13 3 0 399.53 152.09 579.70 o 14 3 0 861.81 514.62 619.87 o 15 3 0 3969.07 4301.62 753.08 o 16 3 0 19.45 -642.28 642.28 o 17 3 0 884.57 434.02 739.74 o 0 4 0 7199.14 7663.55 236.33 o 1 4 0 3636.96 3668.94 187.28 o 2 4 0 6601.80 6507.44 296.57 o 3 4 0 20950.00 22424.44 749.03 o 4 4 0 173.06 209.90 154.29 o 5 4 0 6003.42 5375.29 257.58 o 6 4 0 8316.05 8199.16 273.84 o 7 4 0 4360.33 4277.61 253.33 o 8 4 0 1312.22 1357.25 237.11 o 9 4 0 2784.69 2641.85 367.93 o 10 4 0 234.22 110.73 346.32 o 11 4 0 274.87 898.33 538.88 o 12 4 0 349.62 264.72 522.52 o 13 4 0 3017.31 2874.08 647.03 o 14 4 0 1720.49 1372.30 655.19 o 15 4 0 759.73 547.41 659.79 o 16 4 0 47.39 -581.09 886.44 o 17 4 0 556.81 -704.70 704.70 o 1 5 0 50219.97 53695.14 961.01 o 2 5 0 12732.57 12795.67 307.66 o 3 5 0 3335.60 3482.72 230.19 o 4 5 0 10084.12 9741.48 329.21 o 5 5 0 2412.70 2452.45 243.15 o 6 5 0 14652.28 14373.29 446.06 o 7 5 0 7896.42 7834.82 314.87 o 8 5 0 4.39 -22.84 229.69 o 9 5 0 2942.35 3166.52 385.54 o 10 5 0 217.34 9.67 369.08 o 11 5 0 913.13 1001.51 525.44 o 12 5 0 50.48 199.07 509.22 o 13 5 0 87.54 -52.76 550.82 o 14 5 0 880.77 374.85 639.60 o 15 5 0 2.05 -629.17 629.17 o 16 5 0 104.54 -559.30 647.98 o 17 5 0 54.05 -452.71 706.72 o 0 6 0 69700.39 72801.19 592.88 o 1 6 0 8844.21 9291.84 230.00 o 2 6 0 4155.22 4199.65 236.19 o 3 6 0 2659.72 2467.19 234.27 o 4 6 0 8262.01 8552.77 346.09 o 5 6 0 19183.91 19061.42 448.45 o 6 6 0 3137.97 3447.52 309.48 o 7 6 0 1698.27 2097.31 288.55 o 8 6 0 2057.76 2369.41 287.23 o 9 6 0 528.33 477.66 357.46 o 10 6 0 271.12 282.79 365.74 o 11 6 0 3714.89 3307.71 410.02 o 12 6 0 57.81 -44.98 503.51 o 13 6 0 500.91 868.82 566.16 o 14 6 0 14.90 -517.81 612.16 o 15 6 0 14.14 -615.14 643.05 o 16 6 0 7.07 -369.48 701.15 o 17 6 0 0.12 -1023.25 1023.25 o 1 7 0 549.63 659.40 138.71 o 2 7 0 8829.73 8976.26 259.11 o 3 7 0 4.17 31.14 203.90 o 4 7 0 7068.04 7278.07 373.27 o 5 7 0 7090.06 7182.22 400.33 o 6 7 0 16987.98 17309.52 508.71 o 7 7 0 20.71 -259.39 259.39 o 8 7 0 1326.49 1490.83 285.06 o 9 7 0 1024.88 731.15 360.49 o 10 7 0 466.08 713.41 352.48 o 11 7 0 326.18 101.22 349.02 o 12 7 0 2599.59 2533.57 579.38 o 13 7 0 1256.91 1563.48 822.08 o 14 7 0 3373.18 2907.58 651.64 o 15 7 0 59.60 -640.71 640.71 o 16 7 0 45.33 -308.23 686.41 o 0 8 0 145.03 -118.28 232.46 o 1 8 0 3942.48 3626.15 231.46 o 2 8 0 279.85 44.65 160.91 o 3 8 0 86.39 43.14 247.54 o 4 8 0 2588.72 2775.21 325.95 o 5 8 0 332.31 70.78 281.40 o 6 8 0 517.49 443.95 310.93 o 7 8 0 1505.94 1884.22 340.73 o 8 8 0 45.09 -21.30 295.56 o 9 8 0 196.27 -6.91 326.96 o 10 8 0 568.18 790.03 358.10 o 11 8 0 77.33 -193.80 363.39 o 12 8 0 811.81 411.04 618.80 o 13 8 0 1812.21 1862.80 572.88 o 14 8 0 281.55 -156.87 723.28 o 15 8 0 440.53 -154.48 932.25 o 1 9 0 2.78 46.64 207.62 o 2 9 0 5170.08 5267.45 292.52 o 3 9 0 1260.82 1304.76 241.84 o 4 9 0 192.52 43.02 290.98 o 5 9 0 1871.87 2060.93 349.62 o 6 9 0 2274.89 2426.05 368.72 o 7 9 0 9789.79 9362.99 489.19 o 8 9 0 301.81 234.22 284.07 o 9 9 0 2.68 -85.65 324.93 o 10 9 0 1088.61 922.64 440.18 o 11 9 0 49.45 -8.57 420.57 o 12 9 0 1353.16 577.79 672.39 o 13 9 0 34.20 -337.09 649.64 o 14 9 0 1296.22 1064.57 808.31 o 15 9 0 546.17 -542.46 766.39 o 0 10 0 53.19 283.21 501.75 o 1 10 0 4112.05 4596.04 487.75 o 2 10 0 4406.50 4812.40 384.49 o 3 10 0 2420.58 2627.00 350.69 o 4 10 0 732.31 643.59 280.77 o 5 10 0 1670.29 1621.07 411.07 o 6 10 0 793.02 784.18 374.75 o 7 10 0 269.44 238.71 372.45 o 8 10 0 398.46 589.38 358.47 o 9 10 0 4106.77 4365.01 534.44 o 10 10 0 2028.12 2054.03 641.26 o 11 10 0 445.18 402.12 444.39 o 12 10 0 2.29 -487.38 605.33 o 13 10 0 1472.31 1063.37 741.84 o 14 10 0 43.99 -349.07 723.28 o 1 11 0 99.75 77.49 345.19 o 2 11 0 1.19 -103.67 330.64 o 3 11 0 423.11 269.61 401.76 o 4 11 0 445.36 95.45 349.90 o 5 11 0 568.50 760.96 390.89 o 6 11 0 1495.14 1490.16 437.13 o 7 11 0 53.03 -225.20 376.02 o 8 11 0 3.31 -63.47 630.48 o 9 11 0 27.97 -214.45 400.51 o 10 11 0 535.87 431.04 433.15 o 11 11 0 3.67 126.67 444.19 o 12 11 0 280.07 -258.66 644.25 o 13 11 0 47.60 -652.63 652.63 o 0 12 0 177.40 456.84 522.70 o 1 12 0 188.38 284.92 364.32 o 2 12 0 721.93 707.42 388.90 o 3 12 0 370.79 362.48 429.00 o 4 12 0 579.48 464.50 400.68 o 5 12 0 301.41 630.90 401.50 o 6 12 0 3556.91 2967.66 511.71 o 7 12 0 534.31 215.57 414.96 o 8 12 0 18.62 -219.14 629.88 o 9 12 0 583.02 757.41 701.73 o 10 12 0 2.12 -120.95 650.24 o 11 12 0 595.45 1386.69 755.62 o 1 13 0 650.24 466.12 402.12 o 2 13 0 0.04 114.98 389.92 o 3 13 0 2308.10 2232.18 608.03 o 4 13 0 1265.38 1368.04 454.71 o 5 13 0 803.84 857.36 445.71 o 6 13 0 420.52 178.96 414.58 o 7 13 0 89.78 -274.19 396.75 o 8 13 0 41.30 -10.18 710.11 o 9 13 0 982.03 1098.10 755.02 o 10 13 0 91.86 319.13 710.71 o 11 13 0 141.92 360.44 730.47 o 0 14 0 37.72 -15.57 561.02 o 1 14 0 868.08 1140.18 453.33 o 2 14 0 1357.31 1326.35 469.12 o 3 14 0 524.09 589.85 429.96 o 4 14 0 394.99 217.71 405.97 o 5 14 0 1027.61 638.42 451.98 o 6 14 0 833.50 772.99 465.24 o 7 14 0 439.61 244.29 730.47 o 8 14 0 122.83 122.14 730.47 o 9 14 0 1728.91 2278.82 850.22 o 1 15 0 3742.32 3776.09 584.25 o 2 15 0 89.65 -363.63 403.39 o 3 15 0 3580.74 3208.69 593.06 o 4 15 0 5009.17 4663.02 608.64 o 5 15 0 427.50 59.74 459.54 o 6 15 0 1279.72 680.30 482.11 o 0 16 0 1621.17 1413.64 747.83 o 1 16 0 52.20 -13.53 455.89 o 2 16 0 5598.63 4866.60 902.31 o 3 16 0 3164.95 2617.71 771.78 o 4 16 0 12.20 85.02 602.94 o 5 16 0 993.93 -204.17 580.78 o -17 1 1 22.39 -683.85 683.85 o -16 1 1 84.55 -111.99 677.16 o -15 1 1 147.85 -271.52 626.01 o -14 1 1 405.00 157.04 619.16 o -13 1 1 1108.02 1197.45 579.66 o -12 1 1 966.36 1650.45 612.77 o -11 1 1 293.46 193.25 544.74 o -10 1 1 1462.73 1703.20 532.55 o -9 1 1 5307.04 5010.11 550.29 o -8 1 1 4837.41 4506.69 307.24 o -7 1 1 2538.37 2376.41 196.88 o -6 1 1 1561.41 1455.15 153.97 o -5 1 1 584.58 548.01 128.80 o -4 1 1 44.43 187.04 122.31 o -3 1 1 5665.70 5972.38 283.32 o -2 1 1 1734.92 1615.19 105.95 o -1 1 1 1344.71 1461.60 60.76 o 0 1 1 25.37 48.58 29.80 o 1 1 1 485.79 607.33 56.33 o 2 1 1 26561.74 26683.39 622.28 o 3 1 1 17036.59 16783.57 676.80 o 4 1 1 10468.08 10431.51 268.25 o 5 1 1 3172.28 3131.11 191.49 o 6 1 1 3354.70 3120.89 192.47 o 7 1 1 1062.22 1183.55 197.01 o 8 1 1 1044.18 881.71 217.27 o 9 1 1 76.55 324.81 246.83 o 10 1 1 10.81 -71.31 338.80 o 11 1 1 401.94 1064.56 562.44 o 12 1 1 24.70 -14.71 546.42 o 13 1 1 23.03 -500.13 537.88 o 14 1 1 236.12 -389.55 566.52 o 15 1 1 373.76 372.39 632.40 o 16 1 1 141.66 -46.64 645.32 o 17 1 1 11.30 -688.21 688.21 o -17 2 1 147.50 -124.68 706.13 o -16 2 1 9.81 -637.91 637.91 o -15 2 1 582.90 298.76 644.24 o -14 2 1 83.16 -603.35 603.35 o -13 2 1 284.36 113.28 573.40 o -12 2 1 155.92 -395.79 575.51 o -11 2 1 351.27 747.86 574.58 o -10 2 1 2305.31 2522.25 553.85 o -9 2 1 260.98 168.64 286.99 o -8 2 1 10933.31 9789.21 332.89 o -7 2 1 1434.82 1137.19 180.07 o -6 2 1 242.47 431.38 139.74 o -5 2 1 3.46 18.02 117.40 o -4 2 1 16946.87 16926.52 436.77 o -3 2 1 329.44 436.86 131.90 o -2 2 1 20756.83 21100.56 427.70 o -1 2 1 2441.95 2476.41 129.95 o 0 2 1 3532.16 3621.25 125.08 o 1 2 1 11783.91 12251.77 407.79 o 2 2 1 4388.84 4924.48 240.95 o 3 2 1 7890.17 7955.01 350.67 o 4 2 1 492.99 330.23 150.15 o 5 2 1 2322.78 2630.24 173.79 o 6 2 1 623.37 702.71 161.74 o 7 2 1 4921.34 4639.35 250.40 o 8 2 1 592.72 638.32 208.38 o 9 2 1 1954.55 2060.62 270.60 o 10 2 1 43.07 -225.23 334.96 o 11 2 1 511.07 863.32 555.48 o 12 2 1 74.45 -136.20 548.45 o 13 2 1 22.29 -255.19 546.14 o 14 2 1 383.08 -107.59 607.57 o 15 2 1 488.22 79.53 641.80 o 16 2 1 18.10 -618.25 618.25 o 17 2 1 88.86 -685.00 685.00 o -17 3 1 735.93 -241.22 732.08 o -16 3 1 492.74 -140.38 665.64 o -15 3 1 2.88 -635.25 635.25 o -14 3 1 384.36 530.48 635.45 o -13 3 1 47.11 243.43 580.37 o -12 3 1 329.68 648.66 567.74 o -11 3 1 1012.44 986.06 587.56 o -10 3 1 1186.72 1381.48 535.79 o -9 3 1 821.29 901.04 304.14 o -8 3 1 1338.26 1339.62 210.98 o -7 3 1 2756.75 2912.44 208.35 o -6 3 1 2165.32 2334.82 181.18 o -5 3 1 111.61 68.66 121.97 o -4 3 1 964.04 983.16 139.33 o -3 3 1 6487.95 6843.87 247.01 o -2 3 1 2062.85 2351.37 185.53 o -1 3 1 2669.68 2807.23 193.13 o 0 3 1 84.96 32.74 105.87 o 1 3 1 181.64 297.74 129.53 o 2 3 1 5471.86 5577.40 347.61 o 3 3 1 11984.47 12901.84 423.82 o 4 3 1 1948.24 2334.60 186.80 o 5 3 1 630.44 775.47 168.61 o 6 3 1 1013.73 1141.01 175.70 o 7 3 1 9846.37 9907.10 312.64 o 8 3 1 773.38 914.68 227.82 o 9 3 1 4828.13 4987.03 327.05 o 10 3 1 94.44 48.70 346.71 o 11 3 1 821.23 1235.04 564.59 o 12 3 1 58.97 2.11 538.60 o 13 3 1 663.42 601.35 572.46 o 14 3 1 1270.67 1134.15 643.91 o 15 3 1 116.11 274.85 645.24 o 16 3 1 0.14 -627.76 627.76 o 17 3 1 231.44 -687.28 687.28 o -17 4 1 138.22 -434.38 716.14 o -16 4 1 533.69 200.23 684.55 o -15 4 1 56.24 -577.71 647.49 o -14 4 1 69.75 -578.03 619.83 o -13 4 1 31.78 -151.65 568.49 o -12 4 1 1080.01 819.08 557.42 o -11 4 1 1318.80 682.60 551.84 o -10 4 1 2608.11 2655.89 384.53 o -9 4 1 5019.46 4936.93 395.10 o -8 4 1 890.25 877.87 217.48 o -7 4 1 3.06 65.80 168.16 o -6 4 1 1751.36 1679.49 182.50 o -5 4 1 1686.07 1751.81 177.17 o -4 4 1 23506.14 23589.37 504.53 o -3 4 1 3095.76 3088.65 215.96 o -2 4 1 6296.65 6351.79 253.15 o -1 4 1 8724.10 8820.91 225.89 o 0 4 1 2328.76 2498.60 119.85 o 1 4 1 11427.54 11817.09 277.55 o 2 4 1 1555.67 1626.35 146.10 o 3 4 1 3757.06 3835.92 222.59 o 4 4 1 3437.63 3916.55 239.62 o 5 4 1 5110.89 4726.57 255.48 o 6 4 1 7070.54 7133.20 313.41 o 7 4 1 1208.49 1318.22 211.82 o 8 4 1 6776.21 6578.01 332.61 o 9 4 1 220.56 422.22 268.32 o 10 4 1 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3336.74 3859.41 309.55 o 8 5 1 776.69 1142.90 260.25 o 9 5 1 8211.92 8402.49 396.00 o 10 5 1 1.63 -80.07 361.52 o 11 5 1 2765.66 3381.57 420.96 o 12 5 1 17.25 38.56 509.13 o 13 5 1 233.70 76.32 559.47 o 14 5 1 102.63 -430.43 605.31 o 15 5 1 37.29 -625.27 625.27 o 16 5 1 32.20 -644.72 644.72 o 17 5 1 30.81 -1027.45 1027.45 o -17 6 1 248.72 -428.10 1049.00 o -16 6 1 639.20 -559.57 693.95 o -15 6 1 305.30 -172.07 656.83 o -14 6 1 567.33 525.80 638.48 o -13 6 1 308.66 -395.16 589.57 o -12 6 1 352.60 523.97 531.80 o -11 6 1 12.66 -87.45 475.60 o -10 6 1 339.04 296.81 358.70 o -9 6 1 20.10 -24.31 334.14 o -8 6 1 5310.87 5287.92 322.72 o -7 6 1 118.26 157.53 214.12 o -6 6 1 579.86 825.42 254.69 o -5 6 1 3514.74 4184.54 291.32 o -4 6 1 18053.29 18435.90 423.51 o -3 6 1 1025.47 1194.91 210.69 o -2 6 1 17632.98 17265.92 379.13 o -1 6 1 632.02 517.02 121.70 o 0 6 1 21884.32 21924.23 292.33 o 1 6 1 33413.88 33913.86 483.85 o 2 6 1 773.93 846.42 160.81 o 3 6 1 11234.74 11349.42 350.52 o 4 6 1 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