#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2208548.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208548_Fobs loop_ _publ_author_name 'Osi\'nski, Piotr W.' 'Saadi, Jakub' 'Ricken, Stefan' 'Sch\"urmann, Markus' 'Preut, Hans' 'Pietrusiewicz, Michal' 'Eilbracht, Peter' _publ_section_title ; ({-})-Menthyl (S~P~,R~S~)-(2-p-tolylsulfinylethyl)phenylphosphinate ; _journal_coeditor_code CI2010 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1248 _journal_page_last o1249 _journal_volume 62 _journal_year 2006 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.6199 _cell_length_b 16.8245 _cell_length_c 26.8700 _exptl_crystal_F_000 960.00 _reflns_d_resolution_high 0.8402 _[local]_cod_data_source_file ci2010Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ccd2809 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 188.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 593.42 553.76 37.34 o 4 0 0 1055.80 1027.92 83.40 o 1 1 0 7762.36 7882.57 181.91 o 2 1 0 605.96 609.53 33.46 o 3 1 0 5.69 4.36 15.02 o 4 1 0 24.47 17.93 16.96 o 5 1 0 27.07 21.80 20.83 o 1 2 0 873.23 984.07 41.27 o 2 2 0 31.55 20.83 9.69 o 3 2 0 518.66 518.18 32.48 o 4 2 0 2562.71 2607.95 90.77 o 5 2 0 9.36 3.88 21.32 o 1 3 0 549.42 614.53 31.53 o 2 3 0 103.92 88.68 11.63 o 3 3 0 26.84 23.26 14.54 o 4 3 0 378.71 374.13 36.35 o 5 3 0 6.23 7.27 31.49 o 0 4 0 11591.90 10807.54 335.35 o 1 4 0 4094.66 3764.91 113.66 o 2 4 0 1011.54 1047.27 47.54 o 3 4 0 76.47 57.17 17.93 o 4 4 0 1222.19 1190.93 82.92 o 5 4 0 145.39 178.31 34.89 o 6 4 0 14.09 10.17 89.63 o 1 5 0 177.93 185.61 15.99 o 2 5 0 1168.59 1206.47 57.73 o 3 5 0 122.51 146.82 21.80 o 4 5 0 184.15 185.10 24.71 o 5 5 0 80.41 53.30 42.64 o 6 5 0 1.68 11.14 118.22 o 0 6 0 1973.46 1871.44 87.94 o 1 6 0 1368.99 1309.42 50.47 o 2 6 0 632.64 601.16 33.45 o 3 6 0 304.78 346.02 27.14 o 4 6 0 112.29 134.22 21.32 o 5 6 0 42.98 49.90 37.31 o 6 6 0 0.56 -47.00 103.68 o 1 7 0 18.46 17.44 16.96 o 2 7 0 188.35 148.28 20.35 o 3 7 0 58.78 56.69 19.38 o 4 7 0 2.55 -4.36 18.90 o 5 7 0 53.48 35.37 31.01 o 6 7 0 0.24 32.95 114.34 o 0 8 0 175.03 163.79 27.14 o 1 8 0 1316.96 1287.54 54.82 o 2 8 0 429.93 366.90 31.99 o 3 8 0 461.75 502.11 32.96 o 4 8 0 9.53 -15.02 32.95 o 5 8 0 34.81 15.50 47.00 o 6 8 0 0.00 -32.95 114.34 o 1 9 0 83.35 86.25 20.35 o 2 9 0 10.91 17.44 23.74 o 3 9 0 55.35 47.97 19.38 o 4 9 0 1.05 -17.44 34.40 o 5 9 0 1.90 27.62 40.70 o 0 10 0 86.99 114.84 33.43 o 1 10 0 134.07 165.23 24.23 o 2 10 0 27.84 19.38 31.49 o 3 10 0 144.51 150.69 33.43 o 4 10 0 125.45 130.34 34.89 o 5 10 0 0.70 2.42 58.62 o 1 11 0 22.99 23.26 24.23 o 2 11 0 16.54 38.76 34.40 o 3 11 0 100.67 89.64 26.16 o 4 11 0 5.86 -12.60 59.11 o 5 11 0 47.40 59.60 54.27 o 0 12 0 457.28 427.47 56.22 o 1 12 0 425.22 425.52 41.19 o 2 12 0 214.67 158.94 29.56 o 3 12 0 7.93 24.23 58.14 o 4 12 0 21.99 42.15 57.17 o 5 12 0 16.63 36.34 55.23 o 1 13 0 28.17 12.11 35.85 o 2 13 0 12.36 7.27 71.22 o 3 13 0 62.24 56.69 50.39 o 4 13 0 15.56 2.42 62.99 o 5 13 0 15.77 37.31 109.01 o 0 14 0 441.90 547.15 109.53 o 1 14 0 32.49 35.37 48.45 o 2 14 0 13.39 -36.34 50.39 o 3 14 0 3.72 32.95 73.64 o 4 14 0 13.94 -8.24 64.92 o 1 15 0 7.13 3.39 37.79 o 2 15 0 23.50 15.99 60.08 o 3 15 0 33.80 30.52 51.36 o 4 15 0 15.36 5.33 53.78 o 0 16 0 341.16 372.17 86.74 o 1 16 0 26.51 29.55 41.67 o 2 16 0 0.04 7.75 66.38 o 3 16 0 8.76 49.42 74.61 o 4 16 0 7.35 2.91 171.51 o 1 17 0 9.20 16.47 60.56 o 2 17 0 17.52 -2.91 64.92 o 3 17 0 1.74 63.95 133.24 o 2 18 0 9.05 5.33 199.13 o 2 19 0 0.11 -25.68 127.42 o 1 0 1 4064.72 4452.61 128.83 o 2 0 1 802.26 709.13 42.20 o 3 0 1 569.19 580.26 34.42 o 4 0 1 489.92 506.97 37.32 o 5 0 1 430.47 400.78 35.86 o -5 1 1 99.56 114.83 27.62 o -4 1 1 17.71 15.02 19.38 o -3 1 1 34.31 56.20 14.54 o -2 1 1 146.57 162.34 16.48 o -1 1 1 1190.72 1280.10 38.88 o 1 1 1 1199.36 1288.88 40.34 o 2 1 1 146.32 154.59 16.48 o 3 1 1 34.75 50.39 17.44 o 4 1 1 17.67 10.17 20.83 o 5 1 1 98.59 111.44 28.10 o -5 2 1 675.36 725.10 52.35 o -4 2 1 675.86 697.05 37.32 o -3 2 1 241.95 244.73 19.87 o -2 2 1 620.00 657.52 34.91 o -1 2 1 831.33 772.79 28.64 o 1 2 1 827.95 815.01 44.17 o 2 2 1 626.87 665.77 29.58 o 3 2 1 237.60 226.31 23.75 o 4 2 1 674.90 635.48 42.66 o 5 2 1 679.11 612.65 47.98 o -6 3 1 5.18 -16.96 73.16 o -5 3 1 26.86 17.44 28.59 o -4 3 1 17.37 2.91 24.23 o -3 3 1 632.63 649.60 48.48 o -2 3 1 637.39 661.87 34.43 o -1 3 1 937.84 914.95 41.26 o 0 3 1 31.76 27.62 7.75 o 1 3 1 947.28 934.38 50.00 o 2 3 1 621.77 610.95 33.46 o 3 3 1 634.38 668.02 32.96 o 4 3 1 17.39 23.26 23.74 o 5 3 1 26.41 -0.97 30.04 o -6 4 1 10.38 15.02 93.99 o -5 4 1 148.22 134.70 37.31 o -4 4 1 350.88 389.15 36.35 o -3 4 1 226.45 234.54 26.65 o -2 4 1 100.60 83.34 13.08 o -1 4 1 1764.69 1754.65 68.03 o 0 4 1 5684.92 5354.83 131.36 o 1 4 1 1766.63 1696.83 52.97 o 2 4 1 102.15 90.61 11.63 o 3 4 1 227.22 251.51 21.81 o 4 4 1 350.19 306.76 37.80 o 5 4 1 150.65 139.06 29.07 o 6 4 1 10.33 20.35 88.18 o -6 5 1 10.60 8.24 106.59 o -5 5 1 38.37 45.54 30.52 o -4 5 1 5.01 -6.30 19.86 o -3 5 1 1.44 -4.85 15.99 o -2 5 1 527.66 539.56 26.66 o -1 5 1 901.34 880.99 47.06 o 0 5 1 143.78 139.57 15.51 o 1 5 1 891.03 825.19 33.47 o 2 5 1 539.94 520.17 34.42 o 3 5 1 0.96 4.36 15.50 o 4 5 1 5.29 15.02 26.65 o 5 5 1 38.49 80.91 36.82 o 6 5 1 10.51 10.17 106.11 o -6 6 1 12.05 -37.79 113.37 o -5 6 1 14.54 6.30 32.46 o -4 6 1 468.64 469.14 34.41 o -3 6 1 73.16 68.80 16.96 o -2 6 1 342.42 344.60 27.63 o -1 6 1 729.31 737.11 34.92 o 0 6 1 433.85 413.53 23.27 o 1 6 1 712.56 696.36 29.58 o 2 6 1 353.61 348.48 27.14 o 3 6 1 71.32 76.56 16.47 o 4 6 1 467.42 457.99 37.80 o 5 6 1 15.00 26.16 30.04 o 6 6 1 12.46 21.80 86.24 o -6 7 1 6.73 30.04 111.92 o -5 7 1 61.92 50.87 40.70 o -4 7 1 12.75 7.27 24.23 o -3 7 1 93.11 97.88 20.84 o -2 7 1 253.00 238.43 26.17 o -1 7 1 628.87 627.86 32.00 o 0 7 1 15.42 8.72 17.44 o 1 7 1 642.09 646.30 29.58 o 2 7 1 260.00 249.58 28.59 o 3 7 1 92.29 85.76 19.87 o 4 7 1 12.07 15.99 16.96 o 5 7 1 61.80 69.29 42.64 o 6 7 1 6.74 8.24 87.69 o -6 8 1 1.31 13.57 97.87 o -5 8 1 1.29 17.93 55.72 o -4 8 1 286.85 329.52 44.10 o -3 8 1 12.78 13.57 16.96 o -2 8 1 59.81 47.00 18.90 o -1 8 1 214.51 202.56 22.78 o 0 8 1 2942.99 2816.36 100.60 o 1 8 1 203.27 198.20 22.29 o 2 8 1 60.78 35.85 25.20 o 3 8 1 13.81 -5.33 17.44 o 4 8 1 284.34 237.93 34.41 o 5 8 1 1.47 -2.91 39.73 o 6 8 1 1.54 -11.63 79.46 o -5 9 1 26.34 20.35 55.23 o -4 9 1 115.09 116.29 33.92 o -3 9 1 44.23 44.58 23.26 o -2 9 1 55.18 41.18 24.71 o -1 9 1 210.76 201.59 23.26 o 0 9 1 2.98 -11.14 16.96 o 1 9 1 214.32 186.08 21.81 o 2 9 1 52.83 33.43 26.16 o 3 9 1 43.61 26.16 23.26 o 4 9 1 113.79 102.24 32.95 o 5 9 1 26.03 14.05 47.00 o -5 10 1 6.99 42.64 62.50 o -4 10 1 15.24 5.33 25.68 o -3 10 1 282.04 283.97 37.31 o -2 10 1 71.88 78.98 23.74 o -1 10 1 272.15 278.65 29.56 o 0 10 1 5.55 5.81 17.93 o 1 10 1 270.31 263.63 29.08 o 2 10 1 72.63 56.21 28.10 o 3 10 1 281.28 292.69 41.19 o 4 10 1 14.63 8.72 31.49 o 5 10 1 7.21 33.92 51.36 o -5 11 1 14.19 52.33 53.30 o -4 11 1 7.59 -29.55 61.53 o -3 11 1 122.21 99.81 28.59 o -2 11 1 9.41 11.14 25.68 o -1 11 1 38.11 66.38 23.74 o 0 11 1 46.11 39.25 20.83 o 1 11 1 37.12 42.64 27.62 o 2 11 1 9.04 26.16 27.62 o 3 11 1 119.89 104.18 44.09 o 4 11 1 8.35 18.41 40.70 o 5 11 1 13.88 -31.49 38.28 o -5 12 1 18.98 64.44 68.32 o -4 12 1 2.17 -16.47 58.62 o -3 12 1 173.43 131.80 54.27 o -2 12 1 139.90 129.86 30.53 o -1 12 1 400.39 437.63 43.62 o 0 12 1 902.46 843.09 54.78 o 1 12 1 408.14 426.48 37.32 o 2 12 1 143.74 87.22 36.83 o 3 12 1 174.36 161.36 52.82 o 4 12 1 2.22 -22.77 43.12 o 5 12 1 18.36 94.96 183.63 o -5 13 1 20.65 3.88 70.25 o -4 13 1 0.53 -20.35 62.99 o -3 13 1 2.74 46.03 47.48 o -2 13 1 106.42 164.74 73.65 o -1 13 1 539.59 513.27 46.04 o 0 13 1 40.64 32.95 33.43 o 1 13 1 546.73 537.50 61.07 o 2 13 1 107.03 103.69 51.84 o 3 13 1 3.02 11.63 53.30 o 4 13 1 0.40 -22.29 56.69 o 5 13 1 20.37 102.72 141.96 o -4 14 1 25.10 38.76 61.05 o -3 14 1 80.56 123.07 71.71 o -2 14 1 150.28 178.80 80.92 o -1 14 1 308.28 333.88 61.06 o 0 14 1 1233.15 1290.24 104.25 o 1 14 1 317.30 288.33 60.57 o 2 14 1 150.10 127.92 53.78 o 3 14 1 82.08 107.08 62.99 o 4 14 1 25.34 34.40 70.25 o -4 15 1 1.90 -9.21 59.11 o -3 15 1 1.37 -8.24 65.41 o -2 15 1 44.02 25.68 57.17 o -1 15 1 11.32 26.65 43.61 o 0 15 1 10.70 -2.91 43.12 o 1 15 1 11.54 -15.02 38.28 o 2 15 1 43.93 25.68 59.11 o 3 15 1 1.22 -24.71 53.30 o 4 15 1 1.64 35.85 62.02 o -3 16 1 16.24 15.99 92.54 o -2 16 1 13.55 -18.41 49.42 o -1 16 1 11.29 4.85 54.26 o 0 16 1 303.60 382.34 67.36 o 1 16 1 11.59 22.77 64.44 o 2 16 1 13.74 45.54 63.47 o 3 16 1 15.67 12.11 78.97 o 4 16 1 75.35 47.00 71.22 o -3 17 1 9.65 59.11 126.46 o -2 17 1 7.52 -40.21 62.02 o -1 17 1 36.72 63.96 55.72 o 0 17 1 45.46 19.38 50.39 o 1 17 1 37.32 49.42 66.86 o 2 17 1 7.62 40.70 90.60 o 3 17 1 9.75 38.76 191.86 o -2 18 1 55.98 96.42 194.29 o -2 19 1 1.21 129.36 167.15 o -1 19 1 19.43 51.84 186.53 o 2 19 1 1.30 59.11 125.97 o 0 20 1 94.03 242.26 167.64 o 1 0 2 22321.16 23034.67 771.37 o 2 0 2 38.97 36.82 11.63 o 3 0 2 423.87 433.80 36.35 o 4 0 2 1378.35 1367.64 60.14 o 5 0 2 50.33 60.56 25.19 o -5 1 2 115.99 116.29 24.71 o -4 1 2 50.43 29.56 19.38 o -3 1 2 109.85 116.29 20.84 o -2 1 2 1092.94 1088.83 56.77 o -1 1 2 6753.46 6954.13 159.56 o 1 1 2 6783.44 6996.48 186.17 o 2 1 2 1100.85 1113.58 49.98 o 3 1 2 110.40 106.60 16.47 o 4 1 2 48.53 34.40 25.68 o 5 1 2 116.17 131.79 30.04 o -5 2 2 110.12 124.52 31.01 o -4 2 2 1288.66 1319.52 60.62 o -3 2 2 387.99 381.92 26.17 o -2 2 2 966.16 980.41 41.72 o -1 2 2 21065.29 20427.26 403.05 o 1 2 2 21029.54 21454.60 538.20 o 2 2 2 994.26 938.24 40.75 o 3 2 2 405.15 413.92 30.53 o 4 2 2 1285.03 1335.04 61.59 o 5 2 2 105.90 122.59 25.68 o -6 3 2 6.57 23.26 90.60 o -5 3 2 99.99 71.23 30.53 o -4 3 2 94.59 82.86 21.32 o -3 3 2 701.86 660.30 54.30 o -2 3 2 310.82 316.02 19.87 o -1 3 2 5940.20 5756.92 149.42 o 0 3 2 693.27 634.85 26.21 o 1 3 2 5891.20 5890.13 170.47 o 2 3 2 308.59 336.86 22.78 o 3 3 2 719.54 681.64 40.24 o 4 3 2 94.50 88.18 26.16 o 5 3 2 101.15 98.84 27.13 o -6 4 2 9.82 4.85 79.94 o -5 4 2 301.86 293.66 33.44 o -4 4 2 324.21 301.91 41.19 o -3 4 2 748.39 760.67 40.24 o -2 4 2 162.29 153.13 15.02 o -1 4 2 661.31 635.38 32.98 o 0 4 2 18045.18 17345.10 387.74 o 1 4 2 635.66 604.80 26.68 o 2 4 2 155.52 182.21 15.99 o 3 4 2 749.57 759.22 49.45 o 4 4 2 322.02 275.26 38.77 o 5 4 2 299.53 247.62 47.49 o -6 5 2 7.81 4.85 92.54 o -5 5 2 158.97 124.53 36.83 o -4 5 2 32.26 27.13 20.83 o -3 5 2 868.00 875.63 40.24 o -2 5 2 232.46 231.16 20.84 o -1 5 2 2479.82 2457.19 76.82 o 0 5 2 61.63 47.97 11.63 o 1 5 2 2422.12 2397.20 76.81 o 2 5 2 230.95 239.89 27.14 o 3 5 2 871.06 908.61 44.12 o 4 5 2 33.03 15.50 33.43 o 5 5 2 158.51 139.55 36.83 o 6 5 2 7.65 -14.54 59.11 o -6 6 2 1.34 7.27 118.70 o -5 6 2 57.27 99.33 34.89 o -4 6 2 112.46 112.90 21.80 o -3 6 2 420.43 407.60 26.17 o -2 6 2 207.53 232.12 23.75 o -1 6 2 219.20 224.87 20.84 o 0 6 2 3112.08 3175.29 90.50 o 1 6 2 236.24 217.12 18.42 o 2 6 2 214.19 219.04 23.75 o 3 6 2 423.82 443.47 32.96 o 4 6 2 108.65 97.39 29.56 o 5 6 2 58.53 93.51 46.51 o 6 6 2 1.44 21.80 91.57 o -6 7 2 1.99 13.57 82.37 o -5 7 2 52.01 39.25 47.97 o -4 7 2 8.60 12.60 25.19 o -3 7 2 162.26 138.10 21.81 o -2 7 2 666.24 663.68 41.21 o -1 7 2 1534.94 1557.37 68.91 o 0 7 2 81.11 73.65 15.51 o 1 7 2 1526.03 1524.84 54.84 o 2 7 2 661.17 654.96 46.54 o 3 7 2 163.23 160.39 19.87 o 4 7 2 8.41 10.66 27.13 o 5 7 2 51.83 46.51 46.03 o 6 7 2 2.02 -16.47 92.54 o -6 8 2 7.04 66.86 109.01 o -5 8 2 13.65 46.03 51.36 o -4 8 2 68.26 74.13 31.01 o -3 8 2 276.95 270.40 30.04 o -2 8 2 78.29 94.00 21.80 o -1 8 2 1312.39 1329.24 55.30 o 0 8 2 7.52 13.57 14.54 o 1 8 2 1329.04 1359.82 56.76 o 2 8 2 82.63 101.27 21.32 o 3 8 2 279.39 261.20 25.20 o 4 8 2 65.10 58.14 30.52 o 5 8 2 13.91 2.91 44.09 o 6 8 2 7.00 25.68 121.61 o -5 9 2 2.97 11.14 61.05 o -4 9 2 2.45 1.45 30.04 o -3 9 2 68.61 57.17 21.32 o -2 9 2 243.35 240.36 24.71 o -1 9 2 47.57 45.55 19.87 o 0 9 2 0.78 -3.39 16.47 o 1 9 2 49.10 46.03 19.87 o 2 9 2 244.84 235.51 27.62 o 3 9 2 70.12 54.27 20.83 o 4 9 2 2.34 11.63 32.46 o 5 9 2 3.13 0.48 47.97 o -5 10 2 9.31 -23.26 63.95 o -4 10 2 151.50 139.55 29.07 o -3 10 2 74.88 88.18 28.59 o -2 10 2 73.07 93.03 29.07 o -1 10 2 110.93 117.74 20.84 o 0 10 2 41.50 17.93 18.41 o 1 10 2 108.90 100.79 24.23 o 2 10 2 69.92 103.69 30.04 o 3 10 2 77.38 48.94 28.59 o 4 10 2 154.46 114.84 55.72 o 5 10 2 9.89 24.23 86.24 o -5 11 2 17.23 9.69 61.53 o -4 11 2 29.54 24.23 43.61 o -3 11 2 9.85 0.97 27.62 o -2 11 2 399.51 428.42 44.10 o -1 11 2 233.10 234.54 33.44 o 0 11 2 19.43 11.63 24.71 o 1 11 2 232.11 225.33 28.11 o 2 11 2 402.87 353.78 34.89 o 3 11 2 9.47 20.35 35.37 o 4 11 2 29.71 67.83 50.87 o 5 11 2 17.30 17.44 120.16 o -5 12 2 12.39 49.90 67.83 o -4 12 2 234.61 234.04 63.48 o -3 12 2 1.40 22.77 34.88 o -2 12 2 277.61 280.09 39.74 o -1 12 2 0.22 -2.42 25.68 o 0 12 2 163.26 156.51 29.07 o 1 12 2 0.14 -5.81 20.35 o 2 12 2 275.84 258.28 45.55 o 3 12 2 1.42 -22.29 62.99 o 4 12 2 231.34 217.08 62.51 o 5 12 2 12.56 14.05 109.50 o -5 13 2 1.42 0.48 53.78 o -4 13 2 24.97 12.11 70.74 o -3 13 2 8.94 25.19 51.36 o -2 13 2 72.55 98.36 64.44 o -1 13 2 26.74 -3.39 41.67 o 0 13 2 171.11 128.41 36.34 o 1 13 2 26.88 45.06 31.98 o 2 13 2 70.10 53.30 54.75 o 3 13 2 9.00 -32.46 72.68 o 4 13 2 24.96 -14.54 47.48 o 5 13 2 1.39 -51.36 124.03 o -4 14 2 67.67 78.49 76.07 o -3 14 2 23.83 38.76 60.56 o -2 14 2 35.85 43.12 38.76 o -1 14 2 388.38 322.75 59.12 o 0 14 2 5.66 -10.66 47.00 o 1 14 2 387.73 378.48 63.00 o 2 14 2 35.97 0.00 51.84 o 3 14 2 23.44 8.24 42.15 o 4 14 2 66.79 104.66 79.95 o -4 15 2 1.49 -25.19 62.99 o -3 15 2 25.16 47.00 72.68 o -2 15 2 27.70 29.07 58.63 o -1 15 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