#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2208709.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208709_Fobs loop_ _publ_author_name 'Banu, Afroza' 'Hossain, G. M. Golzar' _publ_section_title ; Sulfathiazolium nitrate monohydrate ; _journal_coeditor_code SG2017 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1573 _journal_page_last o1574 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.466 _cell_angle_gamma 90.000 _cell_length_a 12.1917 _cell_length_b 7.6348 _cell_length_c 15.3895 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file sg2017Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S92 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 202.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5608.57 5546.41 165.19 o 3 0 0 7805.09 7919.87 221.42 o 4 0 0 1525.48 1482.92 35.77 o 5 0 0 3705.15 3884.34 88.98 o 6 0 0 815.14 1070.08 28.01 o 7 0 0 4652.82 5232.78 109.45 o 8 0 0 745.02 739.69 18.84 o 9 0 0 0.03 3.57 2.97 o 10 0 0 692.86 707.79 26.60 o 11 0 0 151.40 178.35 11.00 o 12 0 0 8.39 20.13 6.69 o 13 0 0 538.01 548.19 31.69 o 14 0 0 447.15 406.16 29.99 o 15 0 0 116.88 106.90 24.71 o 1 1 0 2273.46 2014.07 41.87 o 2 1 0 1121.83 1179.54 22.26 o 3 1 0 1166.86 1265.67 24.25 o 4 1 0 6331.40 6422.07 135.91 o 5 1 0 1436.63 1605.54 30.38 o 6 1 0 234.94 288.19 6.10 o 7 1 0 130.54 134.30 4.88 o 8 1 0 498.17 515.77 15.87 o 9 1 0 1046.43 1063.84 30.19 o 10 1 0 1076.38 1126.07 21.57 o 11 1 0 437.55 474.66 11.76 o 12 1 0 298.43 305.49 21.30 o 13 1 0 8.84 4.48 6.53 o 14 1 0 75.54 48.02 10.33 o 15 1 0 72.22 63.38 9.92 o 0 2 0 364.31 264.53 5.64 o 1 2 0 3723.11 3568.60 48.71 o 2 2 0 730.08 732.47 15.56 o 3 2 0 3818.99 3768.90 86.59 o 4 2 0 111.06 121.99 4.15 o 5 2 0 3028.76 3406.87 118.81 o 6 2 0 1768.27 1983.41 65.40 o 7 2 0 390.25 440.71 10.37 o 8 2 0 13.58 10.25 2.03 o 9 2 0 154.57 169.89 6.93 o 10 2 0 477.50 469.89 12.16 o 11 2 0 638.93 617.66 21.89 o 12 2 0 79.07 82.00 7.66 o 13 2 0 190.62 179.41 17.66 o 14 2 0 57.60 57.34 11.03 o 1 3 0 6565.74 6438.29 81.32 o 2 3 0 523.54 461.72 7.94 o 3 3 0 1827.80 1849.31 43.70 o 4 3 0 7.43 11.29 1.85 o 5 3 0 51.49 72.20 3.43 o 6 3 0 12.47 8.54 1.88 o 7 3 0 156.74 145.22 7.77 o 8 3 0 190.34 204.08 9.45 o 9 3 0 971.20 944.58 44.10 o 10 3 0 0.80 2.00 3.37 o 11 3 0 356.17 354.80 16.60 o 12 3 0 61.39 53.77 8.35 o 13 3 0 10.04 7.48 10.53 o 14 3 0 4.48 1.45 9.86 o 0 4 0 13438.91 12732.66 252.66 o 1 4 0 0.14 4.08 1.93 o 2 4 0 514.49 465.30 7.76 o 3 4 0 420.95 440.33 9.18 o 4 4 0 95.43 101.96 3.97 o 5 4 0 2674.58 2769.66 108.89 o 6 4 0 29.92 25.07 3.46 o 7 4 0 840.51 856.05 38.06 o 8 4 0 104.00 81.37 5.54 o 9 4 0 84.57 75.10 4.65 o 10 4 0 16.23 17.05 3.18 o 11 4 0 5.50 -5.02 5.02 o 12 4 0 123.25 146.92 10.82 o 13 4 0 299.72 316.51 20.06 o 1 5 0 801.93 766.17 14.91 o 2 5 0 96.14 84.22 4.25 o 3 5 0 1092.40 1042.29 32.10 o 4 5 0 2433.38 2265.23 73.40 o 5 5 0 936.26 881.13 32.18 o 6 5 0 2.30 -3.52 3.52 o 7 5 0 42.87 47.91 5.52 o 8 5 0 67.36 59.40 4.90 o 9 5 0 344.87 377.68 31.97 o 10 5 0 116.56 117.69 6.40 o 11 5 0 116.64 97.35 9.93 o 12 5 0 37.84 27.39 8.56 o 13 5 0 1.25 6.76 10.43 o 0 6 0 2280.79 2098.60 81.95 o 1 6 0 280.77 243.64 6.40 o 2 6 0 223.25 229.64 9.33 o 3 6 0 212.29 214.61 6.79 o 4 6 0 158.10 157.72 6.19 o 5 6 0 1328.65 1381.88 61.85 o 6 6 0 233.64 232.44 7.87 o 7 6 0 3.57 4.69 4.32 o 8 6 0 3.67 7.44 4.53 o 9 6 0 4.06 3.94 8.83 o 10 6 0 256.15 247.05 15.93 o 11 6 0 250.41 255.67 16.54 o 12 6 0 75.66 45.05 13.41 o 1 7 0 209.91 224.88 7.60 o 2 7 0 185.61 187.44 8.11 o 3 7 0 36.83 37.72 4.54 o 4 7 0 79.43 71.44 5.79 o 5 7 0 93.81 107.42 7.12 o 6 7 0 211.51 222.35 11.49 o 7 7 0 394.96 357.31 21.56 o 8 7 0 75.40 85.28 10.84 o 9 7 0 102.98 87.22 12.57 o 10 7 0 316.11 300.76 38.03 o 0 8 0 1.44 5.91 7.53 o 1 8 0 49.60 42.04 5.93 o 2 8 0 368.74 375.71 13.56 o 3 8 0 344.28 342.62 16.90 o 4 8 0 1.32 -4.52 6.67 o 5 8 0 291.49 331.39 15.17 o 6 8 0 0.01 6.24 7.49 o 7 8 0 344.97 360.74 24.60 o 8 8 0 39.15 32.59 11.29 o 1 9 0 163.83 191.87 12.71 o 2 9 0 329.00 360.66 17.46 o 3 9 0 114.90 121.33 15.85 o 4 9 0 83.80 76.23 12.27 o 5 9 0 13.35 -6.80 10.08 o 6 9 0 16.96 16.53 15.51 o -15 1 1 196.13 184.50 14.01 o -14 1 1 78.10 79.54 11.10 o -13 1 1 9.37 5.55 9.31 o -12 1 1 796.91 810.86 26.93 o -11 1 1 203.25 197.51 6.86 o -10 1 1 241.68 256.68 6.42 o -9 1 1 64.08 70.67 3.58 o -8 1 1 291.35 288.15 6.38 o -7 1 1 331.48 350.34 8.59 o -6 1 1 100.76 128.38 4.30 o -5 1 1 75.08 81.96 2.56 o -4 1 1 45.31 33.38 1.72 o -3 1 1 2793.00 2923.75 45.60 o -2 1 1 14058.01 13309.09 206.65 o -1 1 1 473.34 463.04 10.47 o 0 1 1 121.73 91.76 4.44 o 2 1 1 3516.91 3598.70 63.42 o 3 1 1 2324.22 2090.51 35.27 o 4 1 1 1838.97 1992.61 43.60 o 5 1 1 869.86 948.69 17.45 o 6 1 1 270.15 255.05 6.21 o 7 1 1 87.63 92.41 3.17 o 8 1 1 10.88 21.53 2.22 o 9 1 1 25.23 30.16 3.17 o 10 1 1 645.89 669.54 15.17 o 11 1 1 851.75 828.52 22.14 o 12 1 1 13.81 11.70 8.32 o 13 1 1 367.11 312.09 18.72 o 14 1 1 0.66 2.97 11.90 o -15 2 1 37.50 45.02 12.73 o -14 2 1 1.84 6.03 7.84 o -13 2 1 2.75 -4.88 4.88 o -12 2 1 115.57 115.00 10.48 o -11 2 1 214.76 185.22 7.65 o -10 2 1 3120.11 3198.34 137.58 o -9 2 1 783.83 804.41 30.32 o -8 2 1 1065.99 1163.58 41.23 o -7 2 1 651.55 630.54 20.75 o -6 2 1 3025.25 2918.62 107.20 o -5 2 1 73.66 103.80 3.32 o -4 2 1 2323.39 2512.33 69.74 o -3 2 1 4219.27 3955.82 80.28 o -2 2 1 6579.30 6337.37 131.94 o -1 2 1 41121.89 36534.80 2225.20 o 0 2 1 2900.87 2541.13 34.33 o 1 2 1 9201.79 8637.31 117.00 o 2 2 1 2.19 25.91 4.96 o 3 2 1 1316.08 1105.07 34.15 o 4 2 1 1540.32 1674.45 39.91 o 5 2 1 5266.82 5916.67 205.41 o 6 2 1 1817.88 2053.65 69.02 o 7 2 1 18.66 31.26 2.47 o 8 2 1 596.64 613.79 17.53 o 9 2 1 350.55 360.47 10.52 o 10 2 1 501.24 524.62 13.75 o 11 2 1 226.97 188.39 7.48 o 12 2 1 58.37 50.41 7.14 o 13 2 1 160.28 167.95 16.67 o 14 2 1 1244.91 1289.56 109.65 o -14 3 1 513.23 508.25 44.72 o -13 3 1 344.66 328.98 30.81 o -12 3 1 154.53 124.80 13.53 o -11 3 1 40.45 35.54 4.21 o -10 3 1 0.69 2.30 3.83 o -9 3 1 760.51 701.63 28.75 o -8 3 1 81.48 73.14 4.74 o -7 3 1 1183.27 1225.81 56.84 o -6 3 1 2585.31 2666.31 129.53 o -5 3 1 1810.14 1992.81 57.29 o -4 3 1 0.10 0.63 1.77 o -3 3 1 353.41 339.71 11.77 o -2 3 1 1050.95 908.81 14.82 o -1 3 1 658.82 499.01 8.14 o 0 3 1 9323.22 8475.40 111.38 o 1 3 1 418.84 551.22 8.28 o 2 3 1 54.46 53.98 2.13 o 3 3 1 2241.70 2213.23 68.54 o 4 3 1 547.40 582.07 19.04 o 5 3 1 922.15 953.45 33.45 o 6 3 1 3085.18 3135.70 130.23 o 7 3 1 200.39 182.65 5.45 o 8 3 1 242.08 199.66 6.40 o 9 3 1 699.68 674.21 26.35 o 10 3 1 1178.83 1324.04 75.13 o 11 3 1 747.93 783.23 48.26 o 12 3 1 53.37 53.55 9.20 o 13 3 1 45.27 32.96 7.67 o 14 3 1 44.46 47.43 9.03 o -14 4 1 4.42 0.01 21.67 o -13 4 1 206.60 187.25 14.33 o -12 4 1 23.32 28.43 6.11 o -11 4 1 49.95 41.03 6.52 o -10 4 1 343.38 373.25 14.71 o -9 4 1 1104.36 1073.36 51.22 o -8 4 1 305.47 276.44 12.25 o -7 4 1 17.49 13.52 3.31 o -6 4 1 1066.62 1036.93 45.97 o -5 4 1 100.46 83.39 3.55 o -4 4 1 782.94 827.46 24.32 o -3 4 1 981.88 990.10 39.03 o -2 4 1 2502.40 2601.62 60.65 o -1 4 1 5.34 12.62 2.19 o 0 4 1 2346.80 2261.37 30.48 o 1 4 1 1442.32 1358.89 19.18 o 2 4 1 157.25 170.64 6.19 o 3 4 1 1869.03 1795.21 55.28 o 4 4 1 87.69 76.65 3.90 o 5 4 1 76.41 63.39 3.51 o 6 4 1 7.55 6.83 2.61 o 7 4 1 4.04 0.00 2.57 o 8 4 1 0.84 2.61 3.73 o 9 4 1 21.99 23.97 2.89 o 10 4 1 148.22 138.01 13.01 o 11 4 1 12.18 19.69 11.52 o 12 4 1 68.76 50.13 8.46 o 13 4 1 123.53 107.60 12.47 o -13 5 1 2.47 4.66 8.54 o -12 5 1 5.11 -5.94 7.47 o -11 5 1 360.45 351.75 31.54 o -10 5 1 0.02 -3.17 5.22 o -9 5 1 277.03 273.94 12.58 o -8 5 1 493.02 454.59 19.48 o -7 5 1 18.62 13.09 3.89 o -6 5 1 314.35 312.67 12.01 o -5 5 1 653.74 639.94 26.39 o -4 5 1 3792.35 3817.70 127.40 o -3 5 1 2040.60 2026.17 65.76 o -2 5 1 38.75 57.30 3.78 o -1 5 1 304.76 286.54 6.25 o 0 5 1 328.39 315.46 6.09 o 1 5 1 543.09 508.38 9.38 o 2 5 1 1413.67 1444.96 24.06 o 3 5 1 1533.52 1669.11 68.22 o 4 5 1 16.21 14.29 2.91 o 5 5 1 1.39 1.68 2.38 o 6 5 1 372.33 336.54 18.14 o 7 5 1 507.50 467.45 22.33 o 8 5 1 150.60 154.42 7.37 o 9 5 1 143.72 128.87 9.83 o 10 5 1 0.56 -0.64 4.11 o 11 5 1 2.44 -2.69 8.36 o 12 5 1 158.77 160.76 14.70 o -12 6 1 3.18 2.75 9.71 o -11 6 1 21.06 13.15 10.95 o -10 6 1 26.51 27.17 8.51 o -9 6 1 9.87 5.79 6.47 o -8 6 1 355.55 361.72 18.97 o -7 6 1 2.65 6.12 4.21 o -6 6 1 295.62 290.93 12.00 o -5 6 1 1581.03 1587.27 72.35 o -4 6 1 146.61 151.28 5.84 o -3 6 1 2167.76 2202.21 58.78 o -2 6 1 0.47 5.76 3.89 o -1 6 1 686.26 690.70 15.67 o 0 6 1 95.06 74.50 4.24 o 1 6 1 10.43 4.73 3.21 o 2 6 1 709.83 680.62 19.09 o 3 6 1 498.26 441.03 14.52 o 4 6 1 1191.04 1285.48 39.69 o 5 6 1 612.44 617.46 25.31 o 6 6 1 113.79 111.12 6.02 o 7 6 1 41.52 41.01 6.06 o 8 6 1 0.14 1.14 4.98 o 9 6 1 9.74 7.08 6.43 o 10 6 1 77.74 86.01 8.82 o 11 6 1 3.30 -5.85 10.54 o -10 7 1 220.92 272.50 26.99 o -9 7 1 189.99 217.13 14.91 o -8 7 1 6.19 1.23 7.36 o -7 7 1 199.33 205.29 13.65 o -6 7 1 695.08 794.50 35.24 o -5 7 1 185.59 183.01 15.29 o -4 7 1 10.37 4.35 4.52 o -3 7 1 1432.92 1426.63 47.94 o -2 7 1 555.79 495.51 12.75 o -1 7 1 98.33 91.37 5.42 o 0 7 1 48.68 59.47 5.52 o 1 7 1 860.02 860.65 21.37 o 2 7 1 1.21 -3.63 3.82 o 3 7 1 114.44 116.84 6.23 o 4 7 1 0.26 1.28 5.45 o 5 7 1 0.09 -4.76 4.76 o 6 7 1 310.94 310.97 21.86 o 7 7 1 0.04 0.33 7.93 o 8 7 1 235.75 237.26 23.03 o 9 7 1 15.28 15.47 9.05 o 10 7 1 454.31 436.14 26.96 o -9 8 1 166.98 179.29 17.14 o -8 8 1 84.62 91.04 11.48 o -7 8 1 30.21 41.26 8.97 o -6 8 1 132.66 145.05 11.67 o -5 8 1 62.90 74.84 8.85 o -4 8 1 129.54 123.77 11.16 o -3 8 1 0.39 11.04 7.18 o -2 8 1 97.58 99.83 7.48 o -1 8 1 30.55 14.98 7.14 o 0 8 1 132.06 132.33 8.44 o 1 8 1 202.53 224.12 18.44 o 2 8 1 13.13 21.93 6.54 o 3 8 1 115.41 117.49 8.00 o 4 8 1 146.77 159.13 13.90 o 5 8 1 232.99 246.28 14.40 o 6 8 1 252.59 285.52 25.91 o 7 8 1 7.30 20.10 11.42 o 8 8 1 43.07 46.89 11.57 o -6 9 1 33.07 23.34 9.82 o -5 9 1 288.31 331.36 19.13 o -4 9 1 1050.74 1166.19 41.89 o -3 9 1 470.94 541.19 23.93 o -2 9 1 46.42 38.92 9.27 o -1 9 1 198.88 194.09 13.22 o 0 9 1 745.18 864.82 32.28 o 1 9 1 119.48 112.05 11.23 o 2 9 1 108.98 98.81 11.55 o 3 9 1 144.26 184.94 14.39 o 4 9 1 268.81 285.41 22.04 o 5 9 1 7.49 -4.23 9.16 o 6 9 1 2.70 -4.98 14.08 o -15 0 2 0.64 0.01 9.62 o -14 0 2 2.46 -3.63 7.56 o -13 0 2 106.56 114.38 12.87 o -12 0 2 164.88 156.81 10.60 o -11 0 2 735.41 805.86 26.98 o -10 0 2 260.65 275.69 12.00 o -9 0 2 13350.72 14783.50 382.11 o -8 0 2 2411.98 2733.00 65.45 o -7 0 2 0.02 0.00 2.61 o -6 0 2 2504.66 2938.51 64.52 o -5 0 2 4823.67 5292.40 120.27 o -4 0 2 3486.05 3467.90 87.37 o -3 0 2 1517.18 1470.02 40.06 o 1 0 2 474.88 501.69 13.95 o 2 0 2 2708.70 2905.32 69.21 o 3 0 2 9361.33 9659.33 214.01 o 4 0 2 607.45 886.16 19.36 o 5 0 2 159.52 145.83 3.96 o 6 0 2 7179.55 8155.15 213.73 o 7 0 2 108.42 124.58 7.08 o 8 0 2 1433.88 1522.93 45.22 o 9 0 2 5732.81 6356.10 170.01 o 10 0 2 3465.95 3603.25 126.00 o 11 0 2 351.17 305.51 16.19 o 12 0 2 174.09 155.48 24.29 o 13 0 2 681.47 611.71 42.33 o 14 0 2 33.34 40.05 12.59 o -15 1 2 128.43 113.91 11.00 o -14 1 2 61.45 67.16 10.50 o -13 1 2 1638.24 1669.33 69.17 o -12 1 2 949.54 1067.51 29.96 o -11 1 2 105.07 104.86 5.71 o -10 1 2 465.77 499.63 11.57 o -9 1 2 344.49 385.70 7.81 o -8 1 2 569.66 678.10 18.32 o -7 1 2 717.74 730.32 17.89 o -6 1 2 6.55 6.71 1.73 o -5 1 2 1995.89 2041.23 37.20 o -4 1 2 1200.89 1314.95 27.75 o -3 1 2 2343.69 2472.44 50.04 o -2 1 2 16.03 15.10 5.03 o -1 1 2 265.78 266.38 4.48 o 0 1 2 6671.59 5933.50 94.80 o 1 1 2 3721.70 3545.07 87.92 o 2 1 2 1110.72 1022.59 19.02 o 3 1 2 272.88 346.63 7.95 o 4 1 2 7.57 9.11 1.61 o 5 1 2 4595.55 4681.25 86.24 o 6 1 2 4.52 10.84 2.72 o 7 1 2 1105.05 1170.16 20.09 o 8 1 2 258.17 268.16 6.48 o 9 1 2 511.46 509.77 11.86 o 10 1 2 14.18 10.27 3.05 o 11 1 2 35.41 37.46 3.12 o 12 1 2 931.39 909.64 39.90 o 13 1 2 472.38 461.47 24.65 o 14 1 2 109.04 117.91 13.51 o -15 2 2 22.90 21.31 9.85 o -14 2 2 35.48 33.30 9.39 o -13 2 2 3.56 1.14 4.61 o -12 2 2 200.61 199.41 8.95 o -11 2 2 98.59 94.39 5.12 o -10 2 2 20.45 20.83 3.22 o -9 2 2 309.97 327.53 9.63 o -8 2 2 706.79 721.96 25.44 o -7 2 2 355.70 401.85 11.34 o -6 2 2 104.73 126.38 4.34 o -5 2 2 640.71 632.74 19.96 o -4 2 2 816.52 887.52 26.03 o -3 2 2 9240.44 9329.81 179.49 o -2 2 2 27.98 27.35 1.86 o -1 2 2 301.31 261.47 3.90 o 0 2 2 907.47 825.82 12.16 o 1 2 2 375.78 327.17 6.74 o 2 2 2 55.44 55.52 2.20 o 3 2 2 2564.41 2704.64 41.80 o 4 2 2 2253.28 2445.66 52.48 o 5 2 2 1025.45 1121.80 37.27 o 6 2 2 785.85 826.66 26.45 o 7 2 2 69.95 84.67 3.82 o 8 2 2 30.54 41.16 4.73 o 9 2 2 38.85 46.56 3.94 o 10 2 2 90.79 71.30 4.57 o 11 2 2 51.58 36.47 4.62 o 12 2 2 8.02 10.15 7.10 o 13 2 2 0.12 -0.32 9.70 o 14 2 2 20.37 18.41 10.92 o -14 3 2 3.28 -2.29 6.87 o -13 3 2 3.35 -2.04 6.00 o -12 3 2 341.52 314.21 16.12 o -11 3 2 0.13 -3.79 3.79 o -10 3 2 399.99 412.09 16.06 o -9 3 2 141.42 127.68 5.10 o -8 3 2 94.37 73.67 4.22 o -7 3 2 0.90 -0.94 2.51 o -6 3 2 72.54 72.59 3.48 o -5 3 2 543.22 586.93 19.67 o -4 3 2 380.51 385.96 8.50 o -3 3 2 35.60 46.58 2.17 o -2 3 2 10.78 7.36 1.89 o -1 3 2 1811.09 1731.41 24.10 o 0 3 2 4335.47 3830.92 50.12 o 1 3 2 91.88 101.79 2.73 o 2 3 2 3254.48 3255.40 66.60 o 3 3 2 754.46 848.49 27.10 o 4 3 2 182.81 210.17 7.19 o 5 3 2 2.71 -2.16 2.16 o 6 3 2 26.72 23.36 2.64 o 7 3 2 25.77 27.65 3.33 o 8 3 2 189.58 158.46 5.55 o 9 3 2 26.49 23.38 3.33 o 10 3 2 616.72 575.84 21.43 o 11 3 2 0.90 6.41 6.14 o 12 3 2 540.27 508.73 47.85 o 13 3 2 21.84 27.02 7.80 o -14 4 2 11.79 -3.07 7.32 o -13 4 2 1.87 -2.31 6.94 o -12 4 2 99.52 102.40 11.14 o -11 4 2 478.85 520.35 25.19 o -10 4 2 36.47 25.73 4.85 o -9 4 2 2928.81 2746.09 161.05 o -8 4 2 557.68 532.11 19.19 o -7 4 2 69.58 74.35 3.67 o -6 4 2 729.92 747.50 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