#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2208733.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208733_Fobs loop_ _publ_author_name 'Janzen, Daron E.' 'Botros, Maikel E.' 'Helton, Gregory P.' 'VanDerveer, Donald G.' 'Grant, Gregory J.' _publ_section_title ; 1,4,10,13-Tetraoxa-7,16-diazoniacyclooctadecane bis(hexafluorophosphate): PF~6~^{-^} acting as a pseudohalide ; _journal_coeditor_code SQ3010 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1550 _journal_page_last o1552 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.647 _cell_angle_gamma 90.000 _cell_length_a 9.2690 _cell_length_b 10.3327 _cell_length_c 12.2638 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.8393 _[local]_cod_data_source_file sq3010Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' grant68a in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 143.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5226.04 4866.59 37.64 o 4 0 0 605.29 633.87 5.24 o 6 0 0 247.36 280.01 3.96 o 8 0 0 137.54 137.59 5.56 o 10 0 0 93.68 81.66 5.21 o 1 1 0 85.89 87.24 1.61 o 2 1 0 7367.35 6609.19 61.42 o 3 1 0 513.26 588.60 3.86 o 4 1 0 2.59 3.38 0.75 o 5 1 0 333.43 305.26 4.59 o 6 1 0 253.88 234.01 3.09 o 7 1 0 4.70 5.67 1.93 o 8 1 0 314.13 306.12 5.95 o 9 1 0 42.47 54.88 3.29 o 10 1 0 70.08 57.75 3.30 o 0 2 0 13011.17 10391.44 97.45 o 1 2 0 3360.27 3533.72 20.32 o 2 2 0 407.78 434.70 7.29 o 3 2 0 23.00 20.91 1.66 o 4 2 0 2537.28 2781.56 15.71 o 5 2 0 397.16 359.56 3.61 o 6 2 0 41.58 32.36 1.83 o 7 2 0 410.41 428.18 6.64 o 8 2 0 55.75 53.91 3.58 o 9 2 0 92.73 84.62 4.56 o 10 2 0 106.55 96.20 4.02 o 1 3 0 247.14 210.91 3.38 o 2 3 0 831.37 832.57 8.59 o 3 3 0 2731.06 2639.55 14.53 o 4 3 0 248.27 289.80 4.72 o 5 3 0 2289.16 2349.12 13.89 o 6 3 0 166.14 171.26 5.63 o 7 3 0 34.65 31.28 2.96 o 8 3 0 758.36 869.58 7.30 o 9 3 0 10.62 13.58 1.50 o 10 3 0 26.73 20.70 3.73 o 0 4 0 863.72 709.33 7.54 o 1 4 0 19.25 25.23 1.64 o 2 4 0 691.60 655.48 6.30 o 3 4 0 404.60 337.91 3.94 o 4 4 0 768.55 704.72 6.19 o 5 4 0 12.62 11.33 1.89 o 6 4 0 1266.37 1317.22 9.23 o 7 4 0 328.22 297.53 4.31 o 8 4 0 1.05 2.92 1.72 o 9 4 0 6.13 5.18 0.96 o 1 5 0 311.78 277.37 4.25 o 2 5 0 684.83 697.29 8.69 o 3 5 0 113.12 102.08 4.50 o 4 5 0 155.62 157.85 3.95 o 5 5 0 1.68 4.71 3.16 o 6 5 0 823.01 870.99 8.16 o 7 5 0 8.99 8.14 1.44 o 8 5 0 515.65 589.38 12.39 o 9 5 0 2.78 5.15 2.00 o 0 6 0 495.25 391.87 9.07 o 1 6 0 2.56 1.46 2.05 o 2 6 0 40.75 29.47 2.10 o 3 6 0 1170.59 1129.88 12.65 o 4 6 0 291.56 290.08 7.38 o 5 6 0 70.61 67.68 3.00 o 6 6 0 63.98 62.16 2.46 o 7 6 0 6.18 1.91 2.09 o 8 6 0 99.47 88.32 3.10 o 9 6 0 1.06 2.44 1.47 o 1 7 0 37.03 33.63 2.89 o 2 7 0 211.22 182.96 3.64 o 3 7 0 642.52 651.02 12.86 o 4 7 0 48.46 35.60 2.53 o 5 7 0 89.75 90.42 4.85 o 6 7 0 6.03 5.30 1.32 o 7 7 0 20.02 26.33 2.21 o 8 7 0 11.81 5.49 2.29 o 0 8 0 949.08 948.83 26.64 o 1 8 0 321.36 331.76 5.14 o 2 8 0 194.75 196.46 3.88 o 3 8 0 0.05 3.26 3.00 o 4 8 0 5.46 5.65 1.90 o 5 8 0 0.04 2.84 2.52 o 6 8 0 16.04 13.38 1.79 o 7 8 0 0.43 4.02 2.36 o 1 9 0 69.52 81.26 3.27 o 2 9 0 819.06 796.19 8.31 o 3 9 0 64.26 76.96 3.18 o 4 9 0 6.01 7.11 2.20 o 5 9 0 37.30 26.75 2.45 o 6 9 0 41.56 39.47 3.17 o 7 9 0 75.86 67.98 4.24 o 0 10 0 472.05 485.07 27.22 o 1 10 0 142.18 129.28 5.96 o 2 10 0 40.13 40.90 2.60 o 3 10 0 140.04 149.44 3.88 o 4 10 0 151.01 144.09 6.79 o 5 10 0 40.08 37.58 3.10 o 6 10 0 20.18 27.18 2.68 o 1 11 0 82.92 71.97 3.29 o 2 11 0 96.34 94.23 4.05 o 3 11 0 64.04 65.70 4.49 o 4 11 0 18.88 12.06 2.40 o 0 12 0 122.38 162.36 8.49 o 1 12 0 131.40 126.25 6.33 o 2 12 0 47.14 47.20 4.29 o -9 0 1 1037.99 999.73 40.59 o -7 0 1 0.88 2.23 3.18 o -5 0 1 4188.28 4407.25 41.12 o -3 0 1 41.05 75.10 2.56 o 1 0 1 6331.90 5983.35 52.21 o 3 0 1 1928.39 2149.07 14.93 o 5 0 1 956.86 1068.58 9.37 o 7 0 1 1650.14 1775.61 14.79 o 9 0 1 429.45 451.52 28.97 o -10 1 1 10.94 4.75 2.35 o -9 1 1 94.16 81.99 3.58 o -8 1 1 47.34 42.61 2.91 o -7 1 1 53.08 73.68 3.99 o -6 1 1 32.27 31.62 2.21 o -5 1 1 10.07 2.58 0.78 o -4 1 1 2950.63 2799.86 23.40 o -3 1 1 135.27 146.64 3.29 o -2 1 1 105.54 153.07 4.40 o -1 1 1 3425.16 3283.09 30.58 o 0 1 1 1491.59 1343.49 9.54 o 1 1 1 5018.52 4465.22 86.27 o 2 1 1 38.99 31.85 3.28 o 3 1 1 3.97 1.35 1.47 o 4 1 1 278.37 344.17 3.05 o 5 1 1 312.47 279.58 2.93 o 6 1 1 101.83 111.47 2.64 o 7 1 1 78.81 50.25 2.51 o 8 1 1 2.59 3.65 2.06 o 9 1 1 265.40 226.19 5.49 o 10 1 1 81.89 70.77 4.35 o -10 2 1 0.20 4.37 2.43 o -9 2 1 352.30 409.79 8.81 o -8 2 1 110.20 78.68 2.08 o -7 2 1 26.86 32.49 1.72 o -6 2 1 321.96 322.25 3.98 o -5 2 1 58.87 48.73 1.59 o -4 2 1 247.12 247.92 4.65 o -3 2 1 1598.40 1416.92 16.80 o -2 2 1 104.42 120.93 4.15 o -1 2 1 1302.65 1333.11 20.44 o 0 2 1 708.21 821.08 10.61 o 1 2 1 20590.82 16730.63 250.07 o 2 2 1 2272.51 2165.45 16.90 o 3 2 1 1228.93 1313.17 11.74 o 4 2 1 29.03 21.16 1.47 o 5 2 1 766.69 789.34 6.06 o 6 2 1 1.73 4.38 1.07 o 7 2 1 2281.97 2505.22 13.88 o 8 2 1 318.30 268.58 4.13 o 9 2 1 152.22 139.75 3.27 o -10 3 1 31.40 24.40 2.83 o -9 3 1 98.64 100.53 3.38 o -8 3 1 95.43 115.15 3.42 o -7 3 1 314.14 370.28 4.32 o -6 3 1 534.47 674.85 8.77 o -5 3 1 663.06 619.30 5.77 o -4 3 1 67.14 50.30 2.32 o -3 3 1 391.09 378.94 3.87 o -2 3 1 1005.90 960.76 6.25 o -1 3 1 7738.62 6823.90 54.16 o 0 3 1 449.53 407.83 6.41 o 1 3 1 472.92 501.25 8.56 o 2 3 1 482.26 482.91 6.74 o 3 3 1 2.52 4.46 1.21 o 4 3 1 255.84 319.65 3.55 o 5 3 1 530.74 530.35 5.20 o 6 3 1 70.45 58.48 2.06 o 7 3 1 179.33 180.71 4.40 o 8 3 1 8.16 2.83 0.80 o 9 3 1 209.68 240.38 5.42 o -10 4 1 0.65 0.99 2.11 o -9 4 1 116.38 145.26 3.86 o -8 4 1 31.64 37.89 1.58 o -7 4 1 159.21 191.29 7.26 o -6 4 1 26.92 21.78 2.63 o -5 4 1 807.36 783.79 8.14 o -4 4 1 0.51 3.33 2.27 o -3 4 1 2609.86 2309.46 15.62 o -2 4 1 2243.92 2118.53 13.07 o -1 4 1 275.58 295.93 3.21 o 0 4 1 12.11 0.51 6.94 o 1 4 1 457.86 536.96 4.68 o 2 4 1 295.51 320.32 5.30 o 3 4 1 675.04 635.86 9.51 o 4 4 1 743.27 765.28 5.88 o 5 4 1 254.17 263.87 4.18 o 6 4 1 7.03 12.31 1.70 o 7 4 1 440.04 495.35 7.04 o 8 4 1 115.34 83.32 2.31 o 9 4 1 69.15 75.09 2.27 o -9 5 1 32.31 36.49 1.67 o -8 5 1 28.20 28.40 2.83 o -7 5 1 8.01 9.04 1.35 o -6 5 1 2.55 5.19 1.76 o -5 5 1 151.16 117.02 3.33 o -4 5 1 108.75 99.51 2.99 o -3 5 1 281.13 223.89 3.55 o -2 5 1 84.11 74.44 2.50 o -1 5 1 776.32 639.59 5.45 o 0 5 1 86.03 99.32 3.85 o 1 5 1 656.21 625.78 7.65 o 2 5 1 1518.62 1457.59 17.86 o 3 5 1 1913.37 2018.57 13.55 o 4 5 1 940.40 988.15 9.11 o 5 5 1 729.56 764.37 10.78 o 6 5 1 37.15 21.07 2.02 o 7 5 1 160.41 170.49 3.47 o 8 5 1 6.38 8.92 1.89 o 9 5 1 31.77 22.81 1.63 o -9 6 1 12.61 17.98 2.29 o -8 6 1 6.35 3.74 1.25 o -7 6 1 154.56 157.48 3.35 o -6 6 1 0.00 3.00 2.38 o -5 6 1 601.55 604.55 6.94 o -4 6 1 24.89 27.14 2.24 o -3 6 1 2205.46 2156.24 13.75 o -2 6 1 1206.31 1221.26 8.56 o -1 6 1 105.85 96.64 2.64 o 0 6 1 14.48 9.84 1.64 o 1 6 1 213.31 165.57 3.21 o 2 6 1 18.29 17.98 1.89 o 3 6 1 1484.89 1568.02 17.67 o 4 6 1 71.67 79.42 3.25 o 5 6 1 37.46 29.41 3.12 o 6 6 1 0.04 3.20 2.29 o 7 6 1 289.29 265.40 7.33 o 8 6 1 32.24 24.07 2.38 o -8 7 1 1.01 1.27 1.79 o -7 7 1 1.89 5.53 1.77 o -6 7 1 45.00 37.01 4.21 o -5 7 1 12.56 14.52 2.93 o -4 7 1 0.07 -7.51 9.15 o -3 7 1 243.79 221.06 7.56 o -2 7 1 713.94 675.89 8.84 o -1 7 1 3807.14 3928.42 31.31 o 0 7 1 552.50 596.12 6.88 o 1 7 1 210.51 194.11 5.02 o 2 7 1 395.44 414.21 5.75 o 3 7 1 470.47 487.31 7.54 o 4 7 1 101.79 113.83 3.60 o 5 7 1 99.76 129.44 4.81 o 6 7 1 0.07 1.75 1.94 o 7 7 1 3.71 10.19 2.44 o 8 7 1 27.10 29.41 3.24 o -8 8 1 4.65 3.01 2.26 o -7 8 1 23.29 21.95 2.96 o -6 8 1 4.20 5.46 1.59 o -5 8 1 105.67 91.21 9.99 o -4 8 1 178.90 185.36 5.42 o -3 8 1 1762.43 1866.50 13.08 o -2 8 1 130.85 152.92 3.52 o -1 8 1 297.87 275.40 5.41 o 0 8 1 288.98 267.49 4.54 o 1 8 1 735.74 725.44 10.03 o 2 8 1 196.84 202.50 3.94 o 3 8 1 199.15 194.41 4.13 o 4 8 1 309.63 326.32 6.85 o 5 8 1 127.69 139.63 3.79 o 6 8 1 4.35 6.13 1.91 o 7 8 1 0.12 2.54 2.55 o -7 9 1 17.10 19.42 2.20 o -6 9 1 4.43 8.46 1.39 o -5 9 1 18.00 26.31 3.07 o -4 9 1 116.91 123.18 6.79 o -3 9 1 786.60 798.62 20.22 o -2 9 1 1450.54 1554.88 11.68 o -1 9 1 681.29 651.83 9.73 o 0 9 1 617.11 635.49 9.91 o 1 9 1 1.19 4.69 1.90 o 2 9 1 310.89 367.07 5.79 o 3 9 1 20.74 15.39 1.81 o 4 9 1 75.57 92.81 3.50 o 5 9 1 2.20 7.19 1.55 o 6 9 1 12.81 10.64 1.61 o -6 10 1 50.41 51.14 7.16 o -5 10 1 31.35 31.85 2.48 o -4 10 1 111.02 115.06 3.53 o -3 10 1 0.47 1.21 2.88 o -2 10 1 2.43 3.21 1.87 o -1 10 1 162.23 143.05 3.67 o 0 10 1 33.71 28.61 2.53 o 1 10 1 0.22 5.14 2.72 o 2 10 1 121.09 117.54 4.82 o 3 10 1 14.85 16.42 2.03 o 4 10 1 43.03 42.80 2.81 o 5 10 1 24.05 35.76 2.95 o -4 11 1 98.41 91.92 4.16 o -3 11 1 31.89 41.07 3.32 o -2 11 1 129.04 120.54 5.14 o -1 11 1 19.70 19.29 2.22 o 0 11 1 181.76 188.78 5.33 o 1 11 1 58.15 70.62 4.14 o 2 11 1 50.40 44.34 2.80 o 3 11 1 5.15 4.69 2.02 o 4 11 1 8.78 3.67 4.09 o -2 12 1 6.44 4.53 1.99 o -1 12 1 2.03 6.05 2.62 o 0 12 1 31.06 30.27 4.48 o 1 12 1 45.03 51.36 4.58 o -10 0 2 13.63 7.08 3.89 o -8 0 2 118.14 112.91 11.89 o -6 0 2 663.72 699.50 12.92 o -4 0 2 96.13 106.88 3.10 o 0 0 2 2490.85 2551.92 23.74 o 2 0 2 653.28 712.98 6.08 o 4 0 2 523.37 541.95 6.14 o 6 0 2 15.92 5.51 1.30 o 8 0 2 75.90 55.25 2.95 o -10 1 2 65.21 45.14 5.85 o -9 1 2 0.76 2.74 2.53 o -8 1 2 500.25 458.75 6.15 o -7 1 2 4.67 12.62 1.76 o -6 1 2 213.43 254.99 5.92 o -5 1 2 1408.14 1495.76 13.06 o -4 1 2 7.18 2.05 1.41 o -3 1 2 36.65 38.56 1.42 o -2 1 2 2802.67 2582.63 22.50 o -1 1 2 61.78 66.39 2.28 o 0 1 2 4763.74 4639.96 40.21 o 1 1 2 3873.95 3583.72 17.33 o 2 1 2 2769.87 2514.35 11.42 o 3 1 2 228.64 194.97 2.23 o 4 1 2 150.08 172.57 2.22 o 5 1 2 397.07 327.75 3.27 o 6 1 2 0.39 0.20 1.71 o 7 1 2 3.12 6.74 1.53 o 8 1 2 40.41 34.26 2.33 o 9 1 2 0.41 4.10 2.01 o -10 2 2 0.10 3.75 2.75 o -9 2 2 90.35 95.65 3.95 o -8 2 2 416.49 408.53 16.96 o -7 2 2 37.45 33.94 2.55 o -6 2 2 36.55 29.64 2.15 o -5 2 2 516.00 513.63 3.72 o -4 2 2 90.98 100.19 2.28 o -3 2 2 2864.06 2853.82 15.62 o -1 2 2 2818.04 2867.72 20.53 o 0 2 2 11801.36 10597.41 68.12 o 1 2 2 1.57 -2.89 9.15 o 2 2 2 454.17 518.51 4.32 o 3 2 2 898.65 825.81 6.13 o 4 2 2 874.96 878.59 6.14 o 5 2 2 502.64 546.04 4.70 o 6 2 2 1569.23 1674.25 10.05 o 7 2 2 127.01 133.60 4.77 o 8 2 2 232.01 227.44 3.92 o 9 2 2 16.50 17.81 1.65 o -10 3 2 251.60 264.93 5.48 o -9 3 2 40.77 24.45 3.59 o -8 3 2 244.36 257.35 10.22 o -7 3 2 4.68 2.18 1.99 o -6 3 2 4.04 2.73 1.13 o -5 3 2 1707.20 1924.84 19.33 o -4 3 2 4036.87 3976.71 23.95 o -3 3 2 158.13 171.64 2.38 o -2 3 2 1754.17 1721.01 15.20 o -1 3 2 2310.55 2120.73 11.56 o 0 3 2 2516.50 2428.97 20.51 o 1 3 2 107.51 77.15 2.19 o 2 3 2 148.52 154.01 2.94 o 3 3 2 1.32 2.45 2.06 o 4 3 2 210.31 244.95 3.36 o 5 3 2 342.61 287.88 4.32 o 6 3 2 2000.67 2161.19 13.58 o 7 3 2 1.03 0.55 2.14 o 8 3 2 355.02 363.17 7.00 o 9 3 2 0.31 4.69 2.31 o -10 4 2 42.70 51.98 5.03 o -9 4 2 0.96 3.84 1.84 o -8 4 2 35.31 41.07 1.68 o -7 4 2 13.79 18.96 1.87 o -6 4 2 440.67 426.07 7.30 o -5 4 2 91.62 87.28 6.35 o -4 4 2 16.65 22.80 2.65 o -3 4 2 9.81 4.02 0.97 o -2 4 2 1399.75 1250.49 8.67 o -1 4 2 1129.54 1126.31 8.10 o 0 4 2 2445.22 2278.29 17.64 o 1 4 2 21.00 27.84 2.05 o 2 4 2 17.94 12.15 3.97 o 3 4 2 47.19 48.53 2.34 o 4 4 2 364.16 318.87 8.06 o 5 4 2 332.18 307.11 8.61 o 6 4 2 60.81 47.37 2.15 o 7 4 2 160.02 151.04 3.41 o 8 4 2 411.80 431.02 4.63 o 9 4 2 11.16 6.98 2.60 o -9 5 2 0.91 3.47 2.08 o -8 5 2 114.44 119.20 4.75 o -7 5 2 34.84 21.86 1.64 o -6 5 2 0.81 4.20 2.00 o -5 5 2 943.89 1040.85 11.57 o -4 5 2 3598.22 3631.00 19.16 o -3 5 2 1132.76 1157.07 13.95 o -2 5 2 47.95 48.99 2.63 o -1 5 2 1562.03 1523.05 10.03 o 0 5 2 124.82 114.90 2.53 o 1 5 2 11.33 4.70 1.26 o 2 5 2 3190.13 3181.24 22.05 o 3 5 2 0.01 -0.20 2.53 o 4 5 2 490.06 485.28 5.51 o 5 5 2 225.60 243.07 9.13 o 6 5 2 1192.73 1318.36 11.25 o 7 5 2 16.79 15.68 2.16 o 8 5 2 2.54 1.97 1.88 o -9 6 2 46.00 39.43 3.28 o -8 6 2 0.82 2.49 1.51 o -7 6 2 6.18 5.93 1.81 o -6 6 2 16.88 14.11 1.76 o -5 6 2 208.15 195.99 3.62 o -4 6 2 94.17 77.64 4.72 o -3 6 2 54.58 53.81 3.82 o -2 6 2 4336.90 4409.13 24.12 o -1 6 2 766.33 783.59 6.34 o 0 6 2 38.83 44.23 3.05 o 1 6 2 274.92 257.74 4.02 o 2 6 2 9.89 1.52 2.13 o 3 6 2 183.79 194.88 6.29 o 4 6 2 1915.67 2115.62 16.30 o 5 6 2 35.87 22.63 2.08 o 6 6 2 27.71 17.85 1.93 o 7 6 2 3.20 4.89 1.44 o 8 6 2 13.31 18.32 1.74 o -8 7 2 3.03 -0.11 2.34 o -7 7 2 137.42 135.63 3.71 o -6 7 2 7.79 6.15 1.56 o -5 7 2 11.44 5.95 1.28 o -4 7 2 640.93 632.18 11.56 o -3 7 2 227.92 233.99 5.68 o -2 7 2 1455.63 1515.00 12.50 o -1 7 2 47.22 56.72 2.72 o 0 7 2 136.75 140.46 3.13 o 1 7 2 34.76 37.69 2.37 o 2 7 2 51.07 51.94 2.56 o 3 7 2 120.72 112.28 3.72 o 4 7 2 5.13 5.88 3.02 o 5 7 2 336.88 383.36 8.30 o 6 7 2 513.01 560.54 8.26 o 7 7 2 12.81 8.42 1.71 o -8 8 2 20.27 19.62 1.95 o -7 8 2 0.03 3.88 1.70 o -6 8 2 159.76 154.81 3.64 o -5 8 2 277.11 303.24 10.25 o -4 8 2 25.82 16.70 3.14 o -3 8 2 209.75 187.13 3.69 o -2 8 2 326.44 338.51 9.33 o -1 8 2 137.54 138.50 6.30 o 0 8 2 481.82 496.90 5.65 o 1 8 2 0.29 6.03 2.77 o 2 8 2 63.63 48.37 2.93 o 3 8 2 3.00 3.90 2.85 o 4 8 2 765.13 852.23 9.97 o 5 8 2 98.68 92.35 3.08 o 6 8 2 9.85 6.58 1.57 o 7 8 2 45.11 44.68 5.51 o -7 9 2 0.06 3.91 2.04 o -6 9 2 0.02 2.74 1.65 o -5 9 2 103.32 89.50 3.22 o -4 9 2 81.87 94.44 3.21 o -3 9 2 0.01 -3.97 4.67 o -2 9 2 372.54 384.98 5.02 o -1 9 2 347.54 371.44 6.37 o 0 9 2 85.54 83.53 3.48 o 1 9 2 165.73 161.57 3.87 o 2 9 2 60.53 64.13 2.87 o 3 9 2 202.79 209.84 4.41 o 4 9 2 33.07 32.19 5.03 o 5 9 2 10.01 18.26 1.98 o 6 9 2 83.58 87.74 3.35 o -6 10 2 18.06 27.21 3.09 o -5 10 2 0.52 4.12 2.75 o -4 10 2 250.56 259.44 4.58 o -3 10 2 266.41 264.25 4.65 o -2 10 2 247.80 254.73 6.23 o -1 10 2 31.61 28.47 2.30 o 0 10 2 221.62 218.42 8.89 o 1 10 2 53.34 47.91 4.00 o 2 10 2 305.79 284.51 9.03 o 3 10 2 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