#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2208807.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208807_Fobs loop_ _publ_author_name 'Xiang, Jiang-Feng' 'Li, Ming' 'Wu, Si-Min' 'Yuan, Liang-Jie' 'Sun, Ju-Tang' _publ_section_title ; Diaquabis(pyridine-2,3-dicarboxylato)copper(II) ; _journal_coeditor_code BT2053 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1122 _journal_page_last m1123 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.945 _cell_angle_gamma 90.000 _cell_length_a 9.2115 _cell_length_b 7.9171 _cell_length_c 10.3631 _exptl_crystal_F_000 438.00 _reflns_d_resolution_high 0.7569 _[local]_cod_data_source_file bt2053Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 60116LM4_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 231.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 516.42 436.92 4.83 o 4 0 0 493.59 795.99 6.14 o 6 0 0 913.24 850.15 8.07 o 8 0 0 2697.08 2677.52 29.19 o 10 0 0 4.43 4.22 1.06 o 12 0 0 60.30 66.80 3.54 o 1 1 0 2072.09 2089.85 13.41 o 2 1 0 456.59 571.07 5.09 o 3 1 0 102.70 80.04 0.92 o 4 1 0 617.95 725.50 4.96 o 5 1 0 298.27 237.17 2.29 o 6 1 0 2.96 1.60 0.24 o 7 1 0 1485.71 1482.77 13.48 o 8 1 0 927.68 936.58 7.98 o 9 1 0 984.51 971.64 8.43 o 10 1 0 20.63 19.95 1.76 o 11 1 0 538.17 565.71 8.39 o 12 1 0 51.18 53.57 2.22 o 0 2 0 1372.17 1118.94 9.39 o 1 2 0 3751.39 4024.71 65.55 o 2 2 0 3736.21 3679.98 23.32 o 3 2 0 843.67 970.07 6.48 o 4 2 0 9239.17 9974.89 236.42 o 5 2 0 100.04 104.48 1.35 o 6 2 0 4.45 10.97 0.47 o 7 2 0 123.06 127.98 2.13 o 8 2 0 118.89 116.41 2.13 o 9 2 0 401.32 388.85 4.86 o 10 2 0 460.35 455.14 5.65 o 11 2 0 0.35 0.46 0.69 o 1 3 0 2442.25 2428.06 16.97 o 2 3 0 2797.99 3187.47 20.29 o 3 3 0 1257.53 1226.66 8.18 o 4 3 0 63.53 81.24 1.05 o 5 3 0 939.17 928.04 7.39 o 6 3 0 146.51 150.82 1.88 o 7 3 0 651.37 645.20 6.71 o 8 3 0 59.17 55.63 1.46 o 9 3 0 717.57 673.57 7.38 o 10 3 0 106.95 97.42 2.96 o 11 3 0 215.85 215.63 4.48 o 0 4 0 156.00 85.88 2.39 o 1 4 0 47.14 57.81 1.01 o 2 4 0 3531.32 3538.04 22.58 o 3 4 0 60.39 65.11 1.01 o 4 4 0 652.46 601.60 4.45 o 5 4 0 375.47 413.24 3.84 o 6 4 0 528.98 505.42 4.62 o 7 4 0 231.06 227.00 2.67 o 8 4 0 198.51 204.24 3.11 o 9 4 0 127.50 129.75 2.52 o 10 4 0 308.62 302.35 4.40 o 11 4 0 14.81 14.43 1.10 o 1 5 0 111.32 78.26 2.31 o 2 5 0 36.16 44.95 0.95 o 3 5 0 1724.41 1686.16 11.27 o 4 5 0 2.80 5.16 0.59 o 5 5 0 1600.71 1569.73 12.13 o 6 5 0 458.01 469.53 4.47 o 7 5 0 168.06 168.29 2.28 o 8 5 0 16.80 14.16 0.89 o 9 5 0 342.13 344.10 4.90 o 10 5 0 33.03 27.89 1.33 o 0 6 0 1940.29 1957.24 29.72 o 1 6 0 25.19 25.00 1.01 o 2 6 0 1720.19 1697.23 11.43 o 3 6 0 49.73 46.88 0.85 o 4 6 0 5.46 9.40 1.11 o 5 6 0 169.74 184.92 2.33 o 6 6 0 1588.92 1550.39 12.28 o 7 6 0 0.02 0.66 0.40 o 8 6 0 80.85 77.94 1.90 o 9 6 0 0.74 0.90 0.56 o 1 7 0 642.35 577.07 7.31 o 2 7 0 22.21 20.01 1.09 o 3 7 0 4.42 3.97 0.71 o 4 7 0 326.64 327.68 3.98 o 5 7 0 190.21 190.25 3.62 o 6 7 0 9.33 7.30 0.89 o 7 7 0 695.00 679.71 9.13 o 8 7 0 44.58 42.38 2.74 o 9 7 0 215.38 227.92 6.77 o 0 8 0 69.64 82.85 3.12 o 1 8 0 2.16 1.43 0.57 o 2 8 0 779.55 731.76 9.13 o 3 8 0 33.36 30.69 1.39 o 4 8 0 598.80 587.59 11.30 o 5 8 0 21.04 22.34 1.34 o 6 8 0 181.98 186.16 3.87 o 7 8 0 13.41 16.45 1.31 o 1 9 0 39.48 51.24 1.90 o 2 9 0 5.94 5.13 0.82 o 3 9 0 410.16 403.08 6.18 o 4 9 0 1.23 -0.97 0.93 o 5 9 0 166.72 170.54 5.48 o 6 9 0 37.69 36.33 2.64 o 0 10 0 82.65 79.34 3.51 o 1 10 0 10.99 8.83 1.02 o 2 10 0 58.46 64.24 2.26 o 3 10 0 0.98 1.45 1.13 o -11 0 1 929.30 919.03 17.09 o -9 0 1 7.93 7.78 0.66 o -7 0 1 3767.36 3809.10 32.82 o -5 0 1 3552.03 3626.79 37.40 o -3 0 1 6069.39 5913.08 60.35 o -1 0 1 116.66 75.33 1.39 o 1 0 1 4609.49 4784.79 70.41 o 3 0 1 576.62 724.52 6.39 o 5 0 1 293.76 263.30 6.13 o 7 0 1 1343.28 1348.42 21.56 o 9 0 1 8.62 8.18 1.26 o 11 0 1 304.13 308.37 7.80 o -12 1 1 249.04 238.54 4.96 o -11 1 1 23.61 21.56 1.16 o -10 1 1 190.00 194.29 2.72 o -9 1 1 480.77 469.46 4.75 o -8 1 1 148.88 145.11 2.37 o -7 1 1 0.03 0.40 0.41 o -6 1 1 271.50 239.90 2.26 o -5 1 1 208.27 230.21 1.82 o -4 1 1 223.50 148.17 1.25 o -3 1 1 6.98 7.79 0.42 o -2 1 1 2918.47 2906.51 17.21 o -1 1 1 171.86 213.51 1.70 o 0 1 1 10673.63 10073.70 667.74 o 1 1 1 2113.73 2297.56 23.53 o 2 1 1 2062.54 2079.34 17.25 o 3 1 1 90.20 120.29 1.64 o 4 1 1 2373.90 2329.50 16.94 o 5 1 1 49.57 60.62 0.78 o 6 1 1 2464.41 2368.22 19.90 o 7 1 1 36.73 42.99 1.33 o 8 1 1 1676.79 1695.20 15.56 o 9 1 1 6.42 5.22 0.80 o 10 1 1 154.16 150.42 3.39 o 11 1 1 28.36 29.44 2.35 o -11 2 1 323.18 351.85 4.91 o -10 2 1 65.36 57.17 1.42 o -9 2 1 498.47 506.29 5.87 o -8 2 1 5.49 6.49 0.62 o -7 2 1 1220.67 1264.24 11.76 o -6 2 1 3.18 3.13 0.29 o -5 2 1 357.83 248.68 2.44 o -4 2 1 14.89 20.21 0.38 o -3 2 1 7550.78 7739.91 49.23 o -2 2 1 125.05 150.35 1.27 o -1 2 1 4835.99 4926.03 35.91 o 0 2 1 7.30 10.96 0.64 o 1 2 1 1346.89 1318.83 10.10 o 2 2 1 452.35 507.89 3.56 o 3 2 1 124.95 79.11 1.15 o 4 2 1 50.04 77.61 1.07 o 5 2 1 130.42 91.91 1.27 o 6 2 1 98.82 92.99 1.35 o 7 2 1 823.14 790.00 7.87 o 8 2 1 128.81 127.12 2.26 o 9 2 1 844.13 843.05 10.75 o 10 2 1 66.54 66.22 4.20 o 11 2 1 339.57 356.17 6.13 o -11 3 1 18.29 17.48 1.13 o -10 3 1 758.95 756.31 8.30 o -9 3 1 22.85 24.98 1.55 o -8 3 1 198.87 193.03 2.94 o -7 3 1 5.97 5.68 0.54 o -6 3 1 127.56 95.02 1.39 o -5 3 1 506.49 573.84 4.87 o -4 3 1 1907.07 1814.39 15.07 o -3 3 1 238.43 305.17 2.40 o -2 3 1 3710.17 3597.72 22.86 o -1 3 1 1348.58 1632.30 9.69 o 0 3 1 34.91 13.28 0.39 o 1 3 1 5.98 4.34 0.22 o 2 3 1 3292.71 3304.94 21.05 o 3 3 1 1.92 0.59 0.21 o 4 3 1 2296.20 2444.93 17.91 o 5 3 1 248.44 304.54 2.98 o 6 3 1 737.19 704.92 5.98 o 7 3 1 5.83 4.77 0.48 o 8 3 1 191.32 198.01 3.01 o 9 3 1 6.22 7.43 0.95 o 10 3 1 344.14 336.75 5.72 o 11 3 1 1.45 0.50 0.72 o -11 4 1 124.41 133.78 2.83 o -10 4 1 18.22 18.88 1.10 o -9 4 1 1158.09 1049.24 10.61 o -8 4 1 7.92 8.71 0.72 o -7 4 1 4.30 6.34 0.48 o -6 4 1 3.15 5.74 1.15 o -5 4 1 763.56 745.23 6.20 o -4 4 1 423.17 439.20 3.41 o -3 4 1 4147.96 4246.60 27.04 o -2 4 1 67.84 69.99 0.73 o -1 4 1 3874.82 3919.30 30.24 o 0 4 1 97.31 106.43 1.00 o 1 4 1 5.76 24.74 0.60 o 2 4 1 27.66 29.51 0.88 o 3 4 1 1297.51 1208.03 8.19 o 4 4 1 323.36 349.21 2.87 o 5 4 1 1261.59 1262.88 9.88 o 6 4 1 39.82 39.64 0.94 o 7 4 1 426.76 443.99 4.33 o 8 4 1 39.62 42.03 1.34 o 9 4 1 440.68 428.44 5.36 o 10 4 1 0.05 1.72 1.92 o 11 4 1 151.78 177.82 4.80 o -10 5 1 250.16 260.43 4.07 o -9 5 1 44.89 40.83 1.44 o -8 5 1 509.83 483.07 5.69 o -7 5 1 40.76 33.51 0.95 o -6 5 1 268.90 274.18 3.01 o -5 5 1 15.24 18.58 1.73 o -4 5 1 33.60 28.36 0.64 o -3 5 1 0.02 0.26 0.19 o -2 5 1 1931.91 1786.15 11.84 o -1 5 1 146.34 137.52 1.42 o 0 5 1 1832.17 1868.17 13.04 o 1 5 1 444.74 521.19 3.54 o 2 5 1 1427.49 1370.82 9.26 o 3 5 1 433.85 456.99 3.60 o 4 5 1 129.00 133.76 1.52 o 5 5 1 403.45 407.49 3.92 o 6 5 1 1272.10 1276.64 10.24 o 7 5 1 27.92 28.03 0.92 o 8 5 1 286.79 281.13 3.92 o 9 5 1 12.76 12.84 0.92 o 10 5 1 208.15 219.64 4.80 o -9 6 1 110.81 114.98 3.15 o -8 6 1 99.93 92.77 2.07 o -7 6 1 895.23 850.79 7.46 o -6 6 1 37.29 36.31 1.01 o -5 6 1 3459.14 3315.05 24.50 o -4 6 1 384.34 386.04 3.30 o -3 6 1 152.75 160.86 1.80 o -2 6 1 131.79 130.07 1.69 o -1 6 1 660.90 624.30 5.29 o 0 6 1 0.30 1.41 0.28 o 1 6 1 1929.96 1889.89 14.06 o 2 6 1 8.08 7.59 0.39 o 3 6 1 379.40 362.23 3.52 o 4 6 1 12.44 12.53 0.58 o 5 6 1 89.23 93.61 3.38 o 6 6 1 106.58 110.59 2.85 o 7 6 1 220.13 240.88 3.50 o 8 6 1 45.39 40.98 2.82 o 9 6 1 169.24 186.43 4.08 o -9 7 1 1.92 1.45 1.19 o -8 7 1 108.74 107.72 4.25 o -7 7 1 25.43 25.49 1.18 o -6 7 1 535.28 524.13 5.93 o -5 7 1 0.65 0.38 0.43 o -4 7 1 301.40 294.74 4.32 o -3 7 1 55.14 51.90 1.11 o -2 7 1 16.40 17.83 0.81 o -1 7 1 299.94 268.47 3.35 o 0 7 1 636.85 656.37 6.57 o 1 7 1 71.39 75.93 1.57 o 2 7 1 1317.90 1248.12 11.38 o 3 7 1 18.20 21.17 0.76 o 4 7 1 944.07 958.42 8.86 o 5 7 1 11.16 11.14 0.76 o 6 7 1 523.69 523.39 6.01 o 7 7 1 0.90 1.65 0.74 o 8 7 1 113.65 110.48 2.41 o -7 8 1 178.86 157.73 3.64 o -6 8 1 17.16 17.94 1.29 o -5 8 1 254.90 251.06 6.77 o -4 8 1 16.63 15.65 1.13 o -3 8 1 579.23 568.94 7.55 o -2 8 1 16.93 18.02 1.14 o -1 8 1 472.95 432.15 6.15 o 0 8 1 28.47 26.80 1.26 o 1 8 1 53.53 58.43 1.84 o 2 8 1 0.27 1.04 0.89 o 3 8 1 196.65 194.73 3.65 o 4 8 1 34.43 35.97 2.35 o 5 8 1 345.18 357.78 8.16 o 6 8 1 18.52 21.17 1.39 o 7 8 1 11.70 12.24 1.59 o -6 9 1 74.44 77.53 3.64 o -5 9 1 0.80 0.39 1.00 o -4 9 1 415.77 406.74 9.16 o -3 9 1 34.43 30.05 2.46 o -2 9 1 22.30 22.07 1.34 o -1 9 1 47.97 40.30 1.68 o 0 9 1 239.21 236.65 4.34 o 1 9 1 0.00 -0.02 0.56 o 2 9 1 193.00 197.66 3.89 o 3 9 1 3.67 3.54 1.56 o 4 9 1 919.14 880.38 15.99 o 5 9 1 18.96 19.61 2.03 o 6 9 1 9.99 13.27 1.80 o -3 10 1 366.70 364.44 8.77 o -2 10 1 10.15 10.51 1.13 o -1 10 1 2.09 1.25 0.73 o 0 10 1 0.15 -0.47 0.59 o 1 10 1 191.82 199.09 4.15 o 2 10 1 36.86 40.47 1.88 o 3 10 1 419.68 429.51 9.87 o -12 0 2 788.62 777.52 15.56 o -10 0 2 436.23 440.37 5.37 o -8 0 2 7.88 7.95 0.62 o -6 0 2 1514.33 1523.52 16.57 o -4 0 2 2093.90 2093.78 21.85 o -2 0 2 11.01 7.56 0.79 o 0 0 2 4241.21 4399.71 64.57 o 2 0 2 1910.16 2340.75 23.49 o 4 0 2 2479.31 2423.88 24.55 o 6 0 2 2243.30 2247.86 36.39 o 8 0 2 2758.23 2769.97 42.16 o 10 0 2 53.32 60.13 2.96 o -12 1 2 4.52 5.11 0.82 o -11 1 2 181.50 200.01 2.93 o -10 1 2 7.93 7.23 0.64 o -9 1 2 45.02 43.94 1.01 o -8 1 2 7.91 11.38 0.58 o -7 1 2 1050.67 1092.36 7.97 o -6 1 2 8.56 9.03 0.45 o -5 1 2 3830.18 3751.07 22.73 o -4 1 2 196.96 216.92 1.68 o -3 1 2 8308.41 7790.29 80.91 o -2 1 2 27.97 20.02 0.33 o -1 1 2 3766.09 3680.75 40.80 o 0 1 2 1343.35 1523.43 15.49 o 1 1 2 8355.71 8633.74 86.49 o 2 1 2 633.45 762.14 6.64 o 3 1 2 335.94 253.85 2.61 o 4 1 2 0.14 0.25 0.24 o 5 1 2 1143.32 1076.04 7.35 o 6 1 2 284.18 316.88 3.45 o 7 1 2 537.87 499.85 5.86 o 8 1 2 8.26 9.28 0.85 o 9 1 2 274.85 282.56 4.81 o 10 1 2 586.45 564.74 8.11 o 11 1 2 2.29 3.96 1.18 o -11 2 2 47.16 47.62 1.39 o -10 2 2 671.39 680.59 10.74 o -9 2 2 12.47 11.02 0.78 o -8 2 2 1013.11 977.32 9.63 o -7 2 2 60.39 58.61 2.90 o -6 2 2 647.77 606.36 5.12 o -5 2 2 67.72 82.85 0.99 o -4 2 2 1514.16 1424.88 8.58 o -3 2 2 41.94 38.46 0.46 o -2 2 2 1045.09 936.47 6.24 o -1 2 2 3.16 6.44 0.34 o 0 2 2 681.56 640.66 5.63 o 1 2 2 57.11 62.71 1.90 o 2 2 2 88.64 59.92 1.22 o 3 2 2 254.11 298.43 2.67 o 4 2 2 3132.66 3327.97 24.03 o 5 2 2 42.56 56.90 1.13 o 6 2 2 960.66 894.69 8.34 o 7 2 2 16.18 19.37 0.78 o 8 2 2 1043.24 1048.90 17.74 o 9 2 2 3.10 2.78 0.70 o 10 2 2 105.39 105.50 2.84 o 11 2 2 4.78 3.89 0.88 o -11 3 2 69.10 75.49 2.08 o -10 3 2 4.13 4.58 0.91 o -9 3 2 450.11 443.25 5.37 o -8 3 2 3.90 9.23 1.83 o -7 3 2 25.43 31.13 1.03 o -6 3 2 196.94 193.42 2.20 o -5 3 2 586.97 545.98 4.68 o -4 3 2 97.72 144.50 1.39 o -3 3 2 6030.96 6427.74 40.66 o -2 3 2 359.88 406.77 3.03 o -1 3 2 5736.59 5779.88 61.99 o 0 3 2 186.35 229.35 3.20 o 1 3 2 91.98 182.09 1.53 o 2 3 2 341.77 387.48 3.21 o 3 3 2 1783.81 1685.23 13.92 o 4 3 2 43.82 43.09 0.83 o 5 3 2 2667.88 2683.30 19.77 o 6 3 2 188.74 215.25 2.45 o 7 3 2 314.60 302.24 3.67 o 8 3 2 28.03 27.95 2.03 o 9 3 2 86.55 92.95 2.71 o 10 3 2 55.72 49.45 1.98 o 11 3 2 275.58 289.67 5.45 o -11 4 2 24.87 30.80 1.44 o -10 4 2 264.68 270.44 4.07 o -9 4 2 10.56 9.90 0.81 o -8 4 2 730.86 665.46 7.16 o -7 4 2 89.34 88.17 1.80 o -6 4 2 654.09 633.29 5.52 o -5 4 2 505.84 486.68 4.36 o -4 4 2 2389.13 2320.49 15.16 o -3 4 2 173.55 203.80 1.85 o -2 4 2 1195.57 1127.21 7.63 o -1 4 2 251.85 286.80 2.33 o 0 4 2 38.15 100.08 1.02 o 1 4 2 377.46 428.35 5.14 o 2 4 2 2193.61 2263.98 14.71 o 3 4 2 16.00 21.96 0.52 o 4 4 2 2158.60 2232.52 16.57 o 5 4 2 38.44 38.68 0.88 o 6 4 2 487.79 493.09 4.75 o 7 4 2 5.87 6.41 0.52 o 8 4 2 20.41 22.84 1.28 o 9 4 2 91.65 86.03 2.48 o 10 4 2 478.38 446.56 7.00 o -10 5 2 1.11 1.28 0.59 o -9 5 2 174.81 176.33 3.05 o -8 5 2 39.77 44.92 1.84 o -7 5 2 369.63 349.20 3.69 o -6 5 2 0.53 1.88 0.35 o -5 5 2 1867.84 1810.60 13.82 o -4 5 2 48.36 43.56 0.80 o -3 5 2 47.32 47.24 0.95 o -2 5 2 114.12 117.26 1.31 o -1 5 2 1416.59 1366.82 10.36 o 0 5 2 178.82 185.53 1.75 o 1 5 2 1980.66 1928.15 14.19 o 2 5 2 95.73 102.55 1.19 o 3 5 2 2311.46 2268.37 14.94 o 4 5 2 916.96 953.66 6.83 o 5 5 2 14.93 16.16 1.10 o 6 5 2 0.00 -0.07 0.30 o 7 5 2 308.75 324.72 4.32 o 8 5 2 162.95 155.40 3.47 o 9 5 2 165.47 177.05 5.54 o 10 5 2 14.42 11.43 1.74 o -9 6 2 39.03 39.76 1.83 o -8 6 2 381.22 368.49 6.14 o -7 6 2 99.06 87.37 1.89 o -6 6 2 436.57 430.37 5.01 o -5 6 2 21.42 20.18 0.93 o -4 6 2 17.62 14.40 0.64 o -3 6 2 44.55 41.29 0.93 o -2 6 2 437.93 428.38 3.56 o -1 6 2 64.29 71.97 1.21 o 0 6 2 1400.78 1353.71 10.42 o 1 6 2 41.63 40.12 0.90 o 2 6 2 698.95 677.46 5.73 o 3 6 2 13.26 12.46 0.57 o 4 6 2 31.21 39.11 2.01 o 5 6 2 173.28 180.49 2.76 o 6 6 2 1734.60 1737.70 15.85 o 7 6 2 84.17 84.89 1.96 o 8 6 2 280.66 296.18 4.21 o 9 6 2 5.81 2.64 1.19 o -8 7 2 3.60 7.27 1.95 o -7 7 2 274.01 248.41 3.65 o -6 7 2 74.02 74.27 1.78 o -5 7 2 504.39 481.65 5.49 o -4 7 2 41.02 43.28 1.26 o -3 7 2 493.97 493.07 4.63 o -2 7 2 139.79 150.30 2.02 o -1 7 2 1269.48 1178.66 9.40 o 0 7 2 58.55 58.48 1.44 o 1 7 2 994.67 1011.96 9.52 o 2 7 2 168.14 169.52 2.55 o 3 7 2 321.94 322.87 3.96 o 4 7 2 65.33 61.59 1.29 o 5 7 2 47.92 58.01 4.94 o 6 7 2 82.44 83.82 1.95 o 7 7 2 231.40 243.18 3.71 o 8 7 2 12.00 15.52 1.28 o -7 8 2 18.50 17.59 1.31 o -6 8 2 171.34 164.56 3.62 o -5 8 2 0.45 0.19 0.60 o -4 8 2 92.62 98.20 2.56 o -3 8 2 37.02 38.64 1.27 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