#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:21:00 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181008 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/88/2208831.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208831_Fobs loop_ _publ_author_name 'Jing, Lin-Hai' 'Qin, Da-Bin' 'Gu, Shao-Jin' 'Zhang, Huan-Xia' 'Mao, Zhi-Hua' _publ_section_title ; Diphenyl naphthalene-1,4-dicarboxylate ; _journal_coeditor_code CI2045 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1717 _journal_page_last o1718 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.150 _cell_angle_gamma 90.000 _cell_length_a 13.9840 _cell_length_b 5.7797 _cell_length_c 22.2830 _exptl_crystal_F_000 768.00 _reflns_d_resolution_high 0.8286 _cod_data_source_file ci2045Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' J76 in space group P 1 21/c 1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 109.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 625.06 563.72 8.41 o 3 0 0 1340.26 1234.29 14.36 o 4 0 0 117.02 114.76 9.98 o 5 0 0 315.44 282.00 13.88 o 6 0 0 765.89 746.21 17.05 o 7 0 0 629.22 685.45 19.53 o 8 0 0 67.69 71.38 12.30 o 9 0 0 482.32 452.70 21.50 o 10 0 0 13.94 4.60 14.56 o 11 0 0 24.72 7.51 16.16 o 12 0 0 54.51 69.60 19.74 o 13 0 0 612.77 645.81 32.89 o 14 0 0 1870.57 2008.02 59.37 o 15 0 0 29.38 71.73 18.63 o 16 0 0 2.88 19.24 19.24 o 1 1 0 510.21 510.50 8.00 o 2 1 0 219.66 209.19 6.70 o 3 1 0 218.43 207.50 7.06 o 4 1 0 801.32 742.35 15.76 o 5 1 0 653.39 631.96 16.85 o 6 1 0 645.39 636.29 17.53 o 7 1 0 8.37 0.01 10.97 o 8 1 0 84.62 59.73 13.52 o 9 1 0 12.68 18.86 12.04 o 10 1 0 0.02 0.01 13.38 o 11 1 0 370.40 365.33 24.43 o 12 1 0 1.65 0.01 17.95 o 13 1 0 11.09 22.55 16.97 o 14 1 0 59.93 71.83 21.66 o 15 1 0 5.84 7.16 20.49 o 16 1 0 90.90 74.28 27.48 o 0 2 0 1042.28 1002.64 15.30 o 1 2 0 541.68 555.39 11.90 o 2 2 0 539.39 532.15 11.96 o 3 2 0 592.26 588.74 13.20 o 4 2 0 4.68 2.72 10.16 o 5 2 0 560.40 564.11 14.39 o 6 2 0 491.79 519.11 14.33 o 7 2 0 450.50 489.76 15.51 o 8 2 0 83.55 83.77 15.42 o 9 2 0 226.79 245.00 19.39 o 10 2 0 162.40 165.36 18.51 o 11 2 0 0.19 3.15 15.78 o 12 2 0 4.67 15.57 15.75 o 13 2 0 2.13 7.59 16.39 o 14 2 0 17.66 0.01 20.62 o 15 2 0 0.54 0.02 19.24 o 16 2 0 2.63 9.83 20.27 o 1 3 0 291.73 324.07 12.88 o 2 3 0 112.50 143.26 9.20 o 3 3 0 370.79 369.84 13.59 o 4 3 0 221.14 222.29 11.93 o 5 3 0 1.50 0.01 14.54 o 6 3 0 11.15 3.50 15.25 o 7 3 0 47.81 34.59 15.63 o 8 3 0 2.12 6.42 14.31 o 9 3 0 32.93 25.45 17.43 o 10 3 0 0.63 4.89 15.53 o 11 3 0 158.03 163.50 22.69 o 12 3 0 9.49 3.85 18.32 o 13 3 0 19.21 2.09 18.72 o 14 3 0 17.38 8.30 19.97 o 15 3 0 0.39 0.02 22.08 o 0 4 0 152.37 149.21 11.52 o 1 4 0 38.85 42.01 9.05 o 2 4 0 15.52 32.64 8.75 o 3 4 0 12.30 0.01 16.66 o 4 4 0 42.00 52.48 9.51 o 5 4 0 6.21 0.01 16.27 o 6 4 0 0.01 0.01 16.55 o 7 4 0 102.65 82.78 11.79 o 8 4 0 3.34 11.63 16.52 o 9 4 0 11.57 23.68 17.86 o 10 4 0 1.87 0.01 20.28 o 11 4 0 35.92 34.70 19.62 o 12 4 0 3.23 0.01 20.48 o 13 4 0 0.09 0.02 20.33 o 1 5 0 97.36 111.25 13.23 o 2 5 0 169.34 173.65 15.52 o 3 5 0 23.70 12.59 19.62 o 4 5 0 40.15 34.36 19.27 o 5 5 0 23.38 36.57 10.03 o 6 5 0 47.01 24.93 21.68 o 7 5 0 4.94 0.64 18.14 o 8 5 0 1.08 0.01 19.12 o 9 5 0 1.21 0.01 18.50 o 10 5 0 1.06 9.73 18.53 o 11 5 0 1.11 27.78 20.00 o 0 6 0 530.59 555.70 26.95 o 1 6 0 38.79 43.55 23.82 o 2 6 0 14.82 26.39 21.71 o 3 6 0 1.79 0.01 23.06 o 4 6 0 20.51 0.01 22.08 o 5 6 0 1.05 0.01 20.51 o 6 6 0 0.20 0.01 23.03 o 7 6 0 16.35 31.82 21.41 o 8 6 0 3.36 12.13 20.05 o -16 1 1 2.89 0.02 21.02 o -15 1 1 256.20 264.94 31.63 o -14 1 1 229.81 263.48 26.31 o -13 1 1 208.70 228.71 25.05 o -12 1 1 503.56 510.10 32.84 o -11 1 1 65.55 61.19 20.31 o -10 1 1 7.37 3.02 15.72 o -9 1 1 638.16 634.77 25.42 o -8 1 1 22.59 23.41 12.64 o -7 1 1 44.32 30.59 12.22 o -6 1 1 121.65 131.58 12.01 o -5 1 1 1938.63 1806.97 25.85 o -4 1 1 137.82 140.96 10.10 o -3 1 1 1445.32 1334.86 18.33 o -2 1 1 239.03 244.55 9.53 o -1 1 1 58.87 63.05 4.98 o 0 1 1 670.18 620.95 10.50 o 1 1 1 3272.78 3174.84 18.89 o 2 1 1 4978.67 4638.76 25.40 o 3 1 1 4869.11 4569.32 27.71 o 4 1 1 20.57 13.94 9.24 o 5 1 1 8.48 7.02 9.23 o 6 1 1 459.02 510.17 15.90 o 7 1 1 1133.04 1167.12 24.65 o 8 1 1 860.71 862.63 23.75 o 9 1 1 80.13 59.60 16.02 o 10 1 1 362.64 361.50 23.31 o 11 1 1 5.48 0.01 16.51 o 12 1 1 0.10 10.78 14.66 o 13 1 1 107.69 132.24 21.49 o 14 1 1 62.60 49.80 22.85 o 15 1 1 13.21 25.85 20.89 o 16 1 1 4.47 0.02 21.75 o -16 2 1 0.34 0.02 22.00 o -15 2 1 0.33 0.02 20.01 o -14 2 1 3.32 0.01 18.41 o -13 2 1 161.14 103.28 28.12 o -12 2 1 168.30 140.13 24.80 o -11 2 1 65.13 63.22 18.56 o -10 2 1 149.45 139.76 21.37 o -9 2 1 11.51 0.86 16.43 o -8 2 1 61.07 51.32 16.43 o -7 2 1 108.64 99.24 15.73 o -6 2 1 322.22 352.58 17.83 o -5 2 1 265.91 309.69 15.20 o -4 2 1 531.50 537.49 17.61 o -3 2 1 486.91 493.85 15.51 o -2 2 1 1827.60 1792.22 23.97 o -1 2 1 123.71 131.88 7.56 o 0 2 1 2234.49 2244.76 22.17 o 1 2 1 297.23 307.78 9.40 o 2 2 1 2286.14 2283.79 67.22 o 3 2 1 1286.41 1347.13 19.49 o 4 2 1 67.82 79.17 7.12 o 5 2 1 43.00 57.79 6.48 o 6 2 1 523.92 548.31 15.18 o 7 2 1 329.89 345.20 12.92 o 8 2 1 34.97 26.78 14.30 o 9 2 1 61.60 47.85 15.25 o 10 2 1 90.75 72.06 19.39 o 11 2 1 0.33 1.58 15.54 o 12 2 1 179.22 212.95 20.85 o 13 2 1 16.27 0.01 18.60 o 14 2 1 0.34 23.27 9.45 o 15 2 1 0.06 0.02 19.27 o 16 2 1 4.60 0.02 22.32 o -15 3 1 2.00 0.02 22.49 o -14 3 1 0.18 0.01 20.74 o -13 3 1 47.23 0.01 23.29 o -12 3 1 49.84 18.53 21.85 o -11 3 1 7.89 7.06 18.62 o -10 3 1 15.82 24.91 17.43 o -9 3 1 98.95 71.69 21.09 o -8 3 1 6.57 12.38 8.18 o -7 3 1 13.38 26.94 9.12 o -6 3 1 143.33 138.53 18.74 o -5 3 1 330.53 338.36 20.39 o -4 3 1 975.47 1009.97 27.76 o -3 3 1 235.84 241.84 17.97 o -2 3 1 198.15 207.20 15.51 o -1 3 1 406.30 395.03 13.07 o 0 3 1 32.91 27.81 6.97 o 1 3 1 114.65 115.22 8.66 o 2 3 1 541.77 580.56 15.13 o 3 3 1 1017.63 997.52 19.73 o 4 3 1 36.90 41.54 8.00 o 5 3 1 1.59 0.01 14.01 o 6 3 1 320.86 330.34 14.05 o 7 3 1 109.94 113.22 10.84 o 8 3 1 49.14 67.95 10.41 o 9 3 1 24.08 19.53 16.53 o 10 3 1 652.52 579.48 29.75 o 11 3 1 162.78 164.06 19.53 o 12 3 1 3.73 13.52 17.16 o 13 3 1 12.56 13.97 19.76 o 14 3 1 0.04 10.59 17.80 o 15 3 1 2.66 0.02 19.00 o -13 4 1 5.96 25.00 20.99 o -12 4 1 14.20 0.01 23.05 o -11 4 1 41.64 0.01 24.13 o -10 4 1 15.65 20.24 18.68 o -9 4 1 15.00 30.72 16.41 o -8 4 1 9.90 48.66 14.82 o -7 4 1 0.14 0.01 19.83 o -6 4 1 23.47 18.63 18.46 o -5 4 1 72.78 49.16 21.18 o -4 4 1 10.33 5.30 16.65 o -3 4 1 26.98 0.01 19.32 o -2 4 1 545.11 508.15 19.14 o -1 4 1 98.46 99.13 10.42 o 0 4 1 129.46 21.23 23.61 o 1 4 1 22.86 10.90 16.37 o 2 4 1 0.60 6.17 15.69 o 3 4 1 937.14 965.54 23.80 o 4 4 1 862.92 853.00 23.23 o 5 4 1 92.20 108.13 12.09 o 6 4 1 79.45 97.52 11.90 o 7 4 1 1.70 0.01 16.96 o 8 4 1 0.03 0.01 17.73 o 9 4 1 39.55 46.67 9.80 o 10 4 1 116.33 139.40 14.34 o 11 4 1 0.51 0.01 21.69 o 12 4 1 36.12 26.37 22.05 o 13 4 1 2.81 0.01 22.22 o -11 5 1 0.34 0.01 27.46 o -10 5 1 29.87 3.74 25.27 o -9 5 1 0.59 0.01 23.26 o -8 5 1 15.71 0.01 21.25 o -7 5 1 4.62 0.01 21.13 o -6 5 1 28.28 7.93 21.51 o -5 5 1 0.07 0.01 19.15 o -4 5 1 77.23 73.33 20.81 o -3 5 1 129.31 131.52 23.25 o -2 5 1 7.96 24.15 17.51 o -1 5 1 67.38 71.61 11.93 o 0 5 1 9.19 2.10 19.98 o 1 5 1 151.01 154.91 14.39 o 2 5 1 419.44 393.26 20.62 o 3 5 1 120.35 109.44 13.08 o 4 5 1 52.28 28.23 20.67 o 5 5 1 28.08 15.21 20.22 o 6 5 1 82.75 35.97 24.30 o 7 5 1 7.12 8.30 17.99 o 8 5 1 0.06 0.01 17.60 o 9 5 1 15.01 21.99 19.05 o 10 5 1 9.93 0.01 21.49 o 11 5 1 0.04 11.93 20.67 o -8 6 1 1.81 0.01 24.31 o -7 6 1 1.56 6.99 20.97 o -6 6 1 1.48 0.01 23.53 o -5 6 1 1.62 6.53 20.39 o -4 6 1 1.93 0.01 21.03 o -3 6 1 11.25 14.49 20.24 o -2 6 1 17.36 0.01 25.48 o -1 6 1 406.60 370.84 20.63 o 0 6 1 1.11 0.01 24.53 o 1 6 1 7.77 18.79 20.44 o 2 6 1 5.26 29.15 19.09 o 3 6 1 0.10 0.01 23.16 o 4 6 1 45.27 26.83 25.43 o 5 6 1 1.57 25.39 18.28 o 6 6 1 1.07 0.01 20.82 o 7 6 1 1.97 0.02 21.19 o 8 6 1 1.62 19.44 21.19 o -16 0 2 80.34 62.39 24.12 o -15 0 2 184.00 189.50 27.18 o -14 0 2 23.57 28.75 19.64 o -13 0 2 427.98 414.09 34.14 o -12 0 2 46.43 31.36 20.65 o -11 0 2 125.18 129.61 18.76 o -10 0 2 287.38 302.05 20.66 o -9 0 2 10.31 0.01 14.40 o -8 0 2 327.56 339.11 16.60 o -7 0 2 29.08 22.56 11.73 o -6 0 2 8.63 13.18 9.08 o -5 0 2 1094.23 996.53 18.48 o -4 0 2 854.52 898.31 15.54 o -3 0 2 4502.93 4524.96 67.20 o -2 0 2 7421.96 6596.67 26.09 o -1 0 2 407.36 417.90 6.79 o 0 0 2 1303.97 1197.49 3.82 o 1 0 2 106.33 125.51 4.05 o 2 0 2 1272.31 1207.56 11.44 o 3 0 2 739.30 685.08 10.29 o 4 0 2 288.20 263.37 11.10 o 5 0 2 31.02 27.73 9.57 o 6 0 2 1393.32 1407.20 23.59 o 7 0 2 1887.58 2013.11 29.74 o 8 0 2 279.18 265.29 17.76 o 9 0 2 0.01 0.01 12.56 o 10 0 2 91.57 102.33 16.28 o 11 0 2 8.40 34.23 13.38 o 12 0 2 183.97 207.57 21.72 o 13 0 2 75.00 130.80 18.01 o 14 0 2 7.61 9.70 19.56 o 15 0 2 90.94 78.06 25.39 o 16 0 2 151.20 166.08 30.39 o -16 1 2 0.33 10.97 20.78 o -15 1 2 18.99 5.72 22.59 o -14 1 2 156.27 173.35 25.21 o -13 1 2 52.05 36.72 21.78 o -12 1 2 272.24 285.20 25.89 o -11 1 2 3.35 0.01 17.12 o -10 1 2 343.05 327.60 24.35 o -9 1 2 543.66 554.63 24.74 o -8 1 2 107.39 130.78 14.58 o -7 1 2 3.27 0.01 12.12 o -6 1 2 88.50 84.06 10.52 o -5 1 2 143.55 137.44 11.92 o -4 1 2 421.58 396.06 14.45 o -3 1 2 244.91 229.94 11.06 o -2 1 2 283.04 267.73 10.22 o -1 1 2 14.73 20.54 4.01 o 0 1 2 1963.18 2004.53 15.22 o 2 1 2 4149.87 4051.07 25.70 o 3 1 2 2667.15 2566.30 21.21 o 4 1 2 1824.32 1890.47 20.04 o 5 1 2 4238.17 4265.68 33.13 o 6 1 2 44.37 37.27 10.04 o 7 1 2 287.90 301.68 14.77 o 8 1 2 51.19 40.45 14.41 o 9 1 2 2.40 2.74 12.35 o 10 1 2 25.55 35.12 13.95 o 11 1 2 20.32 9.30 16.87 o 12 1 2 12.58 0.55 16.83 o 13 1 2 30.77 58.77 16.83 o 14 1 2 238.77 261.75 27.56 o 15 1 2 51.23 13.00 23.93 o 16 1 2 4.31 0.02 19.55 o -16 2 2 0.30 0.02 21.42 o -15 2 2 1.12 29.50 12.82 o -14 2 2 0.74 0.01 18.05 o -13 2 2 0.10 0.01 19.74 o -12 2 2 80.66 78.29 21.28 o -11 2 2 98.68 102.19 21.19 o -10 2 2 1.38 8.09 16.99 o -9 2 2 238.69 207.66 21.72 o -8 2 2 1699.77 1700.30 39.24 o -7 2 2 130.40 106.54 15.68 o -6 2 2 4.10 5.33 11.32 o -5 2 2 1631.80 1717.05 30.39 o -4 2 2 3746.89 3844.90 39.02 o -3 2 2 2866.68 2905.25 41.17 o -2 2 2 4898.13 5083.33 48.58 o -1 2 2 222.15 234.72 8.70 o 0 2 2 4779.74 4604.72 15.20 o 1 2 2 1999.38 2032.99 21.66 o 2 2 2 436.36 487.46 12.07 o 3 2 2 16.12 0.00 10.22 o 4 2 2 0.61 0.01 10.09 o 5 2 2 1970.37 1911.50 25.05 o 6 2 2 3.95 0.01 11.91 o 7 2 2 49.39 48.34 7.44 o 8 2 2 1.92 18.42 12.26 o 9 2 2 71.46 50.02 16.13 o 10 2 2 152.49 151.55 19.45 o 11 2 2 0.04 0.01 15.60 o 12 2 2 38.90 40.20 19.74 o 13 2 2 3.21 0.01 18.26 o 14 2 2 56.56 56.50 19.36 o 15 2 2 20.00 0.01 20.69 o 16 2 2 57.47 60.28 22.81 o -15 3 2 8.81 26.10 21.46 o -14 3 2 7.15 0.01 20.56 o -13 3 2 22.39 41.68 18.25 o -12 3 2 0.32 0.01 18.85 o -11 3 2 227.39 190.54 27.75 o -10 3 2 36.46 46.16 17.05 o -9 3 2 25.77 14.49 18.35 o -8 3 2 48.19 37.72 19.15 o -7 3 2 43.36 51.37 16.78 o -6 3 2 121.41 118.16 17.20 o -5 3 2 285.11 263.63 21.65 o -4 3 2 6.33 0.01 14.24 o -3 3 2 204.76 221.11 15.26 o -2 3 2 13.48 10.07 13.07 o -1 3 2 1424.87 1408.44 26.87 o 0 3 2 0.34 0.01 12.27 o 1 3 2 155.51 165.69 9.15 o 2 3 2 0.94 0.01 12.07 o 3 3 2 1119.91 1096.47 21.01 o 4 3 2 181.06 188.74 10.48 o 5 3 2 28.12 38.49 7.73 o 6 3 2 22.31 18.14 14.89 o 7 3 2 59.83 49.99 15.68 o 8 3 2 19.70 22.74 14.30 o 9 3 2 5.09 15.64 14.37 o 10 3 2 2.30 18.10 14.74 o 11 3 2 65.28 66.26 11.15 o 12 3 2 14.72 24.60 15.96 o 13 3 2 4.51 0.01 19.59 o 14 3 2 6.59 0.01 21.48 o 15 3 2 8.95 10.69 19.33 o -13 4 2 9.54 0.01 25.79 o -12 4 2 5.02 11.67 22.43 o -11 4 2 8.22 23.79 19.04 o -10 4 2 0.09 0.01 19.55 o -9 4 2 66.15 32.58 22.67 o -8 4 2 37.26 26.07 18.87 o -7 4 2 32.94 54.26 17.95 o -6 4 2 1.39 24.62 14.93 o -5 4 2 276.23 252.12 25.15 o -4 4 2 196.29 173.60 22.43 o -3 4 2 158.37 180.98 20.27 o -2 4 2 47.98 43.94 17.08 o -1 4 2 15.82 12.28 10.24 o 0 4 2 28.06 36.82 8.86 o 1 4 2 161.33 168.07 12.13 o 2 4 2 5.78 0.01 16.66 o 3 4 2 22.71 0.01 18.90 o 4 4 2 24.67 34.82 9.74 o 5 4 2 0.51 0.01 16.13 o 6 4 2 48.22 6.42 20.31 o 7 4 2 11.58 23.06 15.04 o 8 4 2 27.49 48.19 10.54 o 9 4 2 10.94 0.01 18.65 o 10 4 2 19.94 33.11 10.08 o 11 4 2 56.88 34.30 20.47 o 12 4 2 0.97 0.01 20.50 o 13 4 2 5.21 15.02 20.60 o -11 5 2 205.99 106.20 40.13 o -10 5 2 170.54 99.51 32.90 o -9 5 2 71.51 69.34 23.01 o -8 5 2 5.13 0.01 22.84 o -7 5 2 2.68 21.10 19.84 o -6 5 2 14.83 0.01 21.28 o -5 5 2 0.85 0.01 21.46 o -4 5 2 62.00 66.26 23.20 o -3 5 2 11.30 0.01 22.65 o -2 5 2 254.86 260.73 17.32 o -1 5 2 219.50 263.89 17.52 o 0 5 2 26.14 19.03 18.12 o 1 5 2 110.39 106.81 13.87 o 2 5 2 361.58 362.60 19.72 o 3 5 2 616.09 588.88 24.26 o 4 5 2 106.57 94.13 13.00 o 5 5 2 74.60 41.74 21.69 o 6 5 2 5.81 6.74 18.50 o 7 5 2 0.46 0.01 20.04 o 8 5 2 11.83 4.05 19.99 o 9 5 2 0.84 23.53 17.06 o 10 5 2 3.56 0.01 21.29 o 11 5 2 0.52 0.01 23.29 o -8 6 2 0.08 5.66 23.12 o -7 6 2 0.70 25.68 20.04 o -6 6 2 3.20 1.50 20.63 o -5 6 2 0.27 14.56 20.59 o -4 6 2 4.48 0.01 23.63 o -3 6 2 0.13 0.01 22.34 o -2 6 2 202.36 197.63 16.89 o -1 6 2 24.35 36.14 15.17 o 0 6 2 108.85 132.18 16.46 o 1 6 2 6.01 18.18 21.79 o 2 6 2 16.67 32.86 12.37 o 3 6 2 8.18 0.01 21.79 o 4 6 2 2.15 20.56 19.79 o 5 6 2 5.46 0.72 20.73 o 6 6 2 0.93 0.01 21.87 o 7 6 2 8.52 0.01 25.81 o 8 6 2 5.51 0.02 23.47 o -16 1 3 24.06 30.65 22.49 o -15 1 3 43.46 74.66 19.44 o -14 1 3 51.14 61.53 18.68 o -13 1 3 335.98 328.59 32.01 o -12 1 3 506.42 499.37 31.38 o -11 1 3 22.97 0.01 18.79 o -10 1 3 6.73 0.01 14.51 o -9 1 3 261.28 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