#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/88/2208843.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208843_Fobs loop_ _publ_author_name 'Wu, Ya-Ming' 'Dong, Chang-Chuan' 'Liu, Shan' 'Zhu, Hong-Jun' 'Wu, Yi-Zu' _publ_section_title ; 5-Bromo-2-(hydroxymethyl)pyridine ; _journal_coeditor_code CI2059 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2102 _journal_page_last o2103 _journal_volume 62 _journal_year 2006 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.090 _cell_angle_gamma 90.000 _cell_length_a 4.0390 _cell_length_b 8.9740 _cell_length_c 9.2240 _exptl_crystal_F_000 184.00 _reflns_d_resolution_high 0.8118 _[local]_cod_data_source_file ci2059Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' U in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 102.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -10 0 269.76 239.10 14.06 o 1 -10 0 26.14 25.39 11.19 o 2 -10 0 0.41 8.00 12.61 o 1 -9 0 123.67 112.27 12.05 o 2 -9 0 88.30 104.41 13.33 o 0 -8 0 1138.60 1158.27 19.36 o 1 -8 0 19.91 7.38 8.86 o 2 -8 0 16.99 10.27 10.60 o 3 -8 0 30.53 34.60 14.06 o 1 -7 0 424.73 481.27 13.33 o 2 -7 0 266.35 295.87 14.45 o 3 -7 0 31.00 51.69 12.38 o 0 -6 0 1122.07 1203.91 16.03 o 1 -6 0 179.85 213.55 9.15 o 2 -6 0 88.54 107.04 10.17 o 3 -6 0 54.59 75.07 11.19 o 4 -6 0 34.36 13.73 13.43 o 1 -5 0 592.32 675.06 12.64 o 2 -5 0 919.62 1162.85 19.62 o 3 -5 0 115.07 112.97 11.16 o 4 -5 0 6.76 -9.58 9.58 o 0 -4 0 862.25 935.01 11.10 o 1 -4 0 778.32 924.31 13.24 o 2 -4 0 16.71 13.27 6.68 o 3 -4 0 114.66 125.44 9.45 o 4 -4 0 63.32 62.89 10.80 o 1 -3 0 902.87 1166.31 13.47 o 2 -3 0 1408.83 1267.62 16.46 o 3 -3 0 148.11 151.88 8.69 o 4 -3 0 7.47 -8.43 8.46 o 0 -2 0 8839.02 7189.56 86.07 o 1 -2 0 596.74 532.30 8.46 o 2 -2 0 69.19 67.23 4.97 o 3 -2 0 220.16 221.68 9.15 o 4 -2 0 108.06 122.51 10.44 o 1 -1 0 1756.31 1580.64 10.80 o 2 -1 0 1058.70 964.01 11.85 o 3 -1 0 82.04 78.33 6.35 o 4 -1 0 3.62 -5.63 7.77 o 1 0 0 86.26 72.73 2.63 o 2 0 0 0.23 2.50 3.16 o 3 0 0 234.91 196.99 8.10 o 4 0 0 130.24 137.17 10.24 o 1 1 0 1999.88 1674.90 10.60 o 2 1 0 1042.41 926.25 11.36 o 3 1 0 98.08 91.40 6.75 o 4 1 0 2.91 -6.75 8.00 o 1 2 0 576.74 466.81 6.52 o 2 2 0 72.54 61.17 4.61 o 3 2 0 187.08 170.59 8.03 o 4 2 0 102.15 95.12 10.01 o 1 3 0 1062.16 934.74 10.27 o 2 3 0 1408.57 1222.58 14.49 o 3 3 0 162.47 145.27 8.23 o 4 3 0 5.55 7.80 8.33 o 0 4 0 861.11 901.52 10.96 o 1 4 0 725.18 658.54 9.91 o 2 4 0 20.42 17.35 4.84 o 3 4 0 108.81 88.96 8.33 o 4 4 0 58.32 67.40 9.42 o 1 5 0 534.16 479.75 9.98 o 2 5 0 958.47 839.39 14.12 o 3 5 0 109.35 93.11 9.48 o 4 5 0 4.49 -3.39 9.32 o 0 6 0 1160.52 1212.86 16.20 o 1 6 0 174.47 154.19 7.70 o 2 6 0 87.88 74.97 7.51 o 3 6 0 66.35 57.39 9.09 o 4 6 0 35.21 31.41 11.52 o 1 7 0 375.05 356.28 11.19 o 2 7 0 286.84 259.32 11.16 o 3 7 0 28.48 42.14 8.86 o 0 8 0 1155.14 1153.01 19.46 o 1 8 0 26.63 34.57 7.93 o 2 8 0 16.33 -1.45 8.53 o 3 8 0 31.30 23.64 10.17 o 1 9 0 127.47 115.30 10.70 o 2 9 0 84.21 82.91 11.10 o 0 10 0 272.96 246.31 14.03 o 1 10 0 30.48 13.10 10.54 o 2 10 0 1.85 1.22 11.00 o 0 -11 1 30.77 31.30 8.93 o -2 -10 1 24.19 18.80 14.09 o -1 -10 1 44.29 41.19 12.38 o 0 -10 1 67.63 69.71 8.05 o 1 -10 1 75.18 58.05 12.61 o 2 -10 1 13.75 2.77 13.10 o -2 -9 1 56.40 82.54 12.74 o -1 -9 1 437.76 497.50 16.79 o 0 -9 1 1.06 5.57 6.14 o 1 -9 1 1.03 -8.53 8.53 o 2 -9 1 62.19 75.86 11.62 o -3 -8 1 98.72 109.57 15.54 o -2 -8 1 112.80 148.16 13.73 o -1 -8 1 44.94 58.64 9.25 o 0 -8 1 207.19 212.71 9.53 o 1 -8 1 184.58 204.07 11.00 o 2 -8 1 49.00 55.94 10.60 o 3 -8 1 7.47 0.49 13.89 o -3 -7 1 47.55 71.48 13.37 o -2 -7 1 94.98 139.17 11.49 o -1 -7 1 883.81 1005.83 18.70 o 0 -7 1 27.84 27.13 5.17 o 1 -7 1 8.25 21.14 6.55 o 2 -7 1 132.22 158.40 11.29 o 3 -7 1 104.40 163.14 14.98 o -4 -6 1 20.47 38.98 12.54 o -3 -6 1 166.11 242.36 13.86 o -2 -6 1 301.65 392.04 14.45 o -1 -6 1 89.98 105.56 8.07 o 0 -6 1 618.75 654.64 10.91 o 1 -6 1 911.90 1027.82 16.13 o 2 -6 1 122.85 155.54 10.31 o 3 -6 1 9.94 -8.03 8.03 o 4 -6 1 64.87 81.06 13.40 o -4 -5 1 17.08 13.10 10.63 o -3 -5 1 57.44 69.60 10.24 o -2 -5 1 169.27 185.37 10.54 o -1 -5 1 779.05 956.21 15.31 o 0 -5 1 664.54 705.62 11.26 o 1 -5 1 196.69 222.74 8.43 o 2 -5 1 178.35 259.65 10.96 o 3 -5 1 167.06 225.77 12.41 o 4 -5 1 34.10 44.38 11.19 o -4 -4 1 57.92 70.16 11.03 o -3 -4 1 248.02 278.32 12.38 o -2 -4 1 349.21 450.38 12.35 o -1 -4 1 101.09 116.29 6.68 o 0 -4 1 1359.41 1455.18 26.06 o 1 -4 1 2690.88 2898.66 21.53 o 2 -4 1 197.37 259.09 10.54 o 3 -4 1 8.16 -2.63 6.45 o 4 -4 1 118.86 125.87 12.02 o -4 -3 1 30.40 21.01 10.08 o -3 -3 1 14.95 28.74 7.01 o -2 -3 1 289.53 331.49 9.61 o -1 -3 1 2089.39 2610.11 20.15 o 0 -3 1 1734.35 1779.94 52.25 o 1 -3 1 425.30 497.43 8.73 o 2 -3 1 445.60 490.72 10.80 o 3 -3 1 334.81 322.90 11.13 o 4 -3 1 51.88 59.43 9.71 o -4 -2 1 31.78 44.22 9.05 o -3 -2 1 404.19 425.36 11.56 o -2 -2 1 684.66 724.12 11.59 o -1 -2 1 1186.98 1566.12 13.96 o 0 -2 1 1205.03 1314.40 18.37 o 1 -2 1 2493.12 3529.18 21.20 o 2 -2 1 293.77 264.69 7.38 o 3 -2 1 3.90 -1.88 5.43 o 4 -2 1 101.47 101.08 9.88 o -4 -1 1 47.37 61.11 8.59 o -3 -1 1 29.01 26.83 5.96 o -2 -1 1 645.02 631.60 10.08 o -1 -1 1 10584.00 8920.01 114.45 o 0 -1 1 67.21 69.80 1.50 o 1 -1 1 86.16 94.17 3.33 o 2 -1 1 945.96 849.47 11.19 o 3 -1 1 569.08 530.49 12.12 o 4 -1 1 66.78 67.17 8.63 o -4 0 1 10.95 10.70 7.90 o -3 0 1 531.24 516.20 11.46 o -2 0 1 581.76 516.20 8.82 o -1 0 1 695.00 697.75 7.14 o 0 0 1 1002.08 990.04 124.18 o 1 0 1 1262.04 1087.65 8.89 o 2 0 1 292.22 261.52 6.68 o 3 0 1 1.78 -3.16 5.20 o 4 0 1 72.74 61.90 9.48 o -4 1 1 45.20 42.64 8.69 o -3 1 1 22.49 17.78 5.70 o -2 1 1 700.50 627.78 9.78 o 0 1 1 16.61 14.79 1.88 o 1 1 1 98.31 91.60 3.33 o 2 1 1 876.77 759.98 10.67 o 3 1 1 549.10 502.70 11.72 o 4 1 1 66.21 73.19 8.63 o -4 2 1 36.56 31.58 8.86 o -3 2 1 409.24 384.40 10.60 o -2 2 1 794.98 681.19 10.54 o -1 2 1 1253.91 1134.67 10.01 o 0 2 1 1268.41 1378.03 31.54 o 1 2 1 2517.51 2190.48 14.45 o 2 2 1 349.79 292.38 7.54 o 3 2 1 1.14 0.00 5.37 o 4 2 1 105.90 98.58 10.11 o -4 3 1 29.03 28.02 8.82 o -3 3 1 9.03 13.63 5.93 o -2 3 1 319.08 275.52 7.74 o -1 3 1 1939.50 1717.18 13.70 o 0 3 1 1664.20 1693.15 51.08 o 1 3 1 437.23 407.22 7.51 o 2 3 1 367.43 327.70 8.49 o 3 3 1 308.69 285.10 10.11 o 4 3 1 52.50 56.33 9.42 o -4 4 1 57.83 61.44 9.94 o -3 4 1 257.09 239.17 10.01 o -2 4 1 367.80 321.58 8.73 o -1 4 1 105.06 95.25 4.97 o 0 4 1 1371.73 1476.35 56.61 o 1 4 1 2740.15 2498.39 19.20 o 2 4 1 212.56 173.09 7.57 o 3 4 1 5.12 9.22 6.49 o 4 4 1 121.83 107.01 11.59 o -4 5 1 18.56 19.20 9.75 o -3 5 1 60.15 53.21 7.93 o -2 5 1 132.13 100.29 7.24 o -1 5 1 825.84 770.78 11.95 o 0 5 1 670.92 696.57 19.64 o 1 5 1 203.66 198.08 7.47 o 2 5 1 189.87 177.27 7.97 o 3 5 1 163.77 144.34 9.94 o 4 5 1 33.79 28.78 10.14 o -4 6 1 19.74 28.91 10.90 o -3 6 1 171.39 139.47 10.70 o -2 6 1 273.42 252.77 10.27 o -1 6 1 71.77 73.59 6.22 o 0 6 1 596.13 600.52 14.82 o 1 6 1 942.71 892.80 14.78 o 2 6 1 105.14 113.46 8.03 o 3 6 1 7.22 7.01 8.23 o 4 6 1 64.84 66.71 11.85 o -3 7 1 49.78 33.58 9.91 o -2 7 1 75.73 63.18 8.63 o -1 7 1 925.61 881.27 15.74 o 0 7 1 42.75 42.48 4.82 o 1 7 1 7.06 1.71 6.49 o 2 7 1 150.50 141.97 9.52 o 3 7 1 108.55 88.77 11.39 o -3 8 1 98.56 89.56 11.95 o -2 8 1 109.54 101.80 10.01 o -1 8 1 38.69 26.70 8.03 o 0 8 1 188.57 179.37 7.16 o 1 8 1 191.74 192.84 10.34 o 2 8 1 46.26 29.50 9.38 o 3 8 1 4.76 -9.15 9.48 o -2 9 1 65.61 50.05 10.57 o -1 9 1 436.15 388.32 14.39 o 0 9 1 3.52 16.00 5.89 o 1 9 1 1.27 19.39 8.43 o 2 9 1 58.16 49.19 10.70 o -2 10 1 33.18 35.33 12.08 o -1 10 1 46.79 48.33 10.63 o 0 10 1 61.17 62.98 7.72 o 1 10 1 70.76 59.17 11.26 o 2 10 1 17.03 10.08 11.98 o 0 11 1 29.43 35.17 8.65 o -1 -10 2 5.05 15.97 11.66 o 0 -10 2 13.90 18.62 11.08 o 1 -10 2 54.55 37.50 11.72 o -2 -9 2 47.28 65.42 12.61 o -1 -9 2 83.22 106.91 11.49 o 0 -9 2 119.26 123.96 7.86 o 1 -9 2 34.47 42.21 9.75 o 2 -9 2 7.08 16.33 10.96 o -3 -8 2 48.07 73.23 14.42 o -2 -8 2 207.93 273.77 15.05 o -1 -8 2 5.04 10.11 9.05 o 0 -8 2 12.97 10.12 5.43 o 1 -8 2 227.72 230.34 11.26 o 2 -8 2 173.37 190.70 12.61 o 3 -8 2 23.09 57.85 12.94 o -3 -7 2 42.13 53.44 13.43 o -2 -7 2 75.39 76.16 11.03 o -1 -7 2 270.75 317.69 12.48 o 0 -7 2 465.30 498.59 25.02 o 1 -7 2 99.73 111.25 8.59 o 2 -7 2 22.57 24.89 9.09 o 3 -7 2 137.60 163.05 15.24 o -4 -6 2 17.87 22.78 13.07 o -3 -6 2 61.22 79.28 12.28 o -2 -6 2 424.86 507.74 15.47 o -1 -6 2 122.10 132.39 9.15 o 0 -6 2 162.60 175.13 5.62 o 1 -6 2 292.54 286.84 9.94 o 2 -6 2 301.08 329.94 12.77 o 3 -6 2 38.36 60.35 12.84 o 4 -6 2 16.04 14.32 12.22 o -4 -5 2 23.87 22.75 11.26 o -3 -5 2 159.39 188.30 12.81 o -2 -5 2 186.11 239.83 11.29 o -1 -5 2 1060.47 1228.60 17.81 o 0 -5 2 1322.76 1356.39 48.61 o 1 -5 2 155.69 153.37 7.11 o 2 -5 2 53.17 55.64 8.56 o 3 -5 2 321.14 381.01 15.11 o 4 -5 2 35.17 46.56 11.06 o -4 -4 2 10.20 -2.57 9.05 o -3 -4 2 70.41 84.02 9.42 o -2 -4 2 776.14 1002.14 17.32 o -1 -4 2 529.91 670.42 12.54 o 0 -4 2 805.70 878.01 12.10 o 1 -4 2 317.08 277.82 7.54 o 2 -4 2 569.86 760.37 16.13 o 3 -4 2 72.88 79.78 8.66 o 4 -4 2 14.43 13.80 9.78 o -4 -3 2 38.88 68.45 9.71 o -3 -3 2 214.59 209.96 10.21 o -2 -3 2 533.40 636.57 13.14 o -1 -3 2 1602.30 2010.01 18.73 o 0 -3 2 2285.63 2314.10 31.95 o 1 -3 2 311.40 288.62 6.78 o 2 -3 2 39.61 41.02 5.00 o 3 -3 2 485.50 460.98 12.51 o 4 -3 2 55.72 84.42 10.04 o -4 -2 2 14.95 27.59 9.02 o -3 -2 2 211.00 215.46 10.14 o -2 -2 2 1811.09 1933.33 19.20 o -1 -2 2 406.74 453.94 8.46 o 0 -2 2 888.11 931.95 21.17 o 1 -2 2 1595.70 2063.48 16.86 o 2 -2 2 1231.73 1084.75 13.60 o 3 -2 2 118.44 102.50 8.03 o 4 -2 2 11.65 6.16 8.59 o -4 -1 2 125.52 148.72 10.54 o -3 -1 2 91.81 100.49 7.41 o -2 -1 2 445.65 438.27 9.09 o -1 -1 2 881.33 970.14 10.47 o 0 -1 2 1621.02 1788.55 8.29 o 1 -1 2 609.60 643.16 9.15 o 2 -1 2 23.20 23.41 3.79 o 3 -1 2 382.19 342.55 10.37 o 4 -1 2 101.70 91.66 10.24 o -4 0 2 23.80 39.84 8.20 o -3 0 2 374.37 379.50 10.63 o -2 0 2 1895.88 1733.34 16.27 o -1 0 2 46.15 43.46 2.93 o 0 0 2 270.52 357.50 15.66 o 1 0 2 2958.38 2547.61 16.23 o 2 0 2 1623.94 1395.56 14.88 o 3 0 2 129.18 126.50 7.57 o 4 0 2 10.15 2.70 8.53 o -4 1 2 126.27 121.72 9.94 o -3 1 2 100.04 84.35 7.24 o -2 1 2 496.44 459.44 8.99 o -1 1 2 713.74 646.48 7.87 o 0 1 2 1796.60 1937.63 176.68 o 1 1 2 636.41 548.27 7.97 o 2 1 2 23.98 19.10 4.12 o 3 1 2 400.74 346.04 10.77 o 4 1 2 107.25 102.33 10.08 o -4 2 2 12.42 7.90 8.66 o -3 2 2 237.88 239.73 9.12 o -2 2 2 1633.65 1427.30 15.28 o -1 2 2 445.44 376.86 6.55 o 0 2 2 849.05 897.59 24.23 o 1 2 2 1466.06 1219.78 12.28 o 2 2 2 1129.54 994.21 13.50 o 3 2 2 128.76 120.60 7.97 o 4 2 2 14.21 23.31 8.23 o -4 3 2 39.96 24.60 9.55 o -3 3 2 231.22 206.54 9.42 o -2 3 2 565.99 498.59 10.17 o -1 3 2 1526.06 1375.61 13.10 o 0 3 2 2462.09 2463.46 35.82 o 1 3 2 347.16 290.07 7.21 o 2 3 2 46.39 35.43 5.20 o 3 3 2 507.78 444.03 12.38 o 4 3 2 62.06 73.32 9.88 o -4 4 2 10.84 12.35 9.02 o -3 4 2 70.89 57.26 7.90 o -2 4 2 750.28 667.06 12.31 o -1 4 2 539.09 511.89 9.19 o 0 4 2 800.09 862.73 9.68 o 1 4 2 274.21 224.75 7.34 o 2 4 2 543.68 516.79 11.52 o 3 4 2 75.86 75.27 8.03 o 4 4 2 14.80 26.67 9.48 o -4 5 2 23.24 26.08 9.81 o -3 5 2 168.14 165.19 9.55 o -2 5 2 163.04 151.19 7.90 o -1 5 2 1112.48 997.20 13.76 o 0 5 2 1289.40 1282.33 10.93 o 1 5 2 155.63 132.49 7.38 o 2 5 2 51.16 42.57 6.65 o 3 5 2 323.44 311.08 12.58 o 4 5 2 32.21 47.45 10.60 o -4 6 2 18.66 22.09 10.31 o -3 6 2 44.14 43.99 9.15 o -2 6 2 480.05 457.56 12.15 o -1 6 2 114.59 128.87 7.31 o 0 6 2 176.42 178.65 5.83 o 1 6 2 315.44 276.08 10.04 o 2 6 2 308.58 275.22 11.33 o 3 6 2 34.18 24.92 9.61 o 4 6 2 13.42 -6.78 10.73 o -3 7 2 42.41 6.39 10.63 o -2 7 2 57.62 52.09 8.46 o -1 7 2 297.78 268.54 10.54 o 0 7 2 434.10 451.83 25.86 o 1 7 2 92.32 90.81 8.10 o 2 7 2 18.42 12.97 8.20 o 3 7 2 132.20 134.70 11.52 o -3 8 2 48.54 50.41 10.80 o -2 8 2 215.61 208.09 11.72 o -1 8 2 4.65 13.76 7.34 o 0 8 2 19.98 25.46 5.59 o 1 8 2 238.16 238.74 11.82 o 2 8 2 174.57 197.65 11.85 o 3 8 2 22.23 20.64 10.90 o -2 9 2 48.91 39.77 10.90 o -1 9 2 66.30 61.50 10.11 o 0 9 2 125.51 123.18 7.71 o 1 9 2 33.83 41.32 10.27 o 2 9 2 3.89 8.82 10.27 o -1 10 2 8.03 22.62 9.94 o 0 10 2 14.05 20.74 8.13 o 1 10 2 52.51 51.33 12.02 o -1 -10 3 47.19 62.76 13.60 o 0 -10 3 11.87 20.41 17.07 o 1 -10 3 6.25 10.73 10.57 o -2 -9 3 5.55 25.45 12.15 o -1 -9 3 41.89 43.43 11.62 o 0 -9 3 151.50 160.05 13.24 o 1 -9 3 173.62 165.32 11.95 o 2 -9 3 12.11 4.25 11.36 o -3 -8 3 13.67 -6.16 11.19 o -2 -8 3 104.12 129.07 13.66 o -1 -8 3 176.89 212.70 13.01 o 0 -8 3 34.14 34.63 6.26 o 1 -8 3 25.63 19.59 8.46 o 2 -8 3 217.47 215.30 13.27 o 3 -8 3 53.01 49.35 14.19 o -3 -7 3 67.94 93.34 13.53 o -2 -7 3 47.85 49.42 11.98 o -1 -7 3 106.59 113.82 10.50 o 0 -7 3 347.95 338.65 9.68 o 1 -7 3 321.21 328.79 11.29 o 2 -7 3 17.86 32.60 8.46 o 3 -7 3 50.33 51.86 13.01 o -4 -6 3 22.10 6.32 13.93 o -3 -6 3 95.69 123.57 13.04 o -2 -6 3 302.93 383.18 14.42 o -1 -6 3 503.64 575.66 14.88 o 0 -6 3 62.93 71.80 4.90 o 1 -6 3 113.77 108.98 7.38 o 2 -6 3 498.31 497.56 13.63 o 3 -6 3 118.35 180.69 15.34 o -4 -5 3 26.63 33.75 12.58 o -3 -5 3 176.61 217.60 13.30 o -2 -5 3 79.09 98.81 9.45 o -1 -5 3 245.20 280.59 10.67 o 0 -5 3 357.51 328.93 19.01 o 1 -5 3 615.16 654.49 12.02 o 2 -5 3 53.97 47.68 7.18 o 3 -5 3 56.81 61.77 9.71 o 4 -5 3 52.62 58.64 11.52 o -4 -4 3 76.61 51.99 12.25 o -3 -4 3 298.78 351.01 13.70 o -2 -4 3 537.57 659.95 14.82 o -1 -4 3 723.03 809.07 14.32 o 0 -4 3 118.31 118.64 4.16 o 1 -4 3 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