#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/88/2208877.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208877_Fobs loop_ _publ_author_name 'Hartung, Jens' 'Greb, Marco' 'Svoboda, Ingrid' 'Fuess, Hartmut' _publ_section_title ; 5-cis-Bromo-2,2,6,6-tetramethyltetrahydropyran-3-carboxylic acid ; _journal_coeditor_code FL2009 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1918 _journal_page_last o1919 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.740 _cell_angle_gamma 90.000 _cell_length_a 30.5390 _cell_length_b 10.0510 _cell_length_c 7.7480 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.8118 _[local]_cod_data_source_file fl2009Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' HAR76 (MGSH12)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 290.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3404.30 2962.06 22.94 o 4 0 0 18215.85 15028.78 73.49 o 6 0 0 30061.99 27331.67 174.52 o 8 0 0 73564.52 68624.90 252.01 o 10 0 0 36994.24 34243.15 359.56 o 12 0 0 4146.94 4022.26 61.81 o 14 0 0 8875.90 8257.38 91.12 o 16 0 0 44178.94 39928.09 221.38 o 18 0 0 6508.95 6602.48 93.67 o 20 0 0 3605.55 3782.62 79.24 o 22 0 0 8579.03 8239.81 112.60 o 24 0 0 5096.40 5106.32 99.61 o 26 0 0 5936.76 5741.37 144.08 o 28 0 0 1.13 -40.41 59.91 o 30 0 0 205.07 175.15 19.22 o 32 0 0 1083.73 1081.54 24.50 o 34 0 0 2036.43 2194.30 51.09 o 36 0 0 173.57 210.71 25.92 o 1 1 0 5897.11 6571.72 227.49 o 3 1 0 1433.43 1404.46 53.50 o 5 1 0 12325.86 12471.40 69.15 o 7 1 0 758.28 815.03 26.03 o 9 1 0 446.35 394.55 16.56 o 11 1 0 4211.14 3991.33 244.91 o 13 1 0 11580.64 10924.26 100.42 o 15 1 0 143.08 155.00 8.30 o 17 1 0 1540.08 1353.27 27.72 o 19 1 0 79.64 126.69 65.94 o 21 1 0 5456.20 4999.45 108.00 o 23 1 0 61.03 74.73 13.39 o 25 1 0 62.22 106.07 18.52 o 27 1 0 2843.33 2773.37 57.55 o 29 1 0 1016.89 1052.98 22.90 o 31 1 0 130.44 104.67 47.76 o 33 1 0 1.56 5.14 62.59 o 35 1 0 224.88 154.11 181.55 o 37 1 0 149.83 101.01 68.09 o 0 2 0 72506.74 79351.55 323.57 o 2 2 0 8739.77 9635.48 171.74 o 4 2 0 7997.45 8771.65 82.35 o 6 2 0 7881.94 7731.23 455.02 o 8 2 0 335.52 298.93 23.50 o 10 2 0 27801.82 26348.19 969.19 o 12 2 0 4866.24 5269.36 140.54 o 14 2 0 442.45 283.04 8.12 o 16 2 0 2490.44 2255.91 137.00 o 18 2 0 2745.59 2811.92 227.97 o 20 2 0 135.88 189.13 13.89 o 22 2 0 265.21 230.24 14.18 o 24 2 0 2098.09 2075.77 42.92 o 26 2 0 1735.16 1840.11 40.77 o 28 2 0 426.94 326.07 21.68 o 30 2 0 11.27 -71.80 71.80 o 32 2 0 204.69 223.51 23.21 o 34 2 0 91.17 16.24 77.59 o 36 2 0 38.67 -53.51 87.12 o 1 3 0 12946.00 13505.15 449.47 o 3 3 0 20697.71 21833.49 424.01 o 5 3 0 53656.31 55163.19 1098.82 o 7 3 0 5097.13 5554.60 56.72 o 9 3 0 962.37 1269.04 43.21 o 11 3 0 45440.85 44241.69 199.53 o 13 3 0 20026.93 19593.18 289.60 o 15 3 0 7972.54 7849.32 391.09 o 17 3 0 3494.83 3484.59 105.37 o 19 3 0 7111.06 6453.33 110.63 o 21 3 0 7751.58 7388.50 113.17 o 23 3 0 3787.14 3767.05 82.07 o 25 3 0 7.68 41.58 18.24 o 27 3 0 8896.98 8755.01 150.16 o 29 3 0 1780.98 1949.01 78.00 o 31 3 0 371.58 484.29 25.00 o 33 3 0 109.80 23.44 81.52 o 35 3 0 483.37 543.96 79.86 o 0 4 0 3444.47 3360.82 65.37 o 2 4 0 1501.86 1899.69 65.32 o 4 4 0 269.75 317.08 6.73 o 6 4 0 5813.36 6598.95 145.33 o 8 4 0 58.54 90.59 10.00 o 10 4 0 1818.92 1951.25 58.67 o 12 4 0 114.12 199.32 32.83 o 14 4 0 2568.81 2516.43 66.75 o 16 4 0 3395.88 3531.80 66.07 o 18 4 0 633.44 530.48 13.09 o 20 4 0 832.53 773.36 38.71 o 22 4 0 940.07 784.03 26.56 o 24 4 0 127.33 133.78 17.65 o 26 4 0 102.75 115.25 19.87 o 28 4 0 9.36 -75.88 81.83 o 30 4 0 5.39 7.89 78.46 o 32 4 0 690.58 651.96 74.12 o 34 4 0 187.55 124.16 41.33 o 1 5 0 9105.69 9517.04 170.02 o 3 5 0 1349.11 926.11 19.52 o 5 5 0 3788.52 3323.09 55.19 o 7 5 0 421.77 498.13 10.54 o 9 5 0 15.26 -22.73 29.00 o 11 5 0 865.56 703.36 15.88 o 13 5 0 2859.57 2637.34 171.50 o 15 5 0 5779.78 5639.09 319.36 o 17 5 0 2303.15 2105.41 45.99 o 19 5 0 1052.01 934.26 30.00 o 21 5 0 1399.72 1252.49 28.26 o 23 5 0 132.52 12.01 56.85 o 25 5 0 2.00 11.50 61.63 o 27 5 0 745.49 663.25 24.02 o 29 5 0 273.98 354.05 34.60 o 31 5 0 74.39 120.88 33.66 o 33 5 0 6.25 65.28 82.07 o 0 6 0 16669.20 15786.67 171.98 o 2 6 0 1605.41 1448.51 29.78 o 4 6 0 789.92 818.03 16.78 o 6 6 0 8178.59 8294.32 91.02 o 8 6 0 7350.42 7465.34 89.86 o 10 6 0 5998.55 5779.38 163.51 o 12 6 0 233.85 247.91 11.77 o 14 6 0 7927.92 7522.82 152.93 o 16 6 0 3770.19 3487.87 107.81 o 18 6 0 58.72 57.16 16.55 o 20 6 0 321.79 323.31 16.34 o 22 6 0 2504.64 2224.81 50.89 o 24 6 0 566.53 589.00 20.16 o 26 6 0 848.63 865.93 26.22 o 28 6 0 34.89 -77.59 77.59 o 30 6 0 424.09 443.67 30.90 o 32 6 0 488.01 471.62 40.63 o 1 7 0 1823.01 1967.36 39.34 o 3 7 0 358.78 373.83 12.78 o 5 7 0 1258.78 1441.84 31.22 o 7 7 0 946.59 933.11 21.32 o 9 7 0 887.71 863.53 19.17 o 11 7 0 45.40 44.70 16.54 o 13 7 0 2696.73 2653.16 52.15 o 15 7 0 34.07 -12.94 60.87 o 17 7 0 123.43 142.52 25.22 o 19 7 0 17.50 -25.67 64.50 o 21 7 0 1426.59 1342.68 28.87 o 23 7 0 81.92 76.82 64.60 o 25 7 0 48.02 67.78 67.66 o 27 7 0 149.36 -10.76 78.32 o 29 7 0 288.47 295.19 28.12 o 0 8 0 423.17 299.26 18.95 o 2 8 0 735.31 593.12 18.38 o 4 8 0 165.66 143.63 22.30 o 6 8 0 790.44 705.72 16.64 o 8 8 0 525.54 463.96 20.34 o 10 8 0 3801.56 3475.34 71.67 o 12 8 0 1316.30 1270.78 26.38 o 14 8 0 380.42 334.87 18.10 o 16 8 0 626.22 536.91 35.94 o 18 8 0 9.96 36.95 57.53 o 20 8 0 5.48 -18.68 18.68 o 22 8 0 17.95 86.67 25.75 o 24 8 0 257.51 243.56 22.77 o 26 8 0 54.90 7.80 33.80 o 28 8 0 23.39 69.25 88.64 o 1 9 0 103.94 61.27 41.87 o 3 9 0 1865.83 1638.27 34.33 o 5 9 0 1106.83 1057.82 22.81 o 7 9 0 296.12 294.12 17.01 o 9 9 0 204.05 185.33 18.81 o 11 9 0 698.06 720.03 18.88 o 13 9 0 693.07 667.46 19.83 o 15 9 0 768.91 709.11 31.49 o 17 9 0 166.28 153.56 19.79 o 19 9 0 805.57 776.38 36.61 o 21 9 0 511.51 434.61 22.29 o 23 9 0 79.87 -39.98 78.22 o 25 9 0 162.47 194.97 26.76 o 0 10 0 182.16 192.17 25.17 o 2 10 0 640.55 609.44 30.10 o 4 10 0 0.30 1.16 18.10 o 6 10 0 329.91 311.60 31.34 o 8 10 0 452.73 437.22 20.50 o 10 10 0 204.11 189.38 19.38 o 12 10 0 0.20 27.63 64.42 o 14 10 0 84.79 31.26 66.57 o 16 10 0 49.08 48.03 29.20 o 18 10 0 238.95 247.24 24.90 o 20 10 0 8.42 -2.65 79.25 o 22 10 0 25.05 -12.20 33.92 o 1 11 0 0.67 40.41 66.39 o 3 11 0 42.32 -9.76 27.38 o 5 11 0 606.37 481.10 23.16 o 7 11 0 67.18 -45.07 80.20 o 9 11 0 0.90 17.42 68.11 o 11 11 0 34.25 71.88 74.76 o 13 11 0 74.61 26.38 36.75 o 15 11 0 175.16 132.69 36.85 o 17 11 0 37.11 -21.52 84.24 o 0 12 0 523.87 496.70 38.47 o 2 12 0 72.12 -37.35 140.92 o 4 12 0 0.72 -19.45 82.30 o 6 12 0 123.64 130.69 27.80 o 8 12 0 265.59 248.89 26.35 o -37 1 1 47.24 90.34 118.19 o -35 1 1 52.99 45.55 35.79 o -33 1 1 18.89 27.66 95.32 o -31 1 1 2839.78 2608.68 89.96 o -29 1 1 1204.94 1059.25 38.47 o -27 1 1 312.03 322.52 26.03 o -25 1 1 3793.47 3630.80 113.89 o -23 1 1 5224.78 4832.45 134.27 o -21 1 1 1266.52 1057.43 30.05 o -19 1 1 1277.61 1268.55 39.14 o -17 1 1 6964.82 6202.44 125.56 o -15 1 1 7790.28 6465.63 117.05 o -13 1 1 4488.83 3555.29 82.02 o -11 1 1 24.83 23.06 7.66 o -9 1 1 18582.03 16851.75 135.42 o -7 1 1 34634.45 34274.56 189.40 o -5 1 1 16766.24 17492.77 113.12 o -3 1 1 67361.84 72084.69 330.08 o -1 1 1 45603.00 45158.53 239.35 o 1 1 1 796.30 859.51 24.31 o 3 1 1 14521.63 16369.50 100.87 o 5 1 1 16142.91 17711.26 116.66 o 7 1 1 23748.73 24060.90 158.68 o 9 1 1 13119.98 11988.58 120.11 o 11 1 1 4248.88 3399.77 75.51 o 13 1 1 124.82 105.56 11.29 o 15 1 1 15862.03 13782.63 178.68 o 17 1 1 13260.29 12033.08 182.41 o 19 1 1 3690.91 3277.46 97.04 o 21 1 1 200.66 244.91 20.19 o 23 1 1 3798.62 3477.00 98.00 o 25 1 1 10658.78 9730.65 199.54 o 27 1 1 617.84 568.29 28.42 o 29 1 1 11.01 -28.71 28.71 o 31 1 1 2285.63 2190.84 64.50 o 33 1 1 1245.54 1291.42 38.86 o 35 1 1 673.13 717.20 40.96 o -36 2 1 868.85 954.93 42.88 o -34 2 1 491.33 486.27 33.97 o -32 2 1 39.32 38.86 29.19 o -30 2 1 2985.45 3142.71 90.25 o -28 2 1 1481.29 1515.18 44.50 o -26 2 1 796.44 691.07 28.14 o -24 2 1 33.31 49.38 20.77 o -22 2 1 1790.40 1676.44 45.46 o -20 2 1 5639.92 4836.28 122.98 o -18 2 1 11184.13 9550.72 150.45 o -16 2 1 9.52 -44.98 44.98 o -14 2 1 10838.28 9978.23 129.20 o -12 2 1 11637.42 10691.99 122.98 o -10 2 1 14675.19 13986.48 130.73 o -8 2 1 173.39 303.76 9.19 o -6 2 1 90.50 127.09 6.03 o -4 2 1 17842.15 20477.19 132.26 o -2 2 1 80449.23 95693.87 394.30 o 0 2 1 1366.17 1357.27 32.16 o 2 2 1 9432.26 11456.47 89.67 o 4 2 1 44094.38 49831.35 240.41 o 6 2 1 21162.27 22504.57 150.16 o 8 2 1 3652.71 3267.41 61.15 o 10 2 1 12022.31 12829.33 129.30 o 12 2 1 17295.45 17475.54 173.80 o 14 2 1 9851.42 9624.13 141.74 o 16 2 1 1762.80 1683.23 50.82 o 18 2 1 2809.39 2746.11 76.95 o 20 2 1 10878.62 10857.94 194.37 o 22 2 1 5262.64 4834.56 141.45 o 24 2 1 24.72 10.62 79.34 o 26 2 1 3110.18 2890.91 83.64 o 28 2 1 143.28 171.60 30.63 o 30 2 1 2060.39 2060.02 64.50 o 32 2 1 172.38 266.25 33.30 o 34 2 1 126.35 42.01 129.68 o 36 2 1 583.07 551.44 44.12 o -35 3 1 101.24 120.20 127.96 o -33 3 1 3.08 -104.99 116.18 o -31 3 1 115.84 110.73 32.16 o -29 3 1 66.64 73.31 96.66 o -27 3 1 0.31 -18.38 27.66 o -25 3 1 45.21 70.25 24.31 o -23 3 1 26.43 53.79 70.15 o -21 3 1 856.44 798.55 24.12 o -19 3 1 0.49 0.00 15.79 o -17 3 1 109.19 94.08 13.69 o -15 3 1 1.02 22.20 11.77 o -13 3 1 84.67 60.39 10.24 o -11 3 1 917.12 811.37 24.88 o -9 3 1 1701.12 2256.02 56.37 o -7 3 1 16.68 -11.01 26.03 o -5 3 1 0.46 14.07 23.26 o -3 3 1 4373.26 5118.60 69.29 o -1 3 1 18.71 70.63 6.41 o 1 3 1 46.98 19.43 22.01 o 3 3 1 672.54 742.95 21.44 o 5 3 1 57.89 50.91 6.51 o 7 3 1 2499.52 2445.32 57.33 o 9 3 1 12041.96 13362.78 134.65 o 11 3 1 2204.43 2616.91 69.58 o 13 3 1 12993.38 14028.12 155.61 o 15 3 1 730.87 622.26 18.28 o 17 3 1 495.38 433.63 16.46 o 19 3 1 1.48 -56.37 62.21 o 21 3 1 35.78 28.90 74.74 o 23 3 1 295.11 275.91 23.64 o 25 3 1 63.19 18.57 30.91 o 27 3 1 189.91 154.18 33.50 o 29 3 1 41.43 80.10 31.39 o 31 3 1 32.65 -13.78 113.41 o 33 3 1 1.44 60.96 39.43 o 35 3 1 8.44 -140.97 140.97 o -34 4 1 99.86 100.49 41.92 o -32 4 1 13.96 -91.40 115.23 o -30 4 1 1022.90 1011.11 40.20 o -28 4 1 1289.42 1267.59 41.54 o -26 4 1 268.57 274.67 28.33 o -24 4 1 0.35 56.18 73.21 o -22 4 1 1266.11 1287.50 38.95 o -20 4 1 6430.20 6031.52 136.95 o -18 4 1 196.11 168.63 16.65 o -16 4 1 57.49 5.93 50.05 o -14 4 1 1669.94 1678.16 47.47 o -12 4 1 11035.10 10978.24 134.85 o -10 4 1 3713.37 3696.64 80.10 o -8 4 1 17.29 10.05 9.00 o -6 4 1 5574.39 5311.16 84.70 o -4 4 1 18689.50 19621.02 161.26 o -2 4 1 7897.34 8834.19 104.32 o 0 4 1 209.31 208.73 8.42 o 2 4 1 6085.28 6457.49 89.10 o 4 4 1 28708.48 30130.79 208.73 o 6 4 1 13669.18 13342.21 135.32 o 8 4 1 3039.98 2996.38 71.39 o 10 4 1 13649.08 15758.82 165.09 o 12 4 1 22549.22 22273.83 201.46 o 14 4 1 6700.92 6681.73 124.22 o 16 4 1 271.41 331.33 15.79 o 18 4 1 876.66 837.88 24.88 o 20 4 1 8722.74 8813.81 175.42 o 22 4 1 3261.47 3005.09 98.00 o 24 4 1 60.35 16.17 88.91 o 26 4 1 1591.44 1468.09 40.87 o 28 4 1 1191.00 1230.46 41.25 o 30 4 1 1523.25 1492.49 44.79 o 32 4 1 19.06 46.99 133.03 o 34 4 1 148.00 63.64 46.70 o -33 5 1 242.11 287.40 42.88 o -31 5 1 580.61 607.24 38.19 o -29 5 1 231.45 192.84 33.88 o -27 5 1 43.85 8.90 95.32 o -25 5 1 2553.18 2469.15 71.11 o -23 5 1 2394.39 2423.02 74.36 o -21 5 1 595.79 550.10 22.78 o -19 5 1 68.50 42.49 57.23 o -17 5 1 7635.33 7059.28 136.66 o -15 5 1 16006.29 15572.77 187.67 o -13 5 1 606.17 547.42 19.62 o -11 5 1 890.55 949.67 30.24 o -9 5 1 11256.49 12546.15 150.45 o -7 5 1 15644.07 16445.58 168.15 o -5 5 1 3488.61 3597.59 79.72 o -3 5 1 455.91 494.98 13.02 o -1 5 1 11433.39 12483.84 141.74 o 1 5 1 10133.63 11181.03 134.18 o 3 5 1 3734.19 3784.11 80.58 o 5 5 1 843.16 990.82 27.37 o 7 5 1 2741.52 2751.95 79.15 o 9 5 1 22573.23 24702.40 222.80 o 11 5 1 2426.44 2282.53 66.71 o 13 5 1 434.86 418.89 16.17 o 15 5 1 1982.91 2067.10 59.24 o 17 5 1 2116.27 2184.53 74.65 o 19 5 1 2031.24 2192.85 71.30 o 21 5 1 328.98 286.73 24.31 o 23 5 1 464.32 572.21 27.28 o 25 5 1 2653.49 2437.09 71.49 o 27 5 1 777.02 762.85 35.98 o 29 5 1 70.71 96.37 37.04 o 31 5 1 632.00 618.05 44.41 o 33 5 1 406.38 513.64 47.85 o -32 6 1 20.91 97.04 40.39 o -30 6 1 0.02 7.08 35.60 o -28 6 1 7.01 83.26 95.99 o -26 6 1 79.05 110.54 28.33 o -24 6 1 174.23 175.04 25.36 o -22 6 1 0.06 11.39 75.32 o -20 6 1 310.77 290.56 22.87 o -18 6 1 343.03 349.22 18.95 o -16 6 1 169.44 180.98 17.61 o -14 6 1 1460.52 1464.93 44.60 o -12 6 1 146.68 178.87 15.70 o -10 6 1 952.62 837.69 28.42 o -8 6 1 114.37 123.07 13.97 o -6 6 1 83.19 41.25 46.61 o -4 6 1 46.21 -6.60 46.13 o -2 6 1 95.46 112.45 13.11 o 0 6 1 224.58 253.14 14.45 o 2 6 1 1126.92 1303.96 35.60 o 4 6 1 104.69 190.45 13.02 o 6 6 1 818.46 727.54 20.29 o 8 6 1 482.83 488.37 15.70 o 10 6 1 2.51 13.40 14.93 o 12 6 1 16.05 13.59 16.94 o 14 6 1 192.44 -9.09 65.17 o 16 6 1 331.90 443.87 19.91 o 18 6 1 263.51 256.39 23.93 o 20 6 1 111.74 143.65 26.32 o 22 6 1 5.11 -15.89 90.06 o 24 6 1 133.17 56.66 97.04 o 26 6 1 50.42 95.13 101.25 o 28 6 1 0.28 66.04 114.65 o 30 6 1 47.51 118.00 133.70 o 32 6 1 0.13 -149.68 149.68 o -31 7 1 91.25 42.49 38.57 o -29 7 1 5.19 31.01 34.45 o -27 7 1 11.78 49.67 96.18 o -25 7 1 980.90 949.76 33.78 o -23 7 1 240.20 244.33 28.33 o -21 7 1 727.96 764.38 28.23 o -19 7 1 57.22 56.56 73.98 o -17 7 1 5002.90 4700.67 134.56 o -15 7 1 7169.36 7115.74 149.97 o -13 7 1 24.12 -64.79 64.79 o -11 7 1 1948.33 1743.24 53.50 o -9 7 1 3188.14 3277.17 86.90 o -7 7 1 3131.26 3004.13 83.64 o -5 7 1 938.73 1064.03 32.44 o -3 7 1 167.45 115.51 15.22 o -1 7 1 5097.50 5194.40 114.46 o 1 7 1 6101.57 5969.41 118.96 o 3 7 1 1931.84 1907.66 56.08 o 5 7 1 959.71 994.84 26.41 o 7 7 1 3515.99 3560.17 104.32 o 9 7 1 3951.48 3817.71 113.03 o 11 7 1 437.98 449.52 19.43 o 13 7 1 18.39 24.40 18.76 o 15 7 1 1225.71 1237.35 33.30 o 17 7 1 2225.51 2177.64 66.04 o 19 7 1 1750.51 1830.90 56.08 o 21 7 1 105.79 156.28 29.09 o 23 7 1 282.25 273.42 29.76 o 25 7 1 1486.04 1411.82 48.90 o 27 7 1 287.67 353.91 39.72 o 29 7 1 10.27 -146.04 146.04 o -28 8 1 535.06 569.46 29.37 o -26 8 1 337.64 373.12 26.92 o -24 8 1 150.31 101.52 27.82 o -22 8 1 490.50 433.47 20.88 o -20 8 1 265.67 269.35 19.49 o -18 8 1 680.75 685.40 19.96 o -16 8 1 5.22 -29.97 56.54 o -14 8 1 615.40 599.22 31.20 o -12 8 1 832.50 784.24 18.58 o -10 8 1 1683.77 1658.33 67.38 o -8 8 1 319.90 303.98 14.51 o -6 8 1 383.65 291.48 14.04 o -4 8 1 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