#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2208884.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208884_Fobs loop_ _publ_author_name 'Pl\/oger, Jane M.' 'Petersen, Bo M.' 'Bond, Andrew D.' 'Jeppesen, Jan O.' _publ_section_title ; 4,5-Bis(hydroxymethyl)-1,3-dithiole-2-thione ; _journal_coeditor_code GH2005 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2066 _journal_page_last o2068 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.558 _cell_angle_gamma 90.000 _cell_length_a 13.7118 _cell_length_b 8.9540 _cell_length_c 12.8244 _exptl_crystal_F_000 800.00 _reflns_d_resolution_high 0.7489 _[local]_cod_data_source_file gh2005Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jj0512 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 189.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 13830.18 14440.53 162.23 o 8 0 0 7149.37 7679.65 89.04 o 10 0 0 1433.95 1397.11 29.63 o 12 0 0 5715.70 5631.56 79.63 o 14 0 0 1739.72 1681.97 61.14 o 16 0 0 2950.72 3060.33 63.34 o 3 1 0 10151.22 10311.38 81.57 o 5 1 0 2202.94 2029.57 17.92 o 7 1 0 1229.93 1237.94 12.89 o 9 1 0 3786.19 3701.41 34.84 o 11 1 0 559.96 568.52 9.78 o 13 1 0 160.98 159.87 7.40 o 15 1 0 51.24 51.38 8.64 o 17 1 0 31.88 42.67 10.45 o 0 2 0 11636.17 11947.40 154.48 o 2 2 0 5574.86 5644.44 48.90 o 4 2 0 10.23 4.72 1.56 o 6 2 0 698.25 749.77 8.63 o 8 2 0 225.36 241.05 5.24 o 10 2 0 2411.20 2475.20 39.06 o 12 2 0 171.28 210.30 7.94 o 14 2 0 43.27 46.88 7.41 o 16 2 0 72.01 81.09 10.27 o 1 3 0 7141.07 7314.09 55.49 o 3 3 0 1028.35 1110.01 11.07 o 5 3 0 739.69 683.42 8.27 o 7 3 0 674.30 752.16 9.44 o 9 3 0 2657.57 2740.92 35.89 o 11 3 0 61.13 62.01 5.13 o 13 3 0 208.86 187.76 8.68 o 15 3 0 263.13 263.93 12.65 o 17 3 0 199.88 170.68 13.71 o 0 4 0 35777.26 34542.01 543.63 o 2 4 0 624.82 687.68 8.33 o 4 4 0 16280.08 15795.30 118.49 o 6 4 0 2089.09 2099.68 20.47 o 8 4 0 315.56 337.50 7.05 o 10 4 0 1341.65 1339.19 16.69 o 12 4 0 1649.33 1643.98 31.80 o 14 4 0 301.79 313.02 11.73 o 16 4 0 1793.91 1922.26 33.76 o 1 5 0 0.48 2.21 2.57 o 3 5 0 190.15 196.48 6.00 o 5 5 0 4611.76 4578.76 39.41 o 7 5 0 3385.11 3334.15 30.64 o 9 5 0 389.43 418.35 9.09 o 11 5 0 585.97 555.90 17.32 o 13 5 0 429.31 414.68 12.49 o 15 5 0 484.92 470.30 16.79 o 0 6 0 2201.95 2097.88 38.33 o 2 6 0 1587.06 1569.49 16.68 o 4 6 0 3976.70 3806.90 34.36 o 6 6 0 1681.15 1732.32 18.69 o 8 6 0 261.00 395.33 9.36 o 10 6 0 3117.31 3038.65 42.45 o 12 6 0 70.99 183.96 10.03 o 14 6 0 330.97 309.19 14.49 o 1 7 0 5600.71 5673.47 49.45 o 3 7 0 4080.82 4303.99 39.02 o 5 7 0 3858.52 3755.93 37.25 o 7 7 0 0.25 3.11 5.13 o 9 7 0 2.46 2.83 5.96 o 11 7 0 293.68 314.94 11.91 o 13 7 0 438.92 417.28 16.00 o 0 8 0 826.33 780.55 25.10 o 2 8 0 5.41 171.21 7.01 o 4 8 0 2014.08 1946.06 26.41 o 6 8 0 1014.77 950.11 24.79 o 8 8 0 10.94 17.34 7.20 o 10 8 0 14.19 45.25 9.82 o 12 8 0 44.31 102.33 12.40 o 1 9 0 85.47 97.54 7.56 o 3 9 0 517.42 499.49 12.60 o 5 9 0 95.30 100.11 8.60 o 7 9 0 288.06 254.64 11.31 o 9 9 0 13.62 30.19 10.08 o 11 9 0 224.08 234.60 14.71 o 0 10 0 2292.30 2308.61 42.63 o 2 10 0 142.37 174.94 10.48 o 4 10 0 665.84 684.76 17.07 o 6 10 0 2063.75 2232.34 36.83 o 8 10 0 348.18 369.49 16.39 o 1 11 0 1206.25 1235.91 26.07 o 3 11 0 2171.51 2108.18 35.68 o 5 11 0 528.72 533.60 20.60 o 7 11 0 170.77 146.30 17.10 o -17 1 1 790.48 875.78 21.76 o -15 1 1 153.91 168.08 9.67 o -13 1 1 1444.23 1532.79 23.78 o -11 1 1 1053.15 1036.08 12.97 o -9 1 1 4275.99 4353.86 40.20 o -7 1 1 568.95 760.14 10.16 o -5 1 1 1225.33 1291.73 17.09 o -3 1 1 272.81 292.39 4.07 o 5 1 1 1279.55 1382.29 12.79 o 7 1 1 19196.91 19690.69 155.89 o 9 1 1 191.99 212.23 5.10 o 11 1 1 3598.00 3596.81 37.60 o 13 1 1 4.40 6.48 6.26 o 15 1 1 254.78 293.11 12.46 o 17 1 1 188.64 207.10 13.07 o -16 2 1 40.53 58.30 10.36 o -14 2 1 730.82 654.19 14.78 o -12 2 1 338.28 326.18 8.85 o -10 2 1 843.78 811.39 10.83 o -8 2 1 2449.68 2307.43 21.59 o -6 2 1 1615.42 1683.63 20.50 o -4 2 1 1657.30 1941.64 18.45 o -2 2 1 1351.37 1311.08 11.07 o 0 2 1 2681.34 2900.96 22.65 o 2 2 1 3198.27 3216.87 26.57 o 4 2 1 16078.59 15669.78 116.89 o 6 2 1 1675.76 1734.80 16.21 o 8 2 1 5165.28 5137.55 43.46 o 10 2 1 220.26 215.98 6.06 o 12 2 1 2857.76 2901.41 43.32 o 14 2 1 164.25 156.19 9.81 o 16 2 1 18.43 18.97 9.74 o -17 3 1 1070.37 1137.44 25.70 o -15 3 1 4.68 9.69 7.94 o -13 3 1 3986.50 3947.88 57.43 o -11 3 1 504.50 518.85 10.04 o -9 3 1 873.97 815.09 10.78 o -7 3 1 5779.22 5924.40 50.92 o -5 3 1 1531.33 1639.06 15.66 o -3 3 1 6659.03 6576.77 50.32 o -1 3 1 30944.11 29778.68 667.92 o 1 3 1 5211.31 5251.19 42.99 o 3 3 1 19345.38 18677.46 147.53 o 5 3 1 870.41 886.17 9.73 o 7 3 1 4637.67 4395.60 37.66 o 9 3 1 1337.36 1407.21 16.29 o 11 3 1 71.44 69.45 6.05 o 13 3 1 1251.49 1170.49 26.63 o 15 3 1 609.25 598.38 17.21 o 17 3 1 155.91 171.21 13.61 o -16 4 1 52.95 77.32 11.72 o -14 4 1 36.41 64.01 8.18 o -12 4 1 199.04 221.16 10.08 o -10 4 1 956.74 973.19 13.74 o -8 4 1 569.91 572.66 8.85 o -6 4 1 704.82 771.78 9.83 o -4 4 1 12087.00 12614.62 95.25 o -2 4 1 267.30 298.45 4.74 o 0 4 1 1843.19 2263.44 20.50 o 2 4 1 8314.75 8494.01 68.98 o 4 4 1 651.30 745.07 9.39 o 6 4 1 141.57 151.39 4.41 o 8 4 1 2498.70 2450.48 25.02 o 10 4 1 249.30 242.50 8.22 o 12 4 1 483.37 492.69 12.59 o 14 4 1 53.26 87.22 9.86 o 16 4 1 461.52 411.72 16.32 o -15 5 1 55.15 56.79 9.91 o -13 5 1 948.28 896.28 18.11 o -11 5 1 25.22 18.91 5.38 o -9 5 1 1209.55 1175.37 18.40 o -7 5 1 982.50 938.80 12.07 o -5 5 1 10.80 118.66 4.40 o -3 5 1 128.56 149.90 6.01 o -1 5 1 1098.61 1173.85 13.19 o 1 5 1 89.43 97.26 3.74 o 3 5 1 3711.51 3525.73 31.21 o 5 5 1 2808.15 2825.67 27.89 o 7 5 1 788.99 812.42 19.93 o 9 5 1 967.60 950.20 14.74 o 11 5 1 13.15 25.14 6.20 o 13 5 1 298.23 279.12 12.24 o 15 5 1 273.70 265.80 20.01 o -14 6 1 542.45 547.56 17.70 o -12 6 1 1820.41 1757.01 26.74 o -10 6 1 23.02 94.07 6.59 o -8 6 1 3276.75 3113.57 32.02 o -6 6 1 12.96 17.80 4.02 o -4 6 1 4883.14 4851.86 42.52 o -2 6 1 1248.74 1195.24 16.74 o 0 6 1 916.41 945.18 14.37 o 2 6 1 155.80 179.92 5.28 o 4 6 1 5620.59 5620.54 48.44 o 6 6 1 665.10 689.70 12.36 o 8 6 1 9106.48 8807.46 93.76 o 10 6 1 21.23 27.15 6.71 o 12 6 1 1454.05 1490.13 24.28 o 14 6 1 0.71 24.12 10.49 o -13 7 1 2179.22 2258.53 37.01 o -11 7 1 838.97 847.94 25.64 o -9 7 1 211.72 258.96 8.94 o -7 7 1 4990.52 4870.67 47.08 o -5 7 1 903.73 914.35 12.97 o -3 7 1 1184.18 1235.91 15.29 o -1 7 1 11750.03 11596.18 95.48 o 1 7 1 40.13 186.07 6.09 o 3 7 1 5995.21 5861.01 54.42 o 5 7 1 2626.80 2684.53 42.19 o 7 7 1 2304.99 2224.11 35.15 o 9 7 1 687.01 700.45 19.05 o 11 7 1 94.18 83.26 9.11 o 13 7 1 271.02 292.55 17.00 o -12 8 1 189.07 195.29 14.54 o -10 8 1 665.63 678.14 18.77 o -8 8 1 46.26 48.23 7.79 o -6 8 1 6.01 111.28 7.54 o -4 8 1 1.83 7.84 5.56 o -2 8 1 2042.77 2024.40 23.53 o 0 8 1 89.96 122.76 6.49 o 2 8 1 3837.31 3804.25 38.25 o 4 8 1 4.34 15.20 5.69 o 6 8 1 1233.80 1296.19 19.41 o 8 8 1 71.48 92.75 13.37 o 10 8 1 30.08 53.79 9.46 o 12 8 1 193.98 196.71 15.19 o -11 9 1 215.60 227.93 14.68 o -9 9 1 164.62 172.23 12.35 o -7 9 1 447.49 473.33 14.19 o -5 9 1 209.18 217.84 9.56 o -3 9 1 1309.09 1371.11 26.19 o -1 9 1 213.77 222.16 9.20 o 1 9 1 29.76 21.73 6.39 o 3 9 1 0.81 1.83 6.55 o 5 9 1 461.91 510.12 14.09 o 7 9 1 23.88 20.74 8.78 o 9 9 1 1951.58 1965.38 33.96 o 11 9 1 154.92 160.13 13.96 o -8 10 1 69.74 64.79 12.11 o -6 10 1 50.97 66.67 10.02 o -4 10 1 13.51 13.16 8.51 o -2 10 1 333.20 318.11 12.12 o 0 10 1 1697.13 1596.19 30.81 o 2 10 1 118.92 124.14 9.79 o 4 10 1 2063.01 2074.98 30.81 o 6 10 1 412.05 442.06 16.00 o 8 10 1 1406.21 1396.38 28.25 o -7 11 1 292.84 287.77 33.62 o -5 11 1 261.93 294.79 17.29 o -3 11 1 252.72 347.73 20.92 o -1 11 1 988.97 1029.00 23.65 o 1 11 1 46.66 175.73 12.03 o 3 11 1 1676.85 1624.60 31.85 o 5 11 1 121.67 143.81 14.03 o -18 0 2 607.58 624.38 28.55 o -16 0 2 247.39 249.34 18.15 o -14 0 2 5349.16 5352.94 78.42 o -12 0 2 1646.50 1649.53 25.88 o -10 0 2 7062.57 6597.20 91.15 o -8 0 2 6289.67 6321.57 96.85 o -6 0 2 1534.98 1487.87 28.55 o -4 0 2 34.45 35.32 2.46 o -2 0 2 11755.56 11781.59 182.36 o 4 0 2 15492.18 16377.27 209.80 o 6 0 2 16040.87 15753.66 176.39 o 8 0 2 1145.19 1229.08 18.09 o 10 0 2 2908.92 2927.66 43.65 o 12 0 2 6.32 21.64 8.70 o 14 0 2 222.85 197.92 13.97 o 16 0 2 249.16 247.43 22.29 o -17 1 2 44.36 55.64 11.41 o -15 1 2 131.45 152.16 9.71 o -13 1 2 586.31 612.47 11.54 o -11 1 2 276.99 314.20 7.10 o -9 1 2 5583.73 5515.34 46.80 o -7 1 2 2027.35 2138.68 19.70 o -5 1 2 11347.52 11169.03 89.07 o -3 1 2 7001.19 7168.30 67.69 o -1 1 2 651.17 722.86 6.61 o 1 1 2 7489.09 7932.47 79.58 o 3 1 2 19774.21 19381.94 1020.00 o 5 1 2 1227.89 1266.49 12.76 o 7 1 2 20605.51 20397.49 161.34 o 9 1 2 64.89 79.39 4.09 o 11 1 2 7411.16 7165.81 76.12 o 13 1 2 116.02 114.56 8.00 o 15 1 2 1026.10 1038.15 35.71 o 17 1 2 113.20 147.39 12.37 o -16 2 2 151.33 155.05 11.85 o -14 2 2 0.73 3.00 6.56 o -12 2 2 144.41 163.58 6.21 o -10 2 2 71.14 69.29 5.65 o -8 2 2 521.25 649.91 8.74 o -6 2 2 88.79 96.17 3.41 o -4 2 2 7.11 5.72 1.75 o -2 2 2 0.05 31.97 1.96 o 0 2 2 193.48 216.37 2.99 o 2 2 2 549.05 545.83 5.48 o 4 2 2 982.40 1064.52 10.70 o 6 2 2 58.23 96.15 3.04 o 8 2 2 37.20 41.96 3.44 o 10 2 2 419.90 557.60 19.38 o 12 2 2 67.31 76.71 7.31 o 14 2 2 718.32 675.42 26.08 o 16 2 2 59.21 60.80 10.90 o -17 3 2 204.98 198.14 15.96 o -15 3 2 173.27 217.69 10.68 o -13 3 2 201.83 220.94 8.02 o -11 3 2 152.81 155.00 5.95 o -9 3 2 3114.38 3223.83 29.58 o -7 3 2 429.03 379.37 8.07 o -5 3 2 7616.17 7807.70 63.69 o -3 3 2 0.22 7.38 1.71 o -1 3 2 514.55 698.99 6.84 o 1 3 2 273.28 351.94 5.00 o 3 3 2 12543.14 13370.00 106.22 o 5 3 2 118.06 112.94 3.29 o 7 3 2 13787.39 13886.03 111.34 o 9 3 2 3.36 43.41 4.18 o 11 3 2 2836.59 2745.83 34.22 o 13 3 2 0.10 67.66 7.79 o 15 3 2 130.43 145.88 11.05 o -16 4 2 2.23 5.45 10.59 o -14 4 2 4121.60 4117.92 69.60 o -12 4 2 207.60 204.76 7.76 o -10 4 2 8916.07 8601.13 72.29 o -8 4 2 281.22 263.62 10.76 o -6 4 2 2909.54 2818.42 28.55 o -4 4 2 57.73 124.05 5.36 o -2 4 2 1978.43 2127.70 19.07 o 0 4 2 18.34 122.89 3.02 o 2 4 2 13865.32 13805.00 110.18 o 4 4 2 0.56 57.44 3.08 o 6 4 2 8643.44 8543.61 70.07 o 8 4 2 211.34 242.86 6.30 o 10 4 2 857.42 828.87 16.21 o 12 4 2 302.17 291.87 11.54 o 14 4 2 180.83 173.14 10.90 o 16 4 2 96.65 130.12 12.87 o -15 5 2 73.34 66.70 10.96 o -13 5 2 469.27 452.89 13.21 o -11 5 2 252.83 254.13 8.31 o -9 5 2 3138.85 3101.78 32.69 o -7 5 2 374.68 533.08 9.03 o -5 5 2 4518.13 4403.94 36.03 o -3 5 2 2237.28 2375.21 20.80 o -1 5 2 4656.47 4853.49 41.44 o 1 5 2 1619.57 1645.96 16.43 o 3 5 2 3.38 27.01 3.09 o 5 5 2 1737.98 1739.90 23.89 o 7 5 2 2869.27 2789.77 30.21 o 9 5 2 54.51 44.87 5.57 o 11 5 2 5265.70 5105.99 61.59 o 13 5 2 50.86 64.56 9.41 o 15 5 2 1724.29 1737.14 41.85 o -14 6 2 4.89 20.48 9.94 o -12 6 2 7.50 37.47 7.84 o -10 6 2 2.79 6.23 5.43 o -8 6 2 475.29 551.08 10.18 o -6 6 2 156.13 164.99 8.18 o -4 6 2 2346.59 2341.82 22.83 o -2 6 2 164.59 198.14 7.54 o 0 6 2 818.77 786.27 10.62 o 2 6 2 525.56 515.16 8.47 o 4 6 2 93.76 127.14 5.16 o 6 6 2 121.53 110.27 5.88 o 8 6 2 2429.81 2312.98 31.63 o 10 6 2 1.36 16.59 6.59 o 12 6 2 1321.19 1277.99 24.90 o 14 6 2 86.53 87.50 11.16 o -13 7 2 164.15 184.30 16.01 o -11 7 2 769.79 794.50 17.69 o -9 7 2 1143.15 1122.87 18.01 o -7 7 2 123.08 140.04 7.24 o -5 7 2 1745.57 1715.15 21.52 o -3 7 2 359.66 373.83 10.15 o -1 7 2 1750.38 1713.59 19.91 o 1 7 2 2313.06 2259.57 24.45 o 3 7 2 111.01 157.75 6.25 o 5 7 2 1621.39 1617.60 21.05 o 7 7 2 107.58 121.04 7.46 o 9 7 2 221.11 221.75 11.41 o 11 7 2 214.56 218.87 11.79 o 13 7 2 101.03 89.42 14.62 o -12 8 2 1.08 59.82 11.68 o -10 8 2 3308.22 3398.47 43.72 o -8 8 2 1.66 49.88 7.66 o -6 8 2 2527.28 2552.93 30.76 o -4 8 2 337.98 325.94 11.04 o -2 8 2 89.32 111.21 6.93 o 0 8 2 761.58 729.71 14.61 o 2 8 2 2690.45 2686.63 31.23 o 4 8 2 1234.77 1128.76 17.37 o 6 8 2 3530.77 3444.82 42.47 o 8 8 2 398.68 422.59 13.01 o 10 8 2 1389.55 1308.82 23.24 o 12 8 2 163.09 183.26 14.22 o -11 9 2 15.02 16.31 11.64 o -9 9 2 206.38 227.58 12.27 o -7 9 2 99.95 173.63 9.97 o -5 9 2 412.88 473.30 12.71 o -3 9 2 28.65 111.40 8.03 o -1 9 2 81.02 138.70 8.51 o 1 9 2 122.77 134.65 8.09 o 3 9 2 338.06 355.91 10.89 o 5 9 2 528.68 532.05 18.37 o 7 9 2 1245.11 1219.76 23.99 o 9 9 2 185.57 206.16 12.47 o 11 9 2 1207.65 1246.09 30.75 o -10 10 2 16.81 32.24 14.56 o -8 10 2 1135.55 1189.31 36.62 o -6 10 2 83.51 130.39 11.78 o -4 10 2 1750.94 1686.70 27.24 o -2 10 2 563.35 626.08 17.29 o 0 10 2 504.45 568.35 18.91 o 2 10 2 357.81 380.26 16.03 o 4 10 2 385.24 466.86 17.37 o 6 10 2 180.07 151.71 12.02 o 8 10 2 1215.47 1143.05 25.44 o -7 11 2 46.87 37.27 12.80 o -5 11 2 0.05 1.36 10.96 o -3 11 2 815.28 844.64 22.02 o -1 11 2 43.97 44.20 14.34 o 1 11 2 2706.58 2665.78 42.08 o 3 11 2 200.16 212.06 15.94 o 5 11 2 1191.82 1198.95 27.31 o -17 1 3 71.85 85.14 10.86 o -15 1 3 853.36 825.01 19.43 o -13 1 3 46.91 89.37 5.86 o -11 1 3 4332.37 4208.82 40.23 o -9 1 3 821.22 857.46 10.63 o -7 1 3 12120.50 11728.68 94.29 o -5 1 3 1366.65 1425.74 14.48 o -3 1 3 930.99 925.55 8.15 o -1 1 3 7824.08 8011.28 56.80 o 1 1 3 1731.49 1752.75 14.55 o 3 1 3 82.12 90.06 3.00 o 5 1 3 8629.97 8744.62 66.01 o 7 1 3 349.96 377.64 6.07 o 9 1 3 1488.49 1492.35 19.34 o 11 1 3 591.68 583.32 13.75 o 13 1 3 228.41 209.83 13.06 o 15 1 3 0.91 2.75 8.32 o -18 2 3 864.58 920.69 28.42 o -16 2 3 0.36 27.41 8.61 o -14 2 3 134.89 152.90 8.85 o -12 2 3 22.65 24.33 4.80 o -10 2 3 1620.41 1682.56 17.89 o -8 2 3 123.74 160.47 4.93 o -6 2 3 23910.48 23069.07 182.34 o -4 2 3 125.74 124.43 3.21 o 0 2 3 5561.64 5880.38 42.29 o 2 2 3 6473.24 6228.63 47.32 o 4 2 3 3317.48 3325.99 25.01 o 6 2 3 9581.42 9931.18 79.87 o 8 2 3 2686.30 2651.31 25.65 o 10 2 3 17173.28 16554.05 188.03 o 12 2 3 119.80 118.94 7.98 o 14 2 3 8653.04 8214.74 99.72 o 16 2 3 26.99 19.19 9.81 o -17 3 3 403.55 397.61 19.08 o -15 3 3 1301.26 1312.13 21.00 o -13 3 3 1.01 7.31 5.58 o -11 3 3 5782.35 5603.75 49.09 o -9 3 3 255.83 249.54 6.02 o -7 3 3 6584.29 6455.95 53.97 o -5 3 3 150.16 126.89 4.35 o -3 3 3 1167.83 1224.08 13.52 o -1 3 3 3111.52 3345.00 25.15 o 1 3 3 2385.33 2544.28 20.70 o 3 3 3 2605.49 2855.25 23.11 o 5 3 3 2504.79 2378.07 25.36 o 7 3 3 976.93 1019.70 12.19 o 9 3 3 787.84 749.53 12.86 o 11 3 3 10.42 10.94 5.76 o 13 3 3 144.24 140.91 9.44 o 15 3 3 272.86 238.77 12.53 o -16 4 3 306.98 341.78 17.23 o -14 4 3 1.29 6.50 7.62 o -12 4 3 741.70 767.30 14.48 o -10 4 3 1472.54 1515.01 20.03 o -8 4 3 729.17 686.02 9.92 o -6 4 3 1717.67 1638.88 15.63 o -4 4 3 3739.02 4074.95 32.91 o -2 4 3 2116.29 2130.55 18.38 o 0 4 3 10035.23 10526.93 79.64 o 2 4 3 290.67 391.07 6.14 o 4 4 3 8937.28 9163.61 74.46 o 6 4 3 0.03 46.00 4.41 o 8 4 3 494.95 622.39 11.60 o 10 4 3 192.93 197.72 8.58 o 12 4 3 31.42 41.18 7.49 o 14 4 3 49.13 84.99 9.92 o -15 5 3 0.24 31.57 10.44 o -13 5 3 6.41 22.86 7.49 o -11 5 3 1302.00 1319.75 17.86 o -9 5 3 65.78 69.01 4.82 o -7 5 3 7695.84 7427.33 58.82 o -5 5 3 1280.71 1286.29 15.75 o -3 5 3 6739.82 6583.00 51.69 o -1 5 3 694.82 666.60 8.92 o 1 5 3 502.53 512.96 7.68 o 3 5 3 38.39 39.83 3.33 o 5 5 3 1968.52 2008.23 21.03 o 7 5 3 548.55 567.03 11.25 o 9 5 3 2044.92 2023.50 26.54 o 11 5 3 1070.69 1076.63 20.60 o 13 5 3 587.86 563.38 21.20 o 15 5 3 695.07 694.36 20.32 o -14 6 3 46.98 65.00 10.90 o -12 6 3 224.84 230.31 10.02 o -10 6 3 3448.72 3361.10 37.76 o -8 6 3 487.92 485.92 11.97 o -6 6 3 8826.51 8681.21 68.32 o -4 6 3 2177.56 2171.17 20.22 o -2 6 3 9865.38 9469.66 78.19 o 0 6 3 1183.17 1161.04 13.53 o 2 6 3 1107.58 1015.38 15.74 o 4 6 3 937.29 939.77 13.83 o 6 6 3 157.47 152.12 7.07 o 8 6 3 18.15 85.70 6.80 o 10 6 3 1714.65 1651.59 27.26 o 12 6 3 5.00 36.22 8.94 o 14 6 3 680.52 721.55 20.18 o -13 7 3 1.49 5.13 10.29 o -11 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