#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2208932.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208932_Fobs loop_ _publ_author_name 'Madsen, Anders' 'Nielsen, Kent A.' 'Bond, Andrew D.' 'Jeppesen, Jan O.' _publ_section_title ; 5-(2-Cyanoethylsulfanyl)-4-methylsulfanyl-1,3-dithiole-2-thione ; _journal_coeditor_code KP2014 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1669 _journal_page_last o1670 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.186 _cell_angle_gamma 90.000 _cell_length_a 5.0793 _cell_length_b 15.7214 _cell_length_c 13.9016 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.8149 _[local]_cod_data_source_file kp2014Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jj0603 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 185.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3919.98 4187.70 279.86 o 3 0 0 70.44 72.07 23.21 o 4 0 0 1474.73 1426.84 116.24 o 1 1 0 921.22 851.11 18.84 o 2 1 0 188.51 204.55 12.25 o 3 1 0 2191.37 2292.56 101.04 o 4 1 0 970.91 884.28 52.45 o 6 1 0 22.39 17.21 13.46 o 1 2 0 727.89 773.22 11.81 o 2 2 0 78.73 93.00 8.61 o 3 2 0 339.43 312.01 16.14 o 4 2 0 0.02 -5.45 12.28 o 5 2 0 31.23 27.64 11.02 o 6 2 0 36.63 39.52 20.56 o 1 3 0 449.28 470.70 7.01 o 2 3 0 5593.41 5428.08 93.84 o 3 3 0 344.70 355.49 10.56 o 4 3 0 752.69 724.64 24.01 o 5 3 0 2563.66 2572.71 129.80 o 6 3 0 81.30 35.81 22.87 o 0 4 0 67.11 51.14 3.34 o 1 4 0 2339.84 2353.09 30.82 o 2 4 0 3993.05 4026.59 68.96 o 3 4 0 306.97 307.74 11.16 o 4 4 0 98.55 104.12 8.70 o 5 4 0 2498.65 2466.17 101.50 o 6 4 0 232.34 312.10 34.59 o 1 5 0 2.60 2.34 2.16 o 2 5 0 0.16 -1.21 2.63 o 3 5 0 554.23 554.03 11.68 o 4 5 0 498.37 486.32 14.74 o 5 5 0 44.82 52.66 9.06 o 0 6 0 2971.60 3042.73 65.15 o 1 6 0 662.82 644.40 10.70 o 2 6 0 21.95 8.76 3.14 o 3 6 0 428.78 438.85 10.90 o 4 6 0 131.63 118.94 9.29 o 5 6 0 45.24 33.41 11.08 o 1 7 0 689.65 656.92 11.26 o 2 7 0 2781.99 2871.07 45.95 o 3 7 0 2408.12 2482.88 48.98 o 4 7 0 929.30 886.95 29.32 o 5 7 0 0.43 -1.63 12.28 o 0 8 0 795.75 677.41 16.55 o 1 8 0 708.55 697.85 12.48 o 2 8 0 544.62 550.67 11.27 o 3 8 0 31.20 28.63 4.88 o 4 8 0 530.96 517.03 18.43 o 5 8 0 217.35 198.21 22.40 o 1 9 0 789.24 830.83 16.26 o 2 9 0 3789.24 3738.57 55.49 o 3 9 0 512.68 522.99 12.67 o 4 9 0 349.11 369.26 19.83 o 5 9 0 174.50 187.81 27.61 o 0 10 0 2.56 -6.08 6.08 o 1 10 0 206.32 216.62 10.07 o 2 10 0 62.91 57.67 6.16 o 3 10 0 310.11 325.13 17.84 o 4 10 0 656.82 650.06 27.89 o 5 10 0 3.75 5.68 22.46 o 1 11 0 39.85 20.13 6.38 o 2 11 0 442.02 444.88 14.86 o 3 11 0 153.56 165.27 12.17 o 4 11 0 5.96 3.31 16.90 o 5 11 0 29.79 37.89 25.80 o 0 12 0 6994.24 6853.59 175.10 o 1 12 0 344.75 322.82 11.92 o 2 12 0 866.45 830.70 29.15 o 3 12 0 35.55 28.94 12.78 o 4 12 0 718.66 684.93 35.05 o 1 13 0 1525.41 1354.86 46.13 o 2 13 0 85.41 83.62 14.29 o 3 13 0 910.85 908.28 45.02 o 4 13 0 879.48 964.48 44.53 o 0 14 0 0.31 5.55 15.41 o 1 14 0 20.15 26.15 12.12 o 2 14 0 174.20 172.28 15.83 o 3 14 0 0.53 7.48 16.06 o 4 14 0 65.13 71.24 25.92 o 1 15 0 26.76 26.78 14.58 o 2 15 0 761.87 879.65 30.00 o 3 15 0 46.10 43.44 19.97 o 0 16 0 1564.31 1478.64 61.38 o 1 16 0 801.52 823.74 33.39 o 2 16 0 539.08 514.28 27.50 o 3 16 0 5.66 5.43 21.98 o 1 17 0 43.46 57.62 21.38 o 2 17 0 10.03 -4.11 21.62 o 0 18 0 7.50 -1.59 35.08 o 1 18 0 134.65 151.54 25.93 o 2 18 0 87.46 110.07 47.16 o 1 19 0 128.61 171.65 48.99 o -6 1 1 58.63 62.10 14.27 o -4 1 1 10.79 4.55 11.15 o -3 1 1 562.96 553.55 36.14 o -2 1 1 761.54 700.28 28.81 o -1 1 1 361.23 401.44 7.31 o 1 1 1 3047.28 3147.59 62.62 o 2 1 1 5106.87 5212.04 125.31 o 3 1 1 71.29 79.46 15.77 o 4 1 1 2535.99 2530.94 93.96 o 6 1 1 5.54 -3.46 14.16 o -6 2 1 5.70 -4.42 18.96 o -5 2 1 327.24 347.22 22.00 o -4 2 1 541.75 531.74 32.74 o -3 2 1 302.61 288.49 8.37 o -2 2 1 1113.56 1163.51 23.53 o -1 2 1 3366.03 3551.67 50.64 o 1 2 1 125.71 123.15 2.88 o 2 2 1 1088.98 985.14 21.10 o 3 2 1 1663.78 1692.05 34.20 o 4 2 1 1571.99 1582.75 44.60 o 5 2 1 0.12 7.03 11.28 o 6 2 1 178.02 191.48 25.79 o -6 3 1 61.79 65.17 23.28 o -5 3 1 77.25 67.09 13.83 o -4 3 1 653.52 646.70 19.17 o -3 3 1 6688.47 6504.40 122.69 o -2 3 1 3936.31 3917.15 68.07 o -1 3 1 18523.08 17848.42 227.77 o 0 3 1 22.41 20.40 1.45 o 1 3 1 1009.77 1021.72 14.53 o 2 3 1 3485.35 3516.08 67.67 o 3 3 1 0.04 0.93 4.20 o 4 3 1 3381.62 3379.88 113.27 o 5 3 1 727.54 704.05 35.04 o 6 3 1 251.95 236.09 30.17 o -6 4 1 4.34 -10.77 23.79 o -5 4 1 99.40 82.18 15.91 o -4 4 1 291.17 297.06 13.76 o -3 4 1 10.23 13.48 4.11 o -2 4 1 1503.99 1556.13 23.16 o -1 4 1 770.83 812.34 11.57 o 0 4 1 1293.14 1307.64 19.38 o 1 4 1 582.85 615.81 9.48 o 2 4 1 1.21 -0.06 2.14 o 3 4 1 192.26 228.07 9.71 o 4 4 1 230.30 216.89 11.37 o 5 4 1 43.44 34.76 15.89 o 6 4 1 59.44 47.23 26.67 o -5 5 1 833.03 802.38 30.06 o -4 5 1 178.54 209.68 9.17 o -3 5 1 62.51 50.92 4.82 o -2 5 1 295.79 333.97 6.66 o -1 5 1 807.43 822.41 12.20 o 0 5 1 221.59 216.44 4.71 o 1 5 1 1334.16 1377.38 20.55 o 2 5 1 862.65 854.45 14.39 o 3 5 1 0.88 0.50 4.07 o 4 5 1 990.54 940.13 26.77 o 5 5 1 98.46 90.00 10.34 o -5 6 1 2103.61 2134.86 71.88 o -4 6 1 1031.54 997.70 28.85 o -3 6 1 216.07 212.30 8.40 o -2 6 1 2583.92 2491.88 38.15 o -1 6 1 9632.28 9501.23 129.10 o 0 6 1 14642.46 14505.45 205.38 o 1 6 1 1635.44 1528.59 22.76 o 2 6 1 2810.91 2847.05 43.90 o 3 6 1 782.56 776.07 16.78 o 4 6 1 115.27 114.19 12.49 o 5 6 1 821.99 868.19 33.96 o -5 7 1 498.80 528.24 24.52 o -4 7 1 132.82 133.15 8.03 o -3 7 1 1807.44 1818.24 35.55 o -2 7 1 173.34 155.28 5.73 o -1 7 1 10.05 5.89 3.04 o 0 7 1 714.66 720.70 11.96 o 1 7 1 614.63 641.30 11.38 o 2 7 1 2353.75 2322.73 40.24 o 3 7 1 405.70 406.79 11.91 o 4 7 1 1141.09 1121.09 30.93 o 5 7 1 9.11 -4.25 16.13 o -5 8 1 59.70 64.15 19.16 o -4 8 1 0.02 -3.57 9.26 o -3 8 1 726.16 726.50 14.48 o -2 8 1 1.81 -0.08 4.04 o -1 8 1 414.81 433.97 8.93 o 0 8 1 84.64 95.91 5.22 o 1 8 1 11.84 5.82 3.93 o 2 8 1 19.65 16.49 4.89 o 3 8 1 5.47 -2.04 4.60 o 4 8 1 2.84 -0.60 9.25 o 5 8 1 12.22 14.81 25.42 o -5 9 1 11.46 20.54 19.69 o -4 9 1 9.95 3.42 12.50 o -3 9 1 3744.68 3688.05 59.20 o -2 9 1 2347.57 2305.59 36.37 o -1 9 1 3396.45 3492.30 59.74 o 0 9 1 187.98 201.97 8.96 o 1 9 1 2419.76 2453.60 40.37 o 2 9 1 1777.64 1835.34 30.49 o 3 9 1 21.15 29.23 6.08 o 4 9 1 1595.09 1509.89 49.87 o 5 9 1 910.74 921.85 187.52 o -5 10 1 1992.52 2065.71 92.49 o -4 10 1 4.84 9.19 14.16 o -3 10 1 167.91 189.50 10.51 o -2 10 1 603.71 606.61 12.82 o -1 10 1 76.33 52.15 5.93 o 0 10 1 7492.84 7307.85 116.94 o 1 10 1 391.14 437.75 11.48 o 2 10 1 6155.83 5989.85 91.99 o 3 10 1 160.11 168.03 9.46 o 4 10 1 1468.11 1300.05 45.40 o 5 10 1 266.31 211.30 27.75 o -5 11 1 6.42 -0.88 24.77 o -4 11 1 21.86 9.29 17.20 o -3 11 1 28.31 27.48 10.04 o -2 11 1 4.32 0.54 6.02 o -1 11 1 289.54 319.65 11.18 o 0 11 1 386.77 396.86 11.62 o 1 11 1 356.57 361.26 16.16 o 2 11 1 20.23 23.63 6.91 o 3 11 1 69.14 72.14 10.82 o 4 11 1 0.76 14.95 17.28 o 5 11 1 127.81 118.99 27.52 o -4 12 1 465.43 450.70 28.43 o -3 12 1 576.94 605.80 23.53 o -2 12 1 190.25 204.37 11.01 o -1 12 1 306.01 334.11 13.36 o 0 12 1 1.97 8.66 7.56 o 1 12 1 482.71 420.50 15.32 o 2 12 1 62.50 79.47 11.13 o 3 12 1 838.71 849.34 25.56 o 4 12 1 49.15 55.42 20.02 o -4 13 1 207.57 177.76 24.98 o -3 13 1 1482.55 1417.86 43.06 o -2 13 1 1177.75 1081.94 33.24 o -1 13 1 189.36 186.74 15.34 o 0 13 1 1708.14 1712.50 36.69 o 1 13 1 366.07 405.28 20.82 o 2 13 1 1332.38 1301.45 57.91 o 3 13 1 10.86 2.89 13.58 o 4 13 1 950.11 937.44 45.22 o -4 14 1 174.28 194.14 28.35 o -3 14 1 207.78 205.07 19.00 o -2 14 1 3.49 -8.02 13.26 o -1 14 1 645.58 648.33 21.37 o 0 14 1 299.62 333.98 16.46 o 1 14 1 42.07 33.58 12.55 o 2 14 1 180.70 196.07 16.45 o 3 14 1 78.32 80.46 17.24 o 4 14 1 120.43 112.81 26.98 o -3 15 1 518.32 526.70 29.54 o -2 15 1 94.48 105.28 16.69 o -1 15 1 1022.79 1057.74 33.12 o 0 15 1 470.36 443.81 21.84 o 1 15 1 65.68 53.53 19.98 o 2 15 1 240.38 234.29 18.91 o 3 15 1 1.20 13.97 19.82 o -3 16 1 30.63 48.13 23.78 o -2 16 1 735.23 698.62 35.69 o -1 16 1 425.80 450.99 25.75 o 0 16 1 36.38 53.16 17.78 o 1 16 1 75.57 73.18 19.90 o 2 16 1 110.55 83.79 19.51 o 3 16 1 794.66 890.73 55.62 o -2 17 1 185.59 229.19 27.37 o -1 17 1 95.92 80.75 21.97 o 0 17 1 0.99 4.30 22.63 o 1 17 1 518.21 549.75 29.68 o 2 17 1 57.75 71.71 22.75 o -2 18 1 199.19 166.76 70.92 o -1 18 1 288.70 296.96 27.45 o 0 18 1 440.08 370.35 32.13 o 1 18 1 162.17 168.40 26.53 o 2 18 1 159.99 123.19 46.61 o 0 19 1 6.85 20.51 29.18 o -4 0 2 2047.94 1992.36 86.53 o -3 0 2 2341.35 2469.59 106.89 o -2 0 2 560.60 569.01 20.69 o -1 0 2 17208.59 16640.84 341.86 o 1 0 2 3961.32 3937.23 93.51 o 2 0 2 7066.12 6965.80 253.86 o 3 0 2 2069.81 2153.09 71.41 o 4 0 2 294.91 281.37 22.12 o 6 0 2 2974.94 2986.11 119.65 o -6 1 2 120.64 93.48 19.71 o -5 1 2 543.86 517.10 34.29 o -4 1 2 716.04 668.76 35.37 o -3 1 2 1821.83 1848.43 41.05 o -2 1 2 1344.50 1331.11 25.92 o -1 1 2 4669.13 4779.70 62.09 o 1 1 2 775.63 802.27 12.96 o 2 1 2 5681.30 5924.00 138.67 o 3 1 2 1222.52 1246.43 29.38 o 4 1 2 837.90 840.68 26.09 o 5 1 2 655.53 614.74 29.77 o 6 1 2 49.59 51.82 21.82 o -6 2 2 8.92 7.99 20.15 o -5 2 2 407.43 385.23 28.88 o -4 2 2 8.77 8.12 6.39 o -3 2 2 1191.49 1238.75 25.09 o -2 2 2 1.67 -2.08 2.08 o -1 2 2 802.44 835.58 11.49 o 0 2 2 481.27 488.76 8.04 o 1 2 2 7.15 4.59 1.55 o 2 2 2 228.25 271.72 6.26 o 3 2 2 2.53 6.60 4.26 o 4 2 2 11.51 5.11 6.93 o 5 2 2 0.21 3.47 12.51 o 6 2 2 29.59 27.01 23.41 o -6 3 2 23.97 4.11 22.29 o -5 3 2 4.33 16.02 13.06 o -4 3 2 320.15 337.24 17.99 o -3 3 2 7876.79 7765.50 155.42 o -2 3 2 66.08 67.76 4.70 o -1 3 2 2872.47 2934.68 38.31 o 0 3 2 8685.12 8863.66 122.02 o 1 3 2 5147.82 5218.04 72.01 o 2 3 2 643.23 678.13 13.15 o 3 3 2 104.16 91.82 6.35 o 4 3 2 5897.38 5616.89 132.42 o 5 3 2 0.15 1.15 17.52 o 6 3 2 31.97 34.76 25.48 o -6 4 2 743.89 848.43 41.06 o -5 4 2 187.92 219.57 34.24 o -4 4 2 238.41 241.06 11.47 o -3 4 2 119.21 127.52 4.65 o -2 4 2 78.94 79.42 3.13 o -1 4 2 1230.13 1235.30 16.97 o 0 4 2 13839.08 13544.52 193.61 o 1 4 2 15947.86 16215.29 222.63 o 2 4 2 4419.04 4692.93 67.66 o 3 4 2 0.57 -1.29 3.50 o 4 4 2 199.59 199.92 8.90 o 5 4 2 15.05 8.36 8.92 o -5 5 2 56.46 54.11 10.09 o -4 5 2 73.85 72.00 7.27 o -3 5 2 74.19 89.18 5.76 o -2 5 2 188.46 184.37 4.88 o -1 5 2 1968.51 2003.57 27.53 o 0 5 2 322.97 342.17 7.04 o 1 5 2 9.58 3.92 2.46 o 2 5 2 227.01 226.28 5.55 o 3 5 2 2208.18 2183.97 41.53 o 4 5 2 3.76 1.54 7.18 o 5 5 2 7.59 -0.68 10.51 o -5 6 2 78.73 93.60 13.68 o -4 6 2 371.96 382.97 14.87 o -3 6 2 2.03 -0.08 4.78 o -2 6 2 163.23 163.08 7.36 o -1 6 2 191.33 220.85 5.35 o 0 6 2 58.46 55.88 3.79 o 1 6 2 164.08 175.03 5.97 o 2 6 2 276.46 269.36 7.07 o 3 6 2 495.16 523.87 13.03 o 4 6 2 5.60 2.77 8.34 o 5 6 2 160.08 176.75 15.03 o -5 7 2 0.10 -4.35 15.55 o -4 7 2 684.42 679.43 19.10 o -3 7 2 1949.57 1890.65 30.89 o -2 7 2 1459.56 1430.50 23.99 o -1 7 2 4979.55 4880.95 71.56 o 0 7 2 336.10 306.00 7.01 o 1 7 2 286.62 311.59 8.77 o 2 7 2 2018.75 2039.38 33.89 o 3 7 2 2056.14 2064.61 43.19 o 4 7 2 906.11 865.43 22.86 o 5 7 2 208.87 244.72 23.39 o -5 8 2 140.74 146.47 21.31 o -4 8 2 94.38 94.02 12.70 o -3 8 2 196.71 188.47 6.99 o -2 8 2 322.78 371.62 8.68 o -1 8 2 65.72 50.22 4.51 o 0 8 2 4401.25 4631.16 65.23 o 1 8 2 581.08 556.87 12.10 o 2 8 2 1.37 -0.55 4.95 o 3 8 2 72.03 71.44 5.81 o 4 8 2 0.51 5.53 10.12 o 5 8 2 22.59 18.08 18.95 o -5 9 2 7.05 28.54 20.01 o -4 9 2 5.14 0.53 12.52 o -3 9 2 3312.88 3277.70 54.66 o -2 9 2 284.34 313.48 10.32 o -1 9 2 2484.33 2444.32 40.97 o 0 9 2 143.66 158.55 6.38 o 1 9 2 1147.16 1182.40 21.16 o 2 9 2 749.01 755.24 15.05 o 3 9 2 254.11 250.02 9.43 o 4 9 2 2503.92 2478.94 76.32 o 5 9 2 306.51 292.61 28.22 o -5 10 2 135.83 157.89 25.84 o -4 10 2 140.72 144.70 16.79 o -3 10 2 400.54 427.63 13.97 o -2 10 2 1408.04 1383.78 28.01 o -1 10 2 108.81 112.50 7.39 o 0 10 2 0.78 -5.82 5.82 o 1 10 2 23.16 12.49 5.81 o 2 10 2 311.40 311.81 9.60 o 3 10 2 411.51 410.69 18.08 o 4 10 2 18.12 16.23 14.99 o 5 10 2 147.04 137.53 26.72 o -5 11 2 216.75 156.86 28.53 o -4 11 2 238.94 273.16 38.34 o -3 11 2 192.78 186.63 11.75 o -2 11 2 33.52 31.39 6.57 o -1 11 2 0.04 3.39 6.35 o 0 11 2 650.06 623.64 27.05 o 1 11 2 4.01 4.12 6.90 o 2 11 2 63.81 51.78 7.55 o 3 11 2 393.79 367.38 16.69 o 4 11 2 269.74 288.14 21.88 o -4 12 2 465.38 496.35 30.35 o -3 12 2 3.40 -4.60 12.15 o -2 12 2 619.97 617.20 25.29 o -1 12 2 2487.61 2530.37 47.92 o 0 12 2 86.59 89.90 8.86 o 1 12 2 2753.04 2671.55 52.16 o 2 12 2 2692.18 2712.47 57.28 o 3 12 2 149.70 153.13 17.02 o 4 12 2 1.85 -6.69 19.04 o -4 13 2 14.57 10.60 21.75 o -3 13 2 838.26 835.26 28.24 o -2 13 2 205.63 188.20 17.07 o -1 13 2 1768.04 1781.29 38.25 o 0 13 2 322.03 327.37 13.48 o 1 13 2 91.34 95.86 11.60 o 2 13 2 2165.31 2158.20 59.23 o 3 13 2 112.58 98.74 15.07 o 4 13 2 429.79 489.01 34.50 o -4 14 2 37.39 24.12 25.09 o -3 14 2 146.02 160.74 17.60 o -2 14 2 82.10 86.14 13.93 o -1 14 2 0.01 -6.32 10.96 o 0 14 2 16.66 18.47 10.20 o 1 14 2 3.65 -0.93 12.84 o 2 14 2 66.69 73.36 15.07 o 3 14 2 61.05 43.32 16.89 o 4 14 2 16.18 5.01 24.57 o -3 15 2 1362.32 1414.49 57.91 o -2 15 2 4.51 -2.68 15.12 o -1 15 2 59.95 61.57 15.30 o 0 15 2 410.92 390.78 30.53 o 1 15 2 339.35 313.49 21.19 o 2 15 2 40.74 33.66 16.45 o 3 15 2 3.44 -3.67 20.43 o -3 16 2 184.69 179.30 25.33 o -2 16 2 36.38 30.05 19.61 o -1 16 2 374.26 409.21 50.17 o 0 16 2 1753.87 1856.42 55.74 o 1 16 2 1409.57 1476.99 53.95 o 2 16 2 227.90 234.09 22.91 o 3 16 2 124.65 75.86 24.03 o -2 17 2 112.31 114.51 26.92 o -1 17 2 23.48 30.50 21.96 o 0 17 2 16.39 20.89 22.72 o 1 17 2 0.24 4.23 21.30 o 2 17 2 1.33 -0.26 25.33 o -2 18 2 185.51 207.52 48.02 o -1 18 2 78.68 83.85 25.23 o 0 18 2 60.58 69.09 26.48 o 1 18 2 1.38 12.64 24.40 o 2 18 2 48.40 42.61 62.18 o 0 19 2 442.18 538.82 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