#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/89/2208946.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208946_Fobs loop_ _publ_author_name 'Refat, Moamen S.' 'Ahmed, Hamdy Al-Didamony' 'El-Zayat, Lamia A.' 'Fukunaga, Takeo' 'Ishida, Hiroyuki' _publ_section_title ; Bis(piperidinium) chloranilate ; _journal_coeditor_code LH2042 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1886 _journal_page_last o1887 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 114.412 _cell_angle_beta 95.561 _cell_angle_gamma 95.070 _cell_length_a 5.1239 _cell_length_b 8.7058 _cell_length_c 10.4508 _exptl_crystal_F_000 200.00 _reflns_d_resolution_high 0.7807 _[local]_cod_data_source_file lh2042Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 06030712' _shelx_refln_list_code 4 _shelx_f_calc_maximum 75.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 22.16 15.27 0.69 o 2 0 0 389.71 372.29 7.74 o 3 0 0 195.59 195.47 5.16 o 4 0 0 160.59 147.64 6.38 o 5 0 0 46.74 50.61 1.84 o 6 0 0 5.45 2.65 0.95 o -6 1 0 59.18 55.18 1.94 o -5 1 0 167.38 166.12 3.51 o -4 1 0 58.63 63.42 2.53 o -3 1 0 2.84 2.88 0.86 o -2 1 0 798.87 815.79 10.53 o -1 1 0 408.84 392.67 3.62 o 1 1 0 195.10 212.23 3.52 o 2 1 0 71.00 77.03 3.00 o 3 1 0 1303.60 1396.94 27.02 o 4 1 0 59.85 56.54 1.66 o 5 1 0 353.18 348.69 5.44 o 6 1 0 23.70 23.31 2.19 o -6 2 0 0.12 -1.24 1.24 o -5 2 0 154.07 160.30 4.02 o -4 2 0 2.66 4.06 1.04 o -3 2 0 53.77 54.71 1.70 o -2 2 0 7.83 9.42 0.67 o -1 2 0 3625.58 3358.61 62.70 o 0 2 0 37.86 51.07 2.28 o 1 2 0 1152.54 1134.65 19.82 o 2 2 0 262.12 249.28 6.70 o 3 2 0 618.27 614.59 16.23 o 4 2 0 50.33 50.84 1.51 o 5 2 0 5.86 5.32 1.38 o 6 2 0 14.49 17.15 5.03 o -6 3 0 201.80 212.37 4.34 o -5 3 0 178.68 182.55 5.98 o -4 3 0 1.23 2.18 0.88 o -3 3 0 47.20 54.31 1.64 o -2 3 0 705.82 805.54 19.18 o -1 3 0 335.12 383.38 6.24 o 0 3 0 2.48 8.01 1.70 o 1 3 0 59.30 61.80 2.76 o 2 3 0 306.46 309.32 6.18 o 3 3 0 14.07 11.84 5.27 o 4 3 0 221.06 206.59 9.26 o 5 3 0 134.65 122.11 9.78 o -6 4 0 16.15 21.06 2.23 o -5 4 0 126.57 125.92 4.46 o -4 4 0 224.76 222.47 8.79 o -3 4 0 403.07 390.05 11.77 o -2 4 0 174.44 167.45 3.10 o -1 4 0 182.42 178.70 3.34 o 0 4 0 7.70 5.98 2.77 o 1 4 0 113.98 120.85 4.00 o 2 4 0 78.31 76.59 4.14 o 3 4 0 52.48 58.77 8.06 o 4 4 0 73.21 72.21 8.13 o 5 4 0 0.25 0.11 3.35 o -6 5 0 42.74 49.95 4.00 o -5 5 0 2.71 0.79 0.91 o -4 5 0 298.94 288.67 10.35 o -3 5 0 75.16 84.50 3.29 o -2 5 0 162.77 163.09 9.71 o -1 5 0 25.03 20.46 1.82 o 0 5 0 344.20 346.73 6.17 o 1 5 0 53.48 45.38 4.74 o 2 5 0 113.68 107.47 6.62 o 3 5 0 97.02 100.67 9.54 o 4 5 0 188.71 178.93 12.24 o 5 5 0 38.81 19.37 19.96 o -5 6 0 69.74 69.76 2.03 o -4 6 0 542.99 517.39 17.08 o -3 6 0 88.81 85.24 5.68 o -2 6 0 29.67 29.81 2.09 o -1 6 0 838.36 827.03 13.14 o 0 6 0 88.59 91.05 3.23 o 1 6 0 393.93 398.10 9.04 o 2 6 0 2.43 2.56 2.55 o 4 6 0 40.59 42.52 8.54 o -5 7 0 12.60 12.15 2.03 o -4 7 0 44.88 47.59 2.58 o -3 7 0 29.22 27.68 1.77 o -2 7 0 23.17 23.32 2.69 o -1 7 0 820.24 821.89 14.24 o 0 7 0 23.08 23.33 3.84 o 1 7 0 68.84 70.04 2.67 o 2 7 0 488.60 485.94 11.14 o 3 7 0 23.27 2.50 7.49 o 4 7 0 52.84 56.25 6.30 o -4 8 0 0.47 1.19 1.16 o -3 8 0 13.93 7.71 1.27 o -2 8 0 114.88 110.52 3.36 o -1 8 0 36.79 36.85 2.87 o 0 8 0 120.20 125.79 3.81 o 1 8 0 89.74 90.98 3.42 o 2 8 0 181.83 183.22 4.39 o 3 8 0 58.75 65.25 6.49 o -3 9 0 91.03 91.08 8.77 o -2 9 0 13.07 9.53 2.82 o -1 9 0 113.16 117.83 3.98 o 0 9 0 71.28 77.06 4.07 o 1 9 0 184.80 185.16 6.73 o 2 9 0 51.01 54.58 3.93 o -2 10 0 26.58 29.60 2.47 o -1 10 0 3.99 1.90 1.86 o 0 10 0 68.96 65.84 3.23 o -1 -10 1 56.55 61.59 4.43 o 0 -10 1 246.91 260.88 12.88 o 1 -10 1 153.54 166.68 7.27 o 2 -10 1 34.25 38.42 3.05 o -2 -9 1 146.76 147.09 5.62 o -1 -9 1 84.33 83.24 3.80 o 0 -9 1 0.90 0.31 2.00 o 1 -9 1 17.06 20.12 5.83 o 2 -9 1 109.73 107.37 3.50 o 3 -9 1 45.48 35.85 3.54 o 4 -9 1 5.68 4.20 2.98 o -3 -8 1 6.12 2.80 4.20 o -2 -8 1 42.22 48.63 4.46 o -1 -8 1 85.29 87.77 4.10 o 0 -8 1 42.35 44.21 3.70 o 1 -8 1 332.18 345.42 9.03 o 2 -8 1 204.82 203.16 4.91 o 3 -8 1 279.01 267.78 17.26 o 4 -8 1 108.52 107.27 7.22 o -4 -7 1 4.92 5.98 4.15 o -3 -7 1 2.54 1.37 2.75 o -2 -7 1 9.87 16.28 3.45 o -1 -7 1 67.68 65.98 3.63 o 0 -7 1 40.87 42.69 2.67 o 1 -7 1 323.99 322.16 6.19 o 2 -7 1 17.95 21.20 1.84 o 3 -7 1 80.55 71.13 2.81 o 4 -7 1 234.06 219.34 9.44 o 5 -7 1 105.21 117.34 3.95 o -4 -6 1 463.36 441.26 15.27 o -3 -6 1 92.51 88.68 5.37 o -2 -6 1 4.78 4.66 2.25 o -1 -6 1 0.36 3.38 2.16 o 0 -6 1 4.02 5.53 2.04 o 1 -6 1 31.17 32.35 2.09 o 2 -6 1 63.38 65.10 3.11 o 3 -6 1 0.19 0.78 1.42 o 4 -6 1 66.83 63.29 2.66 o 5 -6 1 100.23 95.69 7.03 o -5 -5 1 3.23 3.60 3.22 o -4 -5 1 213.62 211.24 8.54 o -3 -5 1 198.33 185.66 5.41 o -2 -5 1 22.53 18.23 2.56 o -1 -5 1 233.07 238.17 6.80 o 0 -5 1 135.98 125.69 3.73 o 1 -5 1 279.39 300.59 6.34 o 2 -5 1 301.92 289.33 6.80 o 3 -5 1 70.87 73.46 3.54 o 4 -5 1 13.38 15.24 1.50 o 5 -5 1 81.43 71.38 6.26 o 6 -5 1 54.55 60.17 9.67 o -5 -4 1 274.70 244.39 21.88 o -4 -4 1 125.24 115.26 5.99 o -3 -4 1 134.19 128.46 10.12 o -2 -4 1 78.04 66.35 4.00 o -1 -4 1 1135.35 1173.21 23.48 o 0 -4 1 937.57 957.74 16.98 o 1 -4 1 58.73 56.96 2.63 o 2 -4 1 6.36 2.42 1.02 o 3 -4 1 55.74 54.69 2.16 o 4 -4 1 38.39 38.67 1.75 o 5 -4 1 254.31 243.61 6.11 o 6 -4 1 14.20 17.80 2.41 o -6 -3 1 3.63 4.15 2.47 o -5 -3 1 6.60 6.63 1.08 o -4 -3 1 9.09 8.09 2.74 o -3 -3 1 32.01 32.58 3.56 o -2 -3 1 130.58 109.30 3.11 o -1 -3 1 196.81 173.53 4.34 o 0 -3 1 374.63 373.41 6.95 o 1 -3 1 855.09 869.32 19.34 o 2 -3 1 9.07 5.74 1.30 o 3 -3 1 668.98 657.26 17.60 o 4 -3 1 150.85 161.03 6.99 o 5 -3 1 8.90 6.93 2.97 o 6 -3 1 3.54 1.13 1.94 o -6 -2 1 2.47 3.46 3.16 o -5 -2 1 19.79 16.21 2.24 o -4 -2 1 4.04 2.28 1.12 o -3 -2 1 463.66 476.86 12.36 o -2 -2 1 1366.27 1438.00 27.44 o -1 -2 1 229.25 217.89 4.35 o 0 -2 1 796.23 809.22 17.43 o 1 -2 1 675.50 734.95 10.21 o 2 -2 1 378.12 371.69 7.88 o 3 -2 1 231.40 235.91 3.08 o 4 -2 1 880.52 866.41 17.64 o 5 -2 1 16.19 15.42 1.69 o 6 -2 1 93.83 90.29 3.55 o -6 -1 1 53.54 57.22 2.68 o -5 -1 1 53.73 53.67 1.82 o -4 -1 1 80.59 79.05 2.16 o -3 -1 1 0.17 0.43 1.18 o -2 -1 1 431.81 436.36 9.21 o -1 -1 1 1844.75 1692.83 29.03 o 1 -1 1 1715.09 1569.74 21.70 o 2 -1 1 743.43 742.87 7.89 o 3 -1 1 59.56 62.11 4.38 o 4 -1 1 133.11 130.62 2.89 o 5 -1 1 196.01 202.07 3.56 o 6 -1 1 78.86 80.07 3.56 o -6 0 1 22.51 24.32 2.19 o -5 0 1 58.66 62.70 1.87 o -4 0 1 23.80 23.98 2.04 o -3 0 1 32.13 27.52 1.22 o -2 0 1 37.12 37.19 1.29 o -1 0 1 175.27 161.22 2.87 o 1 0 1 10.06 7.37 0.77 o 2 0 1 502.12 538.88 7.62 o 3 0 1 421.53 433.97 8.10 o 4 0 1 8.98 9.13 1.30 o 5 0 1 55.38 55.21 2.59 o 6 0 1 119.13 121.12 4.99 o -6 1 1 0.32 -0.05 0.96 o -5 1 1 465.00 473.79 6.94 o -4 1 1 289.85 303.14 5.80 o -3 1 1 303.34 292.11 4.99 o -2 1 1 1541.92 1605.29 23.11 o -1 1 1 362.56 344.98 11.33 o 0 1 1 332.71 315.59 3.37 o 1 1 1 64.11 68.55 3.32 o 2 1 1 123.48 134.98 4.38 o 3 1 1 86.28 94.77 2.17 o 4 1 1 480.14 468.76 6.83 o 5 1 1 14.16 13.32 1.41 o 6 1 1 6.65 6.94 2.02 o -6 2 1 15.74 15.83 1.54 o -5 2 1 297.61 307.02 5.54 o -4 2 1 318.40 311.68 4.63 o -3 2 1 3.88 7.10 0.70 o -2 2 1 1.75 0.59 0.46 o -1 2 1 1571.92 1712.59 22.40 o 0 2 1 1358.57 1388.60 19.55 o 1 2 1 1172.42 1202.63 20.91 o 2 2 1 4.36 6.20 2.09 o 3 2 1 266.45 253.99 8.36 o 4 2 1 152.60 146.96 2.46 o 5 2 1 14.30 6.71 1.88 o 6 2 1 9.91 10.68 2.34 o -6 3 1 52.79 50.95 1.57 o -5 3 1 1.02 2.56 1.77 o -4 3 1 16.10 13.78 1.56 o -3 3 1 449.52 452.45 11.68 o -2 3 1 455.14 466.57 6.65 o -1 3 1 640.05 641.93 7.02 o 0 3 1 632.49 613.72 9.72 o 1 3 1 4.91 2.14 1.30 o 2 3 1 142.95 145.18 5.92 o 3 3 1 16.34 16.67 3.48 o 4 3 1 151.82 140.06 2.96 o 5 3 1 2.44 3.54 2.08 o -6 4 1 11.96 0.12 2.37 o -5 4 1 16.41 14.46 1.41 o -4 4 1 0.45 1.18 0.65 o -3 4 1 23.25 19.94 1.10 o -2 4 1 507.30 524.49 15.20 o -1 4 1 80.88 74.00 1.97 o 0 4 1 401.26 407.11 6.64 o 1 4 1 0.18 0.40 1.06 o 2 4 1 953.60 953.92 27.27 o 3 4 1 942.95 928.42 27.53 o 4 4 1 3.80 7.82 3.20 o 5 4 1 107.90 112.54 5.73 o -5 5 1 101.81 106.40 3.65 o -4 5 1 109.18 106.35 3.18 o -3 5 1 0.88 0.60 0.85 o -2 5 1 28.84 26.28 2.04 o -1 5 1 68.80 67.22 2.12 o 0 5 1 122.30 119.77 3.19 o 1 5 1 255.88 254.39 5.61 o 2 5 1 1.70 -0.21 1.30 o 3 5 1 413.93 422.13 13.97 o 4 5 1 29.91 13.43 12.73 o -5 6 1 56.50 43.69 9.53 o -4 6 1 1.02 2.07 1.18 o -3 6 1 11.82 11.69 1.23 o -2 6 1 351.95 349.03 5.52 o -1 6 1 58.07 55.83 2.92 o 0 6 1 0.56 -0.54 1.71 o 1 6 1 24.34 28.28 2.02 o 2 6 1 66.94 64.05 5.52 o 3 6 1 51.16 56.43 3.51 o 4 6 1 106.88 106.21 7.48 o -5 7 1 43.98 46.46 4.76 o -4 7 1 101.05 93.54 6.80 o -3 7 1 176.61 167.00 3.36 o -2 7 1 33.38 33.67 2.11 o -1 7 1 21.28 23.62 2.33 o 0 7 1 11.77 11.86 1.62 o 1 7 1 93.84 87.84 3.79 o 2 7 1 13.47 5.81 2.52 o 3 7 1 3.49 3.09 1.89 o -4 8 1 36.81 32.65 2.07 o -3 8 1 139.22 144.25 3.31 o -2 8 1 119.30 121.04 4.81 o -1 8 1 145.16 145.01 4.72 o 0 8 1 272.98 281.24 5.53 o 1 8 1 74.16 78.20 4.38 o 2 8 1 1.72 -0.29 2.30 o -3 9 1 3.95 2.97 1.11 o -2 9 1 62.12 60.77 2.40 o -1 9 1 32.96 31.93 10.28 o 0 9 1 18.81 15.20 4.97 o 1 9 1 34.82 36.51 3.35 o -1 -10 2 12.67 10.36 3.20 o 0 -10 2 107.55 109.78 4.01 o 1 -10 2 6.64 3.62 2.08 o 2 -10 2 81.00 79.00 4.19 o 3 -10 2 2.21 1.41 2.12 o -2 -9 2 2.09 1.09 2.45 o -1 -9 2 212.72 214.62 6.95 o 0 -9 2 21.51 19.98 3.83 o 1 -9 2 23.79 24.25 7.76 o 2 -9 2 4.94 5.16 2.77 o 3 -9 2 23.45 21.44 1.93 o 4 -9 2 17.56 14.85 2.07 o -3 -8 2 101.50 107.43 12.63 o -2 -8 2 5.51 2.45 2.34 o -1 -8 2 1.36 5.24 2.33 o 0 -8 2 642.54 663.68 21.32 o 1 -8 2 46.53 47.98 2.57 o 2 -8 2 22.73 25.07 2.34 o 3 -8 2 0.17 0.62 1.51 o 4 -8 2 154.67 147.91 7.75 o -4 -7 2 150.68 165.22 8.98 o -3 -7 2 66.67 67.33 9.21 o -2 -7 2 720.50 682.84 24.29 o -1 -7 2 58.41 53.71 6.85 o 0 -7 2 490.93 491.70 15.70 o 1 -7 2 0.64 1.10 1.75 o 2 -7 2 57.01 64.21 4.49 o 3 -7 2 82.50 72.64 2.65 o 4 -7 2 40.78 34.97 3.75 o 5 -7 2 5.10 4.34 1.69 o -5 -6 2 32.48 20.46 7.45 o -4 -6 2 169.26 157.99 12.05 o -3 -6 2 26.05 31.57 3.93 o -2 -6 2 12.19 11.13 2.53 o -1 -6 2 346.97 330.22 8.12 o 0 -6 2 27.98 28.36 4.69 o 1 -6 2 291.10 294.17 18.36 o 2 -6 2 301.58 298.79 10.92 o 3 -6 2 1189.24 1133.98 52.52 o 4 -6 2 38.78 39.73 2.08 o 5 -6 2 53.42 54.75 3.90 o -5 -5 2 47.10 49.39 4.68 o -4 -5 2 27.70 24.84 3.76 o -3 -5 2 120.55 107.98 6.62 o -2 -5 2 89.43 89.17 3.77 o -1 -5 2 75.09 74.46 4.21 o 0 -5 2 355.19 339.83 9.97 o 1 -5 2 599.13 648.12 30.33 o 2 -5 2 20.70 17.78 1.90 o 3 -5 2 2.87 0.07 1.35 o 4 -5 2 35.57 35.56 1.64 o 5 -5 2 88.95 94.97 3.65 o 6 -5 2 33.47 32.53 3.01 o -5 -4 2 6.93 8.39 2.22 o -4 -4 2 2.72 -1.37 2.39 o -3 -4 2 76.37 70.43 5.21 o -2 -4 2 71.73 66.38 3.45 o -1 -4 2 3.66 3.12 1.83 o 0 -4 2 51.14 61.82 6.91 o 1 -4 2 595.28 640.29 39.32 o 2 -4 2 128.18 115.57 3.14 o 3 -4 2 171.72 166.02 3.99 o 4 -4 2 518.19 503.27 13.19 o 5 -4 2 152.53 160.08 9.52 o 6 -4 2 114.66 116.86 5.42 o -6 -3 2 97.27 98.89 6.13 o -5 -3 2 119.08 121.27 4.45 o -4 -3 2 334.93 343.76 10.09 o -3 -3 2 225.31 216.56 5.64 o -2 -3 2 297.11 297.41 5.49 o -1 -3 2 549.08 579.55 30.18 o 0 -3 2 86.98 87.53 5.29 o 1 -3 2 44.00 44.81 5.06 o 2 -3 2 46.70 55.57 2.02 o 3 -3 2 4.07 3.86 1.26 o 4 -3 2 501.27 473.91 15.48 o 5 -3 2 0.03 -0.27 1.25 o 6 -3 2 33.58 35.22 5.37 o -6 -2 2 96.35 97.60 3.24 o -5 -2 2 15.24 14.14 1.69 o -4 -2 2 500.01 502.95 11.08 o -3 -2 2 333.20 367.19 12.61 o -2 -2 2 532.51 531.52 8.32 o -1 -2 2 3564.00 3262.85 170.51 o 0 -2 2 163.29 160.45 4.28 o 1 -2 2 217.38 231.62 6.55 o 2 -2 2 101.08 99.42 1.80 o 3 -2 2 2.47 3.41 1.13 o 4 -2 2 99.89 94.39 4.37 o 5 -2 2 0.38 -0.50 2.06 o 6 -2 2 0.03 -0.27 1.46 o -6 -1 2 83.43 86.23 4.01 o -5 -1 2 113.42 115.69 2.34 o -4 -1 2 354.37 356.97 5.43 o -3 -1 2 465.64 460.78 8.17 o -2 -1 2 164.26 181.54 3.10 o -1 -1 2 5739.22 5119.06 132.22 o 0 -1 2 885.19 891.68 12.47 o 1 -1 2 27.91 26.28 1.71 o 2 -1 2 394.55 412.82 5.39 o 3 -1 2 51.04 50.62 1.45 o 4 -1 2 60.49 55.32 3.94 o 5 -1 2 2.64 2.12 3.71 o 6 -1 2 2.65 2.08 2.12 o -6 0 2 99.21 93.76 2.54 o -5 0 2 102.37 97.96 1.97 o -4 0 2 53.95 52.41 1.69 o -3 0 2 816.66 826.55 10.87 o -2 0 2 797.85 777.41 11.63 o -1 0 2 2860.37 2435.06 56.69 o 0 0 2 1378.00 1240.52 23.27 o 1 0 2 275.22 158.29 116.62 o 2 0 2 2281.14 2519.83 75.35 o 3 0 2 207.27 207.02 10.51 o 4 0 2 108.49 113.50 3.13 o 5 0 2 0.45 1.33 1.98 o 6 0 2 0.49 1.21 2.01 o -6 1 2 111.27 106.73 3.97 o -5 1 2 90.50 94.80 2.40 o -4 1 2 198.39 198.44 2.96 o -3 1 2 44.55 42.34 1.06 o -2 1 2 316.09 330.20 3.75 o -1 1 2 966.35 973.64 20.29 o 0 1 2 551.97 578.84 6.96 o 1 1 2 156.25 163.56 2.66 o 2 1 2 501.02 528.82 12.78 o 3 1 2 20.23 20.99 2.25 o 4 1 2 133.17 119.04 5.32 o 5 1 2 190.48 200.75 5.47 o 6 1 2 83.31 76.62 3.89 o -6 2 2 19.95 18.26 5.41 o -5 2 2 43.89 44.50 2.20 o -4 2 2 25.56 24.40 1.07 o -3 2 2 198.88 241.76 3.94 o -2 2 2 181.30 218.82 7.71 o -1 2 2 617.02 687.32 7.37 o 0 2 2 1224.45 1271.12 17.22 o 1 2 2 470.64 466.06 8.81 o 2 2 2 293.88 296.68 4.62 o 3 2 2 292.24 276.01 7.87 o 4 2 2 22.45 25.43 2.56 o 5 2 2 47.77 55.79 3.34 o -5 3 2 62.58 63.98 1.33 o -4 3 2 138.61 140.23 3.19 o -3 3 2 117.56 125.75 3.26 o -2 3 2 361.44 388.35 4.61 o -1 3 2 3.55 3.99 0.73 o 0 3 2 76.97 93.76 1.83 o 1 3 2 189.66 200.44 4.59 o 2 3 2 191.77 188.64 4.65 o 3 3 2 743.97 725.00 11.74 o 4 3 2 212.17 217.00 7.03 o 5 3 2 121.67 130.62 5.97 o -5 4 2 390.88 399.81 6.38 o -4 4 2 120.91 122.07 8.35 o -3 4 2 0.59 0.63 0.61 o -2 4 2 21.44 19.58 1.46 o -1 4 2 164.24 152.18 6.74 o 0 4 2 68.09 57.68 2.11 o 1 4 2 27.76 26.21 2.73 o 2 4 2 6.97 8.35 1.66 o 3 4 2 36.68 34.71 1.67 o 4 4 2 19.76 20.05 3.41 o 5 4 2 14.84 11.54 2.94 o -5 5 2 146.58 145.84 9.62 o -4 5 2 11.47 13.34 1.24 o -3 5 2 62.49 69.57 2.19 o -2 5 2 714.55 691.82 11.51 o -1 5 2 30.97 30.45 3.06 o 0 5 2 385.28 385.44 7.23 o 1 5 2 156.55 146.09 3.20 o 2 5 2 1.41 0.95 1.76 o 3 5 2 1.65 0.12 2.37 o 4 5 2 9.73 11.14 3.96 o -5 6 2 12.27 19.36 3.80 o -4 6 2 84.05 68.28 3.94 o -3 6 2 35.76 34.47 1.91 o -2 6 2 1103.77 1049.45 15.93 o -1 6 2 71.59 73.72 2.58 o 0 6 2 3.63 3.62 1.44 o 1 6 2 322.37 301.51 5.22 o 2 6 2 106.45 101.98 2.91 o 3 6 2 181.38 174.07 4.21 o 4 6 2 54.94 54.74 6.28 o -4 7 2 12.45 18.47 3.88 o -3 7 2 18.98 20.72 1.59 o -2 7 2 3.09 2.09 1.04 o -1 7 2 153.08 157.72 3.36 o 0 7 2 41.48 41.57 3.41 o 1 7 2 300.68 282.95 8.64 o 2 7 2 105.53 110.78 4.22 o 3 7 2 25.84 22.62 5.05 o -4 8 2 8.28 13.38 4.13 o -3 8 2 181.56 169.17 7.67 o -2 8 2 4.47 2.87 1.31 o -1 8 2 39.98 39.66 3.78 o 0 8 2 79.79 78.51 13.17 o 1 8 2 39.72 40.16 3.16 o 2 8 2 58.54 58.65 3.38 o -2 9 2 0.12 -0.81 1.41 o -1 9 2 15.81 19.05 7.68 o 0 9 2 32.23 31.92 2.21 o -1 -10 3 47.91 54.86 15.09 o 0 -10 3 41.10 45.08 3.30 o 1 -10 3 142.09 145.31 4.51 o 2 -10 3 126.17 111.48 8.09 o 3 -10 3 29.50 21.25 3.60 o -3 -9 3 61.23 58.28 7.46 o -2 -9 3 24.13 21.87 4.13 o -1 -9 3 0.22 -2.06 2.98 o 0 -9 3 389.91 419.87 20.10 o 1 -9 3 19.10 22.55 2.74 o 2 -9 3 53.74 63.81 2.90 o 3 -9 3 14.73 15.42 1.93 o 4 -9 3 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303.95 304.89 35.22 o 1 -3 9 460.54 434.14 39.96 o 2 -3 9 52.03 59.89 3.48 o 3 -3 9 261.90 201.34 21.28 o 4 -3 9 97.82 115.02 8.07 o -5 -2 9 3.22 3.95 5.53 o -4 -2 9 0.68 -1.78 2.97 o -3 -2 9 70.45 65.39 1.77 o -2 -2 9 0.60 0.54 0.78 o -1 -2 9 11.96 13.66 3.21 o 0 -2 9 57.76 58.25 7.84 o 1 -2 9 219.76 204.18 9.18 o 2 -2 9 58.66 49.37 7.64 o 3 -2 9 196.90 201.73 9.35 o 4 -2 9 76.75 86.70 7.27 o -5 -1 9 5.87 6.17 6.10 o -4 -1 9 27.98 21.05 6.62 o -3 -1 9 28.33 28.34 3.79 o -2 -1 9 73.00 68.56 1.48 o -1 -1 9 13.41 12.51 2.68 o 0 -1 9 506.01 495.88 20.57 o 1 -1 9 18.06 16.21 5.76 o 2 -1 9 115.29 72.55 30.04 o 3 -1 9 18.42 26.15 4.57 o -5 0 9 56.28 61.58 9.41 o -4 0 9 38.48 35.06 4.64 o -3 0 9 19.86 21.19 3.64 o -2 0 9 22.60 21.18 2.48 o -1 0 9 348.79 368.35 13.03 o 0 0 9 212.60 212.14 8.59 o 1 0 9 34.70 27.54 2.06 o 2 0 9 0.07 -1.00 4.41 o 3 0 9 25.13 32.79 4.69 o -4 1 9 95.50 102.87 6.45 o -3 1 9 181.63 198.37 8.02 o -2 1 9 8.89 10.15 1.20 o -1 1 9 15.25 14.88 1.00 o 0 1 9 83.19 86.36 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